Rotary And/or Tiltable Patents (Class 202/238)
  • Patent number: 9005403
    Abstract: A rotary evaporator comprising a motor, a rotary joint movably inserted to a motor rotor of the motor by a sleeve in an axial direction, a collection flask attached to the rotary joint at one end of the joint, with a condenser attached to the other end of the joint. The condenser is adapted to receive a cooling coil from an immersion cooler. The cooling coil is attached to the base unit of the immersion cooler via an insulated hose. The rotary evaporator is adapted to provide various ways to remove heat from the flask in the water bath, whether by mechanically lowering the water bath, dropping fluid from the bath into an underlying reservoir, or raising and lowering the rotary evaporator out of the bath. Where the rotary evaporator is raised and lowered, the immersion cooler can remain in place if the hose connecting the base unit to the cooling coil is sufficiently long, or the condenser includes a flexible portion that accommodates the upward and downward movement.
    Type: Grant
    Filed: September 22, 2010
    Date of Patent: April 14, 2015
    Assignee: Ecodyst, Inc.
    Inventor: George M. Adjabeng
  • Patent number: 8956506
    Abstract: The invention relates to a rotary evaporator comprising a rotary drive having a hub and a clamping insert with a sleeve-like basic shape, in particular a clamping sleeve, for the clamping of a steam leadthrough formed as a hollow glass shaft in the hub of the rotary drive, wherein the clamping insert has a longitudinal axis and a first and a second axial end, wherein the clamping insert has two clamping sections which are arranged spaced apart from one another in the longitudinal direction and which each have an outer cross-section tapering toward the first end and of which the clamping arrangement arranged closer to the second end has a larger maximum outer cross-section.
    Type: Grant
    Filed: January 28, 2010
    Date of Patent: February 17, 2015
    Assignee: Hans Heidolph GmbH & Co. KG
    Inventor: Joachim Carl
  • Patent number: 8894822
    Abstract: A rotary evaporator (1) having a cooler (6), wherein temperature sensors (15, 17) are disposed in the inlet (14) and outlet (16) of the coolant into or out of the cooler (6), and a volume flow rate of the coolant through the cooler (6) is determined. The initiation or termination of condensation in the cooler (6) is derived from an increase or decrease in the difference of the temperatures (X) at the temperature sensors (15, 17). The volume of the condensed distillate (10) is determined from the difference in temperatures (X), and a distillation volume control is performed. By regulating the heating power of the heater (11) and/or the pressure in the system, the loading of the cooler (6) is controlled as a function of the difference in temperatures (X).
    Type: Grant
    Filed: August 29, 2009
    Date of Patent: November 25, 2014
    Assignee: Ika-Werke GmbH & Co. KG
    Inventors: Hubert Pinhack, Martin Spath
  • Patent number: 8864949
    Abstract: A system and method for decontaminating water and generating water vapor includes introducing contaminated water in to a vessel. The water is moved through a series of rotating trays alternately separated by stationary baffles so as to swirl and heat the water to effect the vaporization thereof to produce a vapor having at least some of the contaminants separated therefrom. The vapor is removed from the vessel for condensing apart from the separated contaminants and the remaining water. The vapor may be passed through a turbine connected to an electric generator. Sensors in a controller may be employed to adjust the speed of rotation of the trays or water input into the vessel in response to the sensed conditions. The treated water may be recirculated and reprocessed through the vessel to increase the purification thereof.
    Type: Grant
    Filed: January 18, 2013
    Date of Patent: October 21, 2014
    Assignee: Verno Holdings, LLC
    Inventors: John D. Riley, Dana L. Johnson
  • Patent number: 8608911
    Abstract: A device for desalination of water having an inlet for saltwater, a first inner container arranged rotatable around an axis, a second container having an evaporation surface, a heater for heating of the second container and thereby also the evaporation surface, and a motor arranged to rotate the containers around the axis of rotation. The second container encloses the first inner container and is connected fixed to the first inner container. A mechanism for distributing water on the evaporation surface is constituted by holes arranged in the container wall of the first inner container so that water may pass out to the second container. Holes are also arranged in the container wall of the second container so that steam may pass out from the second container. A condensation surface is arranged for condensation of steam which passes out through the holes in the container of the second container.
    Type: Grant
    Filed: April 6, 2011
    Date of Patent: December 17, 2013
    Inventor: Rolf Ingeson
  • Publication number: 20130327631
    Abstract: A rotary evaporator (1), having an equipment stand (2) with a protruding guide tower (3), a glass structure (4) which has an evaporation tank (5) and can be displaced on the guide tower (3) for lifting and lowering the evaporation tank (5) thereof, and at least one fluid line that is connected to the glass structure (4). In one embodiment, the guide tower (3) has a channel (17) that is oriented in the longitudinal extension of the tower (3) and in which a line section is provided of at least one fluid line that is connected to the glass structure (4) and opens out into or ends in a flexible tube connection. This flexible tube connection is arranged on a bottom-side region of the rotary evaporator, which faces away from the free end of the guide tower (3), and the glass structure (4) is retained on a carriage (21) that can be displaced laterally on the guide tower (3).
    Type: Application
    Filed: July 25, 2012
    Publication date: December 12, 2013
    Applicant: KNF Neuberger GmbH
    Inventors: Erwin Hauser, Erich Becker
  • Patent number: 8591705
    Abstract: A multi-effect evaporator, having an upstream and a downstream end, adapted for distillation of water. It includes a plurality of effects connected in a series manner and arranged into groups. Each group has a common parallel water feed inlet adapted to supply all effects in the group with feed water. The evaporator further includes a main feed water line in fluid communication with the most upstream group. An array of heaters is disposed along the line, adapted for heating the feed water before its entry into the effects of the latter group. Each effect includes means for forwarding the second outlet vapor into one of the heaters for heating the feed water. Each group includes a pump adapted to extract the concentrate from the effects of the group and pump it into the common parallel water feed of an adjacent downstream group.
    Type: Grant
    Filed: March 3, 2011
    Date of Patent: November 26, 2013
    Assignee: I.D.E. Technologies Ltd.
    Inventors: Joseph Weinberg, Avraham Ophir
  • Patent number: 8551295
    Abstract: A reactive distillation apparatus for multistage counter-current rotating bed includes a closed shell, in the center of which a revolving shaft linking each shell section is set, the shaft is provided with two or more rotors in series connection, a feeding inlet, a reflux inlet and an outlet of the gas phase are mounted on the top end face of the shell while a waste liquid outlet and an inlet of the gas phase are set on the bottom end face of the shell, a group of concentric dynamic filler rings with different diameters are installed at intervals along the radial direction, wherein the wall of the dynamic filler rings is holed, and the ring clearance between the dynamic filler rings is configured with static rings fastened on the static disc; a feeding inlet is arranged on the top cover of the shell corresponding to the spray nozzle of raw material liquid; a rotating liquid distributor is arranged on the inner side of the innermost dynamic filler ring of the said lower rotor.
    Type: Grant
    Filed: June 12, 2010
    Date of Patent: October 8, 2013
    Assignee: Beijing University of Chemical Technology
    Inventors: Jian-Feng Chen, Peng-Yuan Zhang, Guang-Wen Chu, Hai-Kui Zou, Wei Wu, Qin Shi
  • Patent number: 8524859
    Abstract: In the production of isobutylene-based elastomers the product obtained from the polymerization process is often in the form of a stream. Described herein are an apparatus and a process for removal of hydrocarbon liquids from the elastomer. The process comprises the steps of obtaining a stream comprising hydrocarbon liquids, either solvents or diluents, and an isobutylene-based elastomer; passing the stream through a kneader to volatize the hydrocarbon liquids from the elastomer.
    Type: Grant
    Filed: March 23, 2011
    Date of Patent: September 3, 2013
    Assignee: ExxonMobil Chemical Patents Inc.
    Inventors: Yu Feng Wang, Richard C-M Yeh
  • Patent number: 8506762
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.
    Type: Grant
    Filed: October 30, 2007
    Date of Patent: August 13, 2013
    Assignee: DEKA Products Limited Partnership
    Inventors: David F. Bednarek, Jason A. Demers, Timothy P. Duggan, James L. Jackson, Scott A. Leonard, David W. McGill, Kingston Owens
  • Publication number: 20130056345
    Abstract: A device for desalination of water having an inlet for saltwater, a first inner container arranged rotatable around an axis, a second container having an evaporation surface, a heater for heating of the second container and thereby also the evaporation surface, and a motor arranged to rotate the containers around the axis of rotation. The second container encloses the first inner container and is connected fixed to the first inner container. A mechanism for distributing water on the evaporation surface is constituted by holes arranged in the container wall of the first inner container so that water may pass out to the second container. Holes are also arranged in the container wall of the second container so that steam may pass out from the second container. A condensation surface is arranged for condensation of steam which passes out through the holes in the container of the second container.
    Type: Application
    Filed: April 6, 2011
    Publication date: March 7, 2013
    Inventor: Rolf Ingeson
  • Patent number: 8377257
    Abstract: A total evaporator for fluids, including a cold chamber to prevent pre-evaporation, an evaporation region connected thereto having narrow flow cross-section for fast evaporation of the fluid, and a subsequent vapor chamber for pulsation damping and the controlled superheating of the vapor, the evaporation region being formed by a gap between concentrically nested cylindrical and/or conical tube sections and heat required for the evaporation and superheating processes is supplied by electric heating and/or by hot fluid and/or by catalytic or homogeneous combustion via the wall of the concentric tubes.
    Type: Grant
    Filed: May 19, 2006
    Date of Patent: February 19, 2013
    Assignee: Universitat Stuttgart
    Inventors: Gerhart Eigenberger, Andreas Freund, Grigorios Kolios, Clemens Merten, Jens Bernnat, Gudrun Friedrich
  • Patent number: 8361277
    Abstract: An evaporator is provided for evaporation of liquid from a solution or liquid mixtures, together with methods of operation of the evaporator. The evaporator comprises a chamber (1); a liquid reservoir (3) for holding a heat transfer liquid exposed to the interior of the chamber; a support (6) for supporting a container (8) in the chamber, such that the liquid sample in the container is exposed to a fluid path (15) for connection to a condenser (16), the fluid path being separated from the chamber interior, and at least a portion of the container is closely thermally coupled to the chamber interior; and means (4) for heating the heat transfer liquid in the reservoir to create heat transfer liquid vapor, which in use condenses and releases latent heat of vaporization to the liquid sample in the container. As the temperature of the sample is dependent on the saturated vapor temperature of the liquid in the reservoir, the temperature of the samples is reliably limited, thereby avoiding overheating.
    Type: Grant
    Filed: March 14, 2007
    Date of Patent: January 29, 2013
    Assignee: Genevac Limited
    Inventor: Donald Roger Lee-Smith
  • Publication number: 20120228119
    Abstract: A distiller is provided. The distiller includes a liquid-tight enclosure and an input source connected thereto for inputting a quantity of water into the liquid-tight enclosure. A plurality of substantially vertical rotatable plates is aligned along a substantially horizontal axis within the liquid-tight enclosure. At least a portion of each of the substantially vertical rotatable plates is submerged within the quantity of water inside the liquid-tight enclosure, and each of the substantially vertical rotatable plates has an opening. At least one manifold, having one or more exit ports, extends through a plurality of the openings of the substantially vertical rotatable plates, wherein a portion of the quantity of water is transferred via the substantially vertical rotatable plates to the manifold during a rotation of the plurality of substantially vertical plates. An output opening is formed in the liquid-tight enclosure, the output opening arranged in fluid communication with the manifold.
    Type: Application
    Filed: May 8, 2012
    Publication date: September 13, 2012
    Inventor: Samuel T. Kjellman
  • Patent number: 8246788
    Abstract: A biomass torrefaction system is provided which enables a continuous torrefaction process that involves the introduction of biomass particles into a rotating reactor drum having a low oxygen environment. The particles are conveyed through the drum by a heated gas stream and simultaneously torrefied thereby. Gas exiting the drum is recirculated back to a heat source for reheating the gas prior to reentering the drum. A method of biomass torrefaction is also provided.
    Type: Grant
    Filed: August 25, 2011
    Date of Patent: August 21, 2012
    Assignee: Teal Sales Incorporated
    Inventors: William B. Teal, Richard J. Gobel, Andrew Johnson
  • Patent number: 8034214
    Abstract: A reciprocating film type evaporator for solvents and other chemicals which eliminates the need for a large powerful motor, and other associated equipment such as rotary gaskets, by using reciprocation, versus 360 degree rotation.
    Type: Grant
    Filed: April 12, 2007
    Date of Patent: October 11, 2011
    Assignee: Tracera LLC
    Inventors: Collin McKinney, Rob Musser
  • Publication number: 20110214979
    Abstract: The present invention discloses a reactive distillation apparatus for multistage counter-current rotating bed and its application, the apparatus comprises a closed shell, in the center of which a revolving shaft linking each shell section is set, the said shaft is provided with two or more rotors in series connection, a feeding inlet, a reflux inlet and an outlet of the gas phase are mounted on the top end face of the shell while a waste liquid outlet and an inlet of the gas phase are set on the bottom end face of the shell, the said shell consists of an upper section of the shell and a lower section of the shell along the axial direction, the said rotor consists of a rotating disc firmly connecting with the revolving shaft and a static disc mounted to the shell, a group of concentric dynamic filler rings but with different diameters are installed at intervals along the radial direction, wherein the wall of the dynamic filler rings is holed, and the ring clearance between the dynamic filler rings is configure
    Type: Application
    Filed: June 12, 2010
    Publication date: September 8, 2011
    Applicant: Beijing University of Chemical Technology
    Inventors: Jian-Feng Chen, Peng-Yuan Zhang, Guang-Wen Chu, Hai-Kui Zou, Wei Wu, Qin Shi
  • Patent number: 7955476
    Abstract: A multiple application recycling and purification device has a coaxial core that is horizontally oriented, non-rotating, cylindrical distillation chamber. The enhanced, completely coaxial configuration continuously cleans the entire distillation chamber and spreads a thin film of liquid to enhance distillation and positively aid in the removal of remaining contaminants. Through a timed and positioned valve, the device removes and purges lower-temperature contaminants. Timed valves and sensors control all phases of the distillation to provide a coaxially integrated, stand-alone, adaptable, scalable and maintenance free distillation unit that self-monitors, self-cleans and economically functions to produce the pure distilled liquid, e.g., water. This device can be modified to purify any numerous array of liquids and can be scaled to produce any amount of purified liquids for either household, commercial, or industrial applications.
    Type: Grant
    Filed: January 18, 2007
    Date of Patent: June 7, 2011
    Assignee: Mansur Corporation
    Inventor: Pierre G. Mansur
  • Publication number: 20100243425
    Abstract: The system contains a liquid-tight enclosure. An input source is connected to the liquid-tight enclosure for inputting water into the liquid-tight enclosure. A heating element is in thermal communication with at least a portion of the water within the liquid-tight enclosure. A plurality of substantially vertical plates are aligned along a substantially horizontal axis within the liquid-tight enclosure. Each of the substantially vertical plates has an opening. A groove is formed along each of the substantially vertical plates. A first end of the groove on each of the substantially vertical plates is proximate to the opening. At least one manifold extends through a plurality of the openings of the substantially vertical plates. The manifold is in fluid communication with a plurality of the first ends of the grooves. An output opening is formed in the liquid-tight enclosure. The output opening is arranged in fluid communication with the manifold.
    Type: Application
    Filed: October 2, 2009
    Publication date: September 30, 2010
    Inventor: Samuel T. Kjellman
  • Publication number: 20100193345
    Abstract: The invention relates to a rotary evaporator comprising a rotary drive having a hub and a clamping insert with a sleeve-like basic shape, in particular a clamping sleeve, for the clamping of a steam leadthrough formed as a hollow glass shaft in the hub of the rotary drive, wherein the clamping insert has a longitudinal axis and a first and a second axial end, wherein the clamping insert has two clamping sections which are arranged spaced apart from one another in the longitudinal direction and which each have an outer cross-section tapering toward the first end and of which the clamping arrangement arranged closer to the second end has a larger maximum outer cross-section.
    Type: Application
    Filed: January 28, 2010
    Publication date: August 5, 2010
    Applicant: HANS HEIDOLPH GmbH & Co. KG
    Inventor: Joachim Carl
  • Patent number: 7749360
    Abstract: A vapor based liquid purification system and process utilizes an evaporator for evaporating a liquid into a vapor and a vapor condenser for condensing the vapor into the processed liquid. The vapor condenser has a stator and a rotor, with the rotor disposed for rotation about the stator. The stator and the rotor each have protrusions proximate to an inlet of the vapor condenser. These protrusions cooperate to draw vapor from the evaporator into the vapor condenser. The stator and the rotor each further have at least one axially extending ridge. These ridges cooperate to move a mixture of the vapor and the processed liquid towards at least one drain in the rotor where the processed liquid is communicated to an outlet of the vapor condenser. A multi-level vapor based purification system may also be utilized.
    Type: Grant
    Filed: April 5, 2006
    Date of Patent: July 6, 2010
    Inventor: Wesley K. Waldron
  • Patent number: 7718033
    Abstract: A one step method and system for producing nanofluids by a particle-source evaporation and deposition of the evaporant into a base fluid. The base fluid such (i.e. ethylene glycol) is placed in a rotating cylindrical drum having an adjustable heater-boat-evaporator and heat exchanger-cooler apparatus. As the drum rotates, a thin liquid layer is formed on the inside surface of the drum. A heater-boat-evaporator having an evaporant material (particle-source) placed within its boat evaporator is adjustably positioned near a portion of the rotating thin liquid layer, the evaporant material being heated thereby evaporating a portion of the evaporant material, the evaporated material absorbed by the liquid film to form nanofluid.
    Type: Grant
    Filed: July 12, 2006
    Date of Patent: May 18, 2010
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Milivoje Kostic, Mihajlo Golubovic, John R. Hull, Stephen U. S. Choi
  • Patent number: 7610768
    Abstract: A rotary multi-stage distiller for recovery of water from wastewater is provided. The rotary multi-stage distiller of the present invention can recover water from a wide variety of aqueous wastewaters such as, but not limited to, urine, condensate from air conditioning systems, wash water containing foaming soaps, seawater or polluted water. The multi-stage distiller can operate under vacuum conditions permitting the distillation to occur at low temperatures. The multi-stage distiller uses centrifugal forces for fluid pumping and for vapor/liquid separation. The multi-stage distiller comprises hydraulic seals for each stage which eliminate contamination of clean, recovered water by condensed waste water during the regeneration process. The multi-stage distiller also comprises a stationary shaft of stacked segments where each segment is associated with an individual stage of the multi-stage distiller.
    Type: Grant
    Filed: November 9, 2005
    Date of Patent: November 3, 2009
    Assignee: Honeywell International Inc.
    Inventors: Alex M. Lubman, Allen K. MacKnight, Volodimir G. Rifert, Ivan V. Zolotukhin, Vladimir I. Usenko, Petr A. Barabash, Aleksandr P. Strikun
  • Patent number: 7611604
    Abstract: The invention relates to a method and a device for the production of pure steam. A falling-film evaporator is used. Of the water-steam mixture leaving the evaporator unit, part of the water is collected at the bottom of the device, and a fraction mainly consisting of steam enters a rising spiral channel for the separation of impurities. In the periphery of the spiral channel apertures are provided for separating impurity-containing droplets, which condense on a surface outside the apertures. The liquid formed is removed from the device. The water phase collected at the bottom enters a recycle line connected to the feed end of the evaporator unit. Feed water is supplied to the recycle line to compensate for pure steam consumption.
    Type: Grant
    Filed: August 28, 2003
    Date of Patent: November 3, 2009
    Assignee: STERIS Europe Inc.
    Inventors: Mauri Salmisuo, Ilkka Olavi Laitinen
  • Patent number: 7597784
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.
    Type: Grant
    Filed: November 13, 2003
    Date of Patent: October 6, 2009
    Assignee: DEKA Products Limited Partnership
    Inventors: David F. Bednarek, Jason A. Demers, Timothy P. Duggan, James L. Jackson, Scott A. Leonard, David W. McGill, Kingston Owens
  • Patent number: 7591930
    Abstract: A thin-film evaporator with a vertical drum (1), a supply line (4) that is arranged in the upper region of the drum (1) and is used to supply a medium to be evaporated, a heating jacket (3) arranged on the periphery of the drum and forming vapors, a discharge line (20) for discharging the residue left in the lower end of the drum, and a condenser (11) supplied with a coolant, for increasing the separating capacity and optionally for performing chemical reactions, is characterized in that an inner device (24) influencing the action of the thin-film evaporator is provided in the path of the vapors from the heating jacket (3) to the condenser (11).
    Type: Grant
    Filed: March 31, 2006
    Date of Patent: September 22, 2009
    Assignee: VTU Holding GmbH
    Inventors: Wolfgang Glasl, Matthaeus Siebenhofer, Michael Koncar
  • Publication number: 20090134004
    Abstract: This invention improves efficiencies of existing distilling devices and provides the opportunity to utilize latent heat for heating or cooling purposes. Sufficient heat sources or cooling sinks can drive the invention for mechanical power production. The innovative use of an elongated chamber hydraulic column positive pressure at the bottom to drive condensation; and pertaining negative pressure in a sealed volume at the top to evince evaporation give a new capability. Repeated mechanical inversions of the chamber allows the evaporated vapor volumes to be compressed and driven to condense by the fluid hydraulic column as a piston, eliminating requirements for seals. This allows operation with many fluid separations and in many physical environmental regimes, both internal to the elongated chamber and externally.
    Type: Application
    Filed: November 26, 2008
    Publication date: May 28, 2009
    Inventor: William J. Asprey
  • Patent number: 7507316
    Abstract: The solar still has a frame, an evaporator within the frame and a glass sheet supported by the frame and spaced above the evaporator. The evaporator has a peripheral flange in contact with the edge of the glass sheet. The glass sheet and peripheral flange are nested within an inwardly facing channel on the frame, the sealing between the glass and the flange being by surface tension of water between the glass and the flange.
    Type: Grant
    Filed: April 1, 2003
    Date of Patent: March 24, 2009
    Inventor: John Ward
  • Patent number: 7503997
    Abstract: A centrifugal evaporator includes a chamber in which sample containers are carried and rotated by a rotor and are pivotally mounted so as to swing up to a substantially horizontal orientation as the rotor rotates. The evaporator includes an infra-red source to direct infra-red radiation towards the rotor and the sample containers carried thereon, to heat at least the latter and any sample material therein. A non-contact temperature sensing infra-red pyrometer having a sensor with a defined field of view is mounted in the chamber, such that while the rotor as such is substantially out of its field of view, each sample container at least partly occupies the pyrometer field of view for a part of each rotation of the rotor. The positions of the infra-red source and the pyrometer components are selected so that the radiation from the infra-red source does not impinge on the pyrometer sensor.
    Type: Grant
    Filed: October 29, 2003
    Date of Patent: March 17, 2009
    Assignee: Genevac Ltd.
    Inventors: Roger Lee-Smith, Richard Smith, Duncan Guthrie
  • Patent number: 7501046
    Abstract: An evaporation sleeve is placed within a solar distillation loop apparatus to increase the amount of water evaporated by the apparatus. The evaporation sleeve is rotationally attached within the above ground portion of the solar distillation loop so the sleeve lifts impure water into the air flow within the system. The evaporation sleeve significantly increases the water surface area available to the air flow within a solar distillation loop.
    Type: Grant
    Filed: May 4, 2005
    Date of Patent: March 10, 2009
    Assignee: The United States of American, as represented by the Secretary of the Interior
    Inventor: James Edward Constantz
  • Patent number: 7465375
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.
    Type: Grant
    Filed: November 13, 2003
    Date of Patent: December 16, 2008
    Assignee: DEKA Products Limited Partnership
    Inventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
  • Patent number: 7427336
    Abstract: A blade heat exchanger includes blades that extend axially with respect to an axis of rotation and are elongated in the radial direction. The blades are arranged about the axis such that, when they are disposed in a housing, they form composite condensation and evaporation chambers that are isolated from each other. The interiors of at least some of the blades form the composite condensation chamber. The exteriors of the blades and the inner surface of the housing cooperate to form the composite evaporation chamber.
    Type: Grant
    Filed: June 17, 2004
    Date of Patent: September 23, 2008
    Assignee: Zanaqua Technologies, Inc.
    Inventor: William H. Zebuhr
  • Patent number: 7300538
    Abstract: Liquid organic material is controllably delivered to a receptacle located in the center of a heated surface capable of horizontally rotating about its central axis. As the heated surface rotates, material deposited within the central receptacle is forced outwardly and across the rotating surface. As the material moves radially, it evaporates into a vapor which is then transported to one or more nozzles. From the nozzles, the vapor is applied to a substrate and condensed. The spinning disk evaporator enables the evaporation of a wider variety of organic liquids greater reliability in continuous operation, a decrease in maintenance, and a larger and more constant material flow rate.
    Type: Grant
    Filed: February 16, 2005
    Date of Patent: November 27, 2007
    Assignee: 3M Innovative Properties Company
    Inventors: Charles Daniel Lemme, Marc G. Langlois
  • Publication number: 20070170049
    Abstract: A multiple application recycling and purification device has a coaxial core that is horizontally oriented, non-rotating, cylindrical distillation chamber. The enhanced, completely coaxial configuration continuously cleans the entire distillation chamber and spreads a thin film of liquid to enhance distillation and positively aid in the removal of remaining contaminants. Through a timed and positioned valve, the device removes and purges lower-temperature contaminants. Timed valves and sensors control all phases of the distillation to provide a coaxially integrated, stand-alone, adaptable, scalable and maintenance free distillation unit that self-monitors, self-cleans and economically functions to produce the pure distilled liquid, e.g., water. This device can be modified to purify any numerous array of liquids and can be scaled to produce any amount of purified liquids for either household, commercial, or industrial applications.
    Type: Application
    Filed: January 18, 2007
    Publication date: July 26, 2007
    Inventor: Pierre G. Mansur
  • Patent number: 7153396
    Abstract: In a rotary evaporator, the rotating speed of the rotating flask is automatically controlled or regulated dependent upon a detected process value, particularly the vibration behavior or the mass moment of inertia of the rotating flask.
    Type: Grant
    Filed: March 14, 2002
    Date of Patent: December 26, 2006
    Inventor: Hans Georg Genser
  • Patent number: 7150807
    Abstract: Method and system for evaporating at least one substance. During at least one dosing phase (TG) a predefined or predefinable quantity of a product (M) which contains at least one substance to be evaporated is imported via a feed system (7, 14, 17, 33, 36) into a revolving vessel (2). The revolving vessel is rotated around an axis of rotation (R) and appropriate process conditions for the evaporation of at least one substance are generated or maintained. The flow (F) of the product (M) is automatically controlled or regulated by the feed system (14, 17) during the dosing phase (TG) in particular as a function of at least one process parameter and/or of at least one characteristic property of the product. The product (M) is imported into the revolving vessel (2) in the course of the dosing phase only during predefined feed periods (t1, t2) that are interrupted by intervening intervals and especially idle intervals (t1, t2).
    Type: Grant
    Filed: July 3, 2002
    Date of Patent: December 19, 2006
    Inventor: Hans Georg Genser
  • Patent number: 7087140
    Abstract: A carbonizing waste processing apparatus is operable to rotate and heat a radiant tube for carbonizing waste therein so as to generate granular char and vapors from the waste, transfer waste into an upstream end of the tube, temporarily impede movement of the waste through the tube at upstream and downstream locations therein so as to ensure that residence time of the waste in the tube is sufficient at the upstream location to carry out evaporation of moisture from the waste and at the downstream location to elevate the temperature of any solids in the waste for completion of carbonization of the waste, discharge the granular char and vapors from the tube, and flow the generated and discharged vapors through a succession of finned heat exchanger tubes so as to condense and separate the vapors into oil, water and methanol.
    Type: Grant
    Filed: August 12, 2002
    Date of Patent: August 8, 2006
    Inventor: Harry H. Menian
  • Patent number: 6908533
    Abstract: An evaporator and condenser unit for use in distilling a liquid, such as water, includes a rotary heat exchanger plate having a plurality of folds or pleats. Adjacent panels of the folded plate define spaces between their oppositely facing surfaces, and these spaces are alternatingly configured as evaporating and condensing chambers. The evaporating chambers, moreover, are defined between adjacent panels that are joined at an outer diameter fold, while the condensing chambers are defined between adjacent panels that are joined at an inner diameter fold. The evaporating chambers are thus closed at their outer diameter ends and open at their inner diameter ends, while the condensing chambers are closed at their inner diameter ends and open at their outer diameter ends.
    Type: Grant
    Filed: January 17, 2002
    Date of Patent: June 21, 2005
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr
  • Patent number: 6860966
    Abstract: A method of removing substantially all solvent from a solution containing a polyphenylene ether polymer resin with little by-product formation (less than 250 ppm) is provided. The method employs a wiped thin film evaporator with a cylindrical heating chamber operating under conditions that satisfy the relationships defined by Equations I and II. 5.3*1024RL? exp(?24123/T)/m<C??I 100?(4960AP/Tm)<C??II; Yields are maximized wherein values for feed rate (m) and percent solids (C) are selected to provide a maximum value for the output, Q, determined from the equation m*C=Q and the melt viscosity of the polyphenylene ether product is less than 50,000 centipoise at the operating temperature of the cylindrical heating chamber.
    Type: Grant
    Filed: November 12, 2001
    Date of Patent: March 1, 2005
    Assignee: General Electric
    Inventors: David Parrillo, Probjot Singh
  • Patent number: 6846387
    Abstract: An evaporator and condenser unit for use in distilling a liquid, such as water, includes a rotary heat exchanger plate having a plurality of accordion-style folds, and having its two ends joined together so as to give the folded plate a generally circular form. The adjacent panels of the folded plate define spaces between their oppositely facing surfaces, and these spaces are alternatingly configured as evaporating and condensing chambers. The evaporating chambers have their inner edges sealed by corresponding folds, while the condensing chambers have their outer edges sealed by corresponding folds. The folded plate is disposed between first and second end plates, and is mounted for rotation about its axis in a housing having a sump containing the liquid to be distilled. Liquid is supplied to the evaporating chambers and compressed vapor is supplied to the condensing chambers. Condensate is removed from the condensing chambers.
    Type: Grant
    Filed: July 5, 2000
    Date of Patent: January 25, 2005
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr
  • Publication number: 20040200580
    Abstract: A method of protectively heating a microtitre well plate from below using infra-red radiation in a centrifugal evaporator, wherein a barrier plate is placed in contact with and surrounding the lower ends of the wells. The barrier plate is adapted to convey heat energy to the wells and contents thereof and is selected to be substantially non-transmittive of radiation having wavelengths in the range 200 nm to 3000 nm, and the surface of the barrier plate which is to receive the wells includes a plurality of sockets in which the closed lower ends of the wells are a snug fit. The plate is adapted to fit between the underside of the wells and a swinging sample holder mount of a centrifugal evaporator, or a shelf of a swinging sample holder mount, having two or more shelves for stacking well plates one above the other in such an evaporator.
    Type: Application
    Filed: August 8, 2003
    Publication date: October 14, 2004
    Inventors: Duncan Guthrie, John Poole, Mike Sherwen
  • Patent number: 6802941
    Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.
    Type: Grant
    Filed: January 18, 2001
    Date of Patent: October 12, 2004
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr
  • Publication number: 20040195083
    Abstract: The solar still has a frame, an evaporator within the frame and a glass sheet supported by the frame and spaced above the evaporator. The evaporator has a peripheral flange in contact with the edge of the glass sheet. The glass sheet and peripheral flange are nested within an inwardly facing channel on the frame, the sealing between the glass and the flange being by surface tension of water between the glass and the flange.
    Type: Application
    Filed: April 1, 2003
    Publication date: October 7, 2004
    Inventor: John Ward
  • Patent number: 6740206
    Abstract: A rotary evaporator including a rotating flask (2) to hold the substances to be evaporated, and a drive (6) to rotate the rotating flask around an axis of rotation (R) that runs through the rotating flask, wherein the rotating flask additionally can be swiveled around a swiveling axis (S) which runs outside of the rotating flask and, relative to the force of gravity (G), runs above the axis of rotation of the rotating flask.
    Type: Grant
    Filed: February 20, 2002
    Date of Patent: May 25, 2004
    Inventor: Hans Georg Genser
  • Patent number: 6716320
    Abstract: A liquid sample 3 held in an open container 2 and including a volatile solvent, is evaporated by continuously removing inert gas rich in vapor by means of a suction tube 5 whose open end is held close to the top surface of the liquid. Vapor in the gas is then extracted in a refrigerated condensing vessel 6, from where the purified gas is fed by a pump 7 for recirculation back into a sealed chamber 1 in which the container is mounted. In a modification, the inert gas is fed directly through a nozzle 17 into the container 2 wile the gas/vapor mixture is extracted from the chamber 1 for recirculation, after passing through a condenser 6 or the like.
    Type: Grant
    Filed: April 17, 2000
    Date of Patent: April 6, 2004
    Inventor: Michael Cole
  • Patent number: 6695951
    Abstract: The present water reclamation system includes a series of concentric thin shells. The shells mount within a housing that can be maintained under vacuum or low pressure. The shells rotate at high velocity. Contaminated liquid from outside the housing is injected into the space between half the shells. The centrifugal force causes the liquid to form a thin film along the inward facing surface of the shell. A compressor lowers the pressure adjacent the thin film causing the liquid to boil. The compressor carries the vapor to the other side of those shells at a slightly higher temperature. There the vapor encounters the wall, which is cooler because its heat was transferred to boil the contaminated liquid. The vapor condenses, and rotation throws the condensate against the adjacent wall where it is collected. When condensing, the heat of condensation transfers to the shell for boiling the incoming contaminated liquid.
    Type: Grant
    Filed: July 18, 2000
    Date of Patent: February 24, 2004
    Inventors: Jack G. Bitterly, Steven E. Bitterly
  • Patent number: 6689251
    Abstract: A distiller (10) that employs a rotary heat exchanger (32) introduces water to be evaporated into evaporation chambers (56). During most of its operation, it collects the water that has passed through the evaporation chamber (56) without evaporating, and it reintroduces the thus-collected liquid back into the evaporation chamber, where it also adds a minor amount of unrecirculated feed liquid to make up for evaporation and concentrate removal. Simultaneously, a minor amount of feed liquid is fed into one side of a transfer pump (116). During this mode of operation, the impurities concentration in the recirculating liquid tends to increase as a result of the evaporation of pure water vapor. Periodically, the erstwhile recirculating liquid is redirected to the other side of the transfer pump (116), where it causes the feed liquid stored in the transfer pump's first side to be fed without accompanying recirculant liquid into the rotary heat exchanger's evaporation chambers.
    Type: Grant
    Filed: January 18, 2001
    Date of Patent: February 10, 2004
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr
  • Patent number: 6605474
    Abstract: A method is described for evaporating liquid samples contained in sample holders mounted within a chamber and rotated by the rotor during an evaporation process in which the pressure in the chamber is reduced below atmospheric and the sample holders are rotated at high speed so as to exert centrifugal force on the contents of the holders. Heat is supplied to elevate the temperature of the liquid component of the samples to assist in the evaporation process. The temperature of the sample material is continuously or regularly monitored during the evaporation process and temperature signals are transmitted to a remote computing means which is programmed to generate a control signal for controlling the supply of heat to the samples and controlling the evaporation process. The temperature may be sensed by a probe in a sample holder containing an evaporating liquid sample, or in an adjoining sample holder containing a buffer liquid.
    Type: Grant
    Filed: March 8, 2000
    Date of Patent: August 12, 2003
    Assignee: Genevac Limited
    Inventor: Michael Cole
  • Publication number: 20030132096
    Abstract: An evaporator and condenser unit for use in distilling a liquid, such as water, includes a rotary heat exchanger plate having a plurality of folds or pleats. Adjacent panels of the folded plate define spaces between their oppositely facing surfaces, and these spaces are alternatingly configured as evaporating and condensing chambers. The evaporating chambers, moreover, are defined between adjacent panels that are joined at an outer diameter fold, while the condensing chambers are defined between adjacent panels that are joined at an inner diameter fold. The evaporating chambers are thus closed at their outer diameter ends and open at their inner diameter ends, while the condensing chambers are closed at their inner diameter ends and open at their outer diameter ends.
    Type: Application
    Filed: January 17, 2002
    Publication date: July 17, 2003
    Inventor: William H. Zebuhr
  • Publication number: 20030000651
    Abstract: In a rotary evaporator, the rotating speed of the rotating flask is automatically controlled or regulated dependent upon a detected process value, particularly the vibration behavior or the mass moment of inertia of the rotating flask.
    Type: Application
    Filed: March 14, 2002
    Publication date: January 2, 2003
    Inventor: Hans Georg Genser