Abstract: A vapor compression distillation system (10) is provided and includes a fluid inlet (12) for receiving a fluid, a fluid outlet (14) for a distillate that has been distilled from the fluid, a heat exchanger (16) connected to the fluid inlet (12) and the fluid outlet (14) to transfer heat from the distillate to the fluid; and an integrated motor/compressor unit (18) connected to the heat exchanger (16) to receive vaporized distillate therefrom and to supply pressurized distillate thereto. The system 10 may further include a coolant system (20) connected to the integrated motor/compressor (18) to supply a coolant flow thereto. The system (10) may also include an air oil mist system (22) that is connected to the integrated motor/compressor unit (18) to supply an air oil mist thereto for bearing lubrication and cooling.

Abstract: A decomposition reaction apparatus or distillation apparatus for acrylic acid in which a column bottom liquid heated in a reboiler (5) is supplied from a supply port (1a) provided on a side wall of a column body (1) having: a top plate (12a) above the supply port (1a); and an impingement plate (12b) provided vertically to the top plate (12a), for preventing scattering of the column bottom liquid to a supply direction. The top plate (12a) is provided such that the top face of the top plate (12a) is inclined downward from a base end to a tip end. The present invention allows: suppression of formation of a polymerized product due to flowing of a liquid or gas heated in a reboiler into a column with a simple structure; and a stable continuous operation of column equipment over a long period of time.

Abstract: The present invention relates to a system that allows an operator to remotely switch between cutting and boring while removing solid carbonaceous residue from large cylindrical vessels called coke drums comprising a cutting head for ejecting high pressure fluids into the coke bed; a flow diversion apparatus; and a shifting apparatus.

Abstract: A system for the extraction, drainage and wet transport of the petroleum coke produced by the coking chambers is described. Such system provides the collection, drainage and transport of the petroleum coke coming from the coking chambers during the cutting phase all the way to the boilers' feeding. The material extracted from the coking chamber (7) through the use of high pressure water is conveyed on the pre-crusher (4) through a connection system (1a). Between the pre-crusher (4) and the draining belt conveyor (2) there is a drainage and containment hopper (1) which has the dual function of accumulation and possible drainage thanks to some holes that serve as weir. The material which falls from above in different sizes, after having being reduced in size by the pre-crusher (4), gets transported by the belt (2) that carries out a first drainage phase through the holes made on the same belt. The coke is collected on the belt while the drained water is collected in a lower collection channel (8).

Abstract: A vertical multitubular heat exchanger that can prevent clogging of a polymerized material and is continuously operable for an extended period of time is provided. The vertical multitubular heat exchanger (1) of the present invention introduces a process fluid containing an easily-polymerizable substance into heat exchanger tubes (28) to perform heat exchange. The vertical multitubular heat exchanger (1) includes a shell (2) extending in a vertical direction, an upper tube sheet (8) and a lower tube sheet (10) respectively disposed at the upper portion (4) and the lower portion (6) of the shell (2), and a plurality of heat exchanger tubes (28) whose outer circumferences (26) of both ends are respectively fixed to the upper tube sheet (8) and the lower tube sheet (10). An upper surface (34) of the upper tube sheet (8) is formed to be sloped and at least one of the heat exchanger tubes (28) is disposed in the vicinity of the lowest position of the upper surface (34) of the upper tube sheet (8).

Abstract: An apparatus including a coke drum for coking hydrocarbon substances, a valve disposed near the bottom of the coke drum, and a discharge conduit for removing coke from the coke drum, wherein the discharge conduit is connected to the valve such that when the valve is open, the coke may be removed via the discharge conduit.

Abstract: A system (10) for pyrolysing material comprises a stationary inlet stage (20), a rotary kiln (60) and a stationary outlet stage (70), with a rotary joint mechanism (30, 80) provided between the inlet stage (20) and the rotary kiln and/or between the rotary kiln and the outlet stage (70). The rotary joint mechanism (30, 80) comprises a face seal between a rotating surface (66) of a first seal member (65, 85) fixed to the kiln (60) and a stationary surface (26) of a second seal member (25, 82) fixed to the respective stage (20, 70).

Abstract: The present invention features an installation system for facilitating the installation and removal of a closure onto and from a pressure vessel, respectively. The installation system comprises a fixed support structure constructed proximate a pressure vessel; a carriage dynamically and continuously supported by the fixed support structure, wherein the carriage also dynamically and adjustably supports a closure, such as a header or a deheader valve, in a continuous manner; an elevation adjustment assembly allowing the carriage and the closure to move in a vertical manner relative to the fixed support structure and the pressure vessel; and a horizontal transfer assembly that dynamically couples the closure to the carriage to enable horizontal, bidirectional transitioning of the closure relative to the carriage.

Abstract: A liquid distributor for use in a column having distillation trays has been developed. The liquid distributor functions to uniformly distribute a descending liquid stream across the tray for interaction with an ascending vapor stream. The liquid distributor has a feed pipe which delivers the liquid stream to an underlying elongated trough. Liquid discharge holes are positioned in the floor of the trough. A perforated v-plate positioned within the trough so that liquid from the feed pipe passes through the perforated v-plate before encountering the floor of the trough. When liquid passes through the perforated v-plate, the stream is divided into smaller streams of lower velocity, providing a more uniform overall flow rate of liquid passing through the trough. Liquid is then delivered from the discharge outlets of the trough onto the upper surface of the tray with a substantially uniform flow rate across the trough.

Abstract: A process for converting organic waste into reusable hydrocarbons and a system for doing so, the system including a feeding mechanism for the waste, a reactor and a residue-disposing mechanism. The waste is to be fed into the reactor in which a molten lead bath is confined in an oxygen-free atmosphere. The system is used to practice a process for the pyrocatalytic conversion of the waste, which process comprises, feeding the waste into a reaction zone of a pyrocatalytic reactor, the waste being essentially free of a halogenated synthetic resinous material, and mixing the waste with a minor proportion by weight of a particulate catalyst in the bath held at a temperature in the range from about 450° C. to 550° C. in an elongated vat. The catalyst consists essentially of a major proportion by weight of particulate bauxite <2 mm, in combination with a minor proportion of aluminum powder <0.

Abstract: An apparatus for the provision of a block flange of a manhole aperture or the like, in particular for fluidized bed reactors for the oxychlorination of ethylene, oxygen and HCl, having a wall flange fixed in the reactor wall, is intended to provide a solution whereby all other auxiliary measures can be dispensed with and the expense associated therewith can be eliminated without the functionality of the system suffering as a result and without undesirable deposits being formed in these areas. This is achieved in that the flange surface (5) pointing inward and downward in the direction of gravity is of beveled design, at least in some areas.

Abstract: An low concentration dope is fed through a nozzle into a concentrating apparatus, and flash evaporation of the low concentration dope is performed at an end of the nozzle. The low concentration dope is concentrated thereby to an concentrating dope which is contained and heated in the concentrating apparatus. Thus part of solvents of the low concentration dope and the concentrating dope is evaporated to a solvent gas. The solvent gas is cooled and condensed in a condensing section of the concentrating apparatus, and thereafter drawn through a first exit from the concentrating apparatus. The concentrating dope is concentrated to a high concentration dope, which is drawn through a second exit from the concentrating apparatus.

Abstract: An apparatus including a coke drum for coking hydrocarbon substances, a valve disposed near the bottom of the coke drum, and a discharge conduit for removing coke from the coke drum, wherein the discharge conduit is connected to the valve such that when the valve is open, the coke may be removed via the discharge conduit.

Abstract: Improved coke chute systems (100) include a lock (130) that receives and automatically secures a coke-receiving conduit (110) to a coke vessel after the lock (130) is switched to a closed position. Contemplated systems may further be combined with a horizontally movable coke chute cover, or a cover that is moved by an actuator (114) that lifts and rotates the cover from a first position to a second position.

Abstract: The invention relates to a method and a device for evacuating hot raw gases which occur in the oven chambers of a coke oven battery during coking. The oven gases are lead from the oven chambers into a hot gas collector. The pressure in the oven chambers is controlled by shut-off and throttling devices which are arranged in the hot gas streams between the raw gas outlet of the oven chambers and the hot gas collector. The positions of the devices are controlled according to the pressure that is measured in the allocated oven chamber. The gas of the hot gas collector is supplied to a steam boiler firing or a fission reactor.

Abstract: An apparatus comprises a movable lock ring and a lock arm that prevents inadvertent movement of the lock ring. Contemplated configurations are especially useful in delayed coking vessels to prevent opening of the vessel while the vessel is in operation.

Abstract: A distillation system is provided for batch thermolytic distillation of lump carbonaceous material, such as lump wood and shredded rubber tires. The system preferably includes multiple distillation units mounted side-by-side. Each unit includes a reactor bath for holding molten tin at approximately 455° C., a two-compartment reservoir for storing molten tin, and a porous basket pivotally mounted within the reactor bath for tipping motion. A process for batch thermolytic distillation of lump carbonaceous material includes rotating the porous basket into a reactor bath by rotating the basket about an axis passing through the reactor bath; putting a charge of wood into the basket; closing a retractable lid onto the reactor bath; filling the reactor bath with molten material to produce gas and char by thermolytic conversion of the charge, draining the reactor bath of molten material while the lid is closed; quenching the char in the reactor bath with steam; opening the lid; and tipping the char from the basket.

Abstract: The present invention features systems and methods for de-heading a coke drum without having to physically remove the head units. This is accomplished using a de-header valves that may be removably coupled to a coke drum. The de-header valve is equipped with, a valve closure and a seat support system capable of forming a continuous contact seal during the coke manufacturing process. Actuation of the valve closure functions to open and close the de-header valve. Once the drum is full, the de-header valve may be actuated (opened), wherein the coke that has accumulated on the blind is sheared by the seat support system, thus effectively de-heading the coke drum and facilitating the decoking process.

Abstract: The present invention features a coke drum de-heading system comprising (a) at least one coke drum having an orifice therein; (b) a de-header valve removably coupled to the coke drum designed to de-head the coke drum; and (c) an exchange system, including an upper and lower bonnet and other elements and members adapted to integrate the de-heading system, and particularly the de-header valve, into the manufacturing system.

Abstract: The invention relates to a levelling bar for coking ovens, for levelling the cones of discharged coal which form under the filling holes of the oven chamber during the filling process. The levelling bar consists of two cheeks, such as plates (1), which extend essentially over the entire length of the ranged at a distance from each other depending on the width of the oven chamber, and parallel to each other. They are also interconnected and are essentially vertical. The levelling bar also has transversal coal carriers (2) which are arranged in the intermediate space delimited by the cheeks (1) at a mutual distance, one behind the other and which only extend over part of the cross-sectional surface of the levelling bar formed between he cheeks (1). The height (3) of the coal carriers (2), which take up the entire interval between the cheeks, is less than the height (H) of the cheeks (1) and the cheek form a gas channel (6) above the coal carriers (2) which is essentially free of built-in components.

Abstract: The invention relates to a device for sealing a leveling door aperture of a coke oven chamber when loading bulk coking coal. The device includes a housing and a leveling door aperture, a leveling arm, composed of at least side panels and cross spacers connecting the side panels, is guided through the housing and the leveling door aperture. The leveling arm supports means for sealing a cross-sectional area of the leveling door aperture or upstream the leveling door aperture. A controllable or adjustable exhauster is joined to the housing and a measurement point is provided for flow rate measurement.

Abstract: The present invention provides for an apparatus for converting an organic liquor into a mixture of hydrocarbons and carbon solids, comprising: a heater for heating the organic liquor, thereby producing a mixture of liquid and vaporized oil; a reactor for converting the mixture of liquid and vaporized oil into carbon solids, and a mixture of hydrocarbons and gases; a first cooler for accepting the carbon solids; and a second cooler for accepting the mixture of hydrocarbons and gases. The apparatus of the present invention finds application in the processing of waste and low-value products to produce useful materials in reliable purities and compositions, at acceptable cost, without producing malodorous emissions, and with high energy efficiency.

Abstract: Apparatus for carrying out mass transfer processes with high-viscosity liquids comprising a vertically arranged vessel (1) having a feeder (4) for the liquid to be treated, an outlet (7) for volatile components and an outlet (6) for the treated liquid, the feeder means (4) being equipped with a distributor element (3) having a multiplicity of orifices (8, 10) for subdividing the high-viscosity liquid to be treated into a multiplicity of individual streams, wherein essentially vertically arranged wire loops (2) are disposed in the vicinity of the orifices (8, 10), along which wire loops the high-viscosity liquid runs off under the action of gravity.

Abstract: An unheading and containment system for unheading and heading a pressure vessel includes an unheading apparatus for removing a cover from a pressure vessel in an unheading operation and a modular enclosure, mechanism to substantially enclose the cover during the unheading operation. The unheading apparatus includes a cover removably secured to the pressure vessel, a lock plate cooperating with the cover, and a cover moving mechanism capable of moving the cover vertically and laterally.

Abstract: An apparatus and method for processing hazardous wastes directly from 55-gallon drums through the use of pyrolysis and steam reforming. The method is based on a pyrolyzer using heat to vaporize organics that are present in the hazardous wastes. The waste is heated in the original drums to avoid the bulk handling of alpha radionuclides and to ensure criticality control. At pyrolysis temperatures, all liquids and organics in the drums will evaporate and volatize. The resulting waste in the drums is a dry, inert, inorganic matrix with carbon char containing radioactive metals. The off-gas produced by pyrolysis mainly consists of water vapor, volatized organics, and acid gases from the decomposition of various plastics and other organics present in the waste drums. The off-gas produced by the pyrolysis is then collected and fed into an off-gas treatment system that is in fluid communication with pyrolyzer operated under oxidizing conditions.

Abstract: The present invention features a coke drum de-heading system that provides unique advantages over prior art de-heading systems, namely the de-heading of a coke drum without having to physically remove the head units. This is essentially accomplished using a specially designed dual seated, linear motion goggle blind gate valve, or de-header valve, that is removably coupled to and seals against the flanged portion of a coke drum much the same way a conventional head unit would be attached. The de-header valve is equipped with, among other things, a sliding blind that is contained and capable of moving within an upper and a lower seat, wherein one of such seats is a floating dynamic, live loaded seat that is capable of automatic adjustment through one or more loading zones so as to seal the blind between the upper and lower seats.

Abstract: A method and system for extracting hydrocarbon fuel products from contaminated soil provides extraction of usable fuel components from waste materials such as oil contaminated materials and soils. The materials (or hydrocarbon portion thereof) are liquified and introduced to a chamber where the liquid material is agitated and a negative relative pressure (vacuum) is applied. The liquid is maintained at a substantially constant temperature and the vacuum draws the off-gas hydrocarbon products out for condensation and further processing, while unconverted char is removed to an ash dump. An auger feed unit with agitator buckets is used to propel the char through a feed while agitating the liquid to enhance the rate of gas removal.

Abstract: A method and system for extracting hydrocarbon fuel products from waste material provides extraction of usable fuel components from waste plastic materials and waste materials such as oil contaminated materials and soils. The materials (or hydrocarbon portion thereof) are liquified and introduced to a chamber where the liquid material is agitated and a negative relative pressure (vacuum) is applied. The liquid is maintained at a substantially constant temperature and the vacuum draws the off-gas hydrocarbon products out for condensation and further processing, while unconverted char is removed to an ash dump. An auger feed unit with agitator buckets is used to propel the char through a feed while agitating the liquid to enhance the rate of gas removal.

Abstract: A closed system that eliminates worker exposure during coker vessel decoking operations and thereby significantly reduces risks to workers also increase coking capacity by reducing the coking cycle time. The closed system preferably comprises a coker vessel with a side entry feed line attached to the vessel above the vessel bottom; a closure housing with laterally moveable closure member therein sealed to the vessel bottom either directly without, or indirectly with an adapting spool member and; a coke chute sealed to the bottom of the closure housing. The system can be remotely and repetitively operated through numerous coking/decoking cycles without removal of any system element.

Abstract: An apparatus safely fills and empties a pressurized vessel charged with flammable and/or reactive gas. The apparatus features an upper flap combination, an intermediate lock vessel having a flushing apparatus, and a lower flap combination. The present invention also relates to a pressurized reactor which is charged with flammable and/or reactive gas and is equipped with a filling lock apparatus and an emptying lock apparatus for the simultaneous preparation of tetrachlorosilane, trichlorosilane and hydrogen. In addition, the present invention relates to a special process for filling and emptying such a reactor.

Abstract: The present invention features a coke drum de-heading system comprising (a) at least one coke drum having an orifice therein; (b) a de-header valve removably coupled to the coke drum designed to de-head the coke drum; and (c) an exchange system, including an upper and lower bonnet and other elements and members adapted to integrate the de-heading system, and particularly the de-header valve, into the manufacturing system.

Abstract: An apparatus including a coke drum for coking hydrocarbon substances, a valve disposed near the bottom of the coke drum, and a discharge conduit for removing coke from the coke drum, wherein the discharge conduit is connected to the valve such that when the valve is open, the coke may be removed via the discharge conduit.

Abstract: A reflection column which contains liquid distributors having at least 500 drip points/m2, which are arranged at an angle of about 90° C. to cloth layers of packing elements located immediately therebelow; and a combination of insulation and protective heating. The column is advantageously used for the rectification of mixtures of high-boiling air- or temperature-sensitive substances requiring effective separation efficiency.

Abstract: This invention is a system for manufacturing char having a continuous operation and optimizing heat generation and retention elements.

Abstract: The invention provides a method and apparatus for decreasing gas flow rates in a sole flue gas system for a coke oven during at least an initial coking operation after charging a coking oven with coal. The method includes providing a duct system between a first coke oven having a first coking chamber and a second coke oven having a second coking chamber to direct at least a portion of gas from a gas space in first coking chamber to the second coke oven thereby reducing a gas flow rate in the first sole flue gas system of the first coke oven. Reduction in sole flue gas flow rates has a beneficial effect on product throughput, the life of the coke oven and environmental control of volatile emissions from coke ovens.

Abstract: Tire pyrolysis systems and processes are provided which include feeding tire shreds to a pyrolysis vessel (40) and pyrolyzing the shreds in a pyrolysis vessel (40) to produce a pyrolysis gas and carbon black mixture. The pyrolysis gas processed by centrifugally separating entrained particles therefrom, separating the pyrolysis gas into a hydrocarbon condensate and a light vapor, removing entrained hydrocarbon condensate from the light vapor, and purifying and refining the hydrocarbon condensate. The carbon black mixture is processed by pulverizing the mixture to break up all strands and clumps of inorganic solids, cooling the carbon black mixture, separating the gross contaminants from the carbon mixture, and purifying and refining the carbon black. The hydrocarbon condensate is purified and refined by removing all remaining contaminants, removing any polycyclic aromatics to produce a clear, colorless plasticizer oil.

Abstract: Hydrogen and Oxygen are ducted in the flame zone of a reactor chamber. A body of water and or steam is admitted into the outer zone of said reactor and with intimate contact with the flame zone will generate steam. Said steam is confluent with steam generated by combustion of said Hydrogen and Oxygen. Net steam flow is used externally for generating power, heating and cooling purposes.

Abstract: The present invention provides a substantially remote operable system for connecting and disconnecting a vessel. The system comprises a substantially remotely operable joint connector for connecting and disconnecting structural units. The system and the method using the system may also comprise a remote operable closure transport for removing a vessel closure from an opening in the vessel, and a substantially remote operable removal system for allowing material to be emptied from the vessel to increase operational efficiency.

Abstract: There is provided a feed distributor for feeding liquid to a liquid distributor. The feed distributor has an elongated body sized to extend across the liquid distributor and an inlet defined in the one of the ends thereof. One or more passageways are provided within the body extending between the ends of the body. Each passageway has an elongated outlet configured to discharge the liquid across the liquid distributor. Each passageway has a taper configured to promote a constant liquid velocity within the passageway. As a result, a uniform liquid distribution of the liquid out of the elongated outlet and therefore to the liquid distributor are promoted.

Abstract: A coke drum head is hinged to a coke drum body using a compound joint such as a trammel pivot, and the head is moved between open and closed positions using an actuator. In moving between open and closed positions, the head traces out a non-circular path which reduces the required headroom relative to a head using a standard pivot.

Abstract: The present invention provides a fully remotely operable system for loading and unloading a vessel. The system comprises a remotely operable joint connector for sealing or unsealing a vessel. It also consists of a remotely operable closure transport for removing a vessel closure from an opening in the vessel, and a remotely operable removal system for allowing material to be emptied from the vessel.

Abstract: The present invention relates to an apparatus and method for withdrawing and dewatering slag from a gasification system. In particular, the present invention relates to a conveying lockhopper and method of using the conveying lockhopper to collect slag and other waste byproducts from the gasifier of a gasification system. The conveying lockhopper is configured to receive slag from a gasifier, simultaneously extract and dewater the slag, and expel the processed slag directly into an awaiting container suitable for carrying the processed slag away. The conveying lockhopper generally comprises a housing with inlet and outlet valves to receive and expel slag, respectively. The housing is inclined at an angle typically between 5 and 60 degrees to the horizontal so that the outlet is at a higher elevation than the inlet. Inside the housing, an auger or similar conveying mechanism conveys the slag from the inlet towards the outlet while simultaneously dewatering the slag.

Abstract: This liquid distributor includes: a primary distributor (13) including liquid-distribution openings and delimiting N1 first compartments (22), each provided with liquid feed elements means (10, 11); and a secondary distributor (14), arranged under the primary distributor (13) and including a dish with openworked perforated bottom which occupies substantially the entire cross-section of the distillation column (2), this dish being subdivided by partitions (25) into N2 second compartments (24), with N2>N1.

Abstract: The invention provides a coke oven charging machine including a mobile frame and a coke oven feed device on the mobile frame. The coke oven feed device includes a movable, elongate charging plate having a first end and a second end, retractable side-walls adjacent the charging plate, first and second end walls adjacent the first and second ends of the charging plate and a shuttle section adjacent the first end of the charging plate for spanning an area between the first end of the charging plate and an entrance to the oven. The shuttle section has opposed shuttle side walls and a shuttle end wall. A charging plate moving device is provided for moving the charging plate into and out of the oven. The charging machine apparatus provides a means for quickly charging coking ovens with a compacted coal charge so that lower quality coals may be used to make metallurgical coke.

Abstract: A coal charging car for a coke-oven battery has a screw-type feeder beneath the coal hopper shiftable on the chassis of the car to allow positioning of the outlet of that feeder over the hole communicating with the coking chamber without moving the car.

Abstract: Methods and compositions are provided which decrease the risk and spillage associated with discharging coke from a coking vessel. The risk to workers is decreased by eliminating the need for workers to be near the coking vessel while the head is being removed. The spillage is decreased by modifying the effective diameter of the coke chute inlet in a manner which allows it to catch any materials discharged from the coking vessel both during and after the opening of the bottom head. The process can enhance drum draining and further eliminate the need for process piping to facilitate the draining of water from the coking vessel.

Abstract: A coal compaction system and method for a non-recovery coke oven having refractory roof, floor, side walls and end doors for coal charging and coke discharge provides an improved coal charging machine carrying a coal conveyor supported intermediate the ends of the conveyor to avoid conveyor sagging and non-uniform depth of a deposited coal bed, a number of pressurized fluid-driven vibratory compactors mounted on an end of the charging machine and spaced-apart across the width of the coal bed and serving to compact the coal bed on a retraction stroke of the charging machine, a pivoted lifting frame mounted on the charging machine above the compactors and from which the compactors individually are suspended and are provided with individual supply of pressurized fluid, and a coke pusher head mounted on the charging machine behind the compactors and serving, when the lifting frame and associated compactors are raised, to push finished coke from the coke oven.

Abstract: In apparatus for thermolytic distillation of lump carbonaceous material, an enclosure contains a degassing bath, a reactor bath and a quenching bath. A closed loop continuous chain conveyor drives a plurality of baskets carrying carbonaceous material through the three baths of the enclosure. The carbonaceous material is degassed in hot distillate, then immersed in molten lead in the absence of oxygen to produce char and vapor by thermolytic distillation. The char is quenched with water in the absence of oxygen. At least a portion of the vapor is condensed to produce combustible distillate.

Abstract: The present invention provides a substantially remote operable system for connecting and disconnecting a vessel. The system comprises substantially a remotely operable joint connector for connecting and disconnecting structural units. The system and the method using the system may also comprise a remote operable closure transport for removing a vessel closure from an opening in the vessel, and a substantially remote operable removal system for allowing material to be emptied from the vessel to increase operational efficiency.

Abstract: A method for heating a low temperature carbonization drum includes generating a low temperature carbonization gas in the drum; combusting a partial flow of the low temperature carbonization gas for generating a heating gas; conducting the heating gas in a heating gas circuit; preheating the cooled heating gas flowing out of the drum; and then returning a controllable partial flow of the cooled heating gas to the drum while re-admixing the controllable partial flow with the heating gas.