Involving Waste Liquid Patents (Class 159/47.3)
  • Patent number: 8066844
    Abstract: A compact and portable liquid concentrator includes a gas inlet, a gas exit and a flow corridor connecting the gas inlet and the gas exit, wherein the flow corridor includes a narrowed portion that accelerates the gas through the flow corridor. A liquid inlet injects liquid into the gas stream at a point prior to the narrowed portion so that the gas-liquid mixture is thoroughly mixed within the flow corridor, causing a portion of the liquid to be evaporated. A demister or fluid scrubber downstream of the narrowed portion removes entrained liquid droplets from the gas stream and re-circulates the removed liquid to the liquid inlet through a re-circulating circuit. Fresh liquid to be concentrated is also introduced into the re-circulating circuit at a rate sufficient to offset the amount of liquid evaporated in the flow corridor.
    Type: Grant
    Filed: March 31, 2011
    Date of Patent: November 29, 2011
    Assignee: Heartland Technology Partners LLC
    Inventors: Bernard F. Duesel, Jr., Michael J. Rutsch
  • Patent number: 8066845
    Abstract: A compact and portable liquid concentrator includes a gas inlet, a gas exit and a flow corridor connecting the gas inlet and the gas exit, wherein the flow corridor includes a narrowed portion that accelerates the gas through the flow corridor. A liquid inlet injects liquid into the gas stream at a point prior to the narrowed portion so that the gas-liquid mixture is thoroughly mixed within the flow corridor, causing a portion of the liquid to be evaporated. A demister or fluid scrubber downstream of the narrowed portion removes entrained liquid droplets from the gas stream and re-circulates the removed liquid to the liquid inlet through a re-circulating circuit. Fresh liquid to be concentrated is also introduced into the re-circulating circuit at a rate sufficient to offset the amount of liquid evaporated in the flow corridor.
    Type: Grant
    Filed: March 31, 2011
    Date of Patent: November 29, 2011
    Assignee: Heartland Technology Partners LLC
    Inventors: Bernard F. Duesel, Jr., Michael J. Rutsch
  • Patent number: 8016977
    Abstract: Dry pond water evaporation systems and methods are used to evaporate large quantities of water from industrial waste water sources, such as water produced by oil and gas wells. Dry pond systems include a water evaporation system that emits waste water into the air as a fine spray or mist to promote evaporation. Water that falls to the ground and any initially dissolved solids are captured in a water capture depression. Water and solids are transferred from the water capture depression to a water collection pool. Water from the water collection pool is recirculated through the water evaporation system to further concentrate the total dissolved solids (TDS). When the TDS are sufficiently concentrated, they may be harvested, such as by evaporating off the water and recovering salts or minerals as a solid.
    Type: Grant
    Filed: March 13, 2009
    Date of Patent: September 13, 2011
    Assignee: Reform Water, LLC
    Inventors: Rodney Rasmussen, Paul C. Cox
  • Patent number: 7988831
    Abstract: A method for purifying an aqueous potassium hydroxide solution having rich silicon impurities has been disclosed in the invention, which is particularly related to a method that utilizes a low-carbon alcohol (such as ethanol) for extracting said aqueous potassium hydroxide solution, and includes the steps of mixing a low-carbon alcohol with an aqueous potassium hydroxide solution having rich silicon impurities; allowing the resulting mixture therefrom to divide into an aqueous phase layer and a low-carbon alcohol phase layer that contains the aqueous potassium hydroxide solution with reduced silicon impurities, and subjecting the low-carbon alcohol phase layer to a separation process for removing the low-carbon alcohol, thereby resulting in an aqueous potassium hydroxide solution having reduced silicon impurities.
    Type: Grant
    Filed: December 19, 2008
    Date of Patent: August 2, 2011
    Assignee: Yeou Fa Chemical Co., Ltd.
    Inventors: Yung Hsiung Hsu, Sage Hsu
  • Publication number: 20110139603
    Abstract: In accordance with one embodiment, a method for treating fractionated water produced by a hydraulic fracturing process is provided. The method includes decanting a fractionated water stream in at least one decanter. The decanter is maintained at a temperature ranging from about 90° F. to about 120° F. The method also includes flashing the decanted water in at least one first flash tank and at least one second flash tank in fluid communication with one another to provide a residual concentrate stream. The first flash tank is operated at a temperature ranging from about 180° F. to about 200° F. and the second flash tank is operated at a temperature ranging from about 140° F. to about 160° F. Both the first flash tank and the second flash tank are maintained at a vacuum pressure. The method also includes evaporating the residual concentrate stream in at least one evaporator kettle to produce a concentrated brine.
    Type: Application
    Filed: September 9, 2010
    Publication date: June 16, 2011
    Applicant: NG INNOVATIONS, INC.
    Inventor: Donald W. Booth
  • Publication number: 20110061816
    Abstract: A compact and portable liquid concentrator includes a gas inlet, a gas exit and a flow corridor connecting the gas inlet and the gas exit, wherein the flow corridor includes a narrowed portion that accelerates the gas through the flow corridor. A liquid inlet injects liquid into the gas stream at a point prior to the narrowed portion so that the gas-liquid mixture is thoroughly mixed within the flow corridor, causing a portion of the liquid to be evaporated. A demister or fluid scrubber downstream of the narrowed portion removes entrained liquid droplets from the gas stream and re-circulates the removed liquid to the liquid inlet through a re-circulating circuit. Fresh liquid to be concentrated is also introduced into the re-circulating circuit at a rate sufficient to offset the amount of liquid evaporated in the flow corridor.
    Type: Application
    Filed: July 29, 2010
    Publication date: March 17, 2011
    Applicant: HEARTLAND TECHNOLOGY PARTNERS LLC
    Inventors: Bernard F. Duesel, JR., Michael J. Rutsch, Craig Clerkin
  • Patent number: 7857940
    Abstract: The present invention relates to a liquid radioactive waste treatment system. The liquid radioactive waste treatment system includes a plurality of evaporation plates and each of the evaporation plates has an uneven surface, in a housing comprised of a glass. A liquid radioactive waste is dispersed via a liquid waste dispersing unit to the evaporation plate, and the liquid radioactive waste is evaporated using solar heat and airflow in the housing.
    Type: Grant
    Filed: December 20, 2006
    Date of Patent: December 28, 2010
    Assignee: Korea Atomic Energy Research Institute
    Inventors: Tae-Kuk Kim, Jong-Sik Shon, Kwong-Pye Hong, Han-Seok Cho
  • Patent number: 7803253
    Abstract: A dehydration method of a water-containing substance using a liquefied matter, including a step (1) of contacting a liquefied matter of a substance which is in a gas phase under a condition at ambient temperature and atmospheric pressure with the water-containing substance, to dissolve contained water in the water-containing substance into the liquefied matter, for obtaining the liquefied matter containing a large amount of water; and a step (2) of vaporizing the substance out of the liquefied matter containing a large amount of water, to thereby separate the substance as the gas from water.
    Type: Grant
    Filed: May 12, 2006
    Date of Patent: September 28, 2010
    Assignee: Central Research Institute of Electric Power Industry
    Inventors: Hideki Kanda, Youichi Urakawa
  • Publication number: 20100230057
    Abstract: Water evaporation devices, systems and methods are used to evaporate large quantities of water from water impoundment ponds or other waste water sources. Water evaporation devices include a water evaporation barrel having an air acceleration chamber that creates venturi suction so as to draw water from a water source into a venturi chamber. Fast moving air and water create fine water droplets within a water atomization chamber, which droplets are then emitted from the water evaporation barrel through a discharge nozzle and into the air as a spray or cloud of fine water droplets. Water evaporation devices and associated systems and methods can be used to efficiently evaporate waster water produced by a wide variety of industrial processes.
    Type: Application
    Filed: March 13, 2009
    Publication date: September 16, 2010
    Applicant: REFORMWATER, LLC
    Inventors: J. Keith Reidhead, Tyson P. Cox
  • Patent number: 7736521
    Abstract: Circulating completion, workover and drilling fluids used in hydrocarbon recovery are filtered after monitoring for viscosity, which frequently causes plugging of filters. A viscometer generates a signal representative of viscosity in the fluid; the signal is used by a programmable controller to divert viscous fluid from the filter, or to take other action to prevent damage to the filter. The viscometer can be used in various positions in the system. Fluids deemed too viscous for the filter can be sent to a viscosity-reducing device, which may be a heating, shear-thinning, or cavitation device, to reduce its viscosity, enabling the fluid to pass through a filter without fouling. After filtering and a return to a lower temperature, the fluid may be treated if necessary to become viscous again for a useful purpose.
    Type: Grant
    Filed: May 21, 2007
    Date of Patent: June 15, 2010
    Assignee: Total Separation Solutions, LLC
    Inventors: Robert L. Sloan, Kevin W. Smith, Harry D. Smith, Jr.
  • Publication number: 20100139871
    Abstract: Dry pond water evaporation systems and methods are used to evaporate large quantities of water from industrial waste water sources, such as water produced by oil and gas wells. Dry pond systems include a water evaporation system that emits waste water into the air as a fine spray or mist to promote evaporation. Water that falls to the ground and any initially dissolved solids are captured in a water capture depression. Water and solids are transferred from the water capture depression to a water collection pool. Water from the water collection pool is recirculated through the water evaporation system to further concentrate the total dissolved solids (TDS). When the TDS are sufficiently concentrated, they may be harvested, such as by evaporating off the water and recovering salts or minerals as a solid.
    Type: Application
    Filed: March 13, 2009
    Publication date: June 10, 2010
    Applicant: REFORMWATER, LLC
    Inventors: Rodney Rasmussen, Paul C. Cox
  • Publication number: 20090294074
    Abstract: The water evaporation system functions to increase the concentration strength of a contaminant solution in wastewater, for more economical disposal. A blower conveys an air stream along an air-conduit, over a nozzle or atomizer. The atomizer converts the incoming dilutely-contaminated water into fine droplets, and injects and distributes the droplets into the airstream. An air-heater is located upstream of the atomizer, and heats the airstream to a temperature of 110° C. at the atomizer. A droplet-collector receives the airstream, and the droplets, and mechanically extracts the liquid droplets from the airstream. The airstream leaves the droplet-collector at 65° C. in a saturated condition. The droplets coalesce, and become the final-water, comprising the strongly concentrated contaminant solution. An exhaust-conduit conveys air that has passed through the droplet-collector to the air-outlet. A heat-exchanger transfers heat from the exhaust airstream into the intake airstream, to supplement the air-heater.
    Type: Application
    Filed: August 12, 2009
    Publication date: December 3, 2009
    Inventor: Talivaldis Forstmanis
  • Patent number: 7604710
    Abstract: A floating water evaporation system for use in disposing of excess water from oil and gas drilling operations is provided. One or more nozzle arrays float on the surface of a wastewater pond a distance away from the pond shoreline. Each nozzle array includes a series of upright risers that extend above a water reservoir tank. Spray nozzles are mounted on each riser. The water reservoir tank is mounted between floating pontoons that elevate the nozzles a distance above the surface of the pond. Water from the pond is pumped through the nozzles to create a patterned spray of small evaporable droplets.
    Type: Grant
    Filed: March 30, 2006
    Date of Patent: October 20, 2009
    Assignee: EvapoRite Systems, Inc.
    Inventors: David J Haslem, Michael E. Dofelmire, Darrin N. Haslem, Michael T. Lawing
  • Patent number: 7591309
    Abstract: An evaporation based method for generation of high pressure steam from produced water in the heavy oil production industry. De-oiled produced water is processed through a high pH/high pressure evaporator driven by a commercial watertube boiler. The vapor produced by the evaporator is suitable for the steam assisted gravity drainage (SAGD) method being utilized by heavy oil recovery installations, without the use of once through steam generators that require extensive chemical treatment, and without requiring atmospheric distillation, which requires high power consuming compressors. Evaporator blowdown may be further treated in a crystallizing evaporator to provide a zero liquid discharge (ZLD) system and, with most produced waters, at least 98% of the incoming produced water stream can be recovered in the form of high pressure steam.
    Type: Grant
    Filed: November 24, 2004
    Date of Patent: September 22, 2009
    Assignee: Aquatech International Corporation
    Inventors: Keith R. Minnich, Mark C. Nicholson, RamKumar Karlapudi, Richard M. Schoen
  • Publication number: 20090218051
    Abstract: Device, system and operation method to perform functions in a semiautomatic manner, which permits the most favorable condition to evaporate a plurality of environmental samples that are diluted in solvents, by means of gas sweeping, preferably nitrogen, and a control electronic system that permits the superficial evaporation of the solvent thanks to exposing a cold sample kept at a constant temperature to a controlled gas flux. Furthermore, safety measures are considered to protect the extract, such as: acoustic and luminous signals that inform when it has been reached a critical moment in the process, reduction of gas flux during the last stage of the evaporation and valves to completely shut off the gas flux if a determined time period is exceeded.
    Type: Application
    Filed: March 15, 2007
    Publication date: September 3, 2009
    Inventors: Francisco Cereceda Balic, Manuel Olivares Salinas, Hector Carrasco Espinosa, Gabriel Cereceda Balic
  • Patent number: 7575656
    Abstract: A system that treats wastewater by subjecting it to a heat source and destroying the microbes present therein and disposes of the wastewater to the atmosphere through evaporation. The components of the system are designed for in-ground or below-grade placement for aesthetic purposes and to eliminate a need for separate structures for housing or enclosing the system. The system does not generate a discharge as part of its regular operation and thus eliminates the need for disposal to an on-site feature or public sewer utility.
    Type: Grant
    Filed: March 20, 2007
    Date of Patent: August 18, 2009
    Inventors: Matthew Glen Moore, William Edgar Moore
  • Patent number: 7572352
    Abstract: Salt-containing water is desalinated by first passing salt-containing water through a heat exchanger disposed in a basin containing solar-heated brine formed by several layers of water lying one above the other in the basin, each of the layers of water forming the brine having a higher salt content than the layer present there above. The heat exchanger is in the lowermost layer of water having a higher temperature than the temperature of the layers of water lying above the lowermost layer of water. The salt-containing water is heated in the basin by solar energy indirect heat exchange with the solar-heated brine to obtain heated salt-containing water. At least part of the heated salt-containing water is evaporated to obtain water vapor, and the water vapor is condensed to obtain desalinated water.
    Type: Grant
    Filed: November 26, 2003
    Date of Patent: August 11, 2009
    Inventor: Hans Josef Van Els
  • Patent number: 7566383
    Abstract: A method and system for recovering heat from a pretreated hot biomass stream is described. The method and system for heat recovery includes a flash cooler connected to a direct contact condenser. A liquid portion of the hot biomass stream flashes into vapors upon the hot biomass stream entering the flash cooler. The flashed vapors are transferred to the direct contact condenser. The flashed vapors and an incoming cold biomass stream subsequently come into contact with each other in the direct contact condenser, thereby causing heat to be transferred from the hot biomass stream to the cold biomass stream. As the heat transfer occurs, the flashed vapors condense onto the surface of the cold biomass.
    Type: Grant
    Filed: June 17, 2005
    Date of Patent: July 28, 2009
    Assignee: Purdue Research Foundation
    Inventors: Rollo J. Everett, Nathan S. Mosier, Jerry L. Weiland, Gary Welch, Michael R. Ladisch
  • Patent number: 7540936
    Abstract: An evaporator for receiving waste fluid stream and producing separate streams of an evaporated fluid and a condensate liquid for use in industrial waste treatment has a curved pathway bounded by a casing having an inlet port through which the waste fluid enters the casing. The casing defines a pathway having a flow direction therein through which the waste fluid stream flows, and within which casing the evaporated fluid is produced. The casing has a drain beneath the pathway through which the condensate passes, and an outlet through which the evaporated fluid is drawn. A series of fins of elongate aerofoil cross-section are located in and extend across the pathway in the flow direction of the waste fluid stream flowing along the pathway. The casing is curved and the fins are arranged parallel to a tangent of the curve.
    Type: Grant
    Filed: September 6, 2002
    Date of Patent: June 2, 2009
    Assignee: Industrial Waste Treatment Limited
    Inventor: Richard Lilleystone
  • Publication number: 20090090473
    Abstract: A vessel-based system and method for disposing of wastewater including bilge water from a bilge of the vessel. The system comprising a treatment unit for receiving and treating the wastewater to produce a substantially oil-free treated water and, an evaporator for receiving the treated water from the treatment unit. The evaporator comprising an evaporation element for transferring heat to the treated water to evaporate the treated water.
    Type: Application
    Filed: October 3, 2007
    Publication date: April 9, 2009
    Inventors: Ian Fielding, John Moriarty
  • Patent number: 7513972
    Abstract: The present invention discloses a comprehensive, efficient, and cost effective portable evaporator unit, method, and system for the treatment of brine. The evaporator unit, method, and system require a pretreatment process that removes heavy metals, crude oil, and other contaminates in preparation for the evaporator unit. The pretreatment and the evaporator unit, method, and system process metals and brine at the site where they are generated (the well site). Thus, saving significant money to producers who can avoid present and future increases in transportation costs.
    Type: Grant
    Filed: May 21, 2004
    Date of Patent: April 7, 2009
    Assignee: Hart Resource Technologies, Inc.
    Inventors: Paul John Hart, Bruce G. Miller, Ronald T. Wincek, Glenn E. Decker, David K. Johnson
  • Publication number: 20090025885
    Abstract: The invention relates to an evaporation apparatus for depositing material on a vertically oriented substrate (10). The apparatus comprises at least one evaporation crucible (100) with the evaporation crucible (100) having an evaporation surface (120) for evaporating the material (300) wherein the evaporation surface is inclined at an inclination angle (?) in relation to the horizontal. The invention further provides a method for evaporating a substrate with the steps of providing a vertically oriented substrate (10); providing a crucible having an evaporation surface (120) for evaporating a material; evaporating the material on the evaporation surface (120) that is inclined at an inclination angle (?) in relation to the horizontal.
    Type: Application
    Filed: July 17, 2008
    Publication date: January 29, 2009
    Applicant: APPLIED MATERIALS, INC.
    Inventors: Wolfgang BUSCHBECK, Michael KOENIG, Stefan KELLER, Stefan BANGERT
  • Publication number: 20090020232
    Abstract: A mobile waste processing system and method is disclosed for processing materials in a tank, typically an underground storage tank. A mobile fluid processing module is disposed adjacent to or over the tank, and sealingly connected to the tank through a tank riser. Support equipment, which may include an electric power module, a chiller module, a heating module, and a control and monitor module, are disposed a distance from the processing module, and connected thereto. A pump and optionally a dispersal nozzle are deployed from the processing module into the tank, and effluent is extracted for processing. The processing trailer includes effluent processing equipment such as an evaporator and demister, condenser, vacuum pump, and interim storage tank. The effluent is processed, and at least a portion is removed. Some of the processed effluent may be returned to the tank.
    Type: Application
    Filed: July 17, 2007
    Publication date: January 22, 2009
    Applicant: COLUMBIA ENERGY & ENVIRONMENTAL SERVICES, INC.
    Inventors: Stephen Wolfe, Brian Brendel
  • Patent number: 7442348
    Abstract: A sulfur-bearing residue treatment system is provided for the recovery of valuable organic components and the reduction of capital costs and operating costs. The treatment system involves the use of a stripping vessel in conjunction with a heating apparatus. All elements of the treatment system may be coupled together to form one integral piece of equipment.
    Type: Grant
    Filed: June 17, 2005
    Date of Patent: October 28, 2008
    Assignee: Rohm and Haas Company
    Inventors: Curtis Instad Carlson, Jr., Michael Stanley DeCourcy, Jamie Jerrick John Juliette, Thomas Albert Kaminski, Nelson Ivan Quiros, Paul Benjamin Schladenhauffen
  • Publication number: 20080190567
    Abstract: The present invention is directed to methods for removing CO2 from air, which comprises exposing sorbent covered surfaces to the air. The invention also provides for an apparatus for exposing air to a CO2 sorbent. In another aspect, the invention provides a method and apparatus for separating carbon dioxide (CO2) bound in a sorbent.
    Type: Application
    Filed: March 15, 2006
    Publication date: August 14, 2008
    Inventor: David J. Winsness
  • Patent number: 7396433
    Abstract: The process separates oil and water from a sludge mixture by directing the sludge mixture into a rapidly rotating friction dryer having a cylindrical chamber with a smooth inner surface and a rotating rotor having rotor arms extending into closely spaced relation to the inner surface of the chamber. The rotor is rapidly rotated to form an annular bed of the sludge material while moving the material particles in the mixture axially and tangentially and while frictionally generating heat between the rotor arms and the sludge material sufficient to evaporate the water in the sludge material to steam. At the same time, the oil in the mixture is heated by the steam and evaporated at a temperature below the normal atmospheric boiling point of the oil. Thereafter, the separated evaporated oil and the steam are removed from the chamber.
    Type: Grant
    Filed: May 16, 2002
    Date of Patent: July 8, 2008
    Assignee: Thermtech AS
    Inventor: Asbjørn Strand
  • Patent number: 7384501
    Abstract: A method for the preparation of pulp by means of alkaline cooking, in which method spent liquor is transferred to pressurized tanks, and at least one liquor is expanded corresponding to a temperature difference of 1 to 5° C. The generated steam is led to turpentine recovery. Thus, the removal of turpentine and gases dissolved in said liquor is effective, the amount of recovered turpentine increases, and pulp of better washability and higher quality is obtained.
    Type: Grant
    Filed: December 20, 2000
    Date of Patent: June 10, 2008
    Assignee: Metso Paper Pori Oy
    Inventors: Päivi Uusitalo, Mikael Svedman, Jukka Vaistomaa, Hannu Haaslahti
  • Publication number: 20080110577
    Abstract: In one aspect of the invention, a method and related system efficiently and effectively recover a significant amount of valuable, useable oil from byproducts formed during a dry milling process used for producing ethanol. The method may include forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct using a multi-stage evaporator, as well as recovering the oil before the final stage of the evaporator. Further, the step of recovering oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil.
    Type: Application
    Filed: September 17, 2007
    Publication date: May 15, 2008
    Inventor: David J. Winsness
  • Publication number: 20080099154
    Abstract: A process for treatment of an aqueous stream to produce a low solute containing distillate stream and a high solute/solids containing blowdown stream utilizing a method to increase the efficiency of an evaporator while providing an essentially scale free environment for the heat transfer surface. Multi-valent ions and non-hydroxide alkalinity are removed from aqueous feed streams to very low levels and then the pH is increased preferably to about 9 or higher to increase the ionization of low ionizable constituents in the aqueous solution. In this manner, species such as silica and boron become highly ionized, and their solubility in the concentrated solution that is present in the evaporation equipment is significantly increased. The result of this is high allowable concentration factors and a corresponding increase in the recovery of high quality reusable water with essentially no scaling.
    Type: Application
    Filed: October 17, 2003
    Publication date: May 1, 2008
    Inventors: Keith R. Minnich, Ramkumar Karlupudi, Richard M. Schoen
  • Patent number: 7291270
    Abstract: A process is disclosed that relates to the removal of impurities and the recovery of a mother liquor and wash filtrate from an oxidizer purge stream produced in the synthesis of carboxylic acid, typically terephthalic. More particularly, the process involves the removal of impurities and the recovery of a mother liquor and wash filtrate from an oxidizer purge stream and then routing the mother liquor and or wash filtrate to an oxidation zone.
    Type: Grant
    Filed: October 28, 2004
    Date of Patent: November 6, 2007
    Assignee: Eastman Chemical Company
    Inventors: Philip Edward Gibson, Kenny Randolph Parker, Howard Wood Jenkins, Jr.
  • Patent number: 7282151
    Abstract: A process is disclosed that relates to the recovery of a metal catalyst from an oxidizer purge stream produced in the synthesis of carboxylic acid, typically terephthalic. More particularly, the process involves recovery of a metal catalyst from an oxidizer purge stream through the use of a pressure filter, the combining of water with a mother liquor to recover the metal catalyst and then subjecting an aqueous mixture so formed to a single stage extraction with an extraction solvent to produce an extract stream comprising organic impurities and a raffinate stream comprising the metal catalyst.
    Type: Grant
    Filed: June 23, 2004
    Date of Patent: October 16, 2007
    Assignee: Eastman Chemical Company
    Inventors: Kenny Randolph Parker, Robert Lin
  • Patent number: 7214290
    Abstract: In the methods for treatment of caustic effluents described in the specification, a spent caustic refinery effluent is supplied to a submerged combustion gas evaporator in which hot combustion gas containing carbon dioxide is injected into the caustic liquid to concentrate the liquid and convert a hydroxide constituent to a carbonate. Where the caustic effluent is from a petroleum refinery, oil in the waste liquid is separated from the aqueous constituent before, during or after concentration.
    Type: Grant
    Filed: September 4, 2002
    Date of Patent: May 8, 2007
    Assignees: Shaw Liquid Solutions LLC., GEI Liquid Solutions LLC.
    Inventors: Bernard F. Duesel, Jr., John P. Gibbons, Michael J. Rutsch
  • Patent number: 7189328
    Abstract: A method for separating dissolved materials, including organic and inorganic solids and volatile constituents, from a liquid or aqueous solvent is disclosed. The method first extracts water from the flow stream being treated using a crystallization apparatus which freezes the water onto a continuous loop wire rope and withdraws the wire rope from the chamber containing the feed stream. The resultant concentrated solution is then subjected to a different process of evaporation by heating at reduced pressures resulting in the efficient separation of the materials in solution from the liquid medium while conserving energy. This procedure is considered highly effective in allowing for the concentration of the materials and then the extraction of the materials in solution and the recycling and reuse of the water or other liquid.
    Type: Grant
    Filed: June 25, 2004
    Date of Patent: March 13, 2007
    Assignee: Eau-Viron Incorporated
    Inventor: James A. Titmas
  • Patent number: 7097736
    Abstract: A process and apparatus for recycling dairy wastewater wherein the wastewater is supplied to at least one first evaporation apparatus to produce a water distillate and sludge. The sludge is then supplied to at least one second evaporation apparatus arranged in series with the first evaporation apparatus. The process results in recycled water and a final sludge.
    Type: Grant
    Filed: November 30, 2000
    Date of Patent: August 29, 2006
    Assignee: Alfa Laval Corporate AB
    Inventors: Torsten Jonsson, Jan Hellstrom, Helena Eliasson, Lars-Ola Myrefelt
  • Patent number: 7022242
    Abstract: Use and reduction of wastewater or “pond water” created by the wet-process phosphoric acid manufacturing there is created a large amount of wastewater or “pond water” to substantially reduce or eliminate the discharge of pond water with contaminants to the environment. By partially treating pond water with known industry standard processes and using the treated pond water for use as required makeup or cooling water in an electric power generator or any other Industry requiring makeup, cooling or process water will substantially reduce or eliminate the need for the phosphoric acid manufacturers to discharge the contaminated water to the environment and reduce the quantity of fresh water that would normally be required by these other industries using the treated pond water for cooling or makeup water.
    Type: Grant
    Filed: April 14, 2003
    Date of Patent: April 4, 2006
    Inventor: Richard Edwin Sacchi
  • Patent number: 7020980
    Abstract: A method of treating a waste stream comprises a vacuum treatment to promote disintegration of the waste material by “flash vapor” production, causing a swiftly vaporizing fraction inside the material to literally explode or shred apart the matrix of the material as a whole. A main processor operates at a level of vacuum that determines a given boiling temperature for a vaporizing fraction, and one which lower than the fraction's boiling temperature for the local vicinity's barometric pressure (eg., atmospheric pressure). The input stream is pre-heated to above the given boiling temperature for that fraction as determined by the main processor's vacuum level without, however, going over the boiling temperature for the local barometric pressure. It is then introduced into the vacuum of the main processor whereby a minor percentage of the vaporizing fraction flashes into vapor, and this presumptively promotes destruction and/or disintegration of the material.
    Type: Grant
    Filed: January 2, 2004
    Date of Patent: April 4, 2006
    Assignee: Micronics, L.L.C.
    Inventors: Randall G. Adams, Marshall R. Franklin
  • Patent number: 7008516
    Abstract: According to a method of desalinating sea water, sea water sampled from deep sea is injected into a decompression chamber of a reduced pressure tank having a steam chamber, steam at an atmospheric pressure superheated to a boiling temperature or higher by high-frequency heating is supplied to the steam chamber at a surrounding of the decompression chamber at an interval of a heat conducting wall therebetween, water in the sea water is evaporated by heating sea water in the decompression chamber and the evaporated water is condensed to thereby provide fresh water. Concentrated sea water remains in the decompression chamber and therefore, the method can be utilized also as a method of concentrating sea water. Salt can be obtained by further evaporating the water of the concentrated sea water as necessary.
    Type: Grant
    Filed: September 26, 2002
    Date of Patent: March 7, 2006
    Inventors: Yoshinobu Kozuka, Yoshimasa Shimbo
  • Patent number: 6955743
    Abstract: The invention relates to a process for recovering and producing chemicals in a pulp production process where organic chemicals, such as formic acid and acetic acid, are used as cooking chemicals. The process of the invention is based on regeneration of cooking acids and formation of additional cooking acids and furfural by evaporating the cooking liquor and then separating acetic acid, formic acid, furfural and water. The separation is preferably carried out by distillation using the furfural formed in the process as a distilling aid in the distillation.
    Type: Grant
    Filed: December 28, 2001
    Date of Patent: October 18, 2005
    Assignee: Chempolis Oy
    Inventors: Esa Rousu, Pasi Rousu, Juha Anttila, Juha Tanskanen, Päivi Rousu
  • Patent number: 6946055
    Abstract: An organic solvent is separated from a waste stream containing supercritical CO2, an organic solvent and etchant contaminants. The process includes separating the supercritical CO2 by subjecting the waste stream to elevated temperature and/or reduced pressure to thereby obtain a first composition containing the supercritical CO2 and a second composition containing the organic solvent and being substantially free of the supercritical CO2; and then removing non-volatile etching contaminants from the second stream search as by at least one of the following: evaporation; distillation; filtration; centrifugation; and settling.
    Type: Grant
    Filed: August 22, 2001
    Date of Patent: September 20, 2005
    Assignee: International Business Machines Corporation
    Inventors: Anilkumar C. Bhatt, Jerome J. Wagner
  • Patent number: 6939444
    Abstract: A sulfur-bearing residue treatment system is provided for the recovery of valuable organic components and the reduction of capital costs and operating costs. The treatment system involves the use of a stripping vessel in conjunction with a heating apparatus. All elements of the treatment system may be coupled together to form one integral piece of equipment.
    Type: Grant
    Filed: June 7, 2002
    Date of Patent: September 6, 2005
    Assignee: Rohm and Haas Company
    Inventors: Curtis Instad Carlson, Jr., Michael Stanley DeCourcy, Jamie Jerrick John Juliette, Thomas Albert Kaminski, Nicole Rendon Koegel, Nelson Ivan Quiros, Paul Benjamin Schladenhauffen, Peter John Schmeidler, Robert R. Maven, William Harry Engle, Jr., Arthur Meisch
  • Patent number: 6923888
    Abstract: The invention relates to a process for treating bleaching liquors from pulping processes based on organic acids. The process is characterized in that inorganic acid, such as nitric acid, phosphoric acid and/or sulphuric acid, is added into a bleaching liquor obtained from the bleaching or a stage closely associated with bleaching, whereby organic acids contained in the bleaching liquor are released into the bleaching liquor. The organic acids are then separated from the bleaching liquor and recycled to the cooking stage to be used as cooking chemicals. The nitrogen-, phosphor- and/or sulphur-containing product thereby produced, from which organic acids have been separated, is recovered to be used as a fertilizer or as raw material for a fertilizer.
    Type: Grant
    Filed: February 27, 2001
    Date of Patent: August 2, 2005
    Assignee: Chempolis Oy
    Inventors: Pasi Rousu, Päivi Rousu, Esa Rousu, Juha Anttila
  • Patent number: 6887345
    Abstract: The present invention relates to a process and a device for evaporating liquids, for example black liquor from cellulose cooking, which contain solid and dissolved substances which are to be concentrated. The liquid is heated to close to boiling temperature in a heat exchanger (1) of the falling-film type. The process is characterized in that the pressure on the liquid side in the falling-film heat exchanger (1) is kept so high that boiling does not take place in this heat exchanger and in that the evaporation takes place, by means of flashing, in a separate expansion tank (7) that has a lower steam.
    Type: Grant
    Filed: November 20, 2001
    Date of Patent: May 3, 2005
    Assignee: Kvaerner Pulping AB
    Inventors: Ismo Hirvonen, Randy Stern
  • Publication number: 20040261952
    Abstract: The present invention discloses a comprehensive, efficient, and cost effective portable evaporator unit, method, and system for the treatment of brine. The evaporator unit, method, and system require a pretreatment process that removes heavy metals, crude oil, and other contaminates in preparation for the evaporator unit. The pretreatment and the evaporator unit, method, and system process metals and brine at the site where they are generated (the well site). Thus, saving significant money to producers who can avoid present and future increases in transportation costs.
    Type: Application
    Filed: May 21, 2004
    Publication date: December 30, 2004
    Inventors: Paul John Hart, Bruce G. Miller, Ronald T. Wincek, Glenn E. Decker, David K. Johnson
  • Patent number: 6821382
    Abstract: A method and apparatus for cleaning condensate, produced during the production of cellulose pulp, including evaporation of spent liquor, utilizing a cleaning plant having several condensers, coupled in series. Process steam from the last evaporation stage and unclean condensate are introduced into a combined stripper/condenser, the process steam and the condensate being brought to flow in opposite directions so that direct heat exchange occurs, resulting in volatile compounds of the condensate being separated and taken up by the steam with simultaneous indirect cooling, resulting in condensation of the main part of the process steam, and the remaining process steam gradually flowing further on, the process steam being successively cooled first resulting in water and turpentine being condensed and collected and subsequently methanol being condensed.
    Type: Grant
    Filed: January 29, 2001
    Date of Patent: November 23, 2004
    Assignee: Papsea AB
    Inventor: Allan Lundgren
  • Publication number: 20040200581
    Abstract: Use and reduction of wastewater or “pond water” created by the wet-process phosphoric acid manufacturing there is created a large amount of wastewater or “pond water” to substantially reduce or eliminate the discharge of pond water with contaminants to the environment. By partially treating pond water with known industry standard processes and using the treated pond water for use as required makeup or cooling water in an electric power generator or any other Industry requiring makeup, cooling or process water will substantially reduce or eliminate the need for the phosphoric acid manufacturers to discharge the contaminated water to the environment and reduce the quantity of fresh water that would normally be required by these other industries using the treated pond water for cooling or makeup water.
    Type: Application
    Filed: April 14, 2003
    Publication date: October 14, 2004
    Inventor: Richard Edwin Sacchi
  • Patent number: 6797125
    Abstract: The present invention relates to a method of treating condensates containing compounds, which are more volatile than water, in an evaporation plant, where liquid, such as effluent liquid from a pulp or paper mill is evaporated in multiple effects and where condensates generated in the evaporation are flashed and purified in a steam stripping column. In the method, the condensates from at least two evaporation effects are combined and flashed together, and the vapor obtained from the flashing is made to contact with a condensate stream to be purified in the stripping column, wherefrom the impurities-containing vapor and the purified condensate stream are discharged.
    Type: Grant
    Filed: November 7, 2002
    Date of Patent: September 28, 2004
    Assignee: Andritz Oy
    Inventors: Risto Honkanen, Jan E Öhman
  • Patent number: 6790313
    Abstract: A method to remove sulfides and other volatile contaminants from liquor vapor condensate in a pulp manufacturing process, where the mentioned liquor vapor condensate is fed into a stripper, which is part of a closed loop system including the stripper, a regenerative thermal oxidization process (RTO) and a SO2 scrubber, in which loop a gas is circulated, preferably air, and such components formed or stripped off, in this loop whereafter the circulating gas is stripped off sulfides and other volatile components from the liquor vapor condensate, whereafter the gas stream is fed into a RTO process, where the stripped off contaminants are combusted are under formation of SO2 and thereafter the SO2 enriched gas is led to a SO2 scrubber, where preferably alkali is used as absorption medium, and thereafter the circulating gas is returned back into the stripper.
    Type: Grant
    Filed: November 9, 2001
    Date of Patent: September 14, 2004
    Assignee: Excelentec Holding AB
    Inventors: Kent K. Sandquist, Olle Wennberg
  • Patent number: 6761799
    Abstract: The present invention relates to a method and an arrangement for use in connection with the combustion of black liquor. In the method the black liquor is concentrated in a multi-effect evaporation plant in order to obtain black liquor at a suitable dry-solids content for combustion and to generate vapor. The concentrated black liquor is taken to be combusted in a recovery boiler, into which combustion air is fed at several levels for the combustion process. It is a characteristic feature of the invention that the air fed to at least one air level is preheated by using vapor generated in the concentration of the black liquor as heat source.
    Type: Grant
    Filed: March 19, 2001
    Date of Patent: July 13, 2004
    Assignee: Andritz Oy
    Inventor: Petri Tikka
  • Publication number: 20040108196
    Abstract: This invention relates to a system for distilling liquor. The system is multilayer and has devices including a top layer, a middle layer, a bottom layer and an outer cooling assembly and four units correspondingly arranged in those devices. The layers all have inner walls made of thermal-conductive and anti-corrosive material. The four units are a heating unit, a cracking unit, a purifying distilling unit and a cooling unit. The heating unit boils water to generate heating steam. The heating steam is introduced into the cracking unit to heat alcoholic paste to generate liquor steam.
    Type: Application
    Filed: December 1, 2003
    Publication date: June 10, 2004
    Inventor: Ching-Piau Lai
  • Patent number: 6712882
    Abstract: A process for treating waste water from an industrial process for producing propylene oxide, which process involves the steps of: (a) subjecting the waste water to a multi-effect evaporation treatment resulting in a vaporous top fraction and a liquid bottom fraction containing the non-volatile contaminants; and (b) condensing at least part of the vaporous top fraction into a liquid stream which is subject to a stripping treatment resulting in an overhead stream containing volatile waste organic material and purified water as the liquid bottom stream.
    Type: Grant
    Filed: April 26, 2002
    Date of Patent: March 30, 2004
    Assignee: Shell Oil Company
    Inventors: Johan Hendrik De Bie, Robert Frank Dee, Raymond Lawrence June, Marinus Van Zwienen