Compressed Vapor As Heat Source Patents (Class 203/24)
  • Patent number: 11103803
    Abstract: A distillation device including: a first distillation column having first top, bottom and upper outlets and first upper and lower inlets; a second distillation column equipped with a top condenser and a bottom reboiler, and having second top, bottom and upper outlets and second upper and lower inlets; a vapor recompressor; a heat exchanger; a first supply line supplying a feedstock to the first lower inlet; a first connection line transferring a first bottom flow to the second lower inlet via the heat exchanger; and a second connection line transferring a second top flow to the top condenser via the heat exchanger after passing through the vapor recompressor. The first bottom flow flowing through the first connection line and the second top flow flowing through the second connection line are heat-exchanged in the heat exchanger. A distillation method of a feedstock using the distillation device.
    Type: Grant
    Filed: June 8, 2018
    Date of Patent: August 31, 2021
    Assignee: LG CHEM, LTD.
    Inventors: Tae Woo Kim, Sung Kyu Lee, Joon Ho Shin, Yeon Uk Choo
  • Patent number: 10016699
    Abstract: Significant energy saving can be achieved for a distillation column even when the distillation column has a large column temperature difference. Provided is a distillation column including a first and second columns, wherein the first column includes a part of a rectifying section or a part of a stripping section; the second column includes, if the first column includes a part of the rectifying section, the rest of the rectifying section and the whole of the stripping section, or the second column includes, if the first column includes a part of the stripping section, the rest of the stripping section and the whole of the rectifying section; and the second column constitutes a mechanical-heat-pump distillation column.
    Type: Grant
    Filed: January 9, 2015
    Date of Patent: July 10, 2018
    Assignee: Toyo Engingeering Corporation
    Inventors: Toshihiro Wakabayashi, Kouichi Tachikawa
  • Patent number: 9851140
    Abstract: A distillation apparatus includes a first distillation column and one or more second distillation columns. A higher-pressure part of the first distillation column includes at least part of a rectifying section, and performs gas-liquid contact at a relatively high pressure. A lower pressure-part of the first distillation column includes at least part of a stripping section and performs gas-liquid contact at a relatively low pressure. A vapor line, which includes a pressurizing means, directs a vapor discharged from a column top of the lower-pressure part to a column bottom of the higher-pressure part. A liquid line directs a liquid discharged from the column bottom of the higher-pressure part to the column top of the lower pressure part. Corresponding heat exchange structures transfer heat in both directions between the rectifying section of the first distillation column and at least one second distillation column.
    Type: Grant
    Filed: November 20, 2014
    Date of Patent: December 26, 2017
    Assignee: TOYO ENGINEERING CORPORATION
    Inventors: Toshihiro Wakabayashi, Takato Nakao
  • Patent number: 9028654
    Abstract: Disclosed herein is a system comprising an evaporation unit comprising a first heat exchanger in fluid communication with a second heat exchanger; where the first heat exchanger is operative to heat an effluent stream comprising an amine solvent and/or amine byproducts and water and to discharge the effluent stream to the second heat exchanger; where the second heat exchanger is operative to convert the effluent stream into a distillate stream and a concentrate stream; and a reverse osmosis unit in fluid communication with the evaporation unit; where the reverse osmosis unit comprises a first reverse osmosis unit that is operative to receive the distillate stream and to separate water from byproducts of the amine solvent such that the water has a purity of greater than 95%, based on the weight of the distillate stream.
    Type: Grant
    Filed: February 29, 2012
    Date of Patent: May 12, 2015
    Assignee: ALSTOM Technology Ltd
    Inventors: Bjoern Ungerer, Christoph Weingaertner, Hans-Peter Dornik
  • Publication number: 20150101921
    Abstract: A process for recovering heat from the separation of hydrocarbons. The overhead vapor stream from a fractionation column is passed to a two stage heat pump compressor. The first stage of compression is used to reboil the fractionation column. The second stage is compressed and cooled passed to a separation zone. The liquid in the separation zone may be passed back to the fractionation column as secondary reflux, and/or recovered as liquid product. Heat may also be removed from the second stage. A suction drum on the first stage may be used to protect the heat pump compressor from any droplets in the overhead stream.
    Type: Application
    Filed: July 29, 2014
    Publication date: April 16, 2015
    Inventors: Stephen T. King, Adam J. Kanyuh, Xin X. Zhu
  • Publication number: 20150075968
    Abstract: A compound multi effect distillation (MED) system of integrated backward and forward fed MED systems. Heated concentrate from the hottest effect of the backward fed MED system is delivered as feed to the hottest effect in the forward fed MED system, to generate a more concentrated brine than possible using any of the systems alone. Furthermore, coupling the systems creates additional operational advantages and increases distillation efficiency.
    Type: Application
    Filed: March 19, 2012
    Publication date: March 19, 2015
    Applicant: I.D.E. TECHNOLOGIES LTD.
    Inventors: Yaniv Schmidt, Joseph Newman, Herman Weiss
  • Patent number: 8951421
    Abstract: For purifying a liquid, the liquid is caused to evaporate in a cyclone in a recirculation circuit. Vapor is discharged via a discharge channel in which a compressor is included. In a heat exchanger downstream of the compressor, supplied vapor condenses and heat thereby released is transferred to liquid in the recirculation circuit. A liquid inlet of the cyclone is placed and directed for delivering a jet having a directional component tangential with respect to an inner surface of the cyclone. The liquid inlet has a section shaped such that in operation the delivered jet is a flat jet having a cross section which in a direction parallel to a nearest generatrix of the inner surface of the cyclone is greater than in a direction perpendicular thereto. The jet contacts the inner surface of the cyclone before drop formation occurs in the jet. A method for purifying a liquid is also described.
    Type: Grant
    Filed: March 2, 2010
    Date of Patent: February 10, 2015
    Assignee: Convex B.V.
    Inventor: Geert Jan Zanstra
  • Publication number: 20150014149
    Abstract: An accelerated vapor recompression apparatus 10 converts incoming flow 35a to a concentrate 35c by developing a concentration profile 146 within a tank 30 holding a liquid 23 containing dissolved solids. The resulting curve 160 of saturation temperature of the stratified liquid 23 (such as a brine 23 or other material 23) moves away from the curve 162 corresponding to fully mixed conditions. The shift 174, 180 in saturation temperature results in increased boiling without increased energy from a heater 70 or compressor 50. A method 90, 200 of control of the system provides interventions 203, 204, 205, 206 at different levels 92, 94, 96, 98 of control, ranging from mass flows 35 to work of a compressor 50, heat from a heater 70, and a predictive processing 215 of feedback 217 for controlling commands 216 algorithmically.
    Type: Application
    Filed: September 29, 2014
    Publication date: January 15, 2015
    Inventors: J. Clair Batty, Neil W. Richardson, David A. Bell, Christopher M. Miller
  • Publication number: 20140374235
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.
    Type: Application
    Filed: September 8, 2014
    Publication date: December 25, 2014
    Inventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
  • Patent number: 8888963
    Abstract: A water vending apparatus is disclosed. The water vending system includes a water vapor distillation apparatus and a dispensing device. The dispensing device is in fluid communication with the fluid vapor distillation apparatus and the product water from the fluid vapor distillation apparatus is dispensed by the dispensing device.
    Type: Grant
    Filed: January 28, 2013
    Date of Patent: November 18, 2014
    Assignee: DEKA Products Limited Partnership
    Inventors: Dean Kamen, Christopher C. Langenfeld, Ryan K. LaRocque, Andrew A. Schnellinger, Prashant Bhat, Stanley B. Smith, III, Otis L. Clapp, Jeremy M. Swerdlow
  • Publication number: 20140311888
    Abstract: The invention relates to a vapor-compression method. The aim of the invention is to provide such a method respectively a system with which a distillation with a further reduced energy requirement is possible, which simultaneously operates reliably, with little maintenance, and with only little available power, in particular when starting, and which is able to handle fluctuations in the available power. This is achieved in that an aqueous solution is preheated and fed to an evaporator at a lower end in order to generate vapor. The vapor is conducted from an upper end of the evaporator to a compressor (V) in order to be compressed. The vapor that is compressed in the compressor (V) is used to supply energy to the evaporator. The vapor that is thus cooled or optionally at least partly condensed is used to preheat the aqueous solution.
    Type: Application
    Filed: November 16, 2012
    Publication date: October 23, 2014
    Inventor: Fariba Khandanian
  • Patent number: 8845865
    Abstract: An accelerated vapor recompression apparatus 10 converts incoming flow 35a to a concentrate 35c by developing a concentration profile 146 within a tank 30 holding a liquid 23 containing dissolved solids. The resulting curve 160 of saturation temperature of the stratified liquid 23 (such as a brine 23 or other material 23) moves away from the curve 162 corresponding to fully mixed conditions. The shift 174, 180 in saturation temperature results in increased boiling without increased energy from a heater 70 or compressor 50. A method 90, 200 of control of the system provides interventions 203, 204, 205, 206 at different levels 92, 94, 96, 98 of control, ranging from mass flows 35 to work of a compressor 50, heat from a heater 70, and a predictive processing 215 of feedback 217 for controlling commands 216 algorithmically.
    Type: Grant
    Filed: January 31, 2013
    Date of Patent: September 30, 2014
    Assignee: Purestream Services, LLC
    Inventors: J. Clair Batty, Neil W. Richardson, David A. Bell, Christopher M. Miller
  • Patent number: 8828192
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.
    Type: Grant
    Filed: October 5, 2012
    Date of Patent: September 9, 2014
    Assignee: DEKA Products Limited Partnership
    Inventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
  • Patent number: 8771478
    Abstract: A modular distillation apparatus including at least one heat exchanger that preheats contaminated liquids: a heater that heats the contaminated liquid from the heat exchanger; an evaporator condenser adapted o boil the contaminated liquid coming out of the heater to produce water vapor and contaminant concentrate, and condenser the water vapor into distilled water; a vacuum chamber capable of operating at below atmospheric pressure, the vacuum chamber housing the evaporator condenser and including at least one partition to separate the distilled water from the contaminate concentrate; a vapor compressor operably associated with the vacuum chamber to receive water vapor from the evaporator condenser in the vacuum chamber and pump the water vapor at pressure back through the evaporator condenser, wherein the heat exchanger recovers sensible heat from outgoing condensed distilled water and contaminant concentrate recycled from the vacuum chamber.
    Type: Grant
    Filed: April 24, 2008
    Date of Patent: July 8, 2014
    Assignee: Equus Environmental Ltd.
    Inventor: Dudley Edgar James Ward
  • Publication number: 20140166263
    Abstract: Systems and methods generate steam in hydrocarbon recovery operations and may further enable emulsion separation and product upgrading. The methods rely on indirect boiling of water by contact with a thermal transfer liquid heated to a temperature sufficient to vaporize the water. Examples of the liquid include oils, recovered hydrocarbons, liquid metals and brine. Heating of the liquid may utilize circulation of the liquid across or through a furnace, heat exchangers, or a gas-liquid contactor supplied with hot gas. Further, a solvent for bitumen introduced into the water may also vaporize upon contact with the thermal transfer liquid.
    Type: Application
    Filed: December 5, 2013
    Publication date: June 19, 2014
    Applicant: CONOCOPHILLIPS COMPANY
    Inventors: Peter N. SLATER, Christopher R. COPELAND
  • Patent number: 8673158
    Abstract: The invention relates to a method for purifying wastewaters of melamine systems. The method is characterized in that triazine-containing wastewater is subjected to a thermal pretreatment stage, whereupon the vapors are condensed from the gas phase of the thermal pretreatment stage, and the liquid phase of the thermal pretreatment stage is subjected to a thermal hydrolysis stage while NH3 is isolated from the obtained liquid phase containing H2O, CO2, and NH3. The inventive method makes it possible to compensate varying wastewater qualities, thus allowing the melamine system and wastewater station to be operated in a constant and safe fashion. Furthermore, the strain on the subsequent thermal hydrolysis stage is relieved with the aid of the thermal pretreatment stage of the inventive method.
    Type: Grant
    Filed: June 13, 2006
    Date of Patent: March 18, 2014
    Assignee: AMI Agrolinz Melamine International GmbH
    Inventors: Wolfgang Ruech, Christoph Neumüller, Thomas Wallek
  • Patent number: 8647477
    Abstract: Water can be separated from a liquid composition (e.g., salt water) by directing a carrier gas flow through an evaporator and directly contacting the carrier gas flow with the liquid composition in the evaporator to humidify the carrier gas with water evaporated from the liquid composition, producing a humidified gas flow, which is then compressed by injecting a fluid that includes steam and/or an organic compound at an elevated pressure at least five times greater than the pressure in the evaporator and at a temperature at least as high as a saturation temperature of the steam/organic compound at the elevated pressure of the fluid. After being compressed, the humidified gas flow is directed through at least one condenser where water is condensed from the compressed humidified gas flow and collected; and the dehumidified gas flow is re-circulated back through the evaporator for reuse as the carrier gas.
    Type: Grant
    Filed: February 15, 2011
    Date of Patent: February 11, 2014
    Assignees: Massachusetts Institute of Technology, King Fahd University of Petroleum and Minerals
    Inventors: Prakash N. Govindan, Karan H. Mistry, John H. Lienhard, Syed M. Zubair
  • Patent number: 8603301
    Abstract: A method and apparatus for producing high purity distillate in evaporators. is useful for evaporation of waters where volatile silica or organic compounds are encountered such as in production of hydrocarbons from geological formations. An evaporator having a contaminant reduction system is provided. The contaminant reduction system includes an upflow first mist eliminator portion to remove entrained liquid droplets and produce an intermediate purity water vapor stream. A continuous spray system provides a spray of dilute caustic solution in a selected spray configuration for mass transfer contact with the passing intermediate purity water vapor stream, to remove volatile silica compounds therefrom, and produce a partially decontaminated steam stream having mist particles therein. An upflow second mist eliminator portion is provided to remove the residual mist particles, and produce a high purity water vapor stream. The high purity water vapor stream is condensed to provide a high purity distillate stream.
    Type: Grant
    Filed: September 29, 2010
    Date of Patent: December 10, 2013
    Assignee: General Electric Company
    Inventors: William F. Heins, Gregg L. Wilson
  • Patent number: 8506762
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.
    Type: Grant
    Filed: October 30, 2007
    Date of Patent: August 13, 2013
    Assignee: DEKA Products Limited Partnership
    Inventors: David F. Bednarek, Jason A. Demers, Timothy P. Duggan, James L. Jackson, Scott A. Leonard, David W. McGill, Kingston Owens
  • Patent number: 8496787
    Abstract: A method and apparatus for eliminating brine effluent from desalination plants by distillation, is disclosed. To eliminate the brine the salt is converted into a solid and all of the water in the brine is converted to distilled water. The key to achieving this is reducing or eliminating the scale formation in the heating chamber. In one embodiment the process can be used to reduce or eliminate scale formation in a vapor compression sea water desalinization system and there-by use this system to produce drinking water. This process requires no chemical additives but relies entirely upon separation of the process of vaporization of the fluid involved, from the process of heating of the fluid. In one embodiment of this apparatus sea water can be desalinated and the resulting products can be dry salt and pure water leaving no brine return to the ocean.
    Type: Grant
    Filed: July 26, 2009
    Date of Patent: July 30, 2013
    Inventor: Michael John Lord
  • Publication number: 20130186741
    Abstract: An accelerated vapor recompression apparatus 10 converts incoming flow 35a to a concentrate 35c by developing a concentration profile 146 within a tank 30 holding a liquid 23 containing dissolved solids. The resulting curve 160 of saturation temperature of the stratified liquid 23 (such as a brine 23 or other material 23) moves away from the curve 162 corresponding to fully mixed conditions. The shift 174, 180 in saturation temperature results in increased boiling without increased energy from a heater 70 or compressor 50. A method 90, 200 of control of the system provides interventions 203, 204, 205, 206 at different levels 92, 94, 96, 98 of control, ranging from mass flows 35 to work of a compressor 50, heat from a heater 70, and a predictive processing 215 of feedback 217 for controlling commands 216 algorithmically.
    Type: Application
    Filed: January 31, 2013
    Publication date: July 25, 2013
    Applicant: PURESTREAM SERVICES, LLC
    Inventor: Purestream Services, LLC
  • Publication number: 20130168225
    Abstract: The aim of the invention is to improve the energetic efficiency of the distiller by effective utilization of the residual heat. The invention relates to distillator with a thermal energy recycling in the closed loop energy circulation and to methods for thermal energy recycling of the distiller by returning the residual heat to the initial environment via the heat pump. The invention also further relates to reuse of the heat loss of the distiller using the heat pump which returns the residual heat to the initial environment. In distillers and methods according to present invention the heat energy and thermal losses are used repeatedly again in a closed loop energy circulation. If the problem of intensive energy consumption is resolved the distiller according to this invention can be appropriately utilized for instance in production of drinking water from the seawater or from any available natural water, as well as at the finishing stage of the noncomplicated wastewater treatment process.
    Type: Application
    Filed: September 8, 2011
    Publication date: July 4, 2013
    Applicant: HEAT RECYCLERS, OU
    Inventors: Tarmo Oikimus, Konstantin Oikimus, Mart Eensalu
  • Publication number: 20130146438
    Abstract: In a process for concentrating aqueous hydrogen peroxide solution to give two hydrogen peroxide streams of different concentration in an apparatus comprising a preevaporator (1), a distillation column (2) and a vapour compressor (3), in which the aqueous hydrogen peroxide solution to be concentrated (4) is continuously fed into the preevaporator, vapour (5) produced by evaporation in the preevaporator is fed to the distillation column, bottom product (6) obtained in the preevaporator is withdrawn as a first concentrated hydrogen peroxide stream (7), vapour (8) produced in the distillation column is withdrawn from the distillation column at the top of the column, compressed by means of the vapour compressor and used for heating the preevaporator and the bottom product (9) obtained in the distillation column is withdrawn as a second concentrated hydrogen peroxide stream (10), two concentrated hydrogen peroxide solutions having differing concentrations in the range from 50 to 70% by weight of hydrogen peroxide c
    Type: Application
    Filed: July 29, 2011
    Publication date: June 13, 2013
    Applicant: Evonik Degussa GmbH
    Inventors: Hubertus Eickhoff, Florian Lode, Eduardo Arevalo, Marc Brendel, Claudia Wallert
  • Patent number: 8444830
    Abstract: A desalination process including heating brine in a preheating chamber and transferring the brine to a rotary kiln to be sprayed against the wall structure of the rotary kiln to boil to steam and a residue of salt/impurities, the exiting steam being pressurized in a compressor and passed to an externally powered heater to be heated and then fed to a hollow wall structure of the rotating kiln in which the steam condenses to pure water to be transferred to the preheating chamber to preheat the incoming brine, the rotating kiln being arranged to rotate past a scraper to remove salt/impurities from the wall structure for collection at the base of the kiln.
    Type: Grant
    Filed: June 17, 2008
    Date of Patent: May 21, 2013
    Inventor: Garth Davey
  • Patent number: 8328995
    Abstract: A method and a system to produce a distillate stream from an aqueous stream containing at least one dissolved solid by a thermal distillation process using at least one of a heated aqueous stream from a turbine system intercooler and a stack heater as a heat source.
    Type: Grant
    Filed: February 9, 2007
    Date of Patent: December 11, 2012
    Assignee: Black & Veatch Holding Company
    Inventor: Michael J. Eddington
  • Patent number: 8323457
    Abstract: Systems and methods for separating a multi-component fluid are provided. The method can include introducing a multi-component fluid to a dividing wall column. The multi-component fluid can be heated to provide a first product, a second product, an intermediate distillate, and a process fluid. At least a portion of the first product can be compressed to provide a compressed first product. Heat can be indirectly transferred from the compressed first product to at least a portion of the intermediate distillate to provide a heated intermediate distillate. The heated intermediate distillate can be recycled to the dividing wall column. The compressed first product can be expanded.
    Type: Grant
    Filed: October 28, 2009
    Date of Patent: December 4, 2012
    Assignee: Kellogg Brown & Root LLC
    Inventors: Derek William Townsend, Cyril Collins
  • Patent number: 8282790
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.
    Type: Grant
    Filed: October 29, 2007
    Date of Patent: October 9, 2012
    Assignee: DEKA Products Limited Partnership
    Inventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
  • Patent number: 8246789
    Abstract: A treatment system for a watery material that includes: a dewatering tank in which liquefied matter of a material that is gaseous at a normal temperature and a normal pressure is contacted with the watery material and the watery material is separated into the resultant watery material and a liquid phase that contains an aqueous component from the watery material; an evaporator that vaporizes the material that is gaseous at a normal temperature and a normal pressure from the liquid phase; a separator that separates a gas of the material thus vaporized from effluent water; a condenser that condenses the gas into liquefied matter, two or more external heat sources selected from atmosphere, sewage, warm effluent water, and ground water; an external heat temperature detector that detects temperatures of external heats of the external heat sources; and an external heat supply destination controlling unit.
    Type: Grant
    Filed: March 6, 2008
    Date of Patent: August 21, 2012
    Assignees: Central Research Institute of Electric Power Industry, Tsukishima Kikai Co., Ltd.
    Inventors: Hideki Kanda, Hisao Makino, Mayumi Morita, Keizo Takegami, Akio Yoshikoshi, Masazumi Takahashi
  • Publication number: 20120097520
    Abstract: The invention provides a process and apparatus for the separation of a gaseous feed comprising a mixture of hydrocarbons and nitrogen gas, the process comprising the steps of: (i) cooling and at least partially condensing the gaseous feed; (ii) feeding the cooled and at least partially condensed feed from step (i) to a fractionation column comprising reboil to produce an overhead hydrocarbon vapour stream enriched in nitrogen and a condensed hydrocarbon product stream low in nitrogen, wherein prior to the fractionation, the feed stream is divided into at least two streams including: a) a first stream which is expanded and fed to the fractionation column; b) a second stream which is expanded, heated and fed to a lower stage of the fractionation column than the first stream, (iii) removing a hydrocarbon product stream low in nitrogen from the fractionation column; and (iv) removing a hydrocarbon vapour stream enriched in nitrogen from the fractionation column.
    Type: Application
    Filed: March 23, 2010
    Publication date: April 26, 2012
    Applicant: COSTAIN OIL, GAS & PROCESS LIMITED
    Inventors: Grant Leigh Johnson, Adrian Joseph Finn, Terence Ronald Tomlinson
  • Patent number: 8128787
    Abstract: Processes for removing water from organic solvents, such as ethanol. The processes include distillation in two columns operated at sequentially higher pressure, followed by treatment of the overhead vapor by one or two membrane separation steps.
    Type: Grant
    Filed: August 27, 2008
    Date of Patent: March 6, 2012
    Assignee: Nitto Denko Corporation
    Inventors: Nicholas P. Wynn, Yu Huang, Masakatsu Urairi, Richard W Baker
  • Publication number: 20120037489
    Abstract: For purifying a liquid, the liquid is caused to evaporate in a cyclone in a recirculation circuit. Vapor is discharged via a discharge channel in which a compressor is included. In a heat exchanger downstream of the compressor, supplied vapor condenses and heat thereby released is transferred to liquid in the recirculation circuit. A liquid inlet of the cyclone is placed and directed for delivering a jet having a directional component tangential with respect to an inner surface of the cyclone. The liquid inlet has a section shaped such that in operation the delivered jet is a flat jet having a cross section which in a direction parallel to a nearest generatrix of the inner surface of the cyclone is greater than in a direction perpendicular thereto. The jet contacts the inner surface of the cyclone before drop formation occurs in the jet. A method for purifying a liquid is also described.
    Type: Application
    Filed: March 2, 2010
    Publication date: February 16, 2012
    Applicant: Convex B.V.
    Inventor: Geert Jan Zanstra
  • Patent number: 8114255
    Abstract: Processes for removing water from organic solvents, such as ethanol. The processes include distillation in two columns operated at sequentially higher pressure, followed by treatment of the overhead vapor by one or two membrane separation steps.
    Type: Grant
    Filed: August 27, 2008
    Date of Patent: February 14, 2012
    Assignee: Membrane Technology & Research, Inc.
    Inventors: Leland M Vane, Franklin R Alvarez, Yu Huang, Richard W Baker
  • Patent number: 8075741
    Abstract: In the water purification process, apparatus, and method, contaminated water vapor is exposed to liquid solvent, which causes a transfer of contaminants from the contaminated water vapor to the liquid solvent. In an advantageous embodiment, this latter step is followed by a second purification step where the decontaminated water in liquid phase is exposed to water vapor which causes a transfer of solvent remaining in the decontaminated water to the water vapor. The energy freed during the condensation of the vapor can advantageously be used for evaporation of the liquids, optionally by compressing the vapors prior to condensation thereof within heat exchangers.
    Type: Grant
    Filed: October 26, 2006
    Date of Patent: December 13, 2011
    Inventor: Daniel Blanchette
  • Patent number: 8075740
    Abstract: A system for treating feedwater includes a fluidized bed heat exchanger unit connected to receive feedwater and a flash concentrator column connected to receive feedwater discharged from the fluidized bed heat exchanger unit. A spray dryer is provided to receive a solids/liquid slurry discharged from the flash concentrator column. Feedwater can be treated by converting dissolved solids in the feedwater to suspended solids, vaporizing a portion of the feedwater to produce a solids/liquid slurry, and separating solids from the solids/liquid slurry.
    Type: Grant
    Filed: June 29, 2009
    Date of Patent: December 13, 2011
    Assignees: AHT Solutions, LLC, Watervap, LLC
    Inventors: Robert E. Bailie, Robert R. Wright
  • Patent number: 7927464
    Abstract: A vapor compression distillation system (10) is provided and includes a fluid inlet (12) for receiving a fluid, a fluid outlet (14) for a distillate that has been distilled from the fluid, a heat exchanger (16) connected to the fluid inlet (12) and the fluid outlet (14) to transfer heat from the distillate to the fluid; and an integrated motor/compressor unit (18) connected to the heat exchanger (16) to receive vaporized distillate therefrom and to supply pressurized distillate thereto. The system 10 may further include a coolant system (20) connected to the integrated motor/compressor (18) to supply a coolant flow thereto. The system (10) may also include an air oil mist system (22) that is connected to the integrated motor/compressor unit (18) to supply an air oil mist thereto for bearing lubrication and cooling.
    Type: Grant
    Filed: July 24, 2007
    Date of Patent: April 19, 2011
    Assignee: Mechanical Equipment Company, Inc.
    Inventors: George V. Gsell, Kim C. Klein
  • Publication number: 20100192875
    Abstract: A system and method are provided for heating, concentrating and/or evaporating a fluid by heating the fluid in a heating subsystem comprising a rotary heating device, such as a water brake dynamometer, and then evaporating all or a portion of the fluid in an evaporation subsystem and/or concentrating the fluid in a concentration subsystem.
    Type: Application
    Filed: November 10, 2009
    Publication date: August 5, 2010
    Inventor: F. ALAN FRICK
  • Publication number: 20100175983
    Abstract: Petroleous production is associated with effluents well known to foul lines, nozzles, and containers while consuming substantial energy to assist in both production and remediation. A heat exchanger and manifold system maximizes flows, minimizes changes in flow cross-section, and maximizes heat transfer area, while recycling both water and heat between processes. Dirty regions and clean regions result from scrubbing horizontal exhaust stacks and evaporation of production water in concert to remediate one another, while recycling a significant portion of the energy consumed by each. The heat exchanger relies on a manifold having many layered conduits, each connected to a single layer level of one or more cylindrical conduits in the exchanger. The cylinders of the exchanger themselves are arranged in multiple layers, each layer of a heat exchanger element being connected to a single layer of the manifold.
    Type: Application
    Filed: January 14, 2010
    Publication date: July 15, 2010
    Applicant: Total Water Management, LLC
    Inventors: J. Clair Batty, David A. Bell, Craig E. Cox
  • Patent number: 7641772
    Abstract: A distillation unit (10) employs a fluid circuit (FIG. 8) in which a counterflow heat exchanger (102, 104, 106, 108, 110) transfers heat from condensate and concentrate to feed liquid to be distilled. The pumping system (100, 238) that drives fluid through the circuit is arranged to keep the pressure in the counterflow heat exchanger's condensate higher than that in its feed-liquid passage. This tends to discourage the contamination that could otherwise occur in the concentrate if the fluid isolation ordinarily maintained between those passages is compromised.
    Type: Grant
    Filed: January 20, 2005
    Date of Patent: January 5, 2010
    Assignee: Zanaqua Technologies, Inc.
    Inventor: William H. Zebuhr
  • Publication number: 20090294272
    Abstract: The invention relates to a method for purifying wastewaters of melamine systems. The method is characterized in that triazine-containing wastewater is subjected to a thermal pretreatment stage, whereupon the vapors are condensed from the gas phase of the thermal pretreatment stage, and the liquid phase of the thermal pretreatment stage is subjected to a thermal hydrolysis stage while NH3 is isolated from the obtained liquid phase containing H2O, CO2, and NH3. The inventive method makes it possible to compensate varying wastewater qualities, thus allowing the melamine system and wastewater station to be operated in a constant and safe fashion. Furthermore, the strain on the subsequent thermal hydrolysis stage is relieved with the aid of the thermal pretreatment stage of the inventive method.
    Type: Application
    Filed: June 13, 2006
    Publication date: December 3, 2009
    Applicant: AMI GROLINZ MELAMINE INTERNATIONAL GMBH
    Inventors: Wolfgang Ruech, Christoph Neumüller, Thomas Wallek
  • Patent number: 7597784
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.
    Type: Grant
    Filed: November 13, 2003
    Date of Patent: October 6, 2009
    Assignee: DEKA Products Limited Partnership
    Inventors: David F. Bednarek, Jason A. Demers, Timothy P. Duggan, James L. Jackson, Scott A. Leonard, David W. McGill, Kingston Owens
  • Patent number: 7594980
    Abstract: Device for distillation, for example extraction of fresh water from sea water, including a number of chambers (3) at least in one row, an inlet (10) for distillation fluid, an outlet (11) for the distillation residue, an outlet (5) for the distillate, and a gas compressor (13). Further, the device includes two pipe systems (1,2), where the first pipe system (1) has an inlet (10) for the distillation fluid and an outlet (11) for the distillation residue, together with an outlet (12) for damp. The second pipe system (2) has a number of chambers (3) in a row, each row (3) having an upper inlet (4) for damp and a lower outlet (5) for distillate. The inlets (4) are connected in parallel, and the outlets (5) are connected in parallel.
    Type: Grant
    Filed: November 29, 2002
    Date of Patent: September 29, 2009
    Assignee: GND Water AS
    Inventor: Olav E. Sandstad
  • Publication number: 20090057128
    Abstract: An improved process for separation of liquid mixtures involves vapor stripping followed by mechanical compression of the vapor which is then exposed to a permeation membrane for separation of the compressed vapor.
    Type: Application
    Filed: August 30, 2007
    Publication date: March 5, 2009
    Inventors: Leland Vane, Franklin R. Alvarez
  • Patent number: 7465376
    Abstract: The invention provides for the removal of impurities from treatment fluid including a base liquid and a variety of impurities contained in the base liquid by conveying the treatment fluid to at least one preheating separating device, including a preheating heat exchanger and a separator unit, before the admixture of a carrier gas to the treatment fluid. The treatment fluid is preheated by the preheating heat exchanger to a temperature below the boiling temperature of a base liquid so that the liquid impurities with lower boiling temperatures than the base liquid are evaporated and expelled thermally, whereby the evaporated and expelled impurities are separated in the separator unit of the preheating separator device. The treatment fluid is then evaporated and separated from impurities having a higher boiling point than the base liquid.
    Type: Grant
    Filed: February 9, 2002
    Date of Patent: December 16, 2008
    Inventors: Joachim Neubert, Karl-Ferdinand Staab
  • Patent number: 7378536
    Abstract: Process for preparing propylene oxide, which comprises at least the steps (iii) and (iv) (iii) separating off propylene oxide from a mixture (M1) comprising propylene oxide and at least one solvent by distillation in a distillation column, giving a bottom stream and a vapor stream consisting essentially of propylene oxide; (iv) compressing the vapor stream obtained in (iii) by means of at least one compressor to give a compressed vapor.
    Type: Grant
    Filed: April 16, 2004
    Date of Patent: May 27, 2008
    Assignee: BASF Aktiengesellschaft
    Inventors: Hans-Georg Goebbel, Peter Bassler, Joaquim Henrique Teles, Peter Rudolf
  • Patent number: 6846390
    Abstract: Methods for using a hydrophobic liquid, such as mineral oil, to compress steam include using a compressor to compress a mixture of steam and the hydrophobic liquid. One embodiment includes the steam to be compressed coming from a boiling aqueous solution in an evaporator. The steam compressed with a hydrophobic liquid is routed to a heat exchanger which thermally communicates with the evaporator to create more steam. The resulting mixture of condensed steam and hydrophobic liquid from the heat exchanger is routed to a water/hydrophobic liquid separator. The hydrophobic liquid is also recycled to the compressor from the water/hydrophobic liquid separator.
    Type: Grant
    Filed: September 9, 2002
    Date of Patent: January 25, 2005
    Inventor: David Bruce Bishkin
  • Publication number: 20040222079
    Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.
    Type: Application
    Filed: June 9, 2004
    Publication date: November 11, 2004
    Inventor: William H. Zebuhr
  • Patent number: 6802941
    Abstract: A distillation unit (10) employs a rotary heat exchanger (32) forming a multiplicity of evaporation chambers (56) into which a liquid to be purified is sprayed for evaporation. Spray arms (58) spray at a steady rate into all of the evaporation chambers (56) simultaneously but not at a rate that is adequate to maintain the wetting required for efficient transfer of heat to the liquid. A scanning sprayer (140) supplements this steady spray with spray from nozzles (142 and 144) into only a few of the evaporation chambers at a time, visiting all of them cyclically. The overall rate of spray from the two sources thus combined to spray the chamber cyclically maintains proper wetting even though on average it is lower than the rate that would be required of a constant-rate spray into all of the evaporation chambers.
    Type: Grant
    Filed: January 18, 2001
    Date of Patent: October 12, 2004
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr
  • Publication number: 20040099521
    Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.
    Type: Application
    Filed: November 13, 2003
    Publication date: May 27, 2004
    Applicant: DEKA Products Limited Partnership
    Inventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
  • Patent number: 6740205
    Abstract: Incoming wastewater is preheated in a heat exchanger before delivery to a flash chamber through an orifice for flashing into water vapor rising into an upper section of the flash chamber which also has a bottom section into which liquid waste oil or other contaminants settles. Rise of such water vapor into the upper chamber section is induced by a vacuum established therein by a vacuum pump withdrawing the water vapor in a superheated and compressed condition for cooling within a condenser from which the incoming wastewater is delivered to a heat exchanger for preheating. The water vapor during rise into the upper section of the flash chamber is filtered to extract contaminates therefrom while liquefied water vapor thereafter formed therein is collected before the remaining water vapor is cooled into the condensate for collection within a distillate tank from which it is withdrawn for overboard discharge after being monitored for oil content.
    Type: Grant
    Filed: November 30, 2000
    Date of Patent: May 25, 2004
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: Henry J. Molintas
  • Patent number: 6689251
    Abstract: A distiller (10) that employs a rotary heat exchanger (32) introduces water to be evaporated into evaporation chambers (56). During most of its operation, it collects the water that has passed through the evaporation chamber (56) without evaporating, and it reintroduces the thus-collected liquid back into the evaporation chamber, where it also adds a minor amount of unrecirculated feed liquid to make up for evaporation and concentrate removal. Simultaneously, a minor amount of feed liquid is fed into one side of a transfer pump (116). During this mode of operation, the impurities concentration in the recirculating liquid tends to increase as a result of the evaporation of pure water vapor. Periodically, the erstwhile recirculating liquid is redirected to the other side of the transfer pump (116), where it causes the feed liquid stored in the transfer pump's first side to be fed without accompanying recirculant liquid into the rotary heat exchanger's evaporation chambers.
    Type: Grant
    Filed: January 18, 2001
    Date of Patent: February 10, 2004
    Assignee: Ovation Products Corporation
    Inventor: William H. Zebuhr