Carbonizing To Form Article Patents (Class 264/29.1)
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Patent number: 11897816Abstract: A process for manufacturing a part made of a ceramic matrix composite material, includes coating an outer surface of a porous preform with a layer of a fugitive material to form a model of the part to be obtained, the fugitive material being wax or resin, the fugitive material layer in the model not exceeding the highest peak of surface undulations of the preform, and ceramic and/or carbon particles being present in the porosity of the preform, coating the model formed with a ceramic powder composition, heat treating the coated model to remove the fugitive material and form a ceramic shell mold by sintering of the ceramic powder composition, introducing a molten composition including silicon into the shell mold to obtain the part in the shell mold, the molten composition infiltrating the porosity of the preform to form the ceramic matrix, and separating the shell mold from the part obtained.Type: GrantFiled: May 15, 2019Date of Patent: February 13, 2024Assignees: SAFRAN, SAFRAN CERAMICS, SAFRAN AIRCRAFT ENGINESInventors: Michaël Podgorski, Bruno Jacques Gérard Dambrine, Emilie Chantal Gisèle Mendez, Wen Zhang, Yvan Rappart, Charles Leleu
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Patent number: 11702370Abstract: Systems, devices, and methods are provided for manufacturing a carbon ceramic brake disc. Generally, a plurality of uncured or partially-cured bulk molding compound preforms or molding compound layers and ventilation cores are placed in a mold cavity and warm-pressed at a first temperature. The ventilation cores are removed from the resulting cured green body. The cured green body is then removed from the mold, and treated through a polymer infiltration and pyrolysis or reactive melt infiltration process. Certain steps can be repeated until a desired target density or weight is attained.Type: GrantFiled: January 10, 2019Date of Patent: July 18, 2023Assignee: SiC Technologies, Inc.Inventor: Clifford B. Leonard
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Patent number: 11679983Abstract: A super-flexible high thermal conductive graphene film and a preparation method thereof are provided. The graphene film is obtained from ultra large homogeneous graphene sheets through processes of solution film-forming, chemical reduction, high temperature reduction, high pressure suppression and so on. The graphene film has a density in a range of 1.93 to 2.11 g/cm3, is formed by overlapping planar oriented graphene sheets with an average size of more than 100 ?m with each other through ?-? conjugate action, and comprises 1 to 4 layers of graphene sheets which have few defects. The graphene film can be repeatedly bent for 1200 times or more, with elongation at break of 12-18%, electric conductivity of 8000-10600 S/cm, thermal conductivity of 1800-2600 W/mK, and can be used as a highly flexible thermal conductive device.Type: GrantFiled: July 20, 2016Date of Patent: June 20, 2023Inventors: Chao Gao, Li Peng, Yanqiu Jiang, Yingjun Liu
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Patent number: 11326255Abstract: A system and method for improved atomic layer deposition. The system includes a top showerhead plate, a substrate and a bottom showerhead plate. The substrate includes a porous microchannel plate and a substrate holder is positioned in the system to insure flow-through of the gas precursor.Type: GrantFiled: February 7, 2014Date of Patent: May 10, 2022Assignee: UChicago Argonne, LLCInventors: Anil U. Mane, Joseph Libera, Jeffrey W. Elam
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Patent number: 11053126Abstract: One aspect is a production process including feeding a feed material composition into a reaction zone at a feeding position, wherein the feed material composition is liquid or gaseous or both; reacting the feed material composition in the reaction zone into a first plurality of particles by a chemical reaction; depositing the first plurality of particles onto a substrate surface of a substrate, thereby obtaining a porous silicon dioxide material, having a pore structure, in the form of up to 20 layers superimposing the substrate surface; at least partially removing the porous silicon dioxide material from the substrate surface; and modifying the pore structure of the porous silicon dioxide material, thereby obtaining the porous silicon dioxide material having a further pore structure.Type: GrantFiled: October 26, 2018Date of Patent: July 6, 2021Assignee: Heraeus Quarzglas GmbH & Co. KGInventors: Sascha Pihan, Jörg Becker, Christian Neumann
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Patent number: 10910638Abstract: A non-amorphous hard carbon material, synthesized from Furan-ring containing compounds, is described. These non-amorphous hard carbon materials have a d002 peak in their X-ray diffraction patterns, corresponding to an interlayer spacing of >3.6 ?, along with a prominent D-band peak in their Raman spectra. BET surface area values between 2 m2/gm and around 100 m2/gm can be obtained by controlling the processing parameters of temperature, time and heating rate. The higher surface area HCs—in Li-ion and Na-ion anode configurations—are capable of high charging rates up to 100 C with a cycle life of up to 1000 cycles. Composites of these non-amorphous hard carbons with silicon and lithium compounds are also disclosed.Type: GrantFiled: August 31, 2018Date of Patent: February 2, 2021Assignee: Farad Power, IncInventors: Shantanu Mitra, Vinod Nair
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Patent number: 10822279Abstract: In some examples, a technique for infiltrating a porous preform with a slurry to form an infiltrated-preform, where the slurry includes a plurality of solid particles, where the plurality of solid particles include a plurality of fine ceramic particles defining an average fine particle diameter, a plurality of coarse ceramic particles defining an average coarse particle diameter, and a plurality of diamond particles, where the average fine particle diameter is less than the average coarse particle diameter, and infiltrating the infiltrated-preform with a molten metal infiltrant to form a ceramic matrix composite (CMC) article.Type: GrantFiled: April 28, 2017Date of Patent: November 3, 2020Assignee: Rolls-Royce High Temperature Composites, Inc.Inventors: Sungbo Shim, Robert Shinavski
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Patent number: 10801118Abstract: An electrolysis cell, particularly for the production of aluminum, contains a cathode, a layer of liquid aluminum arranged on the upper side of the cathode, a melt layer thereon and an anode on the top of the melt layer. The cathode is composed of at least two cathode blocks, wherein at least one of the at least two cathode blocks differs from at least one of the other cathode blocks with regard to the average compressive strength, the average thermal conductivity, the average specific electrical resistivity and/or the apparent density.Type: GrantFiled: April 9, 2013Date of Patent: October 13, 2020Assignee: TOKAI COBEX GMBHInventor: Ghazanfar Abbas
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Patent number: 10782190Abstract: A resistance temperature detector (RTD) that uses a ceramic matrix composite (CMC), such as a silicon carbide fiber-reinforced silicon carbide matrix, as an active temperature sensing element, which can operate at temperatures greater than 1000° C. or even 1600° C. Conductive indium tin oxide or a single elemental metal such as platinum is deposited on a dielectric or insulating layer such as mullite or an environmental barrier coating (EBC) on the substrate. Openings in the layer allow etching of the CMC surface in order to make high quality ohmic contacts with the conductive material, either directly or through a silicide diffusion barrier such as ITO. The RTD can measure both temperature and strain of the CMC. The use of an EBC, which typically is deposited on the CMC by the manufacturer, as the insulating or dielectric layer can be extended to other devices such as strain gages and thermocouples that use the CMC as a sensing element. The EBC can be masked and etched to form the openings.Type: GrantFiled: December 14, 2018Date of Patent: September 22, 2020Assignee: University of Rhode Island Board of TrusteesInventors: Otto J. Gregory, Kevin Rivera, Matthew Thomas Ricci
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Patent number: 10697469Abstract: A casing for a subsea compressor comprises a main body having a central axis; a plurality of interconnection flanges attached to the main body; wherein the main body comprises an inner layer made of corrosion resistant material; an outer layer applied over the inner layer and made of a composite material; wherein the outer layer extends along the entire length of said main body.Type: GrantFiled: June 15, 2016Date of Patent: June 30, 2020Assignee: NUOVO PIGNONE SRLInventors: Manuele Bigi, Simone Marchetti, Luciano Mei, Odd Marius Rosvold, Marco M A Anselmi
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Patent number: 10619949Abstract: A method of making a light weight housing for an internal component is provided. The method including the steps of: forming a first metallic foam core into a desired configuration; forming a second metallic foam core into a desired configuration; inserting an internal component into the first metallic foam core; placing the second metallic foam core adjacent to the first metallic core in order to secure the internal component between the first metallic foam core and the second metallic foam core; applying an external metallic shell to an exterior surface of the first metallic foam core and the second metallic foam core; and securing an inlet fitting and an outlet fitting to the housing, wherein a thermal management fluid path for the internal component into and out of the housing is provided by the inlet fitting and the outlet fitting.Type: GrantFiled: April 12, 2016Date of Patent: April 14, 2020Assignee: UNITED TECHNOLOGIES CORPORATIONInventor: Gary D. Roberge
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Patent number: 10591010Abstract: The invention relates to a method for producing a friction lining material as well as a friction lining material having a porous body, whose pores are filled with a filling material, said porous body being formed on the basis of petroleum coke.Type: GrantFiled: January 19, 2016Date of Patent: March 17, 2020Assignee: SCHUNK HOFFMAN CARBON TECHNOLOGY AGInventor: Klaus Reiser
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Patent number: 10449517Abstract: Chromatography media including a high surface area thermoplastic porous nanofiber and an ion-exchange ligand functionality on the surface of the fiber. The porous nanofibers display a convoluted structure that is comprised of discrete bundles of highly entangled nanofibrils that may be fibrillated or ridged. The porous fibers can be prepared through the extraction of a dissolvable mineral or polymeric porogen that is embedded into the fiber during its manufacture in a melt extrusion process.Type: GrantFiled: August 19, 2015Date of Patent: October 22, 2019Assignee: EMD Millipore CorporationInventors: John Paul Amara, John Boyle, David Yavorsky, Benjamin Cacace
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Patent number: 10442559Abstract: A multi-functional composite structure has a modular design that can be altered depending on an extreme environment in which the structure will be exposed such as hazardous radiation, micro-meteoroid and orbital debris impacts, extreme temperature changes, etc. The material combinations employed in the multi-functional composite structure provide a supporting structure with low weight and maximum protection from radiation, debris impacts and temperature variations.Type: GrantFiled: August 2, 2016Date of Patent: October 15, 2019Assignee: The Boeing CompanyInventors: Jian Dong, Naveed Moayyed Hussain
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Patent number: 10418187Abstract: The carbon porous body of the present disclosure includes micropores and mesopores. A micropore volume determined at a temperature of 77K by as plot analysis of a nitrogen adsorption isotherm is 100 (cm3 (STP)/g) or more. A BET specific surface area determined from the nitrogen adsorption isotherm is 1,000 m2/g or more. The derivative of the nitrogen adsorption isotherm is 300 (cm3 (STP)/g) or more over the range where relative pressure P/P0 in the nitrogen adsorption isotherm is from 0.10 to 0.20 inclusive, and the derivative of the nitrogen adsorption isotherm is 200 (cm3 (STP)/g) or more over the range where the relative pressure P/P0 in the nitrogen adsorption isotherm is from 0.20 to 0.95 inclusive. The amount of nitrogen adsorbed when the relative pressure P/P0 in the nitrogen adsorption isotherm is 0.98 is 1,200 (cm3 (STP)/g) or more.Type: GrantFiled: February 17, 2017Date of Patent: September 17, 2019Assignee: KABUSHIKI KAISHA TOYOTA CHUO KENKYUSHOInventors: Masaki Hasegawa, Nobuhiro Ogihara, Norihiko Setoyama
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Patent number: 10418640Abstract: The method includes dispensing carbon fibers having a length of between about 3 and 12 millimeters from a first hopper into a raizing chamber of a double-hopper, bladed-roiler scattering machine and simultaneously depositing a thermoset resin powder from a second hooper of the scattering machine into the mixing chamber where in the fibers and powder are mixed to homogenous predetermined proportions of between about 40% and 60% each. Then, the mixture is directed to flew onto a moving support belt of a double belt press apparatus and the mixture is compressed between the moving support belt and a moving compression belt of the double belt press apparatus and the mixture passes between the belts for an adequate residence time duration to first melt and then cure the thermoset resin to form the fuel cell precursor substrate. Carbonizing and then graphitizing the precursor substrate forms the final substrate.Type: GrantFiled: December 9, 2013Date of Patent: September 17, 2019Assignee: AUDI AGInventor: Richard D. Breault
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Patent number: 10399908Abstract: The method may include forming fibers with a silicon-based sizing, forming a fibrous preform from the fibers, forming a silicon dioxide coating around the fibers, carbonizing the fibrous preform, and densifying the fibrous preform. In various embodiments, forming the fibers with the silicon-based sizing includes utilizing a mass of the silicon-based sizing that is at least 1.0% of a mass of the fibers.Type: GrantFiled: November 15, 2016Date of Patent: September 3, 2019Assignee: GOODRICH CORPORATIONInventors: Steven Poteet, John Linck, Weiming Lu
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Patent number: 10403900Abstract: A method for producing porous graphite capable of realizing higher durability, output and capacity, and porous graphite. A carbon member having microvoids is obtained by a dealloying step for selectively eluting other non-carbon main components into a metal bath by immersing a carbon-containing material, composed of a compound including carbon or an alloy or non-equilibrium alloy, in the metal bath, wherein the metal bath has a solidifying point lower than the melting point of the carbon-containing material, and is controlled to a temperature lower than the minimum value of a liquidus temperature within a composition fluctuation range extending from the carbon-containing material to carbon by reducing the other non-carbon main components. The carbon member obtained in the dealloying step is graphitized by heating in a graphitization step. The carbon member graphitized in the graphitization step is subjected to activation treatment by an activation step.Type: GrantFiled: September 4, 2015Date of Patent: September 3, 2019Assignees: TOHOKU TECHNO ARCH CO., LTD., TPR INDUSTRY CO., LTDInventors: Hidemi Kato, Seung-Geun Yu, Takeshi Wada
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Patent number: 10331033Abstract: A hardmask composition includes a first material including one of an aromatic ring-containing monomer and a polymer containing a repeating unit including an aromatic ring-containing monomer, a second material including at least one of a hexagonal boron nitride and a precursor thereof, a chalcogenide-based material and a precursor thereof, and a two-dimensional carbon nanostructure and a precursor thereof, the two-dimensional carbon nanostructure containing about 0.01 atom % to about 40 atom % of oxygen, and a solvent.Type: GrantFiled: July 6, 2015Date of Patent: June 25, 2019Assignee: Samsung Electronics Co., Ltd.Inventors: Hyeonjin Shin, Sangwon Kim, Seongjun Park
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Patent number: 10294166Abstract: A method of densifying a CMC article includes the steps of pyrolyzing a CMC article until a desired initial porosity is achieved, coating CMC pores within the CMC article with carbon, pyrolyzing the carbon to form carbon pores, coating the carbon pores with silicon, and heat treating the CMC article to create a silicon carbide filled pore integrated with silicon carbide of the CMC article to densify the CMC article.Type: GrantFiled: September 12, 2014Date of Patent: May 21, 2019Assignee: UNITED TECHNOLOGIES CORPORATIONInventors: Michael G. McCaffrey, Douglas M. Berczik
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Patent number: 10189746Abstract: A ceramic composite can include a first ceramic phase and a second ceramic phase. The first ceramic phase can include a silicon carbide. The second phase can include a boron carbide. In an embodiment, the silicon carbide in the first ceramic phase can have a grain size in a range of 0.8 to 200 microns. The first phase, the second phase, or both can further include a carbon. In another embodiment, at least one of the first ceramic phase and the second ceramic phase can have a median minimum width of at least 5 microns.Type: GrantFiled: May 5, 2017Date of Patent: January 29, 2019Assignee: SAINT-GOBAIN CERAMICS & PLASTICS, INC.Inventors: Diana R. Tierney, Matthew Creedon, Tom J. Trunzo, Kenneth R. Delahunty
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Patent number: 10115497Abstract: This present invention disclosed a compressive graphene hydrogel and relates to a preparation method thereof. The compressive graphene hydrogel is obtained using the oxidized graphene and phytic acid as raw materials, wherein the oxidized graphene is used as the precursor. The obtained graphene hydrogel has a rich micro gap structure, a super large surface area, and high conductivity.Type: GrantFiled: January 21, 2015Date of Patent: October 30, 2018Assignee: FUZHOU UNIVERSITYInventors: Yuying Zheng, Xianbin Liu, Jinxian Lin
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Patent number: 10087519Abstract: A method of making a preform and preform formed by the method. The method includes providing a first pre-preg ply including at least a first fiber and a first resin. The method also includes providing a second pre-preg ply including at least a second fiber and a second resin over at least a portion of the first pre-preg ply. Heat or electromagnetic radiation is used to at least partially cure the first and second resins to form a cured preform. Heat is applied to pyrolyze at least a portion of the resin of the cured preform to form a pyrolyzed preform. A mechanical stimulus including at least one of controlled drying, local explosions, or ultrasonic energy is applied to the pyrolyzed preform. The mechanically treated pyrolyzed preform is subsequently densified by melt infiltration to form a densified preform.Type: GrantFiled: June 21, 2017Date of Patent: October 2, 2018Assignee: General Electric CompanyInventors: Jason Robert Parolini, John McConnell Delvaux, Srikanth Chandrudu Kottilingam, James Joseph Murray, Canan Uslu Hardwicke, Matthew Troy Hafner
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Patent number: 10024610Abstract: A method of making a light weight housing for an internal component is provided. The method including the steps of: forming a first metallic foam core into a desired configuration; forming a second metallic foam core into a desired configuration; inserting an internal component into the first metallic foam core; placing the second metallic foam core adjacent to the first metallic core in order to secure the internal component between the first metallic foam core and the second metallic foam core; applying an external metallic shell to an exterior surface of the first metallic foam core and the second metallic foam core; and securing an inlet fitting and an outlet fitting to the housing, wherein a thermal management fluid path for the internal component into and out of the housing is provided by the inlet fitting and the outlet fitting.Type: GrantFiled: April 12, 2016Date of Patent: July 17, 2018Assignee: UNITED TECHNOLOGIES CORPORATIONInventor: Gary D. Roberge
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Patent number: 10024828Abstract: An adsorbent which enables solid phase extraction of water-soluble molecules with high efficiency and excellent selectivity and an analysis system using the adsorbent, the adsorbent containing a structure represented by the formula I wherein R is a carrier component, the moiety other than R is a side-chain functional group, R and the benzene ring in the side-chain functional group are bonded directly or bonded through one or more atoms, R? is selected from the group consisting of hydroxy group, alkoxy group, amino group, alkylamino group, thiol group and alkyl sulfide group, R? is independently selected from the group consisting of hydroxy group, alkoxy group, alkyl group, amino group, alkylamino group, dialkylamino group, trialkylamino group, thiol group, alkyl sulfide group and hydrogen atom, x is an integer of zero or more and three or less, and n is the number of the side-chain functional groups contained in the carrier component.Type: GrantFiled: May 7, 2014Date of Patent: July 17, 2018Assignee: Hitachi High-Technologies CorporationInventors: Jun Nunoshige, Shinya Ito, Hiroshi Nakano
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Patent number: 10017426Abstract: A technique of forming a carbon-carbon composite that includes infiltrating a preform comprising carbon fibers or carbon-precursor fibers with a pitch and pyrolyzing the pitch using a controlled pressure and temperature ramp rate to control a growth of optical textures as the pitch is pyrolyzed to a coke matrix. Pyrolyzing the pitch may include initiating pyrolysis of at least some of the pitch at a first pressure less than about 2000 psi and a first temperature ramp rate between about 5° C./hr and about 50° C./hr to a first target temperature, and pyrolyzing at least some of the pitch at a second pressure greater than 2000 psi and a second temperature ramp rate between about 5° C./hr and about 50° C./hr to a second target temperature, where the second target temperature is greater than the first target temperature.Type: GrantFiled: April 1, 2016Date of Patent: July 10, 2018Assignee: Honeywell International Inc.Inventors: Slawomir T. Fryska, Neil Murdie, Mark L. La Forest
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Patent number: 9997764Abstract: The present invention provides a novel non-exfoliated graphite powder containing highly oriented grain aggregates (HOGA) having a new morphology and surface chemistry, methods for the production of such graphite powders as well as products containing such novel graphite particles.Type: GrantFiled: May 17, 2017Date of Patent: June 12, 2018Assignee: Imerys Graphite & Carbon Switzerland SAInventors: Michael E. Spahr, Curzio Nessi, Salvatore Stallone, Eberhard Waldhor, Grivei Eusebiu, Nicolas Probst
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Patent number: 9989853Abstract: A hardmask composition includes a first material including one of an aromatic ring-containing monomer and a polymer containing a repeating unit including an aromatic ring-containing monomer, a second material including at least one of a hexagonal boron nitride and a precursor thereof, a chalcogenide-based material and a precursor thereof, and a two-dimensional carbon nanostructure and a precursor thereof, the two-dimensional carbon nanostructure containing about 0.01 atom % to about 40 atom % of oxygen, and a solvent.Type: GrantFiled: July 6, 2015Date of Patent: June 5, 2018Assignee: Samsung Electronics Co., Ltd.Inventors: Hyeonjin Shin, Sangwon Kim, Seongjun Park
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Patent number: 9979028Abstract: A coated substrate for forming fuel cell catalyst layers includes a plurality of substrate particles, an adhesion layer disposed over the substrate particles, and a precious metal layer disposed over the adhesion layer. The substrate particles may be carbon powders, carbon nanorods, carbon nanotubes and combinations thereof; with a preferred aspect ratio from 10:1 to 25:1. The adhesion layer includes a tungsten metal layer and may be formed into a heterogeneous layer comprising a lattice-interrupting layer interposed between two tungsten metal layers. The lattice-interrupting layer reduces mechanical stress to the adhesion layer with extended thickness that may develop when it experiences changing environments, and can be any layer other than the metal layer, for example, Al2O3, Al, or WOx, where x is 1.5 to 3.0. Characteristically, the coated substrate is used in fuel cell applications such as providing the catalyst particles used in the cathode and/or anode catalyst layers.Type: GrantFiled: October 29, 2014Date of Patent: May 22, 2018Assignee: GM GLOBAL TECHNOLOGY OPERATIONS LLCInventors: Anusorn Kongkanand, Ratandeep S. Kukreja, Joel W. Clancey, Andrew Cavanaugh, Steven M. George
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Patent number: 9975775Abstract: The invention is directed to high surface area graphitized carbon and to processes for making high surface area graphitized carbon. The process includes steps of graphitizing and increasing the surface area of (in either order) a starting carbon material to form high surface area graphitized carbon. The step of increasing the surface area optionally comprises an oxidizing step (e.g., through steam etching) or template removal from composite particles. The invention is also directed to catalyst particles and electrodes employing catalyst particles that are formed from the high surface area graphitized carbon.Type: GrantFiled: April 3, 2015Date of Patent: May 22, 2018Assignee: Cabot CorporationInventors: Yipeng Sun, Jian-Ping Shen, Gordon Rice, Paolina Atanassova, Geoffrey D. Moeser
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Patent number: 9938152Abstract: An activated nano-porous carbon is produced using a liquid organic compound as a starting material. A combination of the liquid organic compound with organic acids is mixed with conductive carbon powder and polymerized. The polymerized material is then carbonized and activated using physical or chemical methods. The activated nano-porous carbon obtained using this method has been used to fabricate EDLC devices. The carbon has also shown large surface area (up to ˜2000 m2/gm, depending on the degree of activation) and can be used for various other activated carbon applications.Type: GrantFiled: August 19, 2016Date of Patent: April 10, 2018Assignee: Farad Power, Inc.Inventor: Shantanu Mitra
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Patent number: 9932696Abstract: A circular needle loom comprises a bed plate for receiving a transport layer. Engagement members may be disposed proximate to the bed plate, such that the engagement members interface with a positional structure of the transport layer that is used to position and rotate the transport layer around the bed plate. The engagement members may be configured to rotate the transport layer around the bed plate until a predetermined number of fibers and/or layers are deposited on the transport layer and/or bed plate in order to create a needled preform.Type: GrantFiled: June 23, 2017Date of Patent: April 3, 2018Assignee: GOODRICH CORPORATIONInventor: Jean-Francois Le Costaouec
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Patent number: 9725322Abstract: Hot pressing hollow carbon nanoparticles results in a nano-carbon foam that can be used for energy storage, carbon dioxide capture or water desalination.Type: GrantFiled: July 2, 2015Date of Patent: August 8, 2017Assignee: National University of SingaporeInventors: Arunabha Ghosh, Jonghak Lee, Srinivasan Natarajan, Barbaros Oezyilmaz, Antonio Helio Castro Neto
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Patent number: 9719199Abstract: A circular needle loom comprises a bed plate for receiving a transport layer. Engagement members may be disposed proximate to the bed plate, such that the engagement members interface with a positional structure of the transport layer that is used to position and rotate the transport layer around the bed plate. The engagement members may be configured to rotate the transport layer around the bed plate until a predetermined number of fibers and/or layers are deposited on the transport layer and/or bed plate in order to create a needled preform.Type: GrantFiled: May 23, 2014Date of Patent: August 1, 2017Assignee: Goodrich CorporationInventor: Jean-Francois Le Costaouec
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Patent number: 9676013Abstract: A sub-aqueous capping material comprising a plurality of compacted particles of a reactive solid material having a dispersion aid homogeneously blended therein, the compacted particles having a specific gravity greater than 1.0, a particle size in the range of about 1/16 inch to about 1 inch, and having a time for disintegration, once in contact with water, of 5 hours or less.Type: GrantFiled: March 21, 2014Date of Patent: June 13, 2017Assignee: AMCOL INTERNATIONAL CORPORATIONInventors: Robert J. Trauger, Zhen Wang, James T. Olsta
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Patent number: 9666854Abstract: A graphite powder may include highly oriented grain aggregates, wherein the electrical resistivity of the powder decreases with increasing density. A process for coating a substrate may include providing a coating dispersion including such a graphite powder and applying the coating dispersion to the substrate. An electrode may contain such a graphite powder. A coating dispersion may include such a graphite powder dispersed in a liquid medium. A battery may include such a graphite powder. A compressed body of pure graphite may include such a graphite powder. A lubricant may include such as graphite powder.Type: GrantFiled: October 30, 2015Date of Patent: May 30, 2017Assignee: Imerys Graphite & Carbon Switzerland SAInventors: Michael E. Spahr, Curzio Nessi, Salvatore Stallone, Eberhard Waldhor, Grivei Eusebiu, Nicolas Probst
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Patent number: 9656412Abstract: The present invention provides a method for producing a fiber composite component, the method comprising arranging a first and a second mold in relation to one another in such a way that these together form a first cavity; laying a fiber material on the first and/or second mold; filling the first cavity with a casting material and solidifying the casting material in order to seal the first and second molds to one another and/or to interconnect them; and infiltrating the fiber material with a matrix and curing the matrix to form the fiber composite component.Type: GrantFiled: September 17, 2013Date of Patent: May 23, 2017Assignee: Airbus Operations GmbHInventors: Hauke Seegel, Paulin Fideu, Axel Herrmann
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Patent number: 9624138Abstract: A method of creating a component comprises forming a substrate and depositing a template material within the substrate, such that there are a plurality of template member. The component is heated to a temperature above a melting point of the template material, such that the template material wicks into a porosity of the substrate and forms a component with voids. An average hydraulic diameter of the voids is less than 1 millimeter. A component formed by the method, and the component itself are also disclosed.Type: GrantFiled: March 5, 2015Date of Patent: April 18, 2017Assignee: UNITED TECHNOLOGIES CORPORATIONInventors: Paul Sheedy, Wayde R. Schmidt
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Patent number: 9574125Abstract: Disclosed are a composite graphite heat insulating material with improved thermal conductivity in the thickness direction and a method for manufacturing the same. The composite graphite heat insulating material according to the present invention comprises: an expanded graphite matrix which is compressed in the thickness direction; and high-density compressed and expanded graphite particles which are filled in the pores within the compressed and expanded graphite matrix and have a density of 0.1 g/cm3 or more.Type: GrantFiled: May 29, 2014Date of Patent: February 21, 2017Assignee: GTS CO., LTD.Inventors: Su-Han Lee, Duk-Joon Jung
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Patent number: 9567452Abstract: There is provided a carbon nanofiber aggregate capable of suppressing scatter and having excellent dispersibility and filling property in a thermoplastic resin. A carbon nanofiber aggregate has a maximum void volume P1 (cm3/g) at a pore diameter of 2,500 nm or more and 100,000 nm or less and a maximum void volume P2 (cm3/g) at a pore diameter of 6 nm or more and less than 2,500 nm in pore distribution data measured by mercury porosimetry. The maximum void volume P1 and the maximum void volume P2 satisfy a specific relationship.Type: GrantFiled: October 12, 2012Date of Patent: February 14, 2017Assignee: ASAHI KASEI KABUSHIKI KAISHAInventors: Kazuya Nagata, Yoshiyuki Kashiwagi
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Patent number: 9523163Abstract: Provided is a method for producing a carbon material, the method utilizing a cellulosic material and enables the carbon material, which retains the shape of the cellulosic material, to be produced in high yield. The method for producing a carbon material is characterized by comprising the steps of: allowing a cellulosic material and/or a regenerated cellulosic material to adsorb a sulfonic acid; and heating the cellulosic material and/or the regenerated cellulosic material which has adsorbed the sulfonic acid at a temperature of 600-2800° C. in an inert gas atmosphere.Type: GrantFiled: June 5, 2013Date of Patent: December 20, 2016Assignee: NIPPON PAPER INDUSTRIES CO., LTD.Inventors: Mutsumasa Kyotani, Kazuo Akagi, Shinichi Kimura
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Patent number: 9481073Abstract: Methods of forming polycrystalline diamond include encapsulating diamond particles and a hydrocarbon substance in a canister, and subjecting the encapsulated diamond particles and hydrocarbon substance to a pressure and a temperature sufficient to form inter-granular bonds between the diamond particles. Cutting elements for use in an earth-boring tool includes a polycrystalline diamond material formed by such processes. Earth-boring tools include such cutting elements.Type: GrantFiled: November 2, 2015Date of Patent: November 1, 2016Assignee: Baker Hughes IncorporatedInventor: Anthony A. DiGiovanni
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Patent number: 9428388Abstract: A process for preparing a carbon-carbon composite including the steps of: (a) providing a curable low viscosity aromatic epoxy resin liquid formulation, wherein the formulation has a neat viscosity of less than 10,000 mPa-s at 25° C. prior to adding optional components, prior to curing, and prior to carbonizing; and wherein the formulation being cured has a carbon yield of at least 35 wt % disregarding the weight of the carbon matrix and any optional components present in the composition; (b) contacting a carbon matrix with the formulation of step (a); (c) curing the contacted carbon matrix of step (b); and (d) carbonizing the cured carbon matrix of step (c) to form a carbon-carbon composite; and a carbon-carbon composite made by the process.Type: GrantFiled: May 17, 2013Date of Patent: August 30, 2016Assignee: BLUE CUBE IP LLCInventors: Hamed Lakrout, Maurice J. Marks, Ludovic Valette
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Patent number: 9397350Abstract: Disclosed is a carbon fiber web including polymer nanofibers. Specifically, the carbon fiber web includes: a dispersed structure of carbon fibers; and polymer nanofibers distributed among and bonding the constituent carbon fibers of the dispersed structure. The carbon fiber web exhibits excellent characteristics in terms of flexural strength, gas permeability and electrical properties while possessing a tensile strength sufficient to undergo continuous processes for mass production. Also disclosed are a gas diffusion medium using the carbon fiber web, a gas diffusion layer including the gas diffusion medium, a membrane electrode assembly including the gas diffusion layer, and a fuel cell including the membrane electrode assembly. The use of the carbon fiber web ensures high performance of the membrane electrode assembly and the fuel cell.Type: GrantFiled: June 19, 2013Date of Patent: July 19, 2016Assignee: Korea Institute of Energy ResearchInventors: Yoonjong Yoo, Hyunuk Kim, Kwangsub Song, Hongsoo Kim, Young Ju Lee, Sungjin Lee
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Patent number: 9318295Abstract: A CNT electron source, a method of manufacturing a CNT electron source, and a solar cell utilizing a CNT patterned sculptured substrate are disclosed. Embodiments utilize a metal substrate which enables CNTs to be grown directly from the substrate. An inhibitor may be applied to the metal substrate to inhibit growth of CNTs from the metal substrate. The inhibitor may be precisely applied to the metal substrate in any pattern, thereby enabling the positioning of the CNT groupings to be more precisely controlled. The surface roughness of the metal substrate may be varied to control the density of the CNTs within each CNT grouping. Further, an absorber layer and an acceptor layer may be applied to the CNT electron source to form a solar cell, where a voltage potential may be generated between the acceptor layer and the metal substrate in response to sunlight exposure.Type: GrantFiled: January 13, 2009Date of Patent: April 19, 2016Assignee: THE UNITED STATES OF AMERICA AS REPRESENTED BY THE ADMINISTRATOR OF THE NASAInventor: Cattien V. Nguyen
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Patent number: 9221686Abstract: There are provided a cluster of thin sheet graphite crystals or the like which is useful as an electrode material for lithium ion batteries, hybrid capacitors and the like, and a method for efficiently producing the same at high productivity. The method is one for producing a cluster of thin sheet graphite crystals composed of aggregates in such a state that thin sheet graphite crystals extend from the inside toward the outside, comprising charging a powdery and/or particulate material of an organic compound pre-baked to an extent of containing remaining hydrogen in a graphite vessel, and subjecting the powdery and/or particulate material together with the vessel to hot isostatic pressing treatment (HIP treatment) using a compressed gas atmosphere under the predetermined conditions.Type: GrantFiled: February 18, 2011Date of Patent: December 29, 2015Assignee: INCUBATION ALLIANCE, INC.Inventors: Kazuo Muramatsu, Masahiro Toyoda
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Patent number: 9211504Abstract: Carbon molecular sieves (CMS) membranes having improved thermal and/or mechanical properties are disclosed herein. In one embodiment, a carbon molecular sieve membrane for separating a first and one or more second gases from a feed mixture of the first gas and one or more second gases comprises a hollow filamentary carbon core and a thermally stabilized polymer precursor disposed on at least an outer portion of the core. In some embodiments, the thermally stabilized polymer precursor is created by the process of placing in a reaction vessel the carbon molecular sieve membrane comprising an unmodified aromatic imide polymer, filling the reaction vessel with a modifying agent, and changing the temperature of the reaction vessel at a temperature ramp up rate and ramp down rate for a period of time so that the modifying agent alters the unmodified aromatic imide polymer to form a thermally stabilized polymer precursor.Type: GrantFiled: November 1, 2012Date of Patent: December 15, 2015Assignees: GEORGIA TECH RESEARCH CORPORATION, SHELL OIL COMPANYInventors: Nitesh Bhuwania, William John Koros, Paul Jason Williams
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Patent number: 9194062Abstract: A changing method includes the steps of supplying a carbon fiber material with a surface covered by a thermosetting resin oil, performing a desizing step to remove the thermosetting resin oil from the surface of the carbon fiber material, performing a surfactant coating step to coat a surfactant onto the surface of the carbon fiber material, and performing a sizing step to cover a surface of the surfactant by a thermosetting resin oil, so as to obtain a carbon fiber material with a thermosetting resin oil coated onto the surface of the carbon fiber material.Type: GrantFiled: August 9, 2013Date of Patent: November 24, 2015Assignee: UHT UNITECH CO., LTD.Inventor: Chih-Yung Wang
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Patent number: 9187331Abstract: Disclosed herein is a method for producing an elongated (rolled) carbonaceous film by polymer pyrolysis while suppressing the fusion bonding of the carbonaceous film. The method for producing a carbonaceous film includes the step of heat-treating a polymer film wound into a roll, wherein the heat treatment is performed after the polymer film is wound into a roll to have a gap between adjacent layers of the polymer film at a temperature lower than a pyrolysis onset temperature of the polymer film so that the roll of polymer film as a whole satisfies a relationship that a value obtained by dividing a thickness of a gap between adjacent layers of the polymer film (Ts) by a thickness of the polymer film (Tf) (Ts/Tf) is 0.16 or higher but 1.50 or lower.Type: GrantFiled: March 26, 2012Date of Patent: November 17, 2015Assignee: KANEKA CORPORATIONInventors: Makoto Mishiro, Yusuke Ohta, Takashi Inada, Yasushi Nishikawa
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Patent number: 9045374Abstract: A composition having nanoparticles of silicon carbide and a carbonaceous matrix or silicon matrix. The composition is not in the form of a powder. A composition having silicon and an organic compound having a char yield of at least 60% by weight or a thermoset made from the organic compound. A method of combining silicon and the organic compound and heating to form silicon carbide or silicon nitride nanoparticles.Type: GrantFiled: May 19, 2014Date of Patent: June 2, 2015Assignee: The United States of America, as represented by the Secretary of the NavyInventors: Teddy M. Keller, Andrew Saab, Matthew Laskoski