Abstract: A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.

Abstract: The invention relates to producing articles from granulated foaming polymers and from compositions based thereon, in particular, to a device for forming articles with a limited temperature produced by a heat energy released by water exposed to the action of microwave radiation, which is subsequently used for drying said articles. The inventive method for forming articles from foaming polymers and compositions based thereon consists in forming articles using a heat energy released by water exposed to the action of microwave radiation at a temperature equal to or less than 170° C., wherein said temperature is attained, controlled and limited by adjusting a vapour pressure in a forming chamber.

Abstract: A method for synthesis of high quality colloidal nanoparticles using comprises a high heating rate process. Irradiation of single mode, high power, microwave is a particularly well suited technique to realize high quality semiconductor nanoparticles. The use of microwave radiation effectively automates the synthesis, and more importantly, permits the use of a continuous flow microwave reactor for commercial preparation of the high quality colloidal nanoparticles.

Abstract: A textured, layered mold-formed body is produced with a foil laminate in which a top foil of at most partially crosslinked polymer materials and a sub-foil containing a polymer foam material with a density between 35 and 120 grams per liter and a gel content of less than 80 percent are laminated together. The foil laminate is embossed with a texture and treated with electron beams to give the texture enough stability for a subsequent deep-drawing step in which the mold-formed body is produced.

Abstract: A process for producing a cellulose acylate film comprising: casting a solution of a cellulose acylate having an acyl substitution degree of from 2.85 to 3.00 dissolved in at least one organic solvent onto an endless metal support; cooling the solution at 0° C. to ?50° C. to effect gelation, so as to form a film; peeling the film off from the endless metal support; and drying the film.

Abstract: A drying jig of the present invention is a drying jig for a pillar-shaped honeycomb molded body having a large number of cells longitudinally placed in parallel with one another with a cell wall therebetween, comprising: a fixing member for preventing separation or opening of the drying jig; and a piling member which enables the drying jig to be piled up in multi stage at the time of drying.

Abstract: Systems and methods of nanomaterial transfer are described. A method of nanomaterial transfer involving fabricating a template and synthesizing nanomaterials on the template. Subsequently, the nanomaterials are transferred to a substrate by pressing the template onto the substrate. In some embodiments, the step of transferring the nanomaterials involves pressing the template onto the substrate such that the nanomaterials are embedded below a surface layer of the substrate. In some embodiments, the temperature of the plurality of nanomaterials is raised to assist the transfer of the nanomaterials to the substrate.

Abstract: The present invention is directed toward methods of crosslinking carbon nanotubes to each other using microwave radiation, articles of manufacture produced by such methods, compositions produced by such methods, and applications for such compositions and articles of manufacture. The present invention is also directed toward methods of radiatively modifying composites and/or blends comprising carbon nanotubes with microwaves, and to the compositions produced by such methods. In some embodiments, the modification comprises a crosslinking process, wherein the carbon nanotubes serve as a conduit for thermally and photolytically crosslinking the host matrix with microwave radiation.

Abstract: The present disclosure provides for methods of using compositions having improved microwave absorbing properties to cut textile webs. Specifically, the compositions utilized in the methods of the present disclosure absorb the microwave energy as heat, thereby cutting through the textile web.

Abstract: The invention relates to a method of manufacturing implant parts made of highly cross-linked polyethylene, wherein a blank made of ultra-high-molecular-weight polyethylene is irradiated with ionizing radiation in order to produce radicals in the blank. To optimize the cross-linkage of the highly cross-linked polyethylene and to eliminate free radicals, the blank is subsequently treated by means of microwave radiation and/or ultrasound in such a way that free radicals, which have not recombined, are excited so as to ensure substantially complete recombination of the free radicals. The shape of the treated blank can then be adjusted by means of machining. The invention further relates to implant parts for application in human medicine that have been manufactured as described above.

Abstract: A method for drying a ceramic article comprises providing microwave radiation from a microwave generating source, providing a ceramic honeycomb structure having a middle portion and at least one end, and exposing the ceramic honeycomb structure to the microwave radiation while shielding the at least one end from directly receiving the microwave radiation, such that the radiation absorbed by the middle portion is equal to or greater than the radiation absorbed by the at least one end, and the proper drying of the entire honeycomb structure without heat-induced structural degradation is thus ensured.

Abstract: The invention provides a honeycomb formed structure drying method including causing undried honeycomb formed structures 10 placed on stands 12 to pass through a drying apparatus 1, thereby drying the undried honeycomb formed structures through high-frequency heating, to thereby form dried honeycomb formed structures 11; removing the dried honeycomb formed structures 11 from the stands 12; cooling the stands 12 which have been heated dried in the drying apparatus 1 are cooled to a temperature lower than the gelation temperature of the undried honeycomb formed structures 10; placing newly formed undried honeycomb formed structures 10 on the cooled stands 12; drying the undried honeycomb formed structures by passing through the drying apparatus 1; and repeating these operations. The honeycomb formed structure drying method prevents deformation such as warpage of partition walls of honeycomb formed structures during drying thereof.

Abstract: Process for heating a substrate, which contains, relative to the total weight of the substrate, 0.1 to 70 wt. % of metallic, magnetic, ferrimagnetic, ferromagnetic, antiferromagnetic or superparamagnetic particles having an average particle size of between 1 and 5000 nm, wherein the substrate is exposed to electromagnetic radiation, characterized in that the electromagnetic radiation comprises microwave radiation with a frequency in the range from 1 to 300 GHz and the substrate is simultaneously exposed to a direct-current magnetic field, the field strength of which is at least twice the strength of the earth's magnetic field; use of the process for producing or detaching adhesive bonds; device for the simultaneous production of microwave radiation with a frequency within the range from 1 to 300 GHz and a direct-current magnetic field, the field strength of which is at least twice the strength of the earth's magnetic field.

Abstract: A method is disclosed for pre-conditioning inserts for improved replication during injection molding. The pre-conditioned inserts provide improved bonding with the injection-material and improved replication of complex molding surfaces. The pre-conditioning of the inserts comprises placing the insert in position against the molding surface, followed by heat-soaking the insert. Heat-soaking can be accomplished using infrared energy, preferably broadband infrared energy or energy that is preferentially absorbed by the insert.

Abstract: An apparatus and method for molding balloon catheters is disclosed. The balloon may be molded by providing a polymeric tube within a mold having an interior cavity in the shape of the desired balloon. Microwave energy, which may be generated by a gyrotron, may then be directed toward the mold, to heat the polymeric material without heating the mold. Once heated, pressurized fluid may be injected into the tube to blow the polymeric material against the interior cavity whereupon the material can cool to form the balloon or can be further heatset by additional microwave energy and be cooled to form the balloon. In accordance with one embodiment, microwave energy can also be used without a mold to form a medical device. A polymer extrusion apparatus is disclosed utilizing a microwave energy for heating polymer feedstock material within the extruder tip and die unit just prior to formation of the extrudate product.

Abstract: Injection molding machine utilizes microwave heating. A microwave oven adapted to receive a microwave absorbent plasticizing vessel is utilized with or incorporated into an injection molding system to form a plasticizing unit for heating polymer granules to an injection temperature and injection of the melt into the cavity of the injection mold. The polymer granules may be preheated by conventional heating systems to a temperature at which the granules become microwave absorbent before heating to the injection temperature in the microwave oven. The injection molding machine also contains a hydraulic actuator for injection of the melt. The ceramic materials forming the plasticizing vessel are selected to provide equal heating rates of mold members and relatively uniform heating of polymer to desired injection temperature.

Abstract: The present invention is a microwave preheat press. The microwave preheat press includes a first and a second press section which define a press passage therebetween. A compression belt movable along the press passage is contiguous with one of the press sections. The press passage is configured such that it has an initial press section leading into a final press section. A microwave generator is in communication with a microwave waveguide applicator structure assembly such that microwave energy is created and transmitted through the microwave waveguide assembly into the initial compression section.

Abstract: The present invention is a microwave preheat press. The microwave preheat press includes a first and a second press section which define a press passage therebetween. A compression belt movable along the press passage is contiguous with one of the press sections. The press passage is configured such that it has an initial press section leading into a final press section. A microwave generator is in communication with a microwave waveguide applicator structure assembly such that microwave energy is created and transmitted through the microwave waveguide assembly into the initial compression section.

Abstract: The invention provides porous silicon nitride ceramics that having uniform, fine closed pores and a manufacturing method thereof. Metal Si powder is mixed with a sintering additive, followed by thermal treatment, which is a pre-process for forming a specific grain boundary phase. Two-stage thermal treatment is thereafter performed by microwave heating at a temperature of 1000° C. or more. The metal Si powder is thereafter subjected to a nitriding reaction from its surface, the metal Si is thereafter diffused to nitride formed on the outer shell thereof such that porous silicon nitride ceramics having uniform, fine closed pores can be produced. Having a high ratio of closed pores and being superior in electrical/mechanical characteristics, the porous silicon nitride ceramics can display excellent characteristics if used, for example, for an electronic circuit board that requires an anti-hygroscopicity, a low dielectric constant, a low dielectric loss, and mechanical strength.

Abstract: The present invention is a method of forming a compressed product. The method includes introducing a material into a press that is oscillating between a compression phase and a release phase. The material has a compression recovery response time when compressed and released. The compressed product is formed by repeatedly compressing the material during the compression phase and releasing the material during the release phase.

Abstract: A high-CHDM PET-based support for an imaging element can be annealed relatively rapidly to achieve acceptable core-set and post-process curl properties. The fast annealing response of this material allows effective in-line annealing of the film support, yielding a more efficient manufacturing process with less annealing-induced defects in the imaging support.

Abstract: The present invention provides a protective strap and the method of manufacturing the same. The method includes the steps of providing an elongated strap-like base layer; printing a predetermined drawing on a surface of the base layer, wherein the drawing is formed of a plurality of color bits having a color different from that of the base layer; heating and pressurizing the color bits of the base layer at the same time to enable the base layer to form a plurality of concavities on its surface, wherein each of the color bits is positioned in one of the concavities.

Abstract: A process for producing a honeycomb structure, which comprises adding water to a mixed raw material of a raw material powder and a binder, kneading the mixture to obtain a plastic mixture, molding the plastic mixture into a honeycomb shape to obtain a green honeycomb structure, drying the structure by a step including hot-air drying, and firing the resulting dried honeycomb structure, wherein the binder contains hydroxypropyl methyl cellulose as a major component. The process can produce a crack-free high-quality honeycomb structure rapidly at a low cost.

Abstract: The present invention is a modeling technique wherein a three-dimensional model and its support structure are built by fused deposition modeling, using a thermoplastic blended material containing a polyphenylsulfone (PPSF) polymer and a polycarbonate (PC) polymer to form the model. The PPSF/PC blend exhibits good chemical resistance, thermal stability, and resists build-up in the nozzle of a three-dimensional modeling apparatus. Removal of the support structure from a completed model is facilitated by operating on the material while it is hot.

Abstract: A method is disclosed for pre-conditioning inserts for improved replication during injection molding. The pre-conditioned inserts provide improved bonding with the injection-material and improved replication of complex molding surfaces. The pre-conditioning of the inserts comprises placing the insert in position against the molding surface, followed by heat-soaking the insert. Heat-soaking can be accomplished using infrared energy, preferably broadband infrared energy or energy that is preferentially absorbed by the insert.

Abstract: The present invention relates to a process for melting and adhering material to produce three-dimensional objects by means of selective heating via microwave radiation. Unlike selective laser sintering, the present process uses simple microwave radiation commonly available in any household. The selectivity of heating is achieved by applying one or more susceptors to selected regions of a layer composed of a pulverulent substrate, and then heating the susceptor by means of microwave radiation. The heated susceptor transfers the energy present therein to a pulverulent substrate surrounding the susceptor, and the substrate is thereby melted, providing firm adhesion within the substrate after cooling.

Abstract: A process for the continuous coagulation and drying of rubber latex includes feeding the latex onto an endless conveyor belt which feeds the latex through a coagulator. A combination of microwave energy and hot air raises the temperature of the latex causing it to coagulate in a coagulation time of less than five minutes. The coagulated rubber from the coagulator is fed into a conveyor belt of a stretch unit which stretches the rubber by increasing its speed of travel. The stretched rubber is then conveyed onto the upper belt of a drying unit. The drying rubber is passed from the upper belt onto an intermediate belt and then on to a lower belt before leaving the drying unit. A combination of microwave energy and hot air in the drying unit is used to dry the rubber to a moisture content of less than 1.5%.

Abstract: A moldable article that can be custom-fitted to a particular user. Such an article comprises a thermoplastic material such as ethylene vinyl acetate modified by an antistatic agent selected from the group consisting of polyol amines such as ethoxylated amines, ethoxylated fatty alcohols, phosphoric acid esters, quaternary ammonium salts, and amphoteric compounds such as betaine. The article is heated until the thermoplastic material softens, then pressed against a user's body part. The article is allowed to cool, resulting in a custom-fitted article. Such articles may be repeatedly re-heated and re-molded and may include, e.g., moldable footbeds, racquet handles, shin guards, helmets, and seats.

Abstract: A freeform fabrication method for fabricating a 3-D multi-material or multi-color object from successive layers of a primary body-building powder, at least a modifier material and a binder powder in accordance with a computer-aided design of the object.

Abstract: A method of manufacturing PTFE material includes preparing a mixture of PTFE resin powder and a susceptor material which is compacted and sintered by exciting the susceptor material with microwave energy. Preferably, the compaction and sintering of the mixture is carried out in a continuous process and a vacuum is drawn on the mixture in the heating zone to extract any air from the mixture. The sintered mixture may be advanced, preferably continuously, to a cutting zone where the PTFE material may be cut to any desired length preferably while the mixture is still warm to produce anywhere from thin wafer PTFE components to long tubular PTFE hose, or the like.

Abstract: An apparatus and a method, for drying ceramic molded articles, are disclosed. A drying apparatus (1) comprises a drying chamber (10) for accommodating ceramic molded articles (8), a plurality of microwave generators (20) for supplying microwave energy into the drying chamber, and a conveyor (30) for charging the ceramic molded articles (8) continuously into the drying chamber (10), conveying the ceramic molded articles through the drying chamber, and delivering the ceramic molded articles from the drying chamber. The drying chamber (10) has arranged therein a plurality of the microwave generators (20) and at least a sensor (40) for detecting the distribution of the ceramic molded articles (8) in the drying chamber (10). Each microwave generator (20) is adapted to change the output thereof in accordance with the distribution of the ceramic molded articles (8) detected by the sensor (40).

Abstract: The invention describes a model material for dental purposes which has a linear expansion on setting or curing of at least 0.5%, preferably at least 1%. The model material is preferably a dental plaster which has a relatively high volume expansion on setting compared to dental plasters customary hitherto as a result of the use of appropriate additives and/or make-up liquids. The use of these model materials for producing working models enables the sintering shrinkage occurring during sintering to be compensated for in the production of full-ceramic shaped dental parts.

Abstract: A method for producing a composite product including a substrate material and a binder, wherein either the binder includes a plastics material in an emulsion form, or a plastics material is added to an emulsion including the substrate material. The invention is also directed to composite products including a particulate substrate and particles of a plastics material therein.

Abstract: Methods for temperature control in microwave processing of materials, for example microwave sintering, annealing and other forms of microwave heating, are disclosed in which the material is formed into a selected shape and size such that at least a part of the materials reaches a state of thermal equilibrium at a desired temperature.

Abstract: A method of shaping a heat shrinkable material comprising the steps of providing a blank comprising a heat shrinkable material; applying a substance heatable by microwave radiation to a portion of the blank; and applying microwave radiation to the substance so that the substance is heated. Thus the portion of the blank is heated and the blank is shaped.

Abstract: A bed of particulate solids including some hydrated materials can be converted by controlled irradiation with subinfrared electromagnetic radiation into a unitary porous solid that is mechanically strong enough for easy handling. When the particulate solids include typical mildly acid to alkaline cleaner materials, a block or tablet especially suitable for automatic cleaning machinery, with a very fast dissolution rate in water, can readily be obtained.

Abstract: A PTFE seal and method of fabrication therefor includes preparing a mixture of PTFE resin powder and a susceptor material which is then compacted and sintered by exciting the susceptor material with microwave energy. Preferably, the compaction and sintering of the mixture is carried out in a continuous process and a vacuum is drawn on the mixture in the heating zone to extract any air from the mixture. The sintered mixture is advanced, preferably continuously, to a cutting zone where PTFE wafers are cut from the sintered mixture, preferably while the mixture is still warm.

Abstract: The present invention relates to an improved method of manufacture of molded polymeric devices using variable frequency microwaves. Molded polymeric devices include, for example, contact lenses, corneal rings, intraocular lenses and drug delivery devices such as anterior or posterior chamber inserts. Contact lenses include soft and rigid gas permeable contact lenses as well as, lens blanks lathed into finished contact lenses. Molded polymeric devices further include medical devices such as prosthetics including hip joints. According to the present invention, a mold having a cavity the shape of the desired molded polymeric device, the cavity containing a composition comprising one or several monomers having double polymerizable bonds, is placed in a microwave chamber. The mold can be plastic, glass, ceramic or metal. Plastic is preferred. The mold is then swept with at least one range of microwave frequencies to polymerize the composition, thus forming the molded polymeric device.

Abstract: An apparatus and method for molding balloon catheters is disclosed. The balloon may be molded by providing a polymeric tube within a mold having an interior cavity in the shape of the desired balloon. Microwave energy, which may be generated by a gyrotron, may then be directed toward the mold, to heat the polymeric material without heating the mold. Once heated, pressurized fluid may be injected into the tube to blow the polymeric material against the interior cavity whereupon the material can cool to form the balloon or can be further heatset by additional microwave energy and be cooled to form the balloon. In accordance with one embodiment, microwave energy can also be used without a mold to form a medical device. A polymer extrusion apparatus is disclosed utilizing a microwave energy for heating polymer feedstock material within the extruder tip and die unit just prior to formation of the extrudate product.

Abstract: A method for forming an article in which thermoplastics materials are used as the binding agent. Materials (21) are shredded in a shredder (1), compressed in a compressing chamber (15) and moulded in a moulding chamber (16, 17, 19, 20, 26, 27). The thermoplastics material is heated whilst the material is held under compression and then cooled to bind the material together. In one embodiment superheated steam is supplied via tubes (31) having apertures there along. In another embodiment superheated steam is supplied via apertures in side walls of the mould (58, 59). Blocks (62, 72) formed by the method and apparatus of the invention may find application as construction materials etc. and have good structural, thermal and acoustic properties.

Abstract: A method and an apparatus for manufacturing a ceramic honeycomb molding having many cells formed by arranging cell walls in a honeycomb pattern. Deformation, wrinkles, cracks, etc., of the cell walls and the like are prevented from occurring. The method for manufacturing the ceramic honeycomb molding having many cells formed by arranging cells walls in a honeycomb pattern comprises an extruding process in which clayey honeycomb moldings 1 are extruded, a drying process in which the honeycomb moldings 1 are dried, and a storage process, between the extruding process and the drying process, in which the honeycomb moldings 1 are maintained in a high humidity atmosphere.

Abstract: A method of manufacturing a photochromic molded article which comprises the steps of: filling a mold with a photopolymerizable monomer composition containing a photopolymerizable monomer, a photoinitiator and a photochromic compound capable of coloring upon UV irradiation; pre-heating the composition to a temperature which reduces or prevents coloration of the photochromic compound during the subsequent photopolymerization step; and photopolymerizing the composition under irradiation with a light comprising a UV portion and a UV-visible portion.

Abstract: A method is provided for rapidly forming a cementitious panel. A cementitious mixture is introduced into a mold configured to provide the desired surface appearance and profile of the cementitious panel. The cementitious mixture is then subject to an accelerated curing process by applying microwave energy to the cementitious mixture for a predetermined time period. After a relatively short resting or cooling period, the resulting cementitious panel is ready to be removed from the mold.

Abstract: Apparatus suitable for vitrifying nuclear waste comprises a tunable microwave cavity connected by a first wave guide to a source of microwave energy; cooling coils for cooling the exterior of the cavity; a hopper for loading particulate fusible material to the interior of the cavity; within the cavity a crucible made of melted and re-solidified fusible particulate material; an exit-chamber connected by a second waveguide to a second microwave source; and a pipe for supplying argon gas to the exit chamber so that a plasma torch can be generated. The separating of the crucible form the cavity walls by unmelted material gives significant advantages in case of cleaning and reduced energy consumption.

Abstract: The present invention is a short time curing method of epoxy resin compositions composed of epoxy resins with more than 1.8 epoxy groups and curing agents which can react with epoxy groups and cure the epoxy resins at ambient temperatures or under the temperature raising conditions radiating microwave in the range of 300 MHz to 30 GHz frequency.

Abstract: A single pass, continuous, automated system for producing a pharmaceutical granulation includes multiple feeders to feed powders and liquids, a twin screw processor to granulate, a radio frequency or microwave based drying apparatus to dry the granulation, and at least one mill to process the dried granulation to desired particle sizes. The system incorporates means for monitoring key process parameters on-line, all of which are controlled by a controller provided with feedback at each component of the system. The granulation produced can be compressed into a tablet or incorporated into a capsule, both having a uniform distribution of the active ingredient. The system produces product having consistent properties even when production is scaled up for manufacture of the tablet in commercial volume.

Abstract: A method of bonding tubular members comprising the steps of, providing a first generally tubular member having a bonding portion disposed proximate a bonding end thereof, an ancillary end, and a lumen extending therethrough, the first tubular member including a support member encased in a substrate material, the support member having a plurality of filaments providing a second generally tubular member having a bonding portion disposed proximate a bonding end thereof, an ancillary end, and a lumen extending therethrough, stripping a portion of the substrate material of the first tubular member from the filaments of the support member of the first tubular member proximate the bonding portion thereof to create a plurality of exposed filaments, inserting the exposed filaments into the lumen of the second tubular member, positioning the bonding portion of the first tubular member proximate the bonding portion of the second tubular member, and heating the bonding portion of the first tubular member and the bonding

Abstract: The present invention relates to shape deformable materials, which are capable of (1) being deformed, (2) storing an amount of shape deformation, and (3) recovering at least a portion of the shape deformation when exposed to electromagnetic radiation (EMR) energy. The shape deformable materials can advantageously be in the form of films, fibers, filaments, strands, nonwovens, and pre-molded elements. The shape deformable materials of the present invention may be used to form products, which are both disposable and reusable. More specifically, the shape deformable materials of the present invention may be used to produce products such as disposable diapers, training pants, incontinence products, and feminine care products.

Abstract: Polyamides, polyesters, and polyamideesters are efficiently synthesized in a microwave process with precise temperature control. Compared to conventional thermal polymerizations, the microwave process takes less time and produces polymers with equivalent or superior physical properties.

Abstract: There is provided a process and kit for casting sand that is safe and efficient for children to use in the home. The process involves the steps of mixing sand with a non-toxic binding resin to form a resin/sand mixture; casting the resin/sand mixture into a preferred form; heating the resin/sand mixture in a microwave oven until a sand casting is set; and, letting the sand casting cool.