Melting Out Patents (Class 23/308R)
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Patent number: 5976478Abstract: Internal porosity is created in dense SiO.sub.2 particles by heating a mixture of the particles with B.sub.2 O.sub.3 at a temperature above about 450.degree. C. Resulting SiO.sub.2 particles have altered morphology, internal porosity, and small to negative volume changes when heated.Type: GrantFiled: December 21, 1998Date of Patent: November 2, 1999Assignee: E. I. du Pont de Nemours and CompanyInventors: Donald Keith Swanson, Salvatore Anthony Bruno
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Patent number: 5861134Abstract: Internal porosity is created in dense SiO.sub.2 particles by heating a mixture of the particles with B.sub.2 O.sub.3 above the melting point of both mixture components. Resulting SiO.sub.2 particles have altered morphology, internal porosity, and a negative thermal expansion coefficient when heated.Type: GrantFiled: June 9, 1997Date of Patent: January 19, 1999Assignee: E. I. du Pont de Nemours and CompanyInventor: Donald Keith Swanson
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Process for separating and purifying substances by crystallization from the melt under high pressure
Patent number: 5447541Abstract: Process for separating and purifying substances by crystallization from the melt under high pressuresIn the process for separating or purifying substances by crystallization from melts or highly concentrated solutions under high pressures, gas is dissolved in the melt to be crystallized and is expelled again after the crystallization with reduction in the pressure. Still adhering or occluded impurities are thus removed.Type: GrantFiled: April 20, 1994Date of Patent: September 5, 1995Assignee: Hoechst AktiengesellschaftInventors: Rudolf Steiner, Axel Konig, Siegbert Rittner -
Patent number: 5447542Abstract: In the process for separating and purifying substances by crystallization from the melt under pressure, the melt is subjected to pressure under an inert gas atmosphere and then cooled, whereupon it crystallizes. The residual melt is separated from the resulting crystals, after which the crystals are degassed by reducing the pressure and are caused to sweat, and the sweat oil is separated off.Type: GrantFiled: April 20, 1994Date of Patent: September 5, 1995Assignee: Hoechst AktiengesellschaftInventors: Rudolf Steiner, Axel Konig, Siegbert Rittner
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Patent number: 5338519Abstract: A process is provided for the separation of substances by melt crystallization. The organic mixtures which are difficult to crystallize are heated to a temperature sufficient to obtain a melt with the melt then being moved through a three-dimensional crystallization matrix having a large specific area. The melt is slowly cooled over a temperature range so as to achieve a selective crystallization from the supersaturated melt in the carrier matrix. A deposited crystal phase is thereafter melted and separated from the carrier matrix and removed by centrifugation. The carrier matrix may have a crystallization-promoting microstructure surface and may consist of an openpored foam.Type: GrantFiled: March 24, 1993Date of Patent: August 16, 1994Assignee: Sulzer Brothers LimitedInventors: Slobodan Jancic, Evangelos Sakellariou
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Patent number: 5230769Abstract: A process is provided for the separation of substances by melt crystallization. The organic mixtures which are difficult to crystallize are heated to a temperature sufficient to obtain a melt with the melt then being moved through a three-dimensional crystallization matrix having a large specific area. The melt is slowly cooled over a temperature range so as to achieve a selective crystallization from the supersaturated melt in the carrier matrix. A deposited crystal phase is thereafter melted and separated from the carrier matrix and removed by centrifugation. The carrier matrix may have a crystallization-promoting microstructure surface and may consist of an openpored foam.Type: GrantFiled: December 10, 1991Date of Patent: July 27, 1993Assignee: Sulzer Brothers LimitedInventors: Slobodan Jancic, Evangelos Sakellariou
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Patent number: 4584181Abstract: An apparatus for producing low cost, high purity solar grade Si wherein a reduction reaction, preferably the reduction of SiF.sub.4, by an alkali metal (Na preferred) is carried out inside a reaction chamber. The chamber wall and bottom surfaces are formed of graphite and configured with drainage channels so as to facilitate the continuous separation of the products of reaction (Si and NaF) and removal of the molten salt by discharging the salt through one or more ports at the bottom of the reaction chamber. Such process is especially useful where it is desirable to discharge the reaction salt products from the reactor and retain silicon within the chamber for later removal.Type: GrantFiled: December 27, 1982Date of Patent: April 22, 1986Assignee: SRI InternationalInventors: Leonard Nanis, Angel Sanjurjo
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Patent number: 4559071Abstract: Converting thermally meltable materials to a liquefied state is carried out on a support surface of the unmelted material. As liquefied material is drained from the surface, additional unmelted material is fed onto the surface to maintain a substantially constant layer of the unmelted material.Type: GrantFiled: October 16, 1984Date of Patent: December 17, 1985Assignee: PPG Industries, Inc.Inventors: Gerald E. Kunkle, Joseph M. Matesa
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Patent number: 4492627Abstract: Process for recovery of elemental phosphorus from waste ponds by dredging the waste pond to obtain an aqueous phosphorus slurry, separating particles larger than 2 mm from the slurry, treating the remaining slurry in an initial hydrocyclone and removing an overflow of solids larger than 500 micrometers, treating the underflow from the initial hydrocyclones in smaller diameter hydrocyclones, removing a second overflow enriched in slimes and diminished in phosphorus, removing a second underflow enriched in phosphorus and diminished in slimes and heating it sufficiently to melt the phosphorus therein, treating the heated second underflow in a centrifugal separator, and separating and recovering a stream of coalesced phosphorus from a heavy fraction of impurities.Type: GrantFiled: June 14, 1982Date of Patent: January 8, 1985Assignee: FMC CorporationInventor: David A. Crea
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Patent number: 4151264Abstract: A process of melting down and purifying silicon, which comprises melting silicon in at least half of the amount up to double of the amount of a silicate melt heated by resistance heating up to a temperature of at least 1,420.degree. C., said melt consisting of 2-30% by weight of calcium oxide, 5-35% by weight of magnesium oxide, wherein the sum of calcium oxide and magnesium oxide will be 15-38% by weight, 0.5-28% by weight of aluminum oxide and 45-70% by weight of silicon dioxide, and wherein, to the melt are added at least 0.29% by weight of elementary and/or chemically bound copper, preferably 0.50-3% by weight, calculated on the silicon amount.Type: GrantFiled: January 25, 1978Date of Patent: April 24, 1979Assignee: Wacker-Chemie GmbHInventors: Anton More, Rudolf Riedle, Herbert Straussberger, Willi Streckel, Johann Muschi
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Patent number: 3956414Abstract: Melting and cracking of amorphous polyolefin are carried out with a relatively small quantity of heat consumption and also with easiness in separating sludge, in converting it into oil by maintaining amorphous polyolefin at a high temperature of about 130.degree. - 300.degree.C for a relatively long time alone or together with a petroleum hydrocarbon oil to reduce the viscosity of the resultant melt to 5 - 250 CP, spraying the resultant melt upon lumps of amorphous polyolefin, separating impurities in the lumps as sludge, cracking the resultant molten mixture at a temperature of about 250.degree. - 450.degree.C and recovering oily products. For that purpose an apparatus comprising a combination of a holding tank for melt of amorphous polyolefin, a vessel for melting amorphous polyolefin equipped with a perforated plate or a wire-netting, a revolving shaft, a stirrer, etc.Type: GrantFiled: January 18, 1974Date of Patent: May 11, 1976Inventor: Katsutoshi Oshima