Promoting Circulation Patents (Class 159/901)
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Patent number: 5906714Abstract: A method of separating water from an aqueous emulsion using a minimum of energy includes heating the aqueous emulsion in a sump, conveying concentrated emulsion from the sump to a heat exchanger so as to pass therethrough back to the sump, circulating water vapor and non-condensable gases from the sump through a compressor to raise its temperature and passing the heated water vapor and non-condensable gases through the heat exchanger to condense and heat the concentrated emulsion therein and evaporate water therefrom, a thermostat filled with water and water vapor, together with first and second pressure switches respectively communicating with the sump and the external atmosphere and the heat exchanger and the external atmosphere, maintaining a temperature differential between 0.5.degree. and 3.degree. C. between the aqueous emulsion in the sump and the temperature of the compressed water vapor and noncondensable gases.Type: GrantFiled: October 15, 1996Date of Patent: May 25, 1999Assignees: Agro Milj.o slashed. A/S, OHM Electric Co., Ltd.Inventors: Asger Gramkow, Jeppe Christian Bastholm, Finn Erik Christensen
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Patent number: 5809664Abstract: A spout-fluid bed drying system and process is comprised of a spout-fluid bed dryer having a conical shaped lower section provided with a packing of heat exchange particles. A cyclone separator is connected to the top of the dryer with separated particles collected by a receiver connected to the leg of the cyclone. A vapor fan compresses the air-vapor mixture before it goes to the heat recuperator and mixing chamber. A tube-shell type heat exchanger, wherein effluent gases from the vapor fan are preheated with heat exchange with the outcoming high temperature gases. A combustion and incineration chamber wherein a natural gas burner is installed at the top and the high temperature flame is used to incinerate the effluent gases introduced from the annulus channel of the chamber to have the odors and VOCs destroyed.Type: GrantFiled: November 15, 1996Date of Patent: September 22, 1998Assignee: Societe en Commandite Gaz MetropolitainInventors: Robert Legros, Jamal Chaouki, Xiao Tao Bi, Arturo Macchi, Kebir Ratnani
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Patent number: 5772851Abstract: Volatile components are eliminated from polyacrylate melts by distilling off the volatile components by a process in which the volatile components are distilled off under reduced pressure, entraining agents are added to the melts at above 100.degree. C. and the melts are simultaneously circulated.Type: GrantFiled: June 17, 1996Date of Patent: June 30, 1998Assignee: BASF AktiengesellschaftInventors: Jurgen Barwich, Oral Aydin, Ulrich Erhardt, Walter Holtrup
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Patent number: 5730836Abstract: A method for concentrating a clay slurry by subjecting the slurry to indirect heat exchange within a heat exchanger to elevate the temperature of the slurry while specifically suppressing boiling of the liquid within the heat exchanger. The heated slurry is subsequently subjected to a rapid pressure reduction which causes flash evaporation of part of the liquid. The rapid pressure reduction can occur in a separation vessel.Type: GrantFiled: September 26, 1994Date of Patent: March 24, 1998Assignee: Comalco Aluminium LimitedInventors: Christopher Roy Greig, Peter James Tait, Peter John Noble
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Patent number: 5630913Abstract: A water distillation system (10) includes a boiling chamber (11) and a condensation chamber (12). Water is fed via an inlet pipe (13) to a degassing chamber (15) where volatile gases are removed from the water. The water is evaporated in the boiling chamber (11) and vapour is, in turn, condensed in the condensing chamber (12). Distilled water is collected in a water storage tank (30) and is used, with a pump (28) and entrainment device (27), to provide a substantial vacuum within the system (10).Type: GrantFiled: March 14, 1995Date of Patent: May 20, 1997Inventor: Davoud Tajer-Ardebili
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Patent number: 5535877Abstract: A method and apparatus for removing water from a solution of water and glycol solution. The apparatus finds application in recycling of glycol wherein a water and glycol solution having as much as a 95% water content when introduced to the apparatus leaves the apparatus with a water content in the order of 40% to 60%. The glycol concentrator has a packing medium made from glass shards that provide a labyrinth through which air is circulated in one direction and thin streams of glycol are circulated in generally the opposite direction. It is believed that mixing of the thin streams of solution and air flow steams in the labyrinth results in a thin film evaporation process. The glycol concentrator apparatus has reduced energy requirements when compared with a distilling process.Type: GrantFiled: February 28, 1994Date of Patent: July 16, 1996Inventors: Peter d. Eastcott, Nicole A. Truman, Peter Truman
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Patent number: 5494556Abstract: A method of separating a liquid mixture wherein the liquid mixture is heated; the heated liquid mixture is supplied to a pervaporation membrane module to separate a permeable component of the liquid; a portion of non-permeated liquid is circulated through a circulation pipe into a liquid mixture feeding pipe before a heater, and the remaining portion of the non-permeated liquid is extracted to the outside of the system, and wherein the temperature of the liquid in the liquid mixture feeding pipe in which the non-permeated liquid has been mixed with the liquid mixture or in the circulation pipe for the non-permeated liquid, is measured, and when the measured temperature is out of a predetermined range, new supply of the liquid mixture and/or extraction of the non-permeated liquid is stopped.Type: GrantFiled: November 28, 1994Date of Patent: February 27, 1996Assignees: Mitsubishi Chemical Corporation, Mitsubishi Kasei Engineering CompanyInventors: Masaaki Mita, Masumi Hino, Moriyoshi Kudo
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Patent number: 5478443Abstract: An apparatus for extracting, concentrating, and separating biochemical compounds from plant or animal biological substances. It has a heating vessel for the substance to be treated, and is connected at its lower part to an evaporation circuit. The evaporation circuit is connected to the upper part of the heating vessel and, by a valve, to the bottom of a distillation column. A condenser is connected to a vacuum source and, by a valve to the top of the distillation column. A decanter is connected by a valve to the condenser and then successively to a first tank for recovering essential oil, a second tank for recovering aromatic water, and to the vacuum source. A dual discharge circuit has its first circuit connected by two valves to a third tank for receiving light aromatic compounds and to a fourth tank for receiving regenerated solvents.Type: GrantFiled: May 10, 1993Date of Patent: December 26, 1995Inventor: Pierre O. Cogat
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Patent number: 5474653Abstract: A method for use in an evaporator for selectively controlling the flow of solid particles within the evaporator. The method provides for the separation of solids from a liquid through the use of a separation chamber having a plurality of apertures, each of which has a critical size. In the separation chamber, solid particles which are larger than a critical size are separated from the remainder of the solution. The separated particles exit the separation chamber via a bypass conduit for circulation directly to the sump of the evaporator for recombining with the separated liquid portion which passed through the separation chamber and was subsequently concentrated in the heat exchange tubes. The method prevents solid particles from clogging the system and allows for continuous circulation of the solution and solid particles.Type: GrantFiled: June 16, 1994Date of Patent: December 12, 1995Assignee: Ionics, IncorporatedInventor: Joseph J. Bostjancic
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Patent number: 5445714Abstract: A concentrator for reducing the volume of a mixture containing a solvent and various dissolved and/or undissolved solids includes a chamber adapted to receive the mixture and a heater coupled to the chamber for applying heat to the mixture within the chamber, the heat being provided at a temperature sufficient to vaporize the solvent. A condensing tower receives the vapors from the chamber and including a first stage and at least one second stage. A plurality of walls included in each of the first stage and the second stage of the tower direct the vapors along a torturous path including at least one reversal of direction in each of the stages. A coolant is provided to cool the second stage of the tower but not the first stage in order to facilitate condensation of the vapors in the second stage but not in the first stage of the tower. The coolant may include water in order to facilitate the processing of aqueous solutions.Type: GrantFiled: June 20, 1991Date of Patent: August 29, 1995Assignee: Eco Stills, Inc.Inventor: Henry S. Myers
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Patent number: 5439560Abstract: An apparatus for concentrating a photographic processing solution in which there are provided an evaporation chamber, a heater for heating the solution to generate a vapor in the evaporation chamber, a condensation chamber communicated to the evaporation chamber for recieving the vapor, a cooling device for cooling the vapor to generate a condensation, and an ejector for reducing the pressure in the evaporation chamber and the condensation chamber. There is further provided a heat pump having a heat radiating portion used for the heater and a plurality of heat absorbing portions, one of which is used for the cooling device.Type: GrantFiled: September 26, 1994Date of Patent: August 8, 1995Assignees: Konica Corporation, Sanyo Electric Co., Ltd.Inventors: Masayuki Kurematsu, Nobutaka Goto
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Patent number: 5425849Abstract: A film-type evaporator has an upright container, a heating system arranged on the outside of its jacket, a rotor rotating in the container and an upper part with a vapor chamber and droplet separator. In the upper area of the rotor the product is fed onto the inner container wall and runs down in the form of a thin film in which evaporation takes place. Circulation evaporation with a high thickening capacity is made possible in that the container has an unheated lower part constructed as a receiving flask in which the product is collected and a central part with the heating system, on whose inner wall film-type evaporation takes place, and in that the tubular rotor extends into the lower part and is constructed as a circulating pump, which delivers the product from the lower part on the inside of the tubular rotor into its upper area and centrifugally delivers it there to the inner wall of the central part.Type: GrantFiled: April 8, 1992Date of Patent: June 20, 1995Inventor: Vaclav Feres
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Patent number: 5415732Abstract: A method and apparatus for concentration of a flowable foodstuff can be accomplished by supplying a flowable foodstuff into a vaporization chamber as split into a plurality of free nappes and causing the free nappes to run a predetermined distance to release vapor from their surfaces. After covering this distance, the free nappes of flowable foodstuff are collected into a mass at the bottom of the chamber.Type: GrantFiled: April 7, 1992Date of Patent: May 16, 1995Assignee: Rossi & Catelli S.p.A.Inventor: Camillo Catelli
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Patent number: 5389209Abstract: A process for making a light color maple syrup from a water-containing sap. In a first step, the sap is boiled under normal pressure to evaporate part of the water contained therein in the form of steam, to form the maple syrup and to develop caramelized and sweet characteristics and give flavor and a tinted color to this maple syrup. In a second step, the sap is heated at a temperature lower than the boiling temperature of the sap and atomized through an air circulating column to evaporate another part of the water contained therein. This second step which can be carried out before the first one, permits to concentrate the sap, to increase its sugar content and to avoid further caramelization thereof. The sap which is so obtained with an increased sugar content, may be recycled as long as necessary until a desired sugar concentration corresponding to a predetermined Brix number is reached.Type: GrantFiled: January 21, 1993Date of Patent: February 14, 1995Inventor: Yvon A. Paquette
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Patent number: 5376238Abstract: The process of this invention is directed to recovering diluted aqueous latex paint collected during cleaning of latex paint manufacturing equipment. The collected aqueous diluted latex paint is subjected to vacuum evaporation at temperatures between about 120.degree. F. and 170.degree. F. at reduced pressures of at least about 25 inches of mercury vacuum to produce a distillate containing above 99% by weight water and concentrated latex paint reusable as latex paint or as blend in latex paint products.Type: GrantFiled: August 24, 1992Date of Patent: December 27, 1994Assignee: The Glidden CompanyInventor: John G. Zambory
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Patent number: 5334291Abstract: An apparatus for removing non-volatile residues and impurities from a used solvent includes a self-scrubbing heating distillation subassembly for separating purified solvent for reuse and a controlled waste collector subassembly for overflowing concentrated residues and impurities stripped from the used solvent into an easy-to-service container. The apparatus may be disposed in a parallel in-line relationship with a circulating solvent flow circuit, such as in a dry cleaning operation, to continuously withdraw and purify aliquot portions of the circulating solvent stream, returning good solvent back to the flow circuit and concentrating non-volatile residues and impurities to a removable, environmentally sound serviceable container.Type: GrantFiled: July 9, 1993Date of Patent: August 2, 1994Assignee: Safety-Kleen Corp.Inventors: Gilbert Gavlin, William M. Langdon, deceased, Boris Goltsin, Gunther Erlebacher, Douglas A. Larson
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Patent number: 5316628Abstract: A process for simultaneously exchanging material and for exchanging heat, material change being effected between a gas phase and at least one liquid phase by contact and passage in opposite directions of the gas phase and of the at least one liquid phase and heat exchange being effected between a compartment (I) and another compartment (II). In compartment (I) a plurality of spacer plates defining material exchange passages are arranged and the material exchange is effected by causing the at least one liquid phase to flow over a substantially vertical or inclined wall of a corrugated spacer plate having perforations and by causing at least a fraction of the gas phase to traverse simultaneously said perforations in a substantially ascending direction to contact said at least one liquid phase. The heat exchange is effected by circulating a heat exchange fluid in the compartment (II) which has a common wall with the compartment (I).Type: GrantFiled: April 24, 1991Date of Patent: May 31, 1994Assignee: Institut Francais du PetroleInventors: Jean-Claude Collin, Joseph Larue, Alexandre Rojey, Jean-Charles Viltard
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Patent number: 5312524Abstract: A distillation system for recovery of volatile components of contaminated liquids used in an industrial process includes a tube assembly including outer tubes to which hot bottoms liquids are supplied and inner tubes to which process liquids are supplied for transfer of heat from the bottoms to the process liquids. From the tube assembly the two liquids are discharged into the still through separate, elongated, parallel discharge pipes. The process liquids discharge pipe is positioned above the bottoms liquids discharge pipe and an elongated, metal, angle plate is positioned as an inverted V between the two discharge pipes. Efficiency is improved over prior systems wherein process liquids are added to the still without being preheated by the bottoms fluids, and without the unique still intake manifold.Type: GrantFiled: April 21, 1992Date of Patent: May 17, 1994Assignee: Filter Tech, Inc.Inventor: Lyle B. Barcomb
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Patent number: 5294302Abstract: A device for collecting evaporated matter from a vat which first collects the evaporated matter and then condense the evaporated matter into a liquid which is recovered and recycled.Type: GrantFiled: November 7, 1991Date of Patent: March 15, 1994Inventors: Raymond R. Colton, Raymond R. Gamby, George Spector
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Patent number: 5265432Abstract: An oil purification apparatus for use in conjunction with a refrigeration system. The oil purification apparatus includes an isolation tank for receiving a quantity of contaminated oil from the refrigeration system and holding the oil isolated from the refrigeration system. A separation system including a heater and an agitation mechanism reclaims refrigerant contaminant entrained in the oil. A vapor loop selectively conveys the reclaimed refrigerant from the oil purification apparatus to the refrigeration system.Type: GrantFiled: September 2, 1992Date of Patent: November 30, 1993Assignee: American Standard Inc.Inventors: Gary L. Luepke, Allen J. Dietrich
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Patent number: 5259931Abstract: A system for removing volatile constituents (e.g., hydrocarbons) from a liquid (e.g., water) containing the same by which there is a continuous countercurrent contact between the liquid and a forced air flow. Water collected in a reservoir is continuously pumped to the top of a stripping tower where it is dispersed downwardly over packing material. A blower forces air upwardly in the tower so as to remove the volatile constituents that exit the tower with the exit air. Since the water flow is continuous, multiple passes occur through the tower to enhance separation efficiency. Water from the base of the tower returns to the reservoir via overflow from a standpipe. A lower liquid level sensor in the reservoir initiates operation of the water pump to the tower, and an upper liquid level sensor initiates operations of another pump for pressure discharge from the base of the tower to an exterior site.Type: GrantFiled: February 3, 1992Date of Patent: November 9, 1993Inventor: James R. Fox
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Patent number: 5256251Abstract: A continuous evaporation process for drying water-wet waste solids and sludges, using a paraffin oil solvent, until the waste is dried to a near-zero wastewater product, without experiencing sticky solids. The invention involves (1) mixing the input solids or sludges with a paraffin oil solvent, (2) feeding the mixture into two or more stages of evaporation in parallel to evaporate some of the water present in the input solids or sludges and to extract some of the indigenous solvent-soluble compounds from the solids, (3) feeding the slurry from the parallel stages of evaporation to one or more final evaporation stages in series, and (4) feeding the slurry from the final stages of evaporation to a centrifuge or other device for separating most of the solvent from the solids.Type: GrantFiled: June 10, 1991Date of Patent: October 26, 1993Assignee: Hanover ResearchInventor: Thomas C. Holcombe
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Patent number: 5250151Abstract: An evaporation assembly for concentrating liquids having an evaporation area for conveying a liquid to be concentrated and a heating system for heating and concentrating the liquid conveyed through the evaporation area. The evaporation area includes a liquid inlet for introducing liquid to be concentrated into the evaporation area, and a liquid and vapor outlet for conveying the liquid through the evaporation area. A vapor circulating system is coupled between the liquid inlet end and the liquid and vapor outlet of the evaporation area for increasing the velocity of the liquid to be concentrated for impeding or removing precipitated particles or deposits from the heat exchange surfaces.Type: GrantFiled: March 6, 1992Date of Patent: October 5, 1993Inventor: Joaquin Huercanos
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Patent number: 5242548Abstract: An improved distillation device (1) which uses a combination of centrifugal and positive displacement pumps to purify raw liquid in an area of limited space. The device (1) includes evaporation assembly (2) having a boiling chamber (5), a valve and float switches (15, 16, 17) for maintaining the liquid level (20) in the boiling chamber (5) at a predetermined level, and connecting conduit (21) for directing vapor to a condensation apparatus (3). The condensation assembly (3) includes a condensation chamber (6), a collection chamber (7), and at least one bubble tube (22) connecting the two chambers (6, 7). Leading from the collection chamber (7) is first transfer conduit (50), a tube (51) for permitting vapor to bleed from the collection chamber (7) back to condensation chamber (6), and second transfer conduit (52) for returning only distillate from collection chamber (7) to condensation chamber (6) to cool condensation chamber (6).Type: GrantFiled: January 4, 1993Date of Patent: September 7, 1993Inventor: Philip G. Youngner
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Patent number: 5207869Abstract: A liquid waste reduction system uses an evaporator having two packed columns. A reservoir of the evaporator has three level sensor which monitor the fluid level in the reservoir. An input pump delivers waste liquid to the reservoir. When the fluid level has exceeded a low level, a control unit powers an output pump which pumps liquid from the base of the reservoir to an external storage unit. A distributor pump pumps liquid from the reservoir to the top of the packed columns. A blower forces air upward through the packing material to evaporate water from the liquid. When the fluid level has exceeded a high level, the control unit switches on a heating element which heats the air delivered from the blower to the second packed column, thus accelerating the evaporation process. When the fluid level has exceeded the maximum level, the control unit deactivates the input pump to prevent flooding of the evaporator unit.Type: GrantFiled: February 20, 1991Date of Patent: May 4, 1993Assignee: Clivus Multrum, Inc.Inventors: H. David Harmoning, Guy Marchesseault
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Patent number: 5205906Abstract: A process is presented for the treatment of wastewater containing non-volatile pollutants and volatile chemically oxidizable organic and inorganic pollutants. The process combines efficient evaporation to concentrate the non-volatile compounds and a catalytic oxidation reaction to convert the volatilized organic and inorganic pollutants. A condensate product may be obtained by treating wastewater according to the inventive process that is of distilled water quality and substantially free of minerals and organics.Type: GrantFiled: February 11, 1991Date of Patent: April 27, 1993Assignee: Chemical Waste Management, Inc.Inventors: James F. Grutsch, George A. Mortimer
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Patent number: 5198076Abstract: A low-pressure desalinization in a water chamber having an open end submerged in a water supply such as an ocean. An air exhaust pump draws air out of the water chamber to lower the surface tension of an upper stratum of water, which is thereby converted to vapor and subsequently condensed to nonsalinated water and collected in a U-shaped trap with a pair of sealing, closable valves. Moreover, a velocity enhancing parabolic channel is included for efficiently utilizing the potential energy of the fresh water. The fresh water is conveyed from its height at the top of the water chamber to a turbine via a velocity enhancement parabolic channel which enhances the velocity of the water for the turbine. The desalinator also includes a plurality of strips of sheeting partially immersed in the water being desalinated and drawing water therefrom via capillary action to increase the surface area of the water being subjected to the vacuum.Type: GrantFiled: July 29, 1991Date of Patent: March 30, 1993Assignee: Bowpec IncorporatedInventor: Peter M. Borgren
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Patent number: 5174864Abstract: Controlled heating unit for extracting solvent from sludge by distillation, in particular for dry-cleaning machines, having a sludge tank with a flattened shape which is arranged at the base of a sealed box-like chamber and above which inlets for microwaves generated by a microwave source are present, a mixer for the sludge to be treated, at least one sludge temperature sensor which switches off the microwave source when the sludge reaches a temperature which is proximate to the degradation temperature of the solvent.Type: GrantFiled: October 16, 1990Date of Patent: December 29, 1992Assignee: Sodibo S.p.A.Inventors: Tommaso Arbizzani, Gualtiero Ghelardini
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Patent number: 5160580Abstract: An evaporating process that alternate between different modes of operation, according to the characteristics of the product handled; the product is either force fed into the tube nest, or cascaded through it in a free-falling film.Type: GrantFiled: January 3, 1990Date of Patent: November 3, 1992Assignee: Fenco S.p.A.Inventor: Carlo Sassi
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Patent number: 5156706Abstract: A vertical tube evaporation process for the concentration of saline water and other liquids, including the addition of an anionic mono-molecular dispersant thereto which interacts with materials precipitated during concentration and inhibits the formation of scale or fouling depositions on evaporator surfaces, and wherein the additive is incorporated into the precipitated materials and improves their removal during the descaling or defouling of evaporator surfaces by rendering such precipitates redispersable in fresh water or in a non-saturated liquid used for descaling or defouling of evaporator surfaces.Type: GrantFiled: April 29, 1988Date of Patent: October 20, 1992Inventor: Hugo H. Sephton
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Patent number: 5116473Abstract: An apparatus for use in an evaporator for selectively controlling the flow of solid particles within the evaporator. The apparatus includes a separation chamber having a plurality of apertures, each of which has a critical size. In the separation chamber, solid particles which are larger than a critical size are separated from the remainder of the solution. The separated particles exit the separation chamber via a bypass conduit for circulation directly to the sump of the evaporator for recombining with the separated liquid portion which passed through the separation chamber and was subsequently concentrated in the heat exchange tubes. The apparatus prevents solid particles from clogging the system and allows for continuous circulation of the solution and solid particles.Type: GrantFiled: October 12, 1990Date of Patent: May 26, 1992Assignee: Resources Conservation Co.Inventor: Joseph J. Bostjancic
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Patent number: 5102504Abstract: A device for solvent recovery in an ultrasonic cleaning machine is based on utilization of the negative pressure originating from the liquification of the solvent vapor itself in a heat exchanger and the negative pressure from an ejector. Thus, the solvent vapor in a vapor zone is led out of a distillation vessel, cooled outside of the vessel, liquidfied, once again returned to a solvent vessel and, at the same time, the liquification of the solvent vapor which is incompletely liquified from this cooling and liquification process is accelerated even more in the negative pressure section of the ejector. Accordingly, the amount of water mixed into the recovered solvent is extremely reduced so that satisfactory cleaning in the ultrasonic cleaner can be ensured.Type: GrantFiled: July 12, 1990Date of Patent: April 7, 1992Inventor: Tetsuya Saito
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Patent number: 5082535Abstract: An apparatus for dissolving oil or PCB which exists in the electrical insulation of parts to be cleaned, wherein a solvent is evaporated during a heating phase by an evaporator located with the parts in an autoclave. The solvent vapor condenses on the parts and penetrates into the electrical insulation to form an oil or PCB-solvent mixture. The apparatus provides for a plurality of intermediate pressure reductions which are carried out in the autoclave, and during each intermediatre pressure reduction the solvent is simultaneously evaporated from the oil or PCB-solvent mixture, directly from the autoclave. That is, during each of the pressure reductions, the solvent supply is discontinued and the mixture circulated through a circulating line. Following the completion of each intermediate pressure reduction, the pure oil or PCB present in a condensate vessel is pumped out by an intermediately located feed pump through a connecting line and into a reservoir.Type: GrantFiled: December 6, 1990Date of Patent: January 21, 1992Assignee: Micafil, AGInventors: Gustav Oesch, Paul Gmeiner, Urs Hofer
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Patent number: 5047124Abstract: An apparatus for feeding gas into a heated saline solution for pressure measurement or to pump this solution. The gas is introduced into the solution through a gas bubbling-in pipe having a gas outlet opening. The gas is heated prior to being introduced into the solution and is charged with moisture until the saturation of the gas comes close to or corresponds to the saturation conditions in the solution at the gas outlet opening. This minimizes clogging by crystallization at the feeder pipes carrying the measuring or purge gas.Type: GrantFiled: July 26, 1989Date of Patent: September 10, 1991Assignee: Deutsche Gesellschaft fur Wiederaufarbeitung von Kernbrennstoffen mbHInventor: Karlheinz Haberland
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Patent number: 5000821Abstract: An apparatus for use in an evaporator for selectively controlling the flow of solid particles within the evaporator. The apparatus includes a separation chamber having a plurality of apertures, each of which has a critical size. In the separation chamber, solid particles which are larger than a critical size are separated from the remainder of the solution. The separated particles exit the separation chamber via a bypass conduit for circulation directly to the sump of the evaporator for recombining with the separated liquid portion which passed through the separation chamber and was subsequently concentrated in the heat exchange tubes. The apparatus prevents solid particles from clogging the system and allows for continuous circulation of the solution and solid particles.Type: GrantFiled: May 25, 1988Date of Patent: March 19, 1991Assignee: Resources Conservation CompanyInventor: Joseph J. Bostjancic
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Patent number: 4981555Abstract: The solutions are concentrated by multiple-effect evaporation in indirectly heated evaporators. The highest concentration of the solution is reached in a final evaporator stage, which is heated with live steam. The final evaporators stage includes two to four falling-film evaporators, all of which are heated with live steam. The falling-film evaporators are consecutively flown through by the solution. Vapor is withdrawn from that falling-film evaporator which is the first to be supplied with the solution and at least part of said vapor is directly contacted with the solution as it flows down through the heating zone of at least one other evaporator of the final stage. From that falling-film evaporator of the final stage which is the first to be supplied with the solution the vapor may be fed to all other evaporators of the final stage.Type: GrantFiled: September 21, 1989Date of Patent: January 1, 1991Assignee: Metallgesellschaft AGInventors: Klaus Hohmann, Manfred Mai
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Patent number: 4976825Abstract: A process for recovering N-methylpyrrolidone contained in an N-methylpyrrolidone-containing liquid formed in the process for preparing a polyarylene thioether by the dehalogenosulfidation of a dihalogeno-aromatic compound and an alkali metal sulfide in the presence of N-methylpyrrolidone as the polymerization solvent, which comprises (a) subjecting the N-methylpyrrolidone-containing liquid to distillation to distill and recover the majority of contained N-methylpyrrolidone while recovering a distillation residue having such a flowability that flow transferring of the distillation residue is possible, and (b) supplying the distillation residue to an air-tight mixer for a highly-viscous fluid, which has a vent and is provided with a heater, to treat the distillation residue under the conditions of a temperature in the mixer of 190.degree. to 310.degree. C.Type: GrantFiled: June 23, 1989Date of Patent: December 11, 1990Assignee: Kureha Kagaku Kogyo Kabushiki KaishaInventors: Takao Iwasaki, Katsumi Horikoshi, Yuzo Yoshiji
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Patent number: 4959122Abstract: An apparatus for treating a photographic process waste liquor in which the photographic process waste liquor stored in an evaporating device is heated and concentrated by evaporation with use of a heating device provided in the evaporating device, in that the evaporating device is provided with a precipitate separating device capable of separating a precipitate generated in a concentrated liquid to be formed through concentration by evaporation; a circulation system to feed again the concentrated liquid to the evaporating device through the precipitate separating device; and a discharging device for discharging the precipitate separated at the precipitate separating device.By use of the apparatus for treating photographic process waste liquor, thermal decomposition of the precipitate generated by concentration by evaporation of the photographic process waste liquor and generation of bad odor can be inhibited.Type: GrantFiled: October 26, 1988Date of Patent: September 25, 1990Assignee: Konica CorporationInventors: Masayuki Kurematsu, Shigeharu Koboshi, Nobutaka Goto, Naoki Takabayashi
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Patent number: 4944839Abstract: A falling film evaporator in which some plate elements have their upper portions surrounded by a hood to prevent feed liquor from contacting hot vapor generated in the evaporator and exchanging heat therewith by direct contact. Other elements are located outside the hood.Type: GrantFiled: May 30, 1989Date of Patent: July 31, 1990Assignee: Rosenblad CorporationInventor: Axel E. Rosenblad
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Patent number: 4927494Abstract: A high pressure evaporation vessel which is operated at a predeterminate pressure above atmospheric pressure, is connected to a low pressure expansion vessel which is operated at a predeterminate pressure below the pressure prevailing in the high pressure evaporation vessel, through a U-shaped siphon tube. The U-shaped siphon tube contains a liquid column absorbing the pressure difference existing between the high pressure evaporation vessel and the low pressure expansion vessel.Type: GrantFiled: June 2, 1988Date of Patent: May 22, 1990Assignee: Sulzer-Escher Wyss AGInventors: Robert Winkler, Siro Sala, Takayuki Kobayashi, Shinjiro Yokota
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Patent number: 4925526Abstract: A falling film evaporator having vertical outer tubes with closed upper ends connected to an upper tube plate disposed in the lower region of the evaporator. Other parallel tubes are disposed inside the outer tubes and are connected to a lower tube plate under the upper tube plate. The evaporator also has a mechanism for distributing the material to be evaporated onto the upper ends of the outer tubes in such a way that the material flows down along the tubes and forms a film on the external surface of the tubes. The space between the tube plates, in which the ends of the outer pipes are located, is divided by an intermediate wall into an inlet and an outlet compartments. Heating steam is fed to the inlet compartment. Clean condensate is recovered from the inlet compartment and contaminated condensate from the outlet compartment.Type: GrantFiled: October 3, 1988Date of Patent: May 15, 1990Assignee: A. Ahlstrom CorporationInventor: Reino I. Havukainen
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Patent number: 4915792Abstract: A volatile component is separated from a mixture by vaporization in an evaporator and condensation in a condenser. The vapor is transported by a carrier gas that is circulated in and between the evaporator and the condenser. A flow of a liquid is circulated in subsequent heat transfer steps from contact with the mixture via a cooler, via contact with the carrier gas in the condenser, via a heater, and back to contact with the mixture.Type: GrantFiled: October 11, 1988Date of Patent: April 10, 1990Inventor: Sten Zeilon
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Patent number: 4882009Abstract: A brine concentrator utilizing two separate concentrating devices in combination wherein a first concentrating device comprises a plurality of serpentine pipes interposed within a concentrator tank containing a dilute brine solution and a second concentrating device, including a venturi, is attached to the upper end of the concentrator tank and connected to receive exhaust gases from an exterior source. The brine solution which has been concentrated by the first concentrating device exit the tank through an output opening and is introduced into the venturi via a plurality of nozzles where it is mixed with the exhaust gases.A venting stack is also attached to the upper end of the tank for venting the exhaust gases emitted from the venturi and pre-heating dilute brine solution, which is introduced into the tank through the venting stack. As the solution travels down the stack and into the tank, it comes into contact with the exhaust gases exiting the tank from the venturi.Type: GrantFiled: July 13, 1987Date of Patent: November 21, 1989Assignee: Four Nines, Inc.Inventors: Joseph J. Santoleri, Richard D. Ross
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Patent number: 4879004Abstract: In order to dissolve oil or PCB which exists in the electrical insulation of parts to be cleaned, a solvent is evaporated during a heating phase by an evaporator located with the parts in an autoclave. The solvent vapor condenses on the parts and penetrates into the electrical insulation to form an oil or PCB-solvent mixture. In the heating phase, a plurality of intermediate pressure reductions are carried out in the autoclave, and during each intermediate pressure reduction the solvent is simultaneously distilled out of the oil or PCB-solvent mixture, directly from the autoclave. That is, during each of the pressure reductions, the solvent supply is discontinued and the mixture circulated through a circulating line. Following the completion of each intermediate pressure reduction, the pure oil or PCB present in a condensate vessel is pumped out by an intermediately located feed pump through a connecting line and into a reservoir.Type: GrantFiled: May 4, 1988Date of Patent: November 7, 1989Assignee: Micafil AGInventors: Gustav Oesch, Paul Gmeiner, Urs Hofer
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Patent number: 4836891Abstract: A method for concentrating salt water. Salt water is separated from oil-water mixture which has been produced from a well. Salt water is introduced into a recirculating weir and mixed with more concentrated brine. Brine is recirculated through a thermal syphon apparatus. Recirculation includes passing brine, including some salt water, from weir into boiler vessel. Brine is heated within boiler vessel to a boiling temperature whereby brine, while boiling, generates steam which passes up out of weir. All of foregoing steps are performed at atmospheric pressure. The density of brine is sensed at a location in the lower vicinity of weir. Concentrated brine is released from lower vicinity when density at sensed temperature is at a level corresponding to a brine concentration near the precipitation of salt from solution. Salt water and brine is passed through a magnetic water treating unit. The concentrated brine, as released, is passed into a holding vessel.Type: GrantFiled: May 19, 1986Date of Patent: June 6, 1989Assignee: Evaporation, Inc.Inventors: James H. Files, Donald M. Harrel, John M. Montague, Thomas L. Stansbury Sr., Carlton T. Sikes
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Patent number: 4834874Abstract: An apparatus and method are provided wherein liquid is removed from a liquid-solids mixture by employing both filtration and low pressures to achieve vaporization of liquid. The mixture is introduced to a vessel in which the mixture is filtered so that a substantial portion of the liquid is withdrawn from the vessel. The vessel is then depressurized to an extent necessary to vaporize a substantial portion of the remaining liquid. Such vapor is withdrawn from the vessel. During vaporization, the contents of the vessel are agitated and heated.Type: GrantFiled: June 27, 1988Date of Patent: May 30, 1989Assignee: Phillips Petroleum CompanyInventors: William R. Anthoney, Richard K. Young, Brian H. Limoges
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Patent number: 4830707Abstract: A caustic alkali solution is concentrated to high density or high caustic alkali concentration by evaporation under high pressure at elevated temperature and expansion of the thus obtained concentrated caustic alkali solution to low pressure, preferably below atmospheric pressure. The pressure difference between the high pressure evaporator and the low pressure expansion vessel is absorbed gradually by a pressure difference absorber, preferably comprising a liquid column in a U-shaped siphon tube, so that corrosion and erosion are reduced considerably.Type: GrantFiled: May 27, 1986Date of Patent: May 16, 1989Assignees: Sulzer-Escher Wyss AG, Ube Industries, Ltd.Inventors: Robert Winkler, Siro Sala, Yakayuki Kobayashi, Shinjiro Yokota
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Patent number: 4828717Abstract: The device for reducing the volume of an aqueous waste effluent includes a holding tank, a heating tank for receiving waste effluent from the holding tank and including a heater for heating the waste effluent to a predetermined temperature which is below the boiling point of water and high enough to cause a portion of the water to evaporate and be discharged as water vapors, an agitation pump for continuously recirculating the liquids contents of the heating tank and filter units mounted on top of the heating tank for separating solids and particulate matter from the resulting slurry and returning the filtrate to the heating tank.Type: GrantFiled: April 14, 1988Date of Patent: May 9, 1989Assignee: Arkay Corporation of WisconsinInventors: James A. DeLeeuw, Raymond E. Sims
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Patent number: 4790904Abstract: An atmospheric evaporator for reducing the water content of various chemical solutions, more particularly useful in the electroplating industry, wherein the evaporator includes a solution-secure molded tank in which a removable blower sleeve is mounted having a blower inlet duct and support strut members formed at the opposite end thereof to support a multiplicity of finned evaporator members over which the solution is sprayed. When a large-volume, low RPM blower is mounted to the inlet duct, a straight-line downdraft of both air and solution is created, allowing the air and evaporated water to exhaust through an up-facing outlet duct, thus defining a substantially "U" shaped duct arrangement from the inlet side to the exhaust side of the tank with the heavy chemical particles returning to the process tank from the bottom of the evaporator tank.Type: GrantFiled: May 19, 1987Date of Patent: December 13, 1988Inventor: William Yates
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Patent number: 4778535Abstract: An apparatus for vaporizing and recovering, by condensation, a composite mixture of at least two components, at least one of which is a liquid. The apparatus includes at least one chamber in which the mixture is brought to boiling and includes means to condense the vaporized portion of the mixtures. A liquid of the mixture in the vaporizing chamber is vaporized by heating coils and subjected to circulation to uniformly disperse the mixture. The apparatus may further include a system for continuously filtering the mixture in the vaporizing chamber to remove undesirable particulates, a mixture spray device for spraying the mixture into the vaporizing chamber, and an ultrasonic vibrating means.Type: GrantFiled: September 28, 1982Date of Patent: October 18, 1988Inventor: James W. McCord