To Degas Or Prevent Gas Entrapment Patents (Class 264/102)
  • Patent number: 4900493
    Abstract: A method and apparatus for the production of a synthetic resin skin uses a mold for forming at least two separate skin sections which are then joined prior or after a final heat treatment. The synthetic resin skin sections are produced in at least two separate mold members, and the skin sections are then caused to contact each other along determined faces or margins which are joined under light pressure. Any so-called selvage is easily removed after the joining which intimately bonds the skin sections to each other due to the curing of the synthetic resin.
    Type: Grant
    Filed: June 2, 1986
    Date of Patent: February 13, 1990
    Assignee: YMOS Aktiengesellschaft Industrieprodukte
    Inventors: Hermann A. Bartels, Erich M. Christoph, Ruediger Leipnitz
  • Patent number: 4900494
    Abstract: An apparatus including a single screw extruder for extruding a fused molten mass of thermoplastic material and for reverse degassing the melt. The device includes an extrusion screw rotatable in a hollow cylindrial barrel, and a hopper for introducing the melt into the barrel. The screw has at least one flight for conveying the introduced melt and a return delivery flight disposed upstream, in the direction of extrusion, of the hopper. Reverse degassing of the melt is effected by a vacuum source disposed upstream of the hopper in communication with the return delivery section, and provided with a degassing dome generating a reduced pressure or vacuum. At least one radially adjustable separating member for effecting mechanical separation of fused mass from the gas is provided in at least one location in the return delivery section. The method includes degassing of the melt by producing a reduced pressure in the return delivery section. The gas extracted from the melt is discharged.
    Type: Grant
    Filed: February 15, 1989
    Date of Patent: February 13, 1990
    Assignee: Hermann Berstorff Maschinenbau GmbH
    Inventor: Hans Wobbe
  • Patent number: 4897233
    Abstract: The invention relates to a fibre-reinforced thermoplastic semi-finished product includes a thermoplastically processible polymer and long individual reinforcing fibres which form a coherent skeleton, which product can be processed in stamping presses to give moulded articles having a very high surface quality and very good physical properties, and a process for producing this product.
    Type: Grant
    Filed: April 14, 1988
    Date of Patent: January 30, 1990
    Assignee: Bayer AG
    Inventors: Peter Bier, Karl-dieter Loehr, Dieter Titze
  • Patent number: 4892700
    Abstract: A process for making a multilayered formable plastic composite laminate and a process for its manufacture which includes preparing an acrylic composition which includes the reaction product of a mixture of predominantly an acrylic monomer and a substantially lesser amount of a polymer thereof, at least one free radical reaction initiating reaction catalyst, and optionally, a chain length regulating agent or a cross-linking agent; deaerating the acrylic composition; casting the deaerated acrylic composition upon a sheet or laminate of a thermoplastic material; and curing the cast acrylic composition in several successive stages so as to substantially polymerize the acrylic monomer and to permit penetration of the acrylic composition preferably to a depth of between about 0.001-0.
    Type: Grant
    Filed: October 7, 1987
    Date of Patent: January 9, 1990
    Assignee: Polycast Technology Corporation
    Inventors: Carlos Guerra, John Lee, Mark Johnson
  • Patent number: 4883550
    Abstract: A method of manufacturing a fiber-reinforced shaped article of plastics material for pipeline systems. The article includes an inner casing of a thermoplastic material and an outer casing of a fiber winding impregnated with resin. The tape is wound onto the inner casing so that at least the entire surface thereof is covered. The article is then immersed in a resin bath while a negative pressure is maintained outside of and in the interior of the article. The resin bath is subsequently subjected to atmospheric pressure. The impregnated article is removed from the resin bath and the resin is hardened by ultraviolet light while the article is simultaneously rotated.
    Type: Grant
    Filed: April 26, 1988
    Date of Patent: November 28, 1989
    Assignee: Georg Fischer AG
    Inventors: Friedhelm Overath, Michael Weyer
  • Patent number: 4879078
    Abstract: A uniaxially oriented, polyolefin film is prepared by melt blending a mixture of a polyolefin, an inert filler, a processing aid such as calcium stearate, and optionally a stabilizer, maintaining the moisture level in the melt blend below 700 ppm, casting a film, and uniaxially stretching the film at least about 2 times its original casting dimensions in one direction until the film has a sufficient number of elongated, narrow shaped, microporous voids in order to create a CO.sub.2 and O.sub.2 permeance in the range of 5,000 to 10,000,000 cc/100.sup.2 -atm-day. Such a film is used in a controlled atmosphere packaging container as a panel in a window for a controlled flow or flux of CO.sub.2 and O.sub.2 through its wall in an otherwise gas impermeable container.
    Type: Grant
    Filed: March 14, 1988
    Date of Patent: November 7, 1989
    Assignee: Hercules Incorporated
    Inventor: Mitchell K. Antoon, Jr.
  • Patent number: 4877595
    Abstract: Pyrogenically prepared silicic acid is compressed by a rotary filter equipped with a pressing band.
    Type: Grant
    Filed: February 16, 1988
    Date of Patent: October 31, 1989
    Assignee: Degussa Aktiengesellschaft
    Inventors: Reinhard Klingle, Reinhard Manner
  • Patent number: 4876050
    Abstract: A process for dry fiber winding in the absence of resin and subsequent resin impregnating of objects such as projectile bodies having a recessed area for receiving the windings. The process includes winding the projectile body with dry glass or other dry fibers in the absence of resin, placing the wound projectile body into a heated mold, applying a vacuum, pressure injecting a metered amount of resin into the mold, applying pressure to the resin by means of a pressurized ram to impregnate the fibers, allowing the resin to cure to the gel stage within the mold, removing the projectile body from the mold without distrubing the gel surface, and completing cure of the resin at room temperature or in a curing oven.
    Type: Grant
    Filed: October 5, 1987
    Date of Patent: October 24, 1989
    Assignee: Murdock, Inc.
    Inventor: Jack Horton
  • Patent number: 4873040
    Abstract: Through a method for production of piled mats (1-3) with rubber backing on a vulcanizing press (P) with a stationary vulcanizing heater plate (8) where articles (1-3) to be vulcanized are conveyed into position in and out of the press (P) from one and the other side of it using a heat conducting conveyor belt (9), each of the vulcanized articles (1) will be conveyed as soon as it leaves the press (P) on the conveyor belt (9) after the press vulcanizing operation to one of two cooling and degassing stations (KA1, KA2) while at the same time a next unvulcanized article (2) is conveyed on the same conveyor belt (9) into its position in the press (P) while said next article (2) is conveyed after the press vulcanizing operation to the second of the two cooling and degassing stations (KA1, KA2) while at the same time a next unvulcanized article (3) is conveyed on the conveyor belt (9) into its position in the press (P) in connection with which each article at the cooling and degassing stations is removed after the
    Type: Grant
    Filed: October 13, 1988
    Date of Patent: October 10, 1989
    Assignee: Milliken Research Corporation
    Inventor: Aage Lang
  • Patent number: 4871494
    Abstract: A process for forming high free volume, asymmetric gas separation membranes having graded density skins and macrovoid-free morphology from a solvent system comprising a Lewis acid, Lewis base, and a Lewis acid:base complex which dissolve hydrophobic polymers. The dopes have high total solids, high viscosity and low coagulation (g) values which enhance rapid gelation without the formation of macrovoids and which minimize densification. The dope solvent system complexes are readily disassociated by the coagulation medium and the component molecules are miscible in the medium which provides for rapid desolvation of the formed membrane thus providing a membrane having low residual solvent retention.
    Type: Grant
    Filed: July 6, 1987
    Date of Patent: October 3, 1989
    Assignee: Permea, Inc.
    Inventors: Robert E. Kesting, Alfred K. Fritzsche, Milton K. Murphy, Alan C. Handermann, Clint A. Cruse, Raymond F. Malon
  • Patent number: 4863652
    Abstract: A method for manufacturing molded products of polyethylene terephthalate by injection molding or extrusion molding a material containing polyethylene terephthalate as the principal component characterized by using virgin and/or waste polyethylene terephthalate of average molecular weight of more than 10000 to which polymer such as nylon and/or inorganic fillers can be added as required, and molding said material under the following molding conditions by a general type or vent type molding machine:(a) Control of a temperature of a cylinder of the molding machine in the range of melting temperature of resin plus/minus 35.degree. C., and(b) Control of the staying hour of resin in the cylinder to be within 15 minutes.
    Type: Grant
    Filed: May 18, 1987
    Date of Patent: September 5, 1989
    Inventor: Shao C. Chang
  • Patent number: 4861534
    Abstract: A family of circuit boards are molded, each board having its own unique pattern of recessed circuit paths and component insertion through-holes. A different mold is provided for each different member of the family. The two cavity blocks of each mold cavity contain only the holes that are necessary to define the through-hole pattern for that member of the family. A plurality of core pins or wires are provided at the molding site. Only the core pins that are required by the mold in use at the molding site are rendered operative.
    Type: Grant
    Filed: June 29, 1988
    Date of Patent: August 29, 1989
    Assignee: International Business Machines Corporation
    Inventors: Russell W. Boehm, Rex A. Guinn, Hans J. Koerner
  • Patent number: 4859380
    Abstract: Method and apparatus for producing a fiber-reinforced rubber hose having an inner rubber tube, a tubular reinforcing fiber layer, an outer rubber tube, and a resin cover tube, which are formed in this order on a core mandrel. After the formed cover tube is cooled to a temperature sufficiently low to harden the resin to an extent that substantially inhibits expansion of the outer rubber tube in the hardened cover tube, the unvulcanized inner and outer rubber tubes are microwave-heated to soften the rubber tubes, and to cause a thermal shrinkage of the tubular reinforcing fiber layer, for thereby causing a portion of the inner rubber tube to be forced through a network of an interlaced structure of the reinforcing fiber layer into the outer rubber tube. After the unvulcanized inner and outer rubber tubes are vulcanized, the resin cover tube is removed, and the fiber-reinforced rubber hose is prepared.
    Type: Grant
    Filed: January 19, 1988
    Date of Patent: August 22, 1989
    Assignee: Tokai Rubber Industries, Ltd.
    Inventor: Kazuhiro Ogata
  • Patent number: 4855097
    Abstract: A method for making a part with a smooth surface, such as an exterior automotive body panel, by compression molding a charge containing a curable resin. The charge is placed on the molding surface of one of the dies of a compression mold so that the charge covers 40%-80% of the surface area of the molding surface. The molds are moved to a partially closed position and the mold cavity is quickly evacuated. The mold is then closed so that the dies compress the charge to cause it to fill the mold cavity and, after the resin cures, the part is removed from the mold.
    Type: Grant
    Filed: July 14, 1986
    Date of Patent: August 8, 1989
    Assignee: The Budd Company
    Inventors: Kenneth A. Iseler, Robert E. Wilkinson
  • Patent number: 4853170
    Abstract: A method for producing press-molded articles having a plurality of cavities therein includes a mold cavity which can be filled with a particulate molding compound, which mold cavity contains rods sheathed with expandable tubes which can be expanded by means of a fluid under pressure conveyed into the space between the rods and the tubes: this causes compaction of the molding compound to form the pressed article, which can be removed from the mold after reduction of the fluid pressure to allow detumescence of the expandable tubes and withdrawal of these from the mold cavity so that the mold cavity can be opened to remove the shaped pressed article.
    Type: Grant
    Filed: December 3, 1987
    Date of Patent: August 1, 1989
    Assignees: Hutschenreuther AG, Eugen Buhler
    Inventors: Eugen Buhler, Klaus Strobel, Karl Schwarzmeier
  • Patent number: 4851264
    Abstract: A process for reinforcing porous refractories with fillers, such as carbon particles, is provided. First, filler particles are mixed with a liquid resin to produce a liquid mixture. The mixture is allowed to seep into the pores of the refractory, preferably by immersing the refractory in said mixture in an evacuated tank. The refractory can be removed from the mixture and excess mixture can be allowed to drip from the refractory. The refractory is then cured, preferably by heating. The refractory is strengthened by the process to better withstand heat fluctuations encountered, for example, in the steel refining process.
    Type: Grant
    Filed: December 8, 1986
    Date of Patent: July 25, 1989
    Assignee: Magneco/Metrel, Inc.
    Inventors: Subrata Banerjee, Neal T. Sullivan
  • Patent number: 4842787
    Abstract: A method of molding oriented structural yarn/polymer matrix composite structural articles in which a preform of oriented yarn layers saturated with a resin is placed in a shape-defining mold, which is put in an enclosure, and subjected to heat and pressure to cure the resin, after which a cooling medium may be introduced. To enable the use of lightweight multi-part molds, and a mixture of pressure is distributed evenly, an internal liner is collapsed about the mold prior to curing. The process is extremely productive, and allows for accuracy and reproducibility through the use of real time temperature monitoring and closed loop feedback control.
    Type: Grant
    Filed: December 22, 1986
    Date of Patent: June 27, 1989
    Assignee: Xerkon, Inc.
    Inventors: Henry L. Chess, Jr., Roger A. Engdahl, James A. Wedin
  • Patent number: 4840764
    Abstract: A method for forming a cast replica of an article, including: forming an outer mold around the article with a first molding material, the outer mold having an inner surface substantially conforming to the outer surface of the article; separating the article from the outer mold; applying to the outer mold on its inner surface a predetermined thickness of a second molding material which is separable from the outer mold, the second molding material defining a hollow space at the interior thereof; filling the hollow space with a third molding material separable from the second molding material; allowing the third molding material to cure to form an inner mold; separating the second molding material from the outer mold and the inner mold; locating the inner mold or a reproduction thereof within the outer mold with a space between said outer mold and the inner mold representing the predetermined thickness; filling the space between the inner mold and the outer mold with a fourth molding material; allowing the fourt
    Type: Grant
    Filed: October 12, 1988
    Date of Patent: June 20, 1989
    Inventor: Richard F. Cummins
  • Patent number: 4839120
    Abstract: A method of extruding a ceramic batch supplied from a vacuum auger machine into a formed body by a plunger molding machine, included the steps of loosening and crushing a supplied ceramic batch in the vacuum auger machine, extruding the loosened and crushed ceramic batch from the vacuum auger machine into a formed columnar body which is of a size able to be inserted into a cylinder of the plunger molding machine, and extruding the formed columnar body from the plunger molding machine to form a formed body of a predetermined shape. An apparatus for extruding a ceramic batch includes a vacuum auger machine having of a vacuum kneading section for kneading a ceramic material to produce a ceramic batch, a columnar body forming section for forming the kneaded ceramic material into a columnar body, and a batch transfer section having an auger for transferring the ceramic batch to the columnar body forming section.
    Type: Grant
    Filed: February 18, 1988
    Date of Patent: June 13, 1989
    Assignee: NGK Insulators, Ltd.
    Inventors: Toshio Baba, Hajime Matsushita, Yasuji Katsuragawa
  • Patent number: 4839114
    Abstract: A method of manufacturing a highly electrically conductive plastic material from thermoplastic resin and carbon fill through a two-screw mixer having a screw length of more than twenty times the screw diameter involves continuously inserting a thermoplastic resin into a first zone of the two-screw mixer and compacting and preheating the thermoplastic resin. The resin is then passed into a second zone where it is kneaded and plastified. A particulate carbon fill is continuously inserted into a third zone with the fill constituting 30 to 50% by weight of the mixture and being dispersed in said resin within the third zone. The speed of rotation of the two screw mixer lies in the range between 150 to 250 RPM and the temperatures of the zones lie within the range of 165.degree. C. to 300.degree. C. After passage through the various zones, the mixture is removed via an outlet of an extrusion head.
    Type: Grant
    Filed: December 18, 1985
    Date of Patent: June 13, 1989
    Assignee: Occidental Chemical Corporation
    Inventors: Rene Delphin, Bernard Regnaut
  • Patent number: 4830801
    Abstract: Process for a worm extruder or continuous kneader to produce either a degasses paste or plastic composition is disclosed. A mixture of either solid or liquid organic peroxides in the paste or plastic composition having evaporable constituents are introduced into the device, homogenized and degassed by exposing the mixture to a degassing passage of the extruder. The mixture has a free surface which is more than 40% of the cross-section of the degassing passage and the minimum gas passage cross-section of the return delivery device amounts to at least about 0.1 times the degassing passage cross-section.
    Type: Grant
    Filed: November 12, 1987
    Date of Patent: May 16, 1989
    Assignee: Peroxid-Chemie GmbH
    Inventors: Erwin Rossberger, Josef Weinmaier, Nikolaus Ailler
  • Patent number: 4826931
    Abstract: A resin-molding tablet for use in resin-molding semiconductor devices has a tablet body formed of powdered or particulate resin. The particles of the resin are compacted such as to form voids between adjacent particles. At least the outer peripheral region of the tablet is fused such that the resin particles are welded together to form a continuous layer of fine and impervious structure substantially free of open pores. The internal air trapped in the voids of the tablet is drawn and removed before the tablet is fused so that the tablet is substantially free of air. The tablet is produced by placing a particulate or powdered resin material in a vacuum vessel so as to allow the internal air in the resin material to be drawn outside, and then applying pressure and heat to the resin material so that at least the peripheral region of the mass of the particulate resin is fused to weld together.
    Type: Grant
    Filed: October 9, 1987
    Date of Patent: May 2, 1989
    Assignee: Mitsubishi Denki Kabushiki Kaisha
    Inventors: Kunito Sakai, Sueyosi Tanaka, Yasutugu Tutumi, Yutaka Morita
  • Patent number: 4824631
    Abstract: Uncured elastomeric sheet material (42) is built up on the outer surface of a production article (36) constructed from composite materials. A vacuum bag system (20, 24, 26, 30, 32) is used for holding the uncured elastomer member (60) against the composite article (36) while the elastomer member (60) is being cured under heat and pressure. Such curing causes the elastomer member (60) to shrink. The elastomer member (60) is then resized by cutting it into sections (66). The sections (66) are placed back on the composite article (36) and each is positioned on such article (36) at a location best conforming to it in shape. This leaves gaps (68) between the sections (66). Additional uncured elastomer (70) is applied to fill the gaps (68) and bridge across the gaps (68), to in that manner splice the sections (66) together. A vacuum bag (20, 24, 26, 30, 32) is again applied and the bag assembly (20, 24, 26, 30, 32 ) is again cured under heat and pressure, to cure the additional elastomer material (70).
    Type: Grant
    Filed: May 28, 1987
    Date of Patent: April 25, 1989
    Assignee: The Boeing Company
    Inventor: James F. Yeager
  • Patent number: 4822269
    Abstract: In a vent type injection molding machine of the type comprising a heating cylinder, injection nozzle means having a vent port and connected to the front end of the heating cylinder and a reciprocatable screw for metering a predetermined quantity of resin to be injected, the injection nozzle means comprises a first injection nozzle connected to the heating cylinder, a second injection nozzle coaxial with the first injection nozzle, a spring for urging the second injection nozzle against a stationary metal mold and a housing surrounding the first and second injection nozzles. The vent port is provided through the housing at a point communicating with a space in the housing between the first and second injection nozzles.
    Type: Grant
    Filed: August 20, 1987
    Date of Patent: April 18, 1989
    Assignee: Toshiba Kikai Kabushiki Kaisha
    Inventors: Takashi Kamiyama, Shigeru Fujita
  • Patent number: 4822439
    Abstract: A process is provided for manufacturing ballistic resistant composites of an isophthalic thermoset polyester and woven roving made of magnesia aluminosilicate glass fibers. An impregnating solution is provided whereby prepregs can be conveniently formed and then vacuum bag molded. The ingredients i the impregnating solution are critically selected to provide prescribed viscosities after the elapse of certain periods of time and thereby allow the final articles to be formed in an economical and expedient manner.
    Type: Grant
    Filed: August 24, 1987
    Date of Patent: April 18, 1989
    Assignee: Owens-Corning Fiberglas Corporation
    Inventors: James V. Gauchel, Edward L. Wilson, Edward J. Kerle, Terry R. Beaver
  • Patent number: 4820463
    Abstract: The invention relates to a process for degassing and pelletizing polyolefin particles produced by a gas phase polymerization. The polyolefin particles are submitted to a primary degassing, preferably at the outlet of a reactor for catalytic polymerization in the gas phase. Then the polyolefin particles are subjected to a secondary degassing step comprising agitating the particles by a mechanical stirrer and converting the mechanical energy therefrom into heat such that the temperature of the particles is brought to between 80.degree. and 120.degree. C. which is close to minimum sintering temperature Ts so that the polyolefin particles are substantially freed from the gases accompanying them. The heated degassed polyolefin particles are then pelletized in an extruder of a pelleting unit.
    Type: Grant
    Filed: April 30, 1987
    Date of Patent: April 11, 1989
    Assignee: BP Chemicals Limited
    Inventor: Charles Raufast
  • Patent number: 4816106
    Abstract: A composite structure is prepared in a mold using an elastic diaphragm which allows the application of a uniformly distributed pressure during a curing cycle. The elastic diaphragm seals a resin impregnated lay-up throughout the curing cycle during which the lay-up is heated and compressed, and ensures a constant resin-to-reinforcement ratio by preventing the escape of resin from the lay-up as the viscosity of the resin is lowered during the initial stages of the curing cycle. In instances where entrapped air or volatile removal from the lay-up is necessary, a separate step including the application of a vacuum and/or heat to the lay-up can be performed prior to the final curing cycle.
    Type: Grant
    Filed: October 28, 1986
    Date of Patent: March 28, 1989
    Assignee: Aeritalia Saipa - Gruppo Velivoli da Trasporto
    Inventors: Fabrizio R. S. Turris, Salvatore Pagliuso
  • Patent number: 4810444
    Abstract: A process for the preparation of molded high strength composites comprising fibrous reinforcing material impregnated with a reaction injection molded polyisocyanurate resin. The process comprises first evacuating a mold containing the fibrous reinforcing material said mold equipped with means for accepting an overflow volume of the resin. The mold system is pressurized prior to gelation causing the overflow volume to be forced into a final volume. The molded composites have a high flexural moduli, good physical properties, low void content and smooth surface.
    Type: Grant
    Filed: June 8, 1987
    Date of Patent: March 7, 1989
    Assignee: The Dow Chemical Company
    Inventors: Louis M. Alberino, Peter S. Carleton, Douglas P. Waszeciak
  • Patent number: 4808362
    Abstract: A method of forming a hollow reinforced fiber structure includes the steps of providing fiber reinforced material around a flexible expandable member and placing the resulting package inside of a mold which includes inner surfaces conforming to the shape of the structure being formed. A second expandable means is included in the mold on both sides of the package. After the mold is closed, pressure is applied to force the second expandable means against the fiber reinforced material. Resin is injected into the fiber reinforced material. The pressure is then decreased in the second expandable means as inflatable member is expanded to force the fiber material to conform to the inner surfaces of the mold. The fiber material is then cured to form the structure.
    Type: Grant
    Filed: June 4, 1987
    Date of Patent: February 28, 1989
    Assignee: The Budd Company
    Inventor: Richard B. Freeman
  • Patent number: 4806297
    Abstract: Impact- and solvent-resistant resin blends are prepared from a polyphenylene ether, or blend thereof with a polystyrene, a linear polyester such as a poly(alkylene dicarboxylate), at least one elastomeric polyphenylene ether-compatible impact modifier and at least one polymer containing a substantial proportion of aromatic polycarbonate units as a compatibilizing agent. There may also be present a minor amount of at least one epoxide and/or masked isocyanate such as triglycidyl isocyanurate or a glycidyl methacrylate polymer. The polyphenylene ether is preferably inactivated by reaction with at least one non-volatile carboxylic acid or anhydride and/or by extrusion with vacuum venting.
    Type: Grant
    Filed: January 15, 1988
    Date of Patent: February 21, 1989
    Assignee: General Electric Company
    Inventors: Sterling B. Brown, John B. Yates, III
  • Patent number: 4805914
    Abstract: A game ball, particularly a golf ball, having a liquid core, in which some portion of the dissolved gases in the liquid are removed to decrease the compressability of the liquid core.
    Type: Grant
    Filed: September 4, 1986
    Date of Patent: February 21, 1989
    Inventor: J. William Toland
  • Patent number: 4800049
    Abstract: A process and an apparatus obtain plastic molded objects according to a technique which consists of introducing the plastic into a silicone elastomer mold, then inserting this mold into a high frequency device comprising a turntable "carrousel", a series of high frequency heating presses and a cooling device.The process is characterized by the introduction of plastic into one end of the mold in the form of liquid plastisol under low pressure, i.e., less than 1 Magapascal. The apparatus employs a carrousel, a mold having two male inserts and resting on the carrousel, vacuum-creating means and plastisol injection means.
    Type: Grant
    Filed: May 12, 1987
    Date of Patent: January 24, 1989
    Assignee: Anver
    Inventor: Elie Gras
  • Patent number: 4797236
    Abstract: A method for injection molding a material involving bringing the interior of a tightly sealed injection mold under a high vacuum, then injecting the material into the interior of the injection mold at an ultrahigh speed in the vicinity of a speed at which adiabatic change is exerted on the material in accordance with a predetermined pattern of internal pressure so as to fill the interior of the injection mold with the material, and molding the material under low pressure. An injection molding apparatus used for carrying out the aforementioned method is capable of bringing the interior of the injection mold to a high vacuum.
    Type: Grant
    Filed: December 18, 1985
    Date of Patent: January 10, 1989
    Assignee: Technoplas, Inc.
    Inventor: Hisashi Kojima
  • Patent number: 4792424
    Abstract: The present disclosure is directed to a method of injection molding PVC products from powdered raw material, while employing an injection molding machine having a plasticizing unit having a rotary screw and a rotary screw and an injection unit having a screw which both rotates and reciprocates. The powdered raw material is subjected firstly to a prejellifying treatment during forced transportation through the plasticizing unit in which it is heated and brought to agglomerate in a relatively short time and the agglomerate is subjected to a vacuum after the prejellifying treatment and its introduction into the injection unit at an absolute pressure of less than 50 kPa.
    Type: Grant
    Filed: September 10, 1985
    Date of Patent: December 20, 1988
    Inventor: Henricus G. M. Loman
  • Patent number: 4784814
    Abstract: Molded bodies of thermoset material are produced from monomers, oligomers or higher pre-polymers of reactive resins by pressure reaction injection molding. The molded bodies may contain filler and/or reinforcing material. The process is carried out in a mold consisting of a first, preferably upper half mold and a second, preferably lower half mold, and an inlet socket opening downwardly into the first half mold. The mold is equipped with heating coils adapted for applying separately a lower temperature to the first half mold and a higher temperature to the second one. During the introduction and hardening phase of the reactive mixture, the first half mold is maintained at a lower temperature than the second half mold, the temperature difference amounts to about 40 to 180, and preferably 60 to 120 centigrades.
    Type: Grant
    Filed: July 3, 1986
    Date of Patent: November 15, 1988
    Assignee: Ciba-Geigy Corporation
    Inventors: Hermann Diethelm, Wolfgang Dresen
  • Patent number: 4781870
    Abstract: A mirror--typically of the spherical or aspherical variety--is replicated on a large scale (in the order of 2'.times.4') to an optical accuracy in the range of less than one arc minute. An optical master is created by heat shrinking and holding an acrylic sheet to a steel substrate of the same shape as desired mirror in the constant presence of a vacuum at the steel-acrylic interface. The acrylic is optically polished to complete the master. The master is then appropriately dammed to the mirror dimension and poured with subsequently cured epoxy so that the epoxy forms the optical surface of the replicated mirror. A backing master--created by substantially the same process as the optical master--allows fabrication of a backing, composed of a series of adhesive layers typically sandwiching a core material such as commercial honeycomb therebetween, to be made with a curvature substantially similar to the curvature of the replicated optical surface.
    Type: Grant
    Filed: March 18, 1983
    Date of Patent: November 1, 1988
    Inventor: John W. Talbert
  • Patent number: 4776907
    Abstract: A method of resin bonding opposing surfaces of a pair of members for providing a joint having substantially resin free surfaces adjacent the joint. The adjacent surfaces and the joint are covered in intimate contact with a thin, perforated, flexible, and nonadherent film for perforating resin extruded from the joint during application of bonding pressure. The nonadherent film is covered with a sheet of flexible absorbent material for absorbing the resin perforated through perforations along the film. Bonding pressure is applied to the joint to extrude the resin from the joint. The nonadherent film and the absorbent sheet is then removed from the surfaces adjacent to the joint to facilitate secondary bonding to the adjacent surfaces.
    Type: Grant
    Filed: September 25, 1987
    Date of Patent: October 11, 1988
    Assignee: The Boeing Company
    Inventors: Vincent P. Massions, Arnold E. Florio
  • Patent number: 4770835
    Abstract: A method of molding an article utilizing two types of solid flowable particulate polymer pressurizing media wherein one medium is protected from thermal degradation by a second medium. The method comprises disposing an article precursor within a pressure vessel and disposing a first solid flowable polymer medium that is substantially thermally stable at temperatures in excess of about 316.degree. C. so that it is capable of transferring a substantially uniform, predetermined medium pressure to the surface of the article precursor. A second solid flowable polymer medium is disposed so that it is capable of transferring a substantially uniform, predetermined medium pressure to the first polymer medium. The second medium is caused to produce a substantially uniform medium pressure so that said pressure is transferred to the surface of the article precursor and the article precursor is exposed to temperatures in excess of about 316.degree. C.
    Type: Grant
    Filed: September 10, 1986
    Date of Patent: September 13, 1988
    Assignee: United Technologies Corporation
    Inventor: Robert V. Kromrey
  • Patent number: 4769100
    Abstract: A method of applying a carrier film prepainted with metallic paint containing metal flakes to an automobile body panel in a vacuum forming process.
    Type: Grant
    Filed: September 22, 1986
    Date of Patent: September 6, 1988
    Assignee: General Motors Corporation
    Inventors: William T. Short, Charles C. Mentzer, Howard W. Cox
  • Patent number: 4761264
    Abstract: A method for molding powders which comprises introducing a thin-wall resilient mold inside a ventilative mold support, reducing the outside pressure of the ventilative mold support to less than the atmospheric pressure (760 Torr), putting a thin-wall resilient mold exactly close to the inside wall of the ventilative mold support, supplying powder material into the thin-wall resilient mold, exhausting air existing in the voids formed in the powder material, and taking the ventilative mold support apart to apply cold isostatic press treatment to the thin-wall resilient mold. The shape of the thin-wall resilient mold is similar to the shape of the ventilative mold support.
    Type: Grant
    Filed: June 12, 1987
    Date of Patent: August 2, 1988
    Assignee: Nippon Kokan Kabushiki Kaisha
    Inventors: Hiroaki Nishio, Jun Harada
  • Patent number: 4755341
    Abstract: A method particularly adapted for making a complex shaped composite component that has reduced bridging defects. The method comprises disposing a composite prepreg on to a substantially flat tool. The composite prepreg has a substantially flat section and at least one prepreg member extending from and substantially perpendicular to said flat section. A layer, at least about 125% of said composite prepreg height, of a said flowable particulate silicone rubber is disposed in substantially complete contact with the composite prepreg surface. The particulate silicone rubber has a flow rate of at least 0.6 gram/second through a 1.1 cm diameter pipe 7.6 cm long under applied pressure of 10.34 MPa at room temperature. The layer of solid flowable rubber is covered with a bag to effect a gas tight seal. The bag is exposed to pressures which are transferred to said prepreg by said solid flowable polymer. The composite prepreg is exposed to temperatures to form a composite component.
    Type: Grant
    Filed: September 10, 1986
    Date of Patent: July 5, 1988
    Assignee: United Technologies Corporation
    Inventors: Richard T. Reavely, Peter C. Ogle, Robert V. Kromrey
  • Patent number: 4755343
    Abstract: A flowable particulate polymer-metal mixture that is thermally conductive and is particularly adapted for use as a pressurizing medium in a high pressure elevated temperature molding process. The material comprises a substantially uniform mixture of about 20% to about 90% solid flowable, particulate silicone rubber having a nominal flow rate of at least 0.6 gram/second through a 1.1 cm diameter pipe 7.6 cm long under applied pressure of 10.34 MPa at room temperature. The material also comprises about 10% to about 80% thermally conductive particulate metal that has a melting point less than the molding temperature and is substantially chemically compatible with said silicone rubber. The pressurizing medium is used to mold article precursors into articles by placing an article precursor within a pressure vessel and substantially filling the vessel with a pressurizing mixture.
    Type: Grant
    Filed: September 10, 1986
    Date of Patent: July 5, 1988
    Assignee: United Technologies Corporation
    Inventor: Robert V. Kromrey
  • Patent number: 4751488
    Abstract: A coil is made having a plurality of layers of adjacent metal conductor windings subject to voltage stress, where the windings have insulation therebetween containing a small number of minute disposed throughout its cross-section, where the voids are voids filled with SF.sub.6 gas to substitute for air or other gaseous materials in from about 60% to about 95% of the cross-sectional void volume in the insulation, thus incorporating an amount of SF.sub.6 gas in the cross-section of the insulation effective to substantially increase corona inception voltages.
    Type: Grant
    Filed: June 4, 1981
    Date of Patent: June 14, 1988
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: Thomas J. Lanoue, Clarence L. Zeise, Loren Wagenaar, Dean C. Westervelt
  • Patent number: 4747985
    Abstract: A method for the manufacture of a magnesia-carbon brick comprising the steps of:a. preparing a mixture comprising:1. burned magnesite2. carbon3. binder solution comprising3.1 precondensed novolak resin3.2 solvent for the novolak resin4. a hardener for the resinb. pressing a brick from the said mixture.
    Type: Grant
    Filed: September 11, 1986
    Date of Patent: May 31, 1988
    Assignee: Hoogovens Groep B.V.
    Inventors: Jaap H. Addink, Christian M. J. M. Beelen, Adam Steen, Hendrik M. Verhoog, Jurrie de Boer
  • Patent number: 4746482
    Abstract: The invention relates to a method for the manufacture of molding materials containing polyphenylene ether (PPE) and to the materials obtained according to this method. Molten PPE containing at least 0.1% volatile components is degasified until it reaches a residual content of volatile components of less than 500 ppm. Subsequently, additional molten polymers and/or additives are added to this molten mass at the lowest possible temperature and both components are mixed.
    Type: Grant
    Filed: December 29, 1986
    Date of Patent: May 24, 1988
    Assignee: HULS Aktiengesellschaft
    Inventors: Wilfried Ribbing, Hans Jadamus, Hans-Eberhard von Portatius
  • Patent number: 4744934
    Abstract: A process is provided for reducing black speck formation which occurs during melt processing of oxymethylene polymer compositions containing polyamide stabilizers having a melting or softening point below the melting point of the oxymethylene polymer and for simultaneously removing volatile materials from a molten oxymethylene polymer, according to which from about 0.05 to about 5.0 weight percent based on the weight of the oxymethylene polymer of said polyamide stabilizer and from about 0.05 to about 10.0 weight percent, based on the weight of the oxymethylene polymer, of hindered phenol antioxidant is added while the molten polymer is passed through a rotating disk polymer processor having at least three stages; a first devolatilization stage, then a stabilization stage and then a second devolatilization stage. The molten polymer in the first devolatilization stage is maintained at a temperature above its melting point in the temperature range of from about 160.degree. C. to about 220.degree.
    Type: Grant
    Filed: February 28, 1986
    Date of Patent: May 17, 1988
    Assignee: Hoechst Celanese Corporation
    Inventor: Ronald S. Christy
  • Patent number: 4743420
    Abstract: A mold assembly for producing a container having a closed bottom is disclosed. Inner and outer core members are closely spaced together to provide a cavity for forming a container having a wall thickness on the order of 0.015 inch. The cavity is formed with a plurality of radial flow channels which produce corresponding ribs on the container bottom. The radial channels extend from an axial injection port outwardly to the wall portion of the cavity, where a thickened transition region joins the bottom of the container to the side wall portion thereof. A plurality of vertical flow channels are formed by means of milled flat portions on the surface of the inner core along the length of the side wall. The flow channels cause fluid plastic injected under high pressure to flow radially outwardly, around the bottom corner of the container, and down the vertical flow channels located intermediately of the ends of the ribs.
    Type: Grant
    Filed: September 16, 1986
    Date of Patent: May 10, 1988
    Assignee: Sun Coast Plastics, Inc.
    Inventor: Herbert V. Dutt
  • Patent number: 4740346
    Abstract: A resin transfer molding system includes a plurality of ports for injecting resin into reinforcement material, which preferably comprises fabric, disposed between upper and lower mold pieces to form a structural part. Channels are provided adjacent the fabric reinforcement material and act as reservoirs to permit relatively fast and efficient injection of the resin without excessive applied pressure.
    Type: Grant
    Filed: February 26, 1986
    Date of Patent: April 26, 1988
    Assignee: The Budd Company
    Inventor: Richard B. Freeman
  • Patent number: H559
    Abstract: A method for curing resin in the fabrication of a composite material is described comprising enclosing the composite material within a flexible vacuum enclosure, and substantially simultaneously pressing the material within the enclosure between first and second platens of a press to preselected pressure, evacuating the enclosure, selectively heating one of the platens according to a preselected scheme to preselected cure temperature to cure the resin within the material, and cooling the other platen to maintain a preselected temperature differential between the platens across the thickness of the material, whereby cure of the resin is effected in the material first near the heated platen and progresses through the thickness of the material toward the cooler platen as the material is heated to the cure temperature.
    Type: Grant
    Filed: May 12, 1987
    Date of Patent: December 6, 1988
    Assignee: The United States of America as represented by the Secretary of the Air Force
    Inventor: Scott C. Brown
  • Patent number: H565
    Abstract: A vacuum bag autoclave type procedure for curing layers of phenolic resin pregnated fibrous material to form a composite structural part. A straight up heat rise cure cycle is employed in conjunction with a layup and bagging procedure that ensures a relatively free bleed of excess resin during cure and a high-capacity vacuum system for removal of volatiles generated during cure. This method of fabrication releases the majority of volatiles prior to gelation and produces a part having a pore structure that provides an escape path for gases generated during cure and postcure to prevent delamination.
    Type: Grant
    Filed: April 3, 1985
    Date of Patent: January 3, 1989
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventors: Edward J. Ford, Louis H. Dick, Jose L. Camahort