Abstract: A passive reflective tracking media includes a plurality of multi-layer particles including at least one layer of a high refractive index material and at least one layer of a low refractive index material. The particles are configured to reflect ambient electromagnetic radiation at one or more signature wavelengths. Methods of applying the tracking media to a target object, detecting the tracking media, and fabrication the tracking media are also described.

Abstract: This application relates to vaprochromic coordination polymers useful for analyte detection. The vapochromism may be observed by visible color changes, changes in luminescence, and/or spectroscopic changes in the infrared (IR) signature. One or more of the above chromatic changes may be relied upon to identify a specific analyte, such as a volatile organic compound or a gas. The chromatic changes may be reversible to allow for successive analysis of different analytes using the same polymer. The polymer has the general formula MW[M?X(Z)Y]N wherein M and M? are the same or different metals capable of forming a coordinate complex with the Z moiety; Z is selected from the group consisting of halides, pseudohalides, thiolates, alkoxides and amides; W is between 1-6; X and Y are between 1-9; and N is between 1-5. Optionally, an organic ligand may be bound to M. In alternative embodiments of the invention M may be a transition metal, such as Cu and Zn.

Abstract: A method of preparing hydrophobic silica particles includes the step of reacting together in a single step a mixture of silane ether monomers and organically modified silane ether monomers with a hydrolyzing agent. The method also includes producing hydrophobic silica microparticles and nanoparticles that can include dyes and/or magnetizable components. The silica nanoparticles can be used in the detection, visualization and/or analysis of latent fingerprints.

Abstract: A composition comprising synthetic peptides for use as a peptide retention standard in liquid chromatography applications is disclosed Said synthetic peptides have a broad range of hydrophobicity while maintaining low variation in their molecular weights The synthetic peptides disclosed consist of the ammo acid sequences LGGGGGGDGSR, LGGGGGGDFR, LLGGGGDFG, LLLGGDFR, LLLLDFR, LLLLLDFR A method of predicting the hydrophobicity of an unknown peptide in liquid chromatography using a composition of peptide retention standards and a method of developing a Universal Hydrophobicity Index (UHI) for the measurement of peptide hydrophobicity in liquid chromatography are also described

Abstract: There is provided a method for synthesizing colloidal nanoparticles comprising the step of creating a reactive three-phase foam containing reactants therein for synthesizing the colloidal nanoparticles.

Abstract: Provided are homogeneous liquid systems substantially 1H-NMR inactive and/or devoid of protons and are capable of enhancing the diffusion separation of a mixture, the system is substantially devoid of at least one NMR active nucleus present in the mixture. Further provided are methods of using the homogeneous liquid systems for enhancing the diffusion separation of a mixture and/or generating a diffusion ordered spectrum of a mixture and/or minimizing the peak width in a liquid state diffusion ordered spectrum of a mixture.

Abstract: A temperature indicating paint comprises 4 wt % to 40 wt % sodium alumino sulpho silicate, 1 wt % to 38 wt % nickel antimony titanate and the binder comprises 25 wt % to 50 wt % silicone resin 10 wt % to 30 wt % acrylic resin each excluding solvent. This composition undergoes color changes occur, these are; Blue 520-560° C.; Light Blue 950-990° C.; Light Yellow 1000-1040° C.; Glazed Black 1160-1200° C. The color changes are particularly distinct and enable accurate analysis particularly, but not exclusively, in gas turbine engines.

Abstract: An article identifier or code including at least one photo-responsive dye and a method of encoding or embedding information in same. A reader device for decoding or extracting information in an article identifier or code and verifying or authenticating that information and the associated extraction and authentication methods.

Abstract: This application relates to vaprochromic coordination polymers useful for analyte detection. The vapochromism may be observed by visible color changes, changes in luminescence, and/or spectroscopic changes in the infrared (IR) signature. One or more of the above chromatic changes may be relied upon to identify a specific analyte, such as a volatile organic compound or a gas. The chromatic changes may be reversible to allow for successive analysis of different analytes using the same polymer. The polymer has the general formula MW[M?X(Z)Y]N wherein M and M? are the same or different metals capable of forming a coordinate complex with the Z moiety; Z is selected from the group consisting of halides, pseudohalides, thiolates, alkoxides and amides; W is between 1-6; X and Y are between 1-9; and N is between 1-5. Optionally, an organic ligand may be bound to M.

Abstract: A set of crystallization solutions includes a plurality of crystallization solutions of Crystallization Solution Set I, a plurality of crystallization solutions of Crystallization Solution Set II or a plurality of crystallization solutions of Crystallization Solution Set III.

Abstract: Provided is a simulant material for simulating hazardous materials, including a quantity of at least one explosive material and at least one inert material. The simulant material is a non-explosive material and is in the form of a homogenous, flexible and non-particulated material. Also provided is a method for manufacturing such a simulant material.

Abstract: Methods and systems for preparation of calibrant infusion fluid sources are disclosed. In one embodiment, a precise volume of glucose is injected into a saline-solution filled calibrant infusion fluid source proximate in time to conducting a calibration procedure. The glucose concentration in the calibrant infusion fluid source is subsequently calculated based on the measured weight of the saline-solution, as determined prior to glucose injection, and the volume of glucose injected. This method provides a highly accurate and convenient manner for use in a hospital environment, for example, with an intravenous blood glucose sensor system. In another embodiment, a premixed calibrant infusion fluid source is provided that includes saline solution and a predetermined concentration of glucose. In such embodiments, shelf life problems related to water evaporation are mitigated by hermetically covering or otherwise hermetically containing the calibrant infusion fluid source up until the point of use.

Abstract: In one embodiment, a method for producing a high-purity single crystal of aluminum antimonide (AlSb) includes providing a growing environment with which to grow a crystal, growing a single crystal of AlSb in the growing environment which comprises hydrogen (H2) gas to reduce oxide formation and subsequent incorporation of oxygen impurities in the crystal, and adding a controlled amount of at least one impurity to the growing environment to effectively incorporate at least one dopant into the crystal. In another embodiment, a high energy radiation detector includes a single high-purity crystal of AlSb, a supporting structure for the crystal, and logic for interpreting signals obtained from the crystal which is operable as a radiation detector at a temperature of about 25° C. In one embodiment, a high-purity single crystal of AlSb includes AlSb and at least one dopant selected from a group consisting of selenium (Se), tellurium (Te), and tin (Sn).

Abstract: The invention describes a color-developing composition that contains at least four major components: (1) a leuco dye or a combination of leuco dyes, (2) an electron-withdrawing color-developer agent or a combination of color-developers that can form colored complexes with the leuco dyes, (3) a separator or combination of separators that when present in sufficient amounts, can prevent the formation of the colored complexes between the color-developer and leuco dyes, all contained within (4) an encapsulation matrix that includes at least one film-forming and one aqueous-insoluble polymer. All of the foregoing components are dissolved together in a volatile organic solvent medium to form a homogeneous solution that can be applied as an ink on substrates, which can be incorporated as part of absorbent articles or personal care products.

Abstract: A disposable garment having a multicolored scene graphic is disclosed. In particular embodiments, the multicolored scene graphic includes a focal graphic and a background graphic, wherein the background graphic appears blurry relative to the focal graphic to enhance the conspicuousness of the focal graphic. Methods for making such articles are also disclosed.

Abstract: The present invention provides nanocomposite systems made of metallic nanoparticles stabilized with branched cationic polysaccharides, in particular alditolic or aldonic mono- and oligo-saccharidic derivatives of chitosan, and their preparation obtainable with aqueous solutions of these polysaccharides in the presence or absence of reducing agents. The peculiar chemical and physical-chemical features of these polysaccharides allow to form metallic nanoparticles homogeneously dispersed in the polysaccharidic matrix and an effective stabilization thereof. The properties associated with the nanometric dimensions and the presence of biological signals on polymeric chains may be exploited in applications with antimicrobial activities and of molecular biosensors.

Abstract: A temperature switch comprises a material (14) which melts and concomitantly undergoes a change in an electrical characteristic at a predetermined temperature. The temperature switch also includes at least two electrical contacts (10, 12) for detecting the change in the electrical characteristic. The material (14) comprises an organic cation and an anion and is preferably an ionic liquid.

Abstract: A thermal indicator material which comprises a plurality of polythiophenes having a second low temperature color and a high temperature color. The polythiophenes are structured and arranged to exhibit a color change from the second low temperature color to the high temperature color when the thermal indicator material is exposed to a temperature that meets or exceeds a pre-determined temperature and to exhibit a color change from the high temperature color to a first low temperature color when the thermal indicator material is exposed to a decline in temperature from a temperature that meets or exceeds the predetermined temperature to a temperature of within the range of between about 5 to 20° C. below the pre-determined temperature that occurs in a time period of greater than 2.0 seconds.

Abstract: Particles conveying a code are incorporated into polymer matrix to form a core document substrate. These particles may be colored to create a distinctive look of the document that makes it unique for a particular document issuer and enables visual authentication. Addition of a covert attribute to the particle, such as a UV pigment or hidden layer of material, allows a covert, forensic characteristic and it also allows a mathematical description to be calculated describing the random distribution of a specific area on a document and then captured on it (e.g., in the bar code or magnetic stripe or digital watermark on an ID document).

Abstract: A taggant comprising at least one perfluorocarbon compound surrounded by a polyphosphazene compound. The polyphosphazene compound has the chemical structure: wherein G1 and G2 are pendant groups having different polarities, m is an integer greater than or equal to 100, and each of A and B is independently selected from hydrogen, an alkyl, an alkene, an alkoxide, a polyether, a polythioether, a siloxane, and —X(CH2)nY1(CH2)p1Y2(CH2)p2 . . . Yi(CH2)piCH3, where n ranges from 1 to 6, X and Y are independently selected from oxygen, sulfur, selenium, tellurium, and polonium, and p1 through pi range from 1 to 6. Cyclic polyphosphazene compounds lacking the A and B groups are also disclosed, as are methods of forming the taggant and of detecting an object.

Abstract: A simulant material for simulating hazardous materials is provided. The simulant material includes a quantity of at least one explosive material and at least one inert material. The simulant material is a non-explosive material and is in the form of a homogenous, flexible and non-particulated material. Also provided is a method for manufacturing such a simulant material.

Abstract: The present invention describes the development of thin film calibration strips for microscopy/spectroscopy systems and a simple method/routine to conduct instrument calibration using partially (uniaxially) oriented strip to calibrate microscopy system without the prior knowledge of exact polarization of the strip. The invention describes results from studies including a styryl derivative (LDS 798) embedded in poly(vinyl alcohol) (PVA) film. These films were progressively stretched up to 8 folds. Vertical and horizontal components of absorptions and fluorescence were measured and dichroic ratios were determined for different film stretching ratios. The stretched films have high polarization values for isotropic excitation. The isotropic and stretched PVA films doped with LDS 798 can be used as etalons in near infra red (NIR) spectroscopic measurements.

Abstract: The molecule is prepared by capping phospholipid on a single gold nanoparticle (GNP). Since the thiol-related molecule bounded on GNP shows the characteristic of surface-enhanced Raman scattering (SERS), the phospholipid-capped gold nanoparticle (PLGNP) can be formed as a nanoprobe applied on the detection device integrating optics and chemistry and used in the fields of biomedicine, medical diagnosis and environment for detecting, such as solutions containing salts or proteins.

Abstract: The present invention is directed to a method for the synthesis of deuterium labeled Vitamin D and related compounds with a high level of deuterium incorporation, which are particularly suitable for use as standards for mass spectroscopy.

Abstract: A composite material 1 for temperature measurement is specified, as is a temperature sensor 10 formed from the composite material 1. Additionally specified are processes for producing the composite material 1 and for producing the temperature sensor 10.

Abstract: Disclosed are a method for detecting proteins on a polyacrylamide gel by background staining method using an organic dye composition containing eosin Y or phloxine B, and the organic dye composition for use in the method, which enables the rapid and simple detection of the protein on the polyacrylamide gel with a high sensitivity.

Abstract: A method for the diagnosis of tubular kidney diseases comprising the step of determining the presence or absence or amplitude of at least three polypeptide markers in a urine sample, the polypeptide marker being selected from the markers characterized in Table 1 by values for the molecular masses and migration times.

Abstract: A method for separating and purifying the active hematinic species (AHS) present in iron-saccharidic compositions, including AHS such as sodium ferric gluconate complex, ferric hydroxide-sucrose complex and ferric saccharate complex and others of similar form and function. The method separates the AHS from one or more excipients and, preferably, lyophilizes the separated AHS. Separation of the AHS permits its analytical quantification, further concentration, purification and/or lyophilization as well as preparation of new and useful products and pharmaceutical compositions, including those useful for the treatment of humans and animals.

Abstract: The invention relates to curable compositions which are prepared from polyol components containing one or more polyols and isocyanate components containing one or more isocyanates, which compositions contain at least one indicator having at least one quinonoid group, which indicator signifies the degree of curing by a change of color. The invention also relates to a method for indicating the progress of curing in such curable compositions.

Abstract: Devices are described that include a component comprised of a material having a structure of R1—C(O)—NX—R2, wherein each of R1 and R2 is independently a saturated alkyl having between 7-22 carbon atoms or an aryl, X is H or C(O)—Y, Y together with R1 forms a ring. The material is characterized by a single, sharp melting point, thus making it suitable for use, for example, in thermomechanical actuating devices or in temperature-indicating devices. Also described are compositions comprising two or more materials each having a structure of Rn1—C(O)—NH—R2 wherein, n is an identifying integer corresponding to a material in the composition; wherein for each material n in the composition, Rn1 and Rn2 are a saturated alkyl having between 7-22 carbon atoms, wherein for each material n Rn1 and Rn2 differ by one carbon atom, and wherein the number of carbon atoms in Rn2 of each material n differs by four or less.

Abstract: The present invention relates to a multiple-component material including a substrate and a film layer on the substrate. The film layer includes a color-changing composition to indicate a change in condition, such as a change in pH. The color-changing composition includes a water-insoluble, film-forming polymer, a charged surfactant, a charged colorant and a pH adjuster.

Abstract: An artificial test soil comprises particulate, hair, and fiber components, wherein said particulate component consists of mineral, food, and plant materials, so chosen and proportioned as to correlate to a typical soil found in the home. The test soil may be used to test cleaning products by application of a known amount thereof to a surface, cleaning of said surface, and determination of the amount of said soil removed from said surface.

Abstract: The invention relates to methods of isolating white blood cells (WBCs) from a sample, e.g., whole blood, using magnetic particles that specifically bind to WBCs and a series of specific steps and conditions. The methods can include one or more of decreasing the viscosity of the sample prior to WBC isolation, agitating the sample at specified frequencies, and/or using a sample container arranged such that all of the sample is placed in close proximity (e.g., within 5, 2, 1, or 0.5 mm) to the source of the magnetic field. The new methods provide for isolation of WBC preparations with high yield, purity, and viability. The methods are designed for compatibility with automation protocols for rapid processing of multiple samples.

Abstract: A method of monitoring and evaluating the dry-blending of powders and granular materials via the use of non-dissolvable particulate matter such as mustard seed as a blending aid. The mustard seed is blended into the total batch of dry blend materials and the mustard send can subsequently be extracted by a process of sieving from a known volume of sample taken of the mixture since the mustard seed is larger than the other particles that are being blended. The weight and or sight count of the extracted mustard seed present in the sample is determined and compared with the amount of seed that should be present in a perfect blend to determine if the dry blend materials are thoroughly mixed.

Abstract: The invention relates to a method for analysis by capillary electrophoresis of glycated haemoglobins comprising at least one globin chain comprising a glucose residue bound to the amino acid in the N-terminal position, contained in a biological sample, said method comprising using a buffer composition comprising at least one compound which is capable of specifically complexing glucose residues of one or several glycated haemoglobin(s) and of providing said glycated haemoglobin(s) with several negative electric charges at an alkaline pH. By way of example, this compound may be 3,4- or 3,5-dicarboxyphenylboronic acid, preferably 3,5-dicarboxyphenylboronic acid. Said method may in particular be used to separate and assay haemoglobin HbA1c present in a biological sample optionally comprising other haemoglobins, in particular other minor fractions.

Abstract: A temperature switch comprises a material (14) which melts and concomitantly undergoes a change in an electrical characteristic at a predetermined temperature. The temperature switch also includes at least two electrical contacts (10, 12) for detecting the change in the electrical characteristic. The material (14) comprises an organic cation and an anion and is preferably an ionic liquid.

Abstract: The present invention relates to a process for the work-up of acidic or basic ionic liquids (IL) of the general formula (I), [A]+(1/n)*[Y]???(I) where [A]+ is a quaternary ammonium cation and (1/n)*[Y]n? is one anion equivalent of an n-fold charged anion, which comprises adding a conjugate acid-base pair selected from among compounds of the formula (II), [A]+[X]???(II) where [A]+ has the meaning given for the ionic liquid and [X]? is a conjugate base to the ionic liquid (IL).

Abstract: A liquid reagent in which a methylene blue compound color former is stably stored in a liquid state; and a method of stabilizing a methylene blue compound color former in a liquid state. A methylene blue compound color former is stabilized by causing it to coexist with either a quaternary ammonium compound having a C12 or higher hydrocarbon chain or a salt thereof in a liquid medium. Examples of the methylene blue compound color former include 10-(carboxymethylaminocarbonyl)-3,7-bis(dimethylamino) phenothiazine.

Abstract: A method is described for producing a silver colloid solution comprised of highly stable resulting colloids, the method comprising: adding an aqueous solution of a hydroxylamine salt to an aqueous solution of an alkali, and then dispersing into the mixture an aqueous solution of the metal ions, the hydroxylamine salt being selected such that the anion, when combined with the said metal ions, would form a metal salt having a very low solubility in water, wherein the metal ion solution is introduced into the mixture in such a manner that the metal ions are substantially dispersed throughout the mixture within one second. A maturing period, preferably at elevated temperatures, leads to a stable state in which the characteristics of the colloid undergo no further changes, and it is preferred to make and store the colloid in a polystyrene container for greatest stability.

Abstract: The invention is directed to use of polythiophenes in a method to determine the genuineness of an article which method comprises providing an article treated with a composition comprised of a polythiophene, the polythiophene having a low temperature color and a weak fluorescence and the structure of the polythiophene being designed such that when the composition is placed in a heat-exchange relationship with the article, the low temperature color will change to a high temperature color and the weak fluorescence will change to a strong fluorescence when a pre-determined temperature is met or exceeded in the article, heating the article to a temperature that meets or exceeds the pre-determined temperature and detecting the color and the fluorescence change.

Abstract: A temperature indicating paint comprises 4 wt % to 40 wt % sodium alumino sulpho silicate, 1 wt % to 38 wt % nickel antimony titanate and the binder comprises 25 wt % to 50 wt % silicone resin 10 wt % to 30 wt % acrylic resin each excluding solvent. This composition undergoes colour changes occur, these are; Blue 520-560° C.; Light Blue 950-990° C.; Light Yellow 1000-1040° C.; Glazed Black 1160-1200° C. The colour changes are particularly distinct and enable accurate analysis particularly, but not exclusively, in gas turbine engines.

Abstract: Particles conveying a code are incorporated into polymer matrix to form a core document substrate. These particles may be colored to create a distinctive look of the document that makes it unique for a particular document issuer and enables visual authentication. Addition of a covert attribute to the particle, such as a UV pigment or hidden layer of material, allows a covert, forensic characteristic and it also allows a mathematical description to be calculated describing the random distribution of a specific area on a document and then captured on it (e.g., in the bar code or magnetic stripe or digital watermark on an ID document).

Abstract: A sheath liquid for a particle analyzer used to analyze particles contained in a sample is described. The sheath liquid includes water and a refractive-index adjustment agent with glycerols and/or sulfate. A method for producing the sheath liquid and a method for analyzing particles using the sheath liquid are also described.

Abstract: The present invention relates to a method for improving the hydrolysis stability of an ionic liquid (IL), in which at least one tertiary amine or one quaternary ammonium compound different from the ionic liquid (IL) is added to an ionic liquid (IL).

Abstract: The present invention comprises a method of humidity indication comprising providing a substrate and an area of humidity indication comprising copper bromide, bromide salt, a dye, and cellulose fiber. In another embodiment of the invention, the invention comprises a humidity indicator array comprising a substrate having a plurality of areas of humidity indication on the substrate, wherein each area comprises copper bromide, dye, and bromide salt, wherein the mole ratio of bromide ions to copper ions in the area is about 7.5:1.

Abstract: A sample introduction solution includes nitric acid in an amount between approximately 1 percent and 10 percent by volume, hydrochloric acid in an amount between approximately 0.1 percent and 4 percent by volume, sulfuric acid in an amount between approximately 0.1 percent and 4 percent by volume, and hydrogen peroxide in an amount between approximately 0.1 percent and 8 percent by volume.

Abstract: A pellet 4 for use in spectrometry includes a first powder 41 of a light transmitting material in a compression-molded form, and a second powder 42 which is hydrophilic and water-insoluble and is dispersedly mixed in the first powder. A sample 40 to be subjected to spectrometry is e.g. in a powdery form and dispersedly mixed in the first and the second powders 41 and 42. When the sample 40 is a hydrate, the second powder 42 exerts the effect of accelerating dehydration of the sample 40, so that stable spectrum data on the sample in the dehydrated state is obtained early. This makes it possible to perform a processing such as identification of the sample 40 early and precisely.

Abstract: A Mixture of substances is provided for precise calibration of the mass scale of mass spectrometers equipped with ion sources that operate at atmospheric pressure (AP) with ionization of the analyte molecules, for example by APCI (chemical ionization), or by APPI (photoionization), often at high temperatures of up to 470° C. Out of physical reasons, the mass scale of any time-of-flight mass spectrometer deviates in the lower mass range from the theoretical relation between charge-related mass m/z and flight time t. A closely spaced arrangement of low mass calibration reference points is necessary if high mass accuracy is to be achieved for substances of low molecular weight. APCI and APPI sources are increasingly used in time-of-flight mass spectrometers with orthogonal ion injection (OTOF MS) for the detection of non-polar and weakly polar compounds, in particular, for analyte molecules with relatively low molecular weights.

Abstract: According to an aspect of the invention, a polymerized form of formaldehyde is available in granular form containing a polymerized form of formaldehyde, such as paraformaldehyde, a buffer, such as sodium phosphate dibasic anhydrous, and a stabilizer, such as hydroxymethyl cellulose, or hydroxypropyl methyl cellulose. When added to an aqueous solvent, the paraformaldehyde can dissolve in alkaline solution, and depolymerizes into a formaldehyde solution containing a stabilizer. Optionally a second member of the buffer pair or another buffer or pH adjuster can be used The stabilized depolymerized formaldehyde solution is then ready for use, or can be modified by addition of other substances, such as sodium phosphate monobasic monohydrate. Additionally, an additional buffer may be included in the granular mixture to increase the rate at which the solid dissolves and depolymerizes.

Abstract: Disclosed is an improved post-column fluorimetric determination-boric acid complex anion exchange method which allows analysis of mannose-6-phosphate. The disclosed method is a method for separation analysis of reducing sugars using column chromatography, comprising loading a sample onto an anion exchange column, washing the column by allowing to flow a sufficient volume of a first mobile phase consisting of an aqueous solution of a predetermined concentration of boric acid containing a predetermined concentration of a water-soluble inorganic salt through the column, supplying a second mobile phase with an elevated concentration of the salt to elute the reducing sugars, adding to the eluate a basic amino acid, heating, and continuously measuring and recording the intensity of fluorescent light emitted under irradiation with excitation light.