Of Entrained Particles From A Vapor Or Gas Patents (Class 203/40)
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Patent number: 12163496Abstract: An igniter system and method for igniting a propellant by an optical energy source. The igniter system including an igniter composite and a propellant. The igniter composite including a reactive component and a fluoropolymer. The propellant is coupled to the igniter composite. The igniter composite has a composition including nano-aluminum at ideal stoichiometry in polyvinylidene fluoride. The igniter composite is configured to achieve a sustained ignition from a wavelength emitted from the optical energy source. The wavelength is between around 250 nanometers to around 1100 nanometers.Type: GrantFiled: December 1, 2023Date of Patent: December 10, 2024Assignee: Purdue Research FoundationInventors: Steven Forrest Son, Kyle Uhlenhake, Diane Collard, Mateo Gomez
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Patent number: 11939276Abstract: A nanoparticle of a decomposition product of a transition metal aluminum hydride compound, a transition metal borohydride compound, or a transition metal gallium hydride compound. A process of: reacting a transition metal salt with an aluminum hydride compound, a borohydride compound, or a gallium hydride compound to produce one or more of the nanoparticles. The reaction occurs in solution while being sonicated at a temperature at which the metal hydride compound decomposes. A process of: reacting a nanoparticle with a compound containing at least two hydroxyl groups to form a coating having multi-dentate metal-alkoxides.Type: GrantFiled: December 3, 2020Date of Patent: March 26, 2024Assignee: The Government of the United States of America, as represented by the Secretary of the NavyInventors: Albert Epshteyn, Zachary J. Huba
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Patent number: 11934360Abstract: A database storing data associated with an identifier unique to each sample, the data including first data representative of at least one of composition data, processing data, and property data for the each sample, and second data representative of microstructure data for the each sample. The microstructure data includes a feature determined based on a temperature dependence of magnetization for the each sample.Type: GrantFiled: June 5, 2023Date of Patent: March 19, 2024Assignee: PROTERIAL, LTD.Inventors: Takeshi Nishiuchi, Daisuke Furusawa, Asami Oya
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Patent number: 11873788Abstract: An igniter system and method for igniting a propellant by an optical energy source. The igniter system including an igniter composite and a propellant. The igniter composite including a reactive component and a fluoropolymer. The propellant is coupled to the igniter composite. The igniter composite has a composition including nano-aluminum at ideal stoichiometry in polyvinylidene fluoride. The igniter composite is configured to achieve a sustained ignition from a wavelength emitted from the optical energy source. The wavelength is between around 250 nanometers to around 1100 nanometers.Type: GrantFiled: February 28, 2022Date of Patent: January 16, 2024Assignee: Purdue Research FoundationInventors: Steven Forrest Son, Kyle Uhlenhake, Diane Collard, Mateo Gomez
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Patent number: 11827993Abstract: Provided are methods of forming active materials for electrochemical cells using low-temperature electrochemical deposition, e.g., less than 200° C. Specifically, these processes allow precise control of the morphology, composition, and size of deposited structures. For example, the deposited structure may be doped, alloyed, or surface treated during their deposition using a combination of different precursors. In particular, silicon structure may be pre-lithiated while these structures are being formed. The selection of working electrodes (surface size and properties), electrolyte composition, and other parameters result in different types of structures, e.g., precipitating from the electrolyte or deposited on the electrode. Low-temperature plating does not require a lot of energy and volatile and invisible precursors. Furthermore, this plating produces a more confined waste stream, suitable for post-reaction recycling.Type: GrantFiled: September 17, 2021Date of Patent: November 28, 2023Assignee: GRU Energy Lab Inc.Inventors: Xiahui Yao, Xiaohua Liu, Sa Zhou, Song Han
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Patent number: 11828694Abstract: The present invention relates to an apparatus for real-time continuous measurement of airborne microorganisms including a body unit, a vaporization unit, a liquefaction unit, a coating unit, and a measurement unit. The body unit has an inlet through which airborne microorganisms are introduced and an outlet through which airborne microorganisms are discharged. The vaporization unit vaporizes a lysis solution and supplies the vaporized lysis solution to the inside of the body unit. The liquefaction unit cools the vaporized lysis solution to condense the vaporized lysis solution on the surfaces of the airborne microorganisms. The coating unit applies a light-emitting agent onto the airborne microorganisms lysed by the lysis solution. The measurement unit detects the intensity of light generated by reacting the airborne microorganisms and the light-emitting agent and measures the concentration of the airborne microorganisms.Type: GrantFiled: August 8, 2019Date of Patent: November 28, 2023Assignee: INDUSTRY-ACADEMIC COOPERATION FOUNDATION, YONSEI UNIVERSITYInventors: Jung Ho Hwang, Jang Seop Han, Hyeong Rae Kim, Sang Gwon An
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Patent number: 11780744Abstract: A seawater distillation system for distilling seawater and brine and removing salt. The seawater distillation system includes an apparatus having at least a vessel, a separation assembly, and at least one mist eliminator. The vessel may be adapted to hold a volume of seawater comprising a volume of salt, wherein vessel is one of externally heated and internally heated to evaporate the volume of seawater to a volume of steam and to precipitate the volume of salt. The separation assembly may be operably engaged with the vessel, wherein the separation assembly is configured to separate the volume of salt from the volume of seawater inside of the vessel. The at least one mist eliminator may be operably engaged with the vessel and positioned vertically above the separation assembly, wherein the at least one mist eliminator is configured to eliminate water droplets and salt from the volume of steam.Type: GrantFiled: August 2, 2022Date of Patent: October 10, 2023Assignee: DESERT WATER LLCInventor: Thomas F. Butryn
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Patent number: 11692797Abstract: An explosive device composed of an auxiliary flux compression generator operating to produce a high intensity magnetic field to seed a primary flux compression generator The auxiliary flux compression generator has a first section with a magnetic field supplied by a cylindrical permanent magnet array, the first section is composed of a helical winding having a prescribed pattern configured to convert explosive energy into magnetic energy that will be used as seed magnetic field for the primary flux compression generator.Type: GrantFiled: April 15, 2020Date of Patent: July 4, 2023Assignee: ENIG ASSOCIATES, INC.Inventors: Yil-Bong Kim, Eric N. Enig
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Patent number: 11565194Abstract: Systems for extracting solute from a source material are shown and described. Each of the systems includes: a solvent source container configured to store a cooled solvent, a canister configured to contain the source material and receive solvent to produce an extract solution, and one or more extract containers in communication configured to receive and distill the extract solution, the solvent source container being configured to receive a post-extraction portion of the solvent. In some examples, the one or more extract containers are first and second extract containers that are each selectively coupleable to the canister and are selectively removable for storage of the extract mixture or the solute. In some other examples, the system further includes a cooling mechanism coupled to the solvent source container for cooling the recycled solvent within the solvent collection container.Type: GrantFiled: August 22, 2019Date of Patent: January 31, 2023Inventors: Jason Wasserman, Jess Ordower, Samual Decker
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Patent number: 8986508Abstract: A thermal desalination system adapted to produce distilled water from feed water which may be sea water, based on a forward feed evaporator made up of a main water feed line, a vapor feed line, a distilled water main line and any number of effect groups. The effect groups include any number of effects which in turn include vapor inlets, water inflow lines, concentrate outflow lines that drain into a common concentrate drainage line, a vapor and water outlet in fluid communication with the distilled water main line, and heat transfer means that condense part of an inlet vapor to produce the distilled water.Type: GrantFiled: October 21, 2013Date of Patent: March 24, 2015Assignee: I.D.E. Technologies Ltd.Inventors: Avraham Ophir, Joseph Weinberg
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Patent number: 8951421Abstract: For purifying a liquid, the liquid is caused to evaporate in a cyclone in a recirculation circuit. Vapor is discharged via a discharge channel in which a compressor is included. In a heat exchanger downstream of the compressor, supplied vapor condenses and heat thereby released is transferred to liquid in the recirculation circuit. A liquid inlet of the cyclone is placed and directed for delivering a jet having a directional component tangential with respect to an inner surface of the cyclone. The liquid inlet has a section shaped such that in operation the delivered jet is a flat jet having a cross section which in a direction parallel to a nearest generatrix of the inner surface of the cyclone is greater than in a direction perpendicular thereto. The jet contacts the inner surface of the cyclone before drop formation occurs in the jet. A method for purifying a liquid is also described.Type: GrantFiled: March 2, 2010Date of Patent: February 10, 2015Assignee: Convex B.V.Inventor: Geert Jan Zanstra
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Patent number: 8951392Abstract: A modular portable evaporator system for use in a Steam Assisted Gravity Drainage (SAGD) systems having an evaporator, with a sump including an oil skimming weir, a short tube vertical falling film heat exchanger including an outer shell containing short tubes provided for lower water circulation rate. The system further having external to the evaporator, a compressor for compressing evaporated steam from the tube side of the heat exchanger and routing to the shell side of the same exchanger, a distillate tank to collect hot distilled water, a recirculation pump to introduce liquids from the sump into the heat exchanger and an external suction drum protecting the compressor from liquid impurities. The evaporator system receives produced water from the SAGD process into the sump and provides cleaned hot water to a boiler.Type: GrantFiled: April 15, 2011Date of Patent: February 10, 2015Assignee: 1nSite Technologies Ltd.Inventor: Kenneth James
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Patent number: 8946309Abstract: Process to generate synthesis gas and/or liquid raw materials and/or energy materials from waste and/or biomass by performing the following steps: a) solvolysis of the organic components of waste and/or biomass in an alkaline solution or hydrate smelter at a temperature range of 150° to 250° C. and pressure between 3 and 12 bar, whereby the organic components are converted into at least one liquid phase and the inorganic components are sedimented; b) elimination of the inorganic components from the liquid phase by physical separation methods; c) transfer of the vapors generated during the solvolysis into a rectification column, where the organic components are separated from water; and d) further separation of the organic components by rectification, extraction and sorption and/or conversion by thermal gasification into synthesis gas or burnable gas.Type: GrantFiled: November 20, 2009Date of Patent: February 3, 2015Inventors: Wenzel Bergmann, Thomas Müller
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Patent number: 8864951Abstract: Systems and processes for improving quality and yield of one or more distillate products generated in a distillation column are disclosed. The system comprises a feed inlet distributor that reduces the amount of liquid entrained in vapor rising from the feed zone of the distillation column, a wash zone collection apparatus having an improved design for collecting slop wax falling from a liquid/vapor contacting structure provided in the wash zone, a recirculation subsystem for recirculating at least a portion of the collected slop wax to the top of the wash zone for distribution as wash oil, and a control subsystem. The feed inlet distributor ensures a horizontal fluid flow path free of transverse surfaces thereby minimizing atomization of liquid droplets entrained in vapor in the feed stream.Type: GrantFiled: March 17, 2011Date of Patent: October 21, 2014Assignee: ThioSolv, LLCInventors: Mark C. Anderson, George R. Winter
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Publication number: 20140227548Abstract: There are disclosed energetic nanoparticle compositions and materials containing silicon and other energetic elements, and methods of manufacturing the same, including reacting silicon nanoparticles and unsaturated alkene or alkyne to form covalently bonded surface coatings passivated against surface oxidation, for combination with a fuel, explosive or oxidizer.Type: ApplicationFiled: February 25, 2014Publication date: August 14, 2014Inventor: James J. Myrick
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Patent number: 8776879Abstract: Embodiments presented herein provide an evaporation based zero liquid discharge method for generation of up to 100% quality high pressure steam from produced water in the heavy oil production industry. De-oiled water is processed in an evaporation system producing a distillate that allows steam to be generated with either drum-type boilers operating at higher pressures or once-through steam generators (OTSGs) operating at higher vaporization rates. Evaporator blowdown is treated in a forced-circulation evaporator to provide a zero liquid discharge system that could recycle >98% of the deoiled water for industrial use. Exemplary embodiments of the invention provide at least one “straight sump” evaporator and at least one hybrid external mist eliminator. Embodiments of the evaporation method operate at a higher overall efficiency than those of the prior art by producing distillate at a higher enthalpy which minimizes the high pressure boiler preheating requirement.Type: GrantFiled: June 4, 2013Date of Patent: July 15, 2014Assignee: Aquatech International CorporationInventors: Daniel P. Bjorklund, Gregory J. Mandigo, Richard M. Schoen, James Michael Marlett, Chandrakant Tiwari
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Patent number: 8771477Abstract: Embodiments of the invention provide systems and methods for water purification and desalination. The systems have a preheater, a degasser, multiple evaporation chambers with demisters, heat pipes, and a control system, wherein the control system permits continuous operation of the purification and desalination system without requiring user intervention or cleaning. The systems are capable of recovering hear from each distillation stage, while removing, from a contaminated water sample, a plurality of contaminants including: microbiological contaminants, radiological contaminants, metals, salts, and organics.Type: GrantFiled: September 17, 2009Date of Patent: July 8, 2014Assignee: Sylvan Source, Inc.Inventor: Eugene Thiers
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Publication number: 20140166263Abstract: Systems and methods generate steam in hydrocarbon recovery operations and may further enable emulsion separation and product upgrading. The methods rely on indirect boiling of water by contact with a thermal transfer liquid heated to a temperature sufficient to vaporize the water. Examples of the liquid include oils, recovered hydrocarbons, liquid metals and brine. Heating of the liquid may utilize circulation of the liquid across or through a furnace, heat exchangers, or a gas-liquid contactor supplied with hot gas. Further, a solvent for bitumen introduced into the water may also vaporize upon contact with the thermal transfer liquid.Type: ApplicationFiled: December 5, 2013Publication date: June 19, 2014Applicant: CONOCOPHILLIPS COMPANYInventors: Peter N. SLATER, Christopher R. COPELAND
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Patent number: 8709257Abstract: A method and system for purifying liquid using waste heat is provided. Initially, a liquid is mixed with an anti-sealant agent in a first filtering unit to form a liquid mixture. Thereafter, the liquid mixture is filtered in the first filtering unit to separate foreign objects from the liquid mixture. Subsequently, the liquid mixture is heated in a pipe arrangement connecting the first filtering unit and one or more second filtering units to generate steam. The steam obtained from the heated liquid mixture is then purified in the one or more second filtering units. Thereafter, the purified steam is condensed in the pipe arrangement to obtain the purified liquid.Type: GrantFiled: April 20, 2010Date of Patent: April 29, 2014Assignee: King Abdulaziz City for Science and Technology (KACST)Inventors: Mazen Abdullah Ba-Abbad, Hany Abdulrahman Al-Ansary
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Patent number: 8603301Abstract: A method and apparatus for producing high purity distillate in evaporators. is useful for evaporation of waters where volatile silica or organic compounds are encountered such as in production of hydrocarbons from geological formations. An evaporator having a contaminant reduction system is provided. The contaminant reduction system includes an upflow first mist eliminator portion to remove entrained liquid droplets and produce an intermediate purity water vapor stream. A continuous spray system provides a spray of dilute caustic solution in a selected spray configuration for mass transfer contact with the passing intermediate purity water vapor stream, to remove volatile silica compounds therefrom, and produce a partially decontaminated steam stream having mist particles therein. An upflow second mist eliminator portion is provided to remove the residual mist particles, and produce a high purity water vapor stream. The high purity water vapor stream is condensed to provide a high purity distillate stream.Type: GrantFiled: September 29, 2010Date of Patent: December 10, 2013Assignee: General Electric CompanyInventors: William F. Heins, Gregg L. Wilson
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Publication number: 20130299336Abstract: A method for separating one liquid from a mixed liquid containing at least a first liquid and a second liquid having a different boiling point from that of the first liquid, the method including: spraying the mixed liquid from a spraying means for spraying the mixed liquid, into a container into which a heated gas, having a temperature higher than at least one of the boiling point of the first liquid or the boiling point of the second liquid, is supplied from a heated gas supply means, the container having a discharge port for discharging at least a gas; vaporizing at least the first liquid by allowing the mixed liquid sprayed into the container to contact the heated gas; discharging, through the discharge port of the container, at least a mixed gas that contains the first liquid vaporized in the vaporizing; and separating liquid from the mixed gas.Type: ApplicationFiled: December 14, 2011Publication date: November 14, 2013Applicant: BRIDGESTONE CORPORATIONInventors: Masashi Otsuki, Satoru Okumura, Takahiro Masa
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Patent number: 8562709Abstract: A wire mesh mist collector pad having multiple density zones, the zones being arranged other than to provide a constantly increasing density gradient, provides a reduced pressure drop and increased capacity. For example, the pad can include at least three zones with the zones arranged so that the density gradient in the direction of gas flow through the pad varies from low to high to low or from high to low to high.Type: GrantFiled: December 26, 2011Date of Patent: October 22, 2013Assignee: Amistco Separation Products, Inc.Inventor: Kantilal P. Patel
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Patent number: 8562791Abstract: A system and method for decontaminating water and generating water vapor includes introducing contaminated water in to a vessel. The water is moved through a series of rotating trays alternately separated by stationary baffles so as to swirl and heat the water to effect the vaporization thereof to produce a vapor having at least some of the contaminants separated therefrom. The vapor is removed from the vessel for condensing apart from the separated contaminants and the remaining water. The vapor may be passed through a turbine connected to an electric generator. Sensors in a controller may be employed to adjust the speed of rotation of the trays or water input into the vessel in response to the sensed conditions. The treated water may be recirculated and reprocessed through the vessel to increase the purification thereof.Type: GrantFiled: June 22, 2009Date of Patent: October 22, 2013Assignee: Verno Holdings, LLCInventors: John D. Riley, Dana L. Johnson
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Patent number: 8545704Abstract: Provided is a method for recovering high-concentration and high-purity amine from amine-containing waste water generated from nuclear power plants and thermal power plants. The method includes: capturing amine and concentrating waste water using a cation exchange resin; separating amine from the concentrated amine-containing waste water; and carrying out further separation of amine via distillation. The method may be applied to treat amine, which causes an increase in biochemical oxygen demand (BOD) and total nitrogen concentration, drastically at the time of its generation from waste water of nuclear power plants and thermal power plants. In this manner, the method may prevent an increase in load of existing waste water treating plants and avoid a need for modifying the equipment in the existing plants.Type: GrantFiled: May 30, 2008Date of Patent: October 1, 2013Assignee: Soonchunhyang University Industry Academy Cooperation FoundationInventors: In H. Rhee, Byung G. Park, Hyun J. Jung
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Patent number: 8540960Abstract: A method for producing of ultra-clean and High-purity electronic grade reagents is disclosed. The industrial grade reagents are chemically pretreated and filtered, and the colature is rectified. Heating the steam during the rectification to overheated steam, and filtering the overheated steam used the microporous membrane to remove the solid particulates. Condensing the overheated steam and the secondarily filter to remove the dust in the product. Due to the adoption of the technical scheme, the ultra-clean and High-purity isopropanol produced is in conformity with standard SEMI-C12 and the hydrochloric acid to standard SEMI-C8. And the method is applicable for the large-scale continuous production.Type: GrantFiled: October 28, 2010Date of Patent: September 24, 2013Assignee: Shanghai Chemical Reagent Research InstituteInventors: Jiarong Zhan, Mao Huiping, Hui Shaoliang, Shen Zheyu
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Patent number: 8506762Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.Type: GrantFiled: October 30, 2007Date of Patent: August 13, 2013Assignee: DEKA Products Limited PartnershipInventors: David F. Bednarek, Jason A. Demers, Timothy P. Duggan, James L. Jackson, Scott A. Leonard, David W. McGill, Kingston Owens
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Patent number: 8469091Abstract: Embodiments presented herein provide an evaporation based zero liquid discharge method for generation of up to 100% quality high pressure steam from produced water in the heavy oil production industry. De-oiled water is processed in an evaporation system producing a distillate that allows steam to be generated with either drum-type boilers operating at higher pressures or once-through steam generators (OTSGs) operating at higher vaporization rates. Evaporator blowdown is treated in a forced-circulation evaporator to provide a zero liquid discharge system that could recycle >98% of the deoiled water for industrial use. Exemplary embodiments of the invention provide at least one “straight sump” evaporator and at least one hybrid external mist eliminator. Embodiments of the evaporation method operate at a higher overall efficiency than those of the prior art by producing distillate at a higher enthalpy which minimizes the high pressure boiler preheating requirement.Type: GrantFiled: August 5, 2010Date of Patent: June 25, 2013Assignee: Aquatech International CorporationInventors: Daniel P. Bjorklund, Gregory J. Mandigo, Richard M. Schoen, James Michael Marlett, Chandrakant Tiwari
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Patent number: 8343316Abstract: A vacuum dehydrator for processing an oil containing entrained contaminants such as water, air, and particulates comprises a tower enclosing upper and lower chambers. A random packing is contained in the upper chamber. The oil is preheated to a temperature above the boiling point of water and is introduced into the upper chamber for downward flow through the random packing into the lower chamber. Entrained air and water is retained as water vapor in the upper chamber, and particulates are retained in the random packing. Heated ambient air is introduced into the lower chamber for upward flow through the random packing into the upper chamber, and the upper chamber is cooled to condense the water vapor. Oil and condensed water are pumped respectively from the lower and upper chambers.Type: GrantFiled: November 10, 2009Date of Patent: January 1, 2013Assignee: Siemens Industry, Inc.Inventors: Mortimer Daniel Williams, John G. Donnelly, Eric M. Laliberte, J. Rafael Lazo, Juan Alejandro Segrelles Sacristan, Anselmo Garcia Gracia
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Patent number: 8282790Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In an embodiment of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product, and an electric motor with motor rotor and magnets hermetically sealed within the fluid pressure boundary of the distillation system.Type: GrantFiled: October 29, 2007Date of Patent: October 9, 2012Assignee: DEKA Products Limited PartnershipInventors: Jason A. Demers, Scott A. Leonard, Kingston Owens
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Patent number: 8252148Abstract: A mobile waste processing system and method is disclosed for processing materials in a tank, typically an underground storage tank. A mobile fluid processing module is disposed adjacent to or over the tank, and sealingly connected to the tank through a tank riser. Support equipment, which may include an electric power module, a chiller module, a heating module, and a control and monitor module, are disposed a distance from the processing module, and connected thereto. A pump and optionally a dispersal nozzle are deployed from the processing module into the tank, and effluent is extracted for processing. The processing trailer includes effluent processing equipment such as an evaporator and demister, condenser, vacuum pump, and interim storage tank. The effluent is processed, and at least a portion is removed. Some of the processed effluent may be returned to the tank.Type: GrantFiled: June 15, 2011Date of Patent: August 28, 2012Assignee: Columbia Energy & Environmental Services, Inc.Inventors: Stephen Wolfe, Brian Brendel
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Patent number: 8202403Abstract: A distillation tower for use in a petrochemical or petroleum operation effects liquid and vapor separation by using centrifugal force applied to the feed introduced into a ring from a tangential inlet. The feed is separated into a liquid component that flows into the bottoms section of the tower and a vapor component that flows upwardly through the core of the ring to a wash zone in the tower. De-entrainment devices are provided in the core so that the vapor swirling upwardly impacts the devices and any remaining entrained liquid is separated from the vapor. As a result, overflash with decreased resid can be collected from the wash zone and used as feed suitable for a fluid catalytic cracking operation, for example.Type: GrantFiled: February 19, 2008Date of Patent: June 19, 2012Assignee: ExxonMobil Research & Engineering CompanyInventors: Theodore Sideropoulos, Arun K. Sharma
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Patent number: 8083901Abstract: A de-entrainment device separates entrained liquid from vapor in a fluid stream that flows through a chimney tray in a distillation tower. The separated liquid is collected and shielded from the fluid stream to prevent re-entrainment of the liquid in the vapor flowing upward into the tower. The chimney tray includes risers with hats that have gutters to guide liquid toward the tray deck, channels to collect and drain liquid from the top of the hats to the tray deck, and baffles extending from the risers to shield the liquid collected on the tray deck from the vapor flow.Type: GrantFiled: February 19, 2008Date of Patent: December 27, 2011Assignee: ExxonMobil Research & Engineering CompanyInventors: Arun K. Sharma, Theodore Sideropoulos, Berne K. Stober, Brian D. Albert, Alvin U. Chen, Vikram Singh
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Publication number: 20110240457Abstract: A mobile waste processing system and method is disclosed for processing materials in a tank, typically an underground storage tank. A mobile fluid processing module is disposed adjacent to or over the tank, and sealingly connected to the tank through a tank riser. Support equipment, which may include an electric power module, a chiller module, a heating module, and a control and monitor module, are disposed a distance from the processing module, and connected thereto. A pump and optionally a dispersal nozzle are deployed from the processing module into the tank, and effluent is extracted for processing. The processing trailer includes effluent processing equipment such as an evaporator and demister, condenser, vacuum pump, and interim storage tank. The effluent is processed, and at least a portion is removed. Some of the processed effluent may be returned to the tank.Type: ApplicationFiled: June 15, 2011Publication date: October 6, 2011Applicant: COLUMBIA ENERGY & ENVIRONMENTAL SERVICES, INC.Inventors: Stephen Wolfe, Brian Brendel
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Patent number: 7981253Abstract: An improved de-entrainment device for use in distillation towers, especially vacuum distillation towers used for fractionating petroleum atmospheric resids is in the form of a baffle which is to be located in the portion of the tower below the feed zone and at the top of the flash zone. The baffle is in the form of an apertured plate above the stripping zone and in its preferred form comprises number of radial fins or blades, resembling a static fan with openings between the fins to permit vapors from the lower portions of the tower to pass upwards through the baffle with a minimal pressure drop. The fins of the baffle are preferably oriented at an angle between 30° and 60° away from the incoming feed so that the incoming feed stream skims over the top edges of the fins.Type: GrantFiled: January 26, 2007Date of Patent: July 19, 2011Assignee: ExxonMobil Research & Engineering CompanyInventors: Arun K. Sharma, Theodore Sideropoulos, Rutton D. Patel, Brian D. Albert, Alvin U. Chen
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Patent number: 7959766Abstract: Process for recovering cyclododecatriene (CDT) from a solution containing CDT and high boilers such as deactivated catalyst and polymers, which includes feeding the solution into a preheater and heating it, subsequently depressurizing it through a downstream pressure maintenance device and feeding the resulting two-phase mixture into a helical tube evaporator and there reducing the CDT content of the liquid phase by partial evaporation and discharging a gaseous product stream having an increased concentration of CDT.Type: GrantFiled: June 30, 2006Date of Patent: June 14, 2011Assignee: BASF AktiengesellschaftInventors: Bernd Rumpf, Ortmund Lang, Andrea Haunert, Thomas Genger, Anton Meier
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Publication number: 20110094872Abstract: A method for producing of ultra-clean and High-purity electronic grade reagents is disclosed. The industrial grade reagents are chemically pretreated and filtered, and the colature is rectified. Heating the steam during the rectification to overheated steam, and filtering the overheated steam used the microporous membrane to remove the solid particulates. Condensing the overheated steam and the secondarily filter to remove the dust in the product. Due to the adoption of the technical scheme, the ultra-clean and High-purity isopropanol produced is in conformity with standard SEMI-C12 and the hydrochloric acid to standard SEMI-C8. And the method is applicable for the large-scale continuous production.Type: ApplicationFiled: October 28, 2010Publication date: April 28, 2011Inventors: Jiarong ZHAN, Mao HUIPING, Hui SHAOLIANG, Shen ZHEYU
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Publication number: 20110024282Abstract: A process vessel is provided for separating a multi-component stream. The process vessel includes an inlet for permitting introduction of reaction water stream into the vessel and an outlet for withdrawing a water-rich phase from the vessel. The vessel further includes a plurality of draw-off points for drawing off a phase rich in suspended hydrocarbons from the vessel, the draw-off point(s) being located above the outlet.Type: ApplicationFiled: August 3, 2009Publication date: February 3, 2011Applicant: Sasol Technology (Pty) LtdInventors: Paul Meintjes, Johannes Buys
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Publication number: 20100300869Abstract: The invention involves a micro-fluidic separation device for liquid mixtures with different boiling points. According to the invention it is intended that a head and a sump are formed in a separating channel; further intended is a thermo unit along the entire length of the separating channel consisting preferably of individually controllable heating and/or cooling elements. This makes it advantageously possible to perform a rectification of the liquid mixture with the separating device where individual fractions of the liquid mixture may be removed via the outlets. This allows continuous operations of the separating device at a simultaneously high degree of efficiency of the separation.Type: ApplicationFiled: June 1, 2010Publication date: December 2, 2010Applicant: SIEMENS AKTIENGESELLSCHAFTInventors: Hans-Richard Kretschmer, Oliver Lade, Arkadij M. Elizarov
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Patent number: 7767170Abstract: A process is provided for cracking hydrocarbon feedstock containing resid comprising: heating the feedstock, mixing the heated feedstock with a fluid and/or a primary dilution steam stream to form a mixture, optionally further heating the mixture, flashing the mixture within a flash/separation vessel to form a vapor phase and a liquid phase, partially condensing the vapor phase by contacting with a condenser within the vessel, to condense at least some coke precursors within the vapor while providing condensates which add to the liquid phase, removing the vapor phase of reduced coke precursors content as overhead and the liquid phase as bottoms, heating the vapor phase, cracking the vapor phase in a radiant section of a pyrolysis furnace to produce an effluent comprising olefins, and quenching the effluent and recovering cracked product therefrom. An apparatus for carrying out the process is also provided.Type: GrantFiled: June 16, 2006Date of Patent: August 3, 2010Assignee: ExxonMobil Chemical Patents Inc.Inventors: Richard C. Stell, George Stephens, Jennifer L. Bancroft, John R. Messinger
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Publication number: 20100175983Abstract: Petroleous production is associated with effluents well known to foul lines, nozzles, and containers while consuming substantial energy to assist in both production and remediation. A heat exchanger and manifold system maximizes flows, minimizes changes in flow cross-section, and maximizes heat transfer area, while recycling both water and heat between processes. Dirty regions and clean regions result from scrubbing horizontal exhaust stacks and evaporation of production water in concert to remediate one another, while recycling a significant portion of the energy consumed by each. The heat exchanger relies on a manifold having many layered conduits, each connected to a single layer level of one or more cylindrical conduits in the exchanger. The cylinders of the exchanger themselves are arranged in multiple layers, each layer of a heat exchanger element being connected to a single layer of the manifold.Type: ApplicationFiled: January 14, 2010Publication date: July 15, 2010Applicant: Total Water Management, LLCInventors: J. Clair Batty, David A. Bell, Craig E. Cox
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Patent number: 7611604Abstract: The invention relates to a method and a device for the production of pure steam. A falling-film evaporator is used. Of the water-steam mixture leaving the evaporator unit, part of the water is collected at the bottom of the device, and a fraction mainly consisting of steam enters a rising spiral channel for the separation of impurities. In the periphery of the spiral channel apertures are provided for separating impurity-containing droplets, which condense on a surface outside the apertures. The liquid formed is removed from the device. The water phase collected at the bottom enters a recycle line connected to the feed end of the evaporator unit. Feed water is supplied to the recycle line to compensate for pure steam consumption.Type: GrantFiled: August 28, 2003Date of Patent: November 3, 2009Assignee: STERIS Europe Inc.Inventors: Mauri Salmisuo, Ilkka Olavi Laitinen
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Patent number: 7597784Abstract: Embodiments of the invention are directed toward a novel pressurized vapor cycle for distilling liquids. In some embodiments of the invention, a liquid purification system is revealed, including the elements of an input for receiving untreated liquid, a vaporizer coupled to the input for transforming the liquid to vapor, a head chamber for collecting the vapor, a vapor pump with an internal drive shaft and an eccentric rotor with a rotatable housing for compressing vapor, and a condenser in communication with the vapor pump for transforming the compressed vapor into a distilled product. Other embodiments of the invention are directed toward heat management, and other process enhancements for making the system especially efficient.Type: GrantFiled: November 13, 2003Date of Patent: October 6, 2009Assignee: DEKA Products Limited PartnershipInventors: David F. Bednarek, Jason A. Demers, Timothy P. Duggan, James L. Jackson, Scott A. Leonard, David W. McGill, Kingston Owens
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Patent number: 7563360Abstract: A top temperature T1 of a distillation tower 1 is held below a liquefying temperature of a light fraction by returning a part of an exhaust gas W, which is cooled by a condenser 5, to the upper zone of the distillation tower 1. A bottom temperature T2 is raised up to 300° C. at highest by returning a part of a liquid product P from a re-boiler 3 to a lower zone of the distillation tower 1. When a liquid hydrocarbon L comes in countercurrent contact with a stripping gas G inside the distillation tower 1 with the temperature profile that an inner temperature gradually falls down along an upward direction, mercury is efficiently transferred from the liquid L to a vapor phase without effusion of the light fraction in accompaniment with the exhaust gas W.Type: GrantFiled: January 26, 2005Date of Patent: July 21, 2009Assignee: Japan Petroleum Exploration Co., Ltd.Inventors: Yoshiyuki Yamaguchi, Senichiro Kaku, Kazutoshi Chaki
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Publication number: 20090101546Abstract: A combination of differently sized structured packings in the wash zone of distillation towers is provides advantages at high vapor rates. The use of a large crimp structured packing below a smaller crimp size structured packing is advantageous for vacuum crude unit service where fouling resistance is desirable and liquid entrainment into the wash zone is a problem at high vapor rates. The tower may be operated at high vapor flux rates or C 0.4 ft/sec or higher (0.12 m/sec). An unexpected characteristic of the combinations is that the entrainment increases only slowly with increasing vapor flux rate up to Cs values of at least 0.55 ft/sec (0.17 m.sec), as compared to other packings such as random packing, grid packing and combinations of grid packing with structured packing which allow entrainment to increase sharply at high vapor rates.Type: ApplicationFiled: September 30, 2008Publication date: April 23, 2009Applicant: ExxonMobil Research and Engineering CompanyInventors: Theodore Sideropoulos, Andrew P. Sullivan, Arun K. Sharma, Berne K. Stober, Vikram Singh, Brian A. Albert
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Publication number: 20090057128Abstract: An improved process for separation of liquid mixtures involves vapor stripping followed by mechanical compression of the vapor which is then exposed to a permeation membrane for separation of the compressed vapor.Type: ApplicationFiled: August 30, 2007Publication date: March 5, 2009Inventors: Leland Vane, Franklin R. Alvarez
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Publication number: 20080314729Abstract: A distillation tower for use in a petrochemical or petroleum operation effects liquid and vapor separation by using centrifugal force applied to the feed introduced into a ring from a tangential inlet. The feed is separated into a liquid component that flows into the bottoms section of the tower and a vapor component that flows upwardly through the core of the ring to a wash zone in the tower. De-entrainment devices are provided in the core so that the vapor swirling upwardly impacts the devices and any remaining entrained liquid is separated from the vapor. As a result, overflash with decreased resid can be collected from the wash zone and used as feed suitable for a fluid catalytic cracking operation, for example.Type: ApplicationFiled: February 19, 2008Publication date: December 25, 2008Applicant: ExxonMobil Research and Engineering Company Law DepartmentInventors: Theodore Sideropoulos, Arun K. Sharma
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Publication number: 20080217158Abstract: Process for recovering cyclododecatriene (CDT) from a solution comprising CDT and high boilers such as deactivated catalyst and polymers, which comprises feeding the solution into a preheater and heating it, subsequently depressurizing it through a downstream pressure maintenance device and feeding the resulting two-phase mixture into a helical tube evaporator and there reducing the CDT content of the liquid phase by partial evaporation and discharging a gaseous product stream having an increased concentration of CDT.Type: ApplicationFiled: June 30, 2006Publication date: September 11, 2008Applicant: BASF AktiengesellschafInventors: Bernd Rumpf, Ortmund Lang, Andrea Haunert, Thomas Genger, Anton Meier
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Patent number: 7381310Abstract: A sea water desalination installation that employs an evaporation-condensation system which operates continuously at a low temperature and which enables the recovery of energy released. The installation includes a cylindrical evaporator having a large evaporation surface and a concentric condenser with a large surface area. Sea water is used to cool the condenser and said water is subsequently sent to the evaporator. A static high-pressure ventilator is used to: (i) drive the vapor/air in a closed circuit between the evaporator and the condenser and (ii), using a calibrated nozzle, create a pressure gradient that is equivalent to the pressure of the saturated vapor at working temperature between said two zones. The aforementioned evaporator and condenser are thermally insulated in relation to one another and to the external environment.Type: GrantFiled: October 11, 2002Date of Patent: June 3, 2008Inventors: Maria Fernando Hernandez Hernandez, Francisco Fernadnez De Mazarambroz Bernabeu
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Patent number: 7279075Abstract: In a thermal separating process between at least one gaseous and at least one liquid stream, of which at least one comprises (meth)acrylic monomers, in a separating column containing sieve trays as separating internals, at least some of the sieve trays are operated above an entrainment fraction of 10% by weight.Type: GrantFiled: August 26, 2003Date of Patent: October 9, 2007Assignee: BASF AktiengesellschaftInventors: Joachim Thiel, Hugues Vandenmersch, Juergen Schroeder, Albrecht Dams
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Patent number: 7175696Abstract: Herein is disclosed a method and an apparatus for preparing a highly purified gas from a crude liquid comprising the gas and one or more of a metal, particulates, water vapor, or a volatile impurity. The method comprises: (a) vaporizing the crude liquid, to yield (i) a first vapor stream comprising the gas and (ii) a first liquid stream comprising the gas; (b) removing water vapor, particulates, or both from the first vapor stream, to yield a second vapor stream comprising the gas; (c) condensing the second vapor stream, to yield a second liquid stream comprising the gas; and (d) sparging the second liquid stream with an inert gas, to yield (i) a third vapor stream comprising the gas and (ii) a third liquid stream comprising the highly purified gas. Also disclosed is a method for preparing an adsorbent to effectively remove water vapor from the gas, as well as an adsorbent so prepared.Type: GrantFiled: February 18, 2003Date of Patent: February 13, 2007Assignees: American Air Liquide, Inc., Air Liquide America L.P.Inventors: Derong Zhou, John P. Borzio, Gregory M. Jursich, Earle R. Kebbekus