Rotary And/or Tiltable Patents (Class 202/238)
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Publication number: 20020148718Abstract: A rotary evaporator including a rotating flask (2) to hold the substances to be evaporated, and a drive (6) to rotate the rotating flask around an axis of rotation (R) that runs through the rotating flask, wherein the rotating flask additionally can be swiveled around a swiveling axis (S) which runs outside of the rotating flask and, relative to the force of gravity (G), runs above the axis of rotation of the rotating flask.Type: ApplicationFiled: February 20, 2002Publication date: October 17, 2002Inventor: Hans Georg Genser
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Publication number: 20020092759Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Publication number: 20020092758Abstract: A distillation unit (10) employs counterflow-heat-exchanger modules (102, 104, 106, 108, and 110) to use the heat from water that has come from a rotary heat exchanger (32) to heat feed water that is being sent to it for distillation. In one of the modules the feed water is heated only by concentrate that results from the distillation process, whereas only condensate heats the feed water in the other modules. By thus employing four different flows in two sets of heat-exchanger modules rather than three flows in a single set, the distillation unit can employ relatively simple counterflow-heat-exchanger modules and easily adjust flows to achieve a desired output concentration in response to different expected feed concentrations while maintaining optimum feed flows.Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Publication number: 20020092624Abstract: In a distillation unit (10) a rotary heat exchanger (32) receives from a radially inward position feed liquid to be purified and collects on the inner surface of a rotating exterior shell (36) liquid that has passed through its evaporation chambers (56). Stationary scoop tubes (122 and 124) scoop liquid from the resultant liquid layer that forms on the shell (36)'s inner surface, and the kinetic energy of the liquid scooped from the thus-spinning layer drives it radially inward through the scoop tubes (122 and 124) into spray arms (58) for reintroduction into the rotary heat exchanger's evaporation chambers (56).Type: ApplicationFiled: January 18, 2001Publication date: July 18, 2002Inventor: William H. Zebuhr
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Publication number: 20020038760Abstract: An evaporation product discharged from a lower end a falling-film evaporator (1, 2) enters a downpipe (7), makes a 180° turn at a bottom of the downpipe, and moves upward through an annular rising channel (9) defined between the downpipe and an intermediate housing (10). As the evaporation product moves along a spiral path (12) defined by the spiral fins, centrifugal forces urges water droplets and impurities to a radial outward periphery where they pass through openings (13) in the intermediate shell as pure steam continues through the spiral path and out a pure steam outlet (21). A cooling jacket (15) chills a peripheral wall of an outer shell (14) adjacent the holes such that the discharged water droplets condense on the outer shell and flow down a reject water return path to a reject water reservoir at the bottom of the outer shell.Type: ApplicationFiled: September 21, 2001Publication date: April 4, 2002Applicant: STERIS EUROPE, INC.Inventor: Mauri J. Salmisuo
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Publication number: 20020017450Abstract: A liquid having certain undesired elements therein is distilled in a distillation column to form a vapor stream. This vapor stream is fed by means of an inert gas drive to a first container having an array of semi-permeable screens which are rotated at a speed of 3,000-10,000 rpm to generate vertical spiral vortexes which act on the vapor to separate out heavier impurities. An inert gas is employed to drive the vapor stream from the first container to the bottom of a second container having a narrower diameter array of semi-permeable screens, these screens being driven at a velocity of 6000-100,000 rpm. In the second container, the molecular species is separated from the main vapor stream by virtue of the exposure of the vapor to large centrifugal gravity forces generated by the horizontal velocity vectors of the rotating screens.Type: ApplicationFiled: August 1, 2001Publication date: February 14, 2002Inventor: Ernest Csendes
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Publication number: 20020008009Abstract: Liquid organic material is controllably delivered to a receptacle located in the center of a heated surface capable of horizontally rotating about its central axis. As the heated surface rotates, material deposited within the central receptacle is forced outwardly and across the rotating surface. As the material moves radially, it evaporates into a vapor which is then transported to one or more nozzles. From the nozzles, the vapor is applied to a substrate and condensed. Relative to existing devices and methods, the present invention enables the evaporation of a wider variety of organic liquids, greater reliability in continuous operation, a decrease in maintenance, and a larger and more constant material flow rate.Type: ApplicationFiled: September 6, 2001Publication date: January 24, 2002Applicant: 3M Innovative Properties CompanyInventors: Charles Daniel Lemme, Marc G. Langlois
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Patent number: 6309508Abstract: Liquid organic material is controllably delivered to a receptacle located in the center of a heated surface capable of horizontally rotating about its central axis. As the heated surface rotates, material deposited within the central receptacle is forced outwardly and across the rotating surface. As the material moves radially, it evaporates into a vapor which is then transported to one or more nozzles. From the nozzles, the vapor is applied to a substrate and condensed. Relative to existing devices and methods, the present invention enables the evaporation of a wider variety of organic liquids, greater reliability in continuous operation, a decrease in maintenance, and a larger and more constant material flow rate.Type: GrantFiled: January 15, 1998Date of Patent: October 30, 2001Assignee: 3M Innovative Properties CompanyInventors: Charles Daniel Lemme, Marc G. Langlois
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Patent number: 6258215Abstract: The system for the recovery of water from urine aboard spacecraft includes a urine intake and pretreatment unit, a unit for water reclamation from urine and a condensate purification unit. The unit for water reclamation from urine is made on the basis of a rotary multistage vacuum distiller, each stage of which is formed by at least one heat-transfer plate and comprises an evaporation zone and a condensation zone. The stages of the distiller are separated from each other by separation plates, a chamber for collecting condensate and noncondensable gases being disposed downstream of the last stage and communicated with all the condensation zones of all the stages through water seals of condensate overflow and openings for the removal of noncondensable gases in disks mounted in the condensation zones.Type: GrantFiled: July 6, 1999Date of Patent: July 10, 2001Assignee: Otkrytoe aktsionernoe obschestvo “Nauchno-Issledovatelsky I Konstruktosky Institut Kkhimicheskogo Mashinostroenia (A. O. Neikhimmash”)Inventors: Nikolai Mikhailovich Samsonov, Leonid Sergeevich Bobe, Vladimir Gustavovich Rifert, Petr Alexeevich Barabash, Vladimir Viktorovich Komolov, Vadim Iliich Margulis, Vladimir Mikhailovich Novikov, Boris Yakovlevich Pinsky, Nikolai Nikolaevich Protasov, Valentin Vasilievich Rakov, Nikolai Sergeevich Farafonov
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Patent number: 6063242Abstract: An evaporation system for separation of a fluid mixture into its component parts, especially for the reclamation of solvents, has a vacuum pump connected to the evaporator, especially a rotation evaporator, with at least one separator being connected to the suction side of the vacuum pump and at least one secondary condenser being connected at the pressure side of the vacuum pump. A fine regulating valve (8) is installed in the connecting pipe (7) between the rotation evaporator (2) and the separator (9), which is connected in front of the vacuum pump (10), for regulation of the boiling pressure.Type: GrantFiled: August 31, 1998Date of Patent: May 16, 2000Assignee: KNF Neuberger GmbHInventor: Erwin Hauser
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Patent number: 5919339Abstract: A rotary evaporator of the present invention has an insertion area of a rotary joint 33 in a straight shape. This area is movably inserted to a motor rotor 27 of a motor by a sleeve 31 or 31' in an axial direction. Bushes 57 are inserted between the rotary joint 33 and the sleeve 31 or 31' for integrating the rotary joint 33 and the sleeve 31 or 31' by a fastening force generated by a fastening cap 61 or 61' engaged with a screw section of the sleeve 31 or 31'. With the above-described structure, when the outer peripheral surface of the rotary joint 33 is abraded by a sealing member 43, the fastening cap 61 is loosened and the rotary joint 33 is slightly moved to the axial direction so that the rotary joint 33 is moved to an appropriate or an optimum position along the axial direction.Type: GrantFiled: March 14, 1997Date of Patent: July 6, 1999Assignees: Yamato Scientific Co., Ltd, Ikeda Glass Co., LtdInventor: Naoki Ikeda
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Patent number: 5879516Abstract: Improved kugelrohr or apparatus for distilling or separating liquids. It includes a rugged, reliable air oven and drive unit with numerous safety features. One or more external guards eliminate burn hazard and risk of accidental contact. A thermal isolation support isolates the oven from its rest surface. A grounded heating element eliminates shock hazards. The oven is fitted with a grommet or bushing to support a flask connected to one or more additional flasks in a series. The outlet of the last flask in the series is connected to a drive tube via a flexible coupling. The drive tube is connected to a rotary bearing assembly mounted on a drive unit. The oven and the flasks may include impellers for circulating air to enhance heating efficiency.Type: GrantFiled: February 29, 1996Date of Patent: March 9, 1999Inventor: David H. Kasman
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Patent number: 5759356Abstract: An evaporator flask for a rotary evaporator is formed in two portions: a substantially cylindrical bowl and a lid secured to the bowl by a connecting ring. The lid is connected to a rotary drive mechanism, and a conduit passes through a central aperture in the lid to provide fluid communication between the interior of the flask and a condenser. A mechanical scraper or stirrer is affixed to the end of the conduit within the bowl portion of the flask.Type: GrantFiled: February 22, 1996Date of Patent: June 2, 1998Assignee: Buchi Labortechnik AGInventor: Arthur Spring
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Patent number: 5746987Abstract: The present invention is an apparatus for separating volatile from nonvolatile substances, separation of volatile substances, one from the other, and for performing various chemical reactions. In particular, an apparatus which performs these functions utilizing a combination of above ambient temperatures and above one inch of mercury vacuum within a rotating vessel. The apparatus uses a conventional rotary vacuum seal. The apparatus, however, operates well above the maximum operating temperature of the conventional rotary vacuum seal by isolating and cooling the conventional rotary vacuum seal.Type: GrantFiled: January 17, 1997Date of Patent: May 5, 1998Assignee: Thermall Corp.Inventors: Randy Aulbaugh, Gregory G. Hawk
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Patent number: 5744008Abstract: A simple, portable and efficient water desalination device uses deep ocean water, solar energy and the dynamics of generated secondary vortices. The device includes a tower, a heat exchanger positioned inside the tower near the top of the tower, a cold water source, a cold water receiving tank, a condensate catchment grille, a freshwater collecting tank, a rotor extending upward between the side walls of the tower from a lower portion of the tower, a power source for driving the rotor, a warm salt water pan positioned in the bottom of the tower and a warm salt water source. The cold water source is cold deep ocean water that is siphoned to the top of the tower through rollable, transportable fabric pipes. The warm salt water source is solar heated ocean water. In the tower, a hurricane is simulated by a rotating column that induces a circulation of air which approximates that of a hurricane.Type: GrantFiled: January 2, 1996Date of Patent: April 28, 1998Assignee: Oceanit Laboratories, Inc.Inventor: John P. Craven
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Patent number: 5688377Abstract: Rotating parallel disks create radial cyclonic vortices between them. The axes of these vortices communicate with the bore of a hollow shaft, and a vacuum is drawn in the shaft bore by the action of a centrifugal pump. Particles, mist, and heavy vapors such as mercury, are separated out of a gas stream by the radial vortices, which cause whatever is relatively heavy in the vortex to migrate away from the vortex axis and then contact the rotating disks, whereby they are expelled from the space between the disks. Application to mist elimination for steam is discussed, as are application to cyclonic cracking of hydrocarbons and separation of gaseous waste from intra-lattice fluid.Type: GrantFiled: November 25, 1994Date of Patent: November 18, 1997Inventor: Wilmot H. McCutchen
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Patent number: 5643408Abstract: An apparatus for decontaminating a liquid surfactant of a dioxane having a vapor pressure which is higher than the vapor pressure of the surfactant includes an elevated reservoir for dioxane-contaminated liquid surfactant and an elongate inclined conduit, which has an upper portion for receiving a stream of the contaminated liquid surfactant from the elevated reservoir and a lower portion for discharge of decontaminated liquid surfactant. A heat source is suitable for heating contaminated liquid surfactant in the elongate inclined conduit in an amount sufficient to cause the dioxane contaminant of the liquid surfactant to volatilize, thereby decontaminating the surfactant. A gas source is suitable for directing a gas through the inclined conduit to transport volatilized dioxane out of the conduit. A receptacle is connected to the elongate inclined conduit for receiving the decontaminated liquid surfactant discharged from the inclined conduit.Type: GrantFiled: May 16, 1995Date of Patent: July 1, 1997Assignee: Pharm-Eco Laboratories, Inc.Inventors: Yesh P. Sachdeva, Richard L. Gabriel
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Patent number: 5639354Abstract: A distillation device with a rotating evaporator flask disposed within a heated bath. The heated bath is movable down and away from the evaporator flask to provide space for an evaporator flask support below the evaporator flask. The evaporator flask support holds the evaporator flask while it is connected or disconnected from the rotary drive. In addition, a U-shaped case accommodates the collecting flask and/or evaporator flask. The case supports the flask in an upright manner and facilitates positioning and transporting of the flask.Type: GrantFiled: September 25, 1996Date of Patent: June 17, 1997Assignee: Resona Innovation AGInventor: Adolf Zellweger
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Patent number: 5611895Abstract: An arrangement for discharging and collecting the distillate of rotary vacuum evaporators includes a rotating flask and a line for conducting the distillate from the rotating flask to a cooler for liquefying the distillate. The liquified distillate flows from the cooler into a collector and from the collector into a storage container. A safety check valve constructed as a pressure control valve is provided between the collector and the storage container. An excess pressure producer for increasing the pressure of the distillate is provided between the collector and the pressure control valve, wherein the pressure control valve and the excess pressure producer are constructed so as to interact in such a way that the pressure control valve opens when a sufficient excess pressure of the distillate has been reached.Type: GrantFiled: February 15, 1995Date of Patent: March 18, 1997Inventor: Hans-Georg Genser
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Patent number: 5607558Abstract: An apparatus and method for separating the components of and/or decomposing a liquid material, involving the application of an artificial gravitational field to a liquid material by rotating the liquid material in a rotatable vessel. A non-rotatable mechanical member contacts the liquid material while the liquid material is exposed to the artificial gravitational field. The liquid material is thusly subjected to thermomechanical frictional heating.Type: GrantFiled: March 27, 1995Date of Patent: March 4, 1997Inventor: Olav Ellingsen
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Patent number: 5603809Abstract: A spinning band device for use in a distillation process including a particular pattern of apertures. The band is made of of an elongated strip, either metal screen or Teflon, twisted about its longitudinal center. Both embodiments contain frayed or jagged edges to create turbulences within a mixture and scrape the inner wall of a distillation column. The novel features of this band are the large apertures, which a situated on the longitudinal centerline for the metallic embodiment and scattered on the outer face for the Teflon embodiment, combined with the use of a plurality of spinning blades. Experimental testing and empirical data has proven this type of band to yield a significant increase in fractionating efficiency over the conventional two bladed bands without apertures.Type: GrantFiled: February 3, 1995Date of Patent: February 18, 1997Inventor: Roger R. Roark, Sr.
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Patent number: 5589135Abstract: A height adjustable stand for laboratory equipment, in particular for rotary evaporators, possesses a holder arrangement (6). The holder arrangement is able to be displaced vertically on a stand post (5). By way of a motor driven lifting arrangement (9, 11), the holder device (6) can be vertically raised or lowered. A coupling (12) is provided between the holder arrangement (6) and the lifting arrangement (9, 11) for the powered connection and its release.Type: GrantFiled: September 22, 1992Date of Patent: December 31, 1996Assignee: Buchi Laboratoriums - Technik AGInventor: Erwin Bossart
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Patent number: 5569357Abstract: A vortex evaporator having a holder for holding at least one container presents a chamber wherein liquid is evaporated from a liquid and solid solution in a container. The vortex evaporator also includes a drive mechanism, coupled to the holder, for moving each container in an orbital motion within the chamber to cause the solution in the container to form a vortex configuration. The vortex evaporator further includes a gas supply system for directing gas into the container to increase the evaporation rate of the liquid and a control system for controlling operation of the vortex evaporator. In an alternative embodiment, a vacuum supply system may be utilized instead of the gas supply system. Further, the vortex evaporator will preferably include a heater, at least one liquid level sensor, a heat sensor and a motion dampening assembly all located within the chamber.Type: GrantFiled: April 28, 1994Date of Patent: October 29, 1996Assignee: Labconco CorporationInventors: Lowell L. Kuhn, James F. Ptacek, Gary P. Roepke
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Patent number: 5536374Abstract: An evaporator flask for a rotary evaporator is formed in two portions: a bowl and a lid secured to the bowl by a connecting ring. The lid is connected to a rotary drive means, and a conduit passes through the lid to provide fluid communication between the interior of the flask and a condenser. A mechanical scraper or stirrer is affixed to the end of the conduit within the bowl portion of the flask.Type: GrantFiled: January 19, 1994Date of Patent: July 16, 1996Assignee: Buchi Labortechnik AGInventor: Arthur Spring
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Patent number: 5534118Abstract: A controlled bubble of cavitation is formed within the distilland by opposed centrifugal and centripetal forces in the plane of an afferent mesial passage. Thus a distilland surface forms around the axis of rotation, and saturated vapor is continuously stripped from this distilland surface by the work of a vapor pump, which also creates the centripetal force. The vapor vortex within this cavitation region ejects by centrifugal force whatever in it is denser than pure vapor, including any particles or droplets which may somehow become entrained in the vapor. Bubbling at the distilland surface, which might produce mist, is suppressed by centrifugal force. Vapor is compelled to follow an afferent flow path, and is scrubbed by cyclones in the afferent mesial passage. Scrubbed vapor is then withdrawn from within the distilland along the axis of rotation. No container is necessary for the distilland and no heat is added to produce evaporation.Type: GrantFiled: March 7, 1994Date of Patent: July 9, 1996Inventor: Wilmot H. McCutchen
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Patent number: 5472574Abstract: Bands used in fractionating columns, and more specifically, to the type made from either a metal screen strip or from a Teflon sheet twisted into a helicoid. In addition to previously documented design characteristics, the present spinning band includes a number of additional, circular apertures cut into the face of the metal screen strip and Teflon sheet. The circular apertures, sequentially arranged along the centerline of the band, add to the operating efficiency of the spinning band as it is employed in a fractionation process.Type: GrantFiled: July 9, 1993Date of Patent: December 5, 1995Inventor: Roger R. Roark, Sr.
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Patent number: 5472575Abstract: A rotary evaporator is described utilizing a magnetically driven fluorocarbon cylinder, operating within a solvent container, to create a thin solvent film for rapid evaporation without the usual requirement for rotating the entire solvent container assembly. Infra-red heating is employed for efficient evaporation rates. Solvent heating is controlled during evaporation by a single temperature probe, turning the infra-red heater on and off on demand of the probe. Over heating of the product is prevented by maintaining a solvent residue at or near the conclusion of an evaporation.Type: GrantFiled: February 14, 1994Date of Patent: December 5, 1995Assignee: Maustat CorporationInventors: Martin Parkinson, Francis Gomer
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Patent number: 5340444Abstract: A circulation cooler (10) has a heat exchanger (12) in a housing (11) that contains a cooling liquid and is detachably connected by its forward flow (13) to an inlet line (5), and by its return line (14) to the outlet (6) of a condenser (4) of a distillation apparatus (1). The circulation cooler (10) moreover has a vacuum pump (21) inside its housing (11) and an absorber (28) outside its housing (11). A second condenser (24) is interposed along the cooling agent inlet line (13) between the circulation cooler (10) and the condenser (4) of the distillation apparatus (1), and is connected to a vacuum line (27). The cooling liquid (25) flows successively to the heat exchanger ( 12) through the two condensers (24, 4) , then back to the heat exchanger (12). In both condensers, which are under a vacuum through common vacuum line (26, 27) , the condensation of the liquid substances is effected in the form of main condensation and aftercondensation phases.Type: GrantFiled: June 22, 1993Date of Patent: August 23, 1994Assignee: Peter W. D. van der Heijden LaborbedarfInventor: Peter W. D. van der Heijden
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Patent number: 5338409Abstract: There is described an apparatus for distilling liquids in a vacuum, having a receptacle for a liquid that can be connected to a vacuum pump, a heating arrangement for heating the receptacle causing the liquid to evaporate, a condenser for condensing the vapour, and a collecting vessel for the condensate. To be able to handle the apparatus quickly and more simply and to make it overall more economical and make it possible to carry out continuous distillation, the heating arrangement includes a vacuum-tight receiving chamber (1) for the receptacle (2) and a microwave generator (13, 13.Type: GrantFiled: July 23, 1992Date of Patent: August 16, 1994Assignee: MLS Mikrowellen-Labor-Systeme GmbHInventor: Jacob Heierli
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Patent number: 5334290Abstract: The invention relates to a molecular distillation apparatus of the type comprising a metallic conical rotor (12) rotatably driven and fed in its center with a liquid to be distilled, a vacuum bell (10) defining an enclosure housing the cone and means for inductively heating the rotor which are located beneath and in proximity to the latter.According to the invention, the heating means comprise at least two concentric inductors (100a, 100b, 100c) supplying different thermal power densities to homologous regions of the rotor and an inner inductor (100a) supplies a greater thermal power density to the rotor than the power density supplied to the rotor by an outer inductor (100c).The invention also relates to a process for manufacturing an assembly of a rotor and inductors for such an apparatus.Type: GrantFiled: November 21, 1991Date of Patent: August 2, 1994Assignee: Expanchimie S.A.R.L.Inventors: Jacques Nuns, Alain Girault, Alain Rancurel
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Patent number: 5264079Abstract: A film-type evaporator has a vapor chamber, a rotor rotating therein, at least one evaporating surface extending outwards from the rotor axis and a heating chamber rotating therewith and sealed with respect to the vapor chamber. The starting product is fed onto the evaporating surface close to the rotor axis and spreads outwards in film-like manner due to the centrifugal force on the evaporating surface. A uniform film thickness is achieved in that the evaporating surface is a curved blade surface, which is formed by a generatrix substantially parallel to the rotor axis and whose axial extension is limited by upper and lower stop ledges, and that the concave side of the evaporating surface is directed in the circumferential direction of rotation of the rotor.Type: GrantFiled: February 28, 1992Date of Patent: November 23, 1993Inventor: Vaclav Feres
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Patent number: 5256250Abstract: In a thin film evaporator for the evaporation of solutions, colloids, suspensions, or the like, to concentrates, which has a heatable cylindrical evaporator casing coupled with a rotary drive, which evaporator casing has a feed inlet at one end, in the form of a feed distributor that runs on bearings and is coupled with a rotary drive, and at the other end has a concentrate discharge, the axis of the evaporator casing is arranged horizontally. The distal end of the feed distributor can reach the inside surface of the evaporator casing to within less than 2 cm. Wiper elements can work together with the effective surface of the evaporator casing. This thin film evaporator makes possible an optimal setting of the retention time of the process material to be treated in the evaporator casing and has the effect that the thickness of the layer of the process material changes very little over the entire axial length.Type: GrantFiled: July 20, 1992Date of Patent: October 26, 1993Inventor: Rudolf Pelzer
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Patent number: 5167763Abstract: A spray dryer which has a tank for receiving batches of differing materials to be spray dried. The tank is rotatable about a horizontal axis. The tank has an open top and a cover which is hinged on an axis perpendicular to the tank axis. The cover carries atomizer which has a shaft extending through the cover into the tank when the cover is closed. A spray disk is attached to the atomizer shaft.Type: GrantFiled: November 29, 1990Date of Patent: December 1, 1992Assignee: Sakamoto Engineering Co., Ltd.Inventor: Tetsuo Sakamoto
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Patent number: 4940134Abstract: An apparatus for treating a waste solution generated when a photosensitive material is processed by an automatic developing machine includes a waste solution reservoir which is maintained at a constant level. A drum, partially immersed in the waste solution, is rotated to coat its surface. The drum is heated to produce a waste vapor. The waste vapor is condensed by a condenser and filtered and solid wastes are scraped from the surface of the drum. The condenser has a drain tank for collecting condensate and a non-condensable gas component. The interior of the drain tank is sealed to form an air tight seal and has a vent for exhausting the non-condensable gas component from the interior portion to the outside. The air vent includes an absorption tower to treat the non-condensable gas component.Type: GrantFiled: November 14, 1988Date of Patent: July 10, 1990Assignee: Konishiroku Photo Industry Co., Ltd.Inventors: Syozo Aoki, Satoru Kuse, Shigeharu Koboshi
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Patent number: 4913777Abstract: A rotary evaporator for laboratory scale solvent evaporative procedures is described. A magnetically driven fluorocarbon coated rotor, being open at its base and closed at its top, operating within a container for solvents, creates a thin film for rapid solvent evaporation without the usual requirement for rotating the entire solvent assembly. Rotary seals are eliminated, increased control over bubbling and foaming at higher vacuum is obtained, and continuous solvent addition is simplified.Type: GrantFiled: December 2, 1988Date of Patent: April 3, 1990Inventor: Martin Parkinson
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Patent number: 4853088Abstract: A process and apparatus for separating volatile components from a volatile-containing liquid by a stripping gas flowing countercurrent to the liquid. Separation of the volatile components is enhanced by heating the liquid with radiant solar energy and agitating the liquid as it flows.Type: GrantFiled: April 12, 1988Date of Patent: August 1, 1989Assignee: Marathon Oil CompanyInventor: David D. Conway
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Patent number: 4822455Abstract: A distilling and desalination apparatus comprising an evaporation chamber and a condensing chamber in which the evaporation chamber through a cooling circuit communicates by way of heat exchange with the condensing chamber and rotates in relation thereto. The evaporation chamber is constructed to form a thin fluid film on the inner surface of the evaporation chamber during rotation, surplus water being slung out along the edge and into channels and led tangentially to the rear by blades. The cooling circuit comprises a condensing portion and an evaporation portion, the fluid being evaporated along the inner surface of the coolant condensing portion, and fluid vapors being condensed along the outer surface of the coolant condensing portion, whereupon the drops of fluid are slung outwards and collected.Type: GrantFiled: January 7, 1987Date of Patent: April 18, 1989Assignee: Chas. HudeInventor: Henrik-Gerner Olrik
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Patent number: 4790911Abstract: A rotary evaporator for laboratory scale solvent evaporative procedures is described. A magnetically driven fluorocarbon coated rotor, operating within a container for solvents, creates a thin film for rapid solvent evaporation without the usual requirement for rotating the entire solvent container assembly. Rotary seals are eliminated, increased control over bubbling and foaming at higher vacuum is obtained, and continuous solvent addition is simplified.Type: GrantFiled: December 11, 1987Date of Patent: December 13, 1988Inventor: Martin Parkinson
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Patent number: 4780178Abstract: Rotation driving apparatus usable with a rotary evaporator for holding a sample vessel in a water bath. The driving apparatus includes a stator supported by an elevating member mounted alongside the water bath, and a rotor mounted on the inside of the stator. A hollow support shaft is mounted within the rotor, and the sample vessel is detachably connected to one end of the support shaft. A concentrator can be connected to the other end of the support shaft, for fluid communication with the sample vessel through the hollow support shaft. The support shaft is affixed to the rotor, so that the sample vessel and concentrator are rotated as the rotor turns. A slitted disk is supported by the rotor, and a photosensor produces signals in response to relative movement of the slits. These signals are used for controlling the rotation of the driving apparatus.Type: GrantFiled: February 6, 1987Date of Patent: October 25, 1988Assignee: Yamoto Scientific Co. Ltd.Inventors: Naoki Yoshida, Tatsuhiko Saito, Takao Kawakami
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Patent number: 4770746Abstract: Spinning band fractionating column apparatus is disclosed having a spinning band formed with a magnet embedded in its bottom end in the manner of a magnetic stirring vane for rotation by a rotating external magnetic field at the bottom of the apparatus. Reflux is controlled by an angled drip edge on a rotatable condenser column that passes a portion of dripped condensate to a collecting spout with the portion varying as rotation of the condenser column brings the drip from said edge closer or further from center opposition with the spout.Type: GrantFiled: January 5, 1987Date of Patent: September 13, 1988Assignee: Microscale Organic Laboratory CorporationInventors: Dana W. Mayo, Ronald M. Pike, Robert J. Hinkle
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Patent number: 4764250Abstract: A vacuum evaporator is provided which is connected to the casing of a driving motor for rotating the evaporator piston, wherein the driving motor is vertically adjustable mounted on a bolt fixedly mounted on a pedestal. A supporting sleeve which is freely displaceable on the bolt supports the driving motor thereon and a lever arm supports this sleeve and is articulated on the pedestal. A thread drive is coupled to the lever arm by means of a coupling sleeve arranged on the lever arm and wherein the lever arm is pivotable by the thread drive and the thread drive is adjustable by means of a geared motor.Type: GrantFiled: October 8, 1986Date of Patent: August 16, 1988Inventors: Gunther Riehl, Gunther Vollgold
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Patent number: 4759825Abstract: The invention relates to a rotary evaporator for carrying out a processor-controlled distilling operation. A rotary flask (5), a condenser (8) and a distillate collector receptacle (10) of the rotary evaporator (1) are continually kept under vacuum.According to the invention, the automatically controlled supply of a sample solution to the rotary flask is accomplished by means of a metering receptacle adapted to have the sample solution supplied thereto from a supply container for temporary transitory storage therein prior to transfer of the solution to the vacuum system, or the rotary flask (5), respectively. For discharging the distillate from the distillate collector receptacle (14), an outlet valve associated therewith is operable to connect the collector receptacle to a vacuum conduit (26) for the discharge of the distillate. This provision offers the advantage of permitting substantially discharge of the distillate without requiring the vacuum system to be vented.Type: GrantFiled: July 23, 1986Date of Patent: July 26, 1988Inventors: Bela Medvey, Laszlo Rozsnoki
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Patent number: 4738295Abstract: A method and apparatus of controlling a rotating vacuum evaporation system is disclosed. The rotating flask, containing the medium to be evaporated, is buoyantly supported in a liquid bath and the relative elevation between the flask and the liquid level in the bath is measured. The relative elevation is utilized as the control signal to control the addition of fluid medium to the flask, and to shut off the system when desired.Type: GrantFiled: April 2, 1986Date of Patent: April 19, 1988Inventor: Hans G. Genser
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Patent number: 4731159Abstract: An evaporator comprises a plurality of substantially parallel plates mounted for rotation about a common axis and in which provision is made for a condensible vapor to flow across a first face of each of said plates and for a liquid, at least a portion of which is to be evaporated, to flow across the second face of each of said plate, which plates are arranged to be rotatable at such a mean acceleration, measured in a radial direction with respect to said axis of rotation, greater than the acceleration due to gravity, said first face of each of said plates has a surface designed to discourage formation of a continuous liquid film thereon. The evaporator may be used to concentrate solutions, e.g. of depleted brine or aqueous caustic soda.Type: GrantFiled: December 19, 1985Date of Patent: March 15, 1988Assignee: Imperial Chemical Industries plcInventors: John E. Porter, Colin Ramshaw
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Patent number: 4693304Abstract: A method and apparatus for transferring heat for the purpose of purifying raw feed liquid, vaporizing heat transfer fluids or containing and regulating biological/chemical reactions. The raw feed liquid is directed into an evaporator module submerged in a solar pond or other body of heated liquid. The evaporator module includes a rotating housing through which a plurality of spaced apart substantially horizontal open ended heat transfer tubes extend. A heating liquid is directed through the heat transfer tubes. The raw feedwater is distributed within the evaporator module so as to cause the feedwater to descend into heat transferring contact with the heat transfer tubes and thereby vaporize a portion of the feedwater. The vapor formed in the evaporator module is withdrawn from the evaporator module and directed to a suitable condenser. A preferred embodiment of the evaporator module is disclosed which includes cavitation fins for urging the heated liquid through the evaporator module.Type: GrantFiled: May 23, 1986Date of Patent: September 15, 1987Inventor: Craig S. Volland
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Patent number: 4666564Abstract: Method and apparatus for distilling a liquid mixture to separate a volatile vapor fraction therefrom. The liquid is forced to flow along a meander-like path through a plurality of concentrically arranged chambers of a rotating drum. In the radially outermost chamber, a heating unit is provided which brings the liquid to a boiling temperature to allow formation of vapor. The liquid thus freed of volatile constituents is then discharged from the outermost chamber in which the liquid is subjected to a maximum centrifugal acceleration while the vapor moves radially inwardly under the action of the centripetal force to the innermost chamber from where the vapor containing volatile constituents is discharged.Type: GrantFiled: April 5, 1985Date of Patent: May 19, 1987Assignee: Fried. Krupp Gesellschaft mit beschrankter HaftungInventor: Karl Zeitsch
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Patent number: 4627890Abstract: In a centrifugal mass transfer device comprising a rotary annular permeable element, annular plates are mounted adjacent the radially inner or outer face of the permeable element and gaseous or liquid material flowing from the permeable element across one surface of the annular plates is cooled or heated by a heat exchange fluid on the opposite surface of the plates. In this way condensed or vaporized material is returned to the permeable element.Type: GrantFiled: November 22, 1982Date of Patent: December 9, 1986Assignee: Imperial Chemical Industries PLCInventors: John E. Porter, Colin Ramshaw
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Patent number: 4613409Abstract: A method and apparatus for purifying raw feedwater. The raw feedwater is directed into an evaporator module submerged in a solar pond or other body of heated liquid. The evaporator module includes a rotating housing through which a plurality of spaced apart substantially horizontal open ended heat transfer tubes extend. A heating liquid is directed through the heat transfer tubes. The raw feedwater is distributed within the evaporator module so as to cause the feedwater to descend into heat transferring contact with the heat transfer tubes and thereby vaporize a portion of the feedwater. The vapor formed in the evaporator module is withdrawn from the evaporator module and directed to a suitable condensor.A preferred embodiment of the evaporator module is disclosed which includes cavitation fins or urging the heated liquid through the evaporator module.Type: GrantFiled: August 19, 1985Date of Patent: September 23, 1986Inventor: Craig S. Volland
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Patent number: 4597835Abstract: A still comprises a housing, a hollow rotor rotatably mounted in the housing and having one or more outlets for liquid at the periphery thereof, means for rotating the rotor about its axis, a plurality of concentric lamellar bodies of thermally conductive material mounted in the hollow interior of said rotor so as to provide a labyrinthine path within the rotor for liquid moving radially outwardly under centrifugal force and for vapor moving radially inwardly with respect to the rotor, vaporizing means for vaporizing liquid to be distilled, liquid inlet means for introducing liquid to a radially inner part of the hollow interior of said rotor, vapor outlet means communicating with a radially inner part of the hollow interior of said rotor, and liquid outlet means for removal of liquid from the housing, whereby in use vapor is constrained to move radially inwardly and liquid to move radially outwardly under centrifugal force within said rotor, fractionation occurring at least in part by condensation of vapor oType: GrantFiled: November 28, 1984Date of Patent: July 1, 1986Inventor: John Moss
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Patent number: 4569724Abstract: A sealing means for a vacuum distillation apparatus is provided having a vapor tube rotatably and sealably mounted within a vacuum tube through which vapor passes.Type: GrantFiled: September 30, 1982Date of Patent: February 11, 1986Inventor: Raymond A. Firestone