By Vibration Or Agitation Patents (Class 264/9)
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Patent number: 12226790Abstract: An acoustic force assisted painting system includes a housing, a nozzle, and at least one first transducer. The conduit is configured to receive paint from an external source. The nozzle is disposed in the housing. The nozzle has an inlet that is fluidly connected to the conduit and is configured to receive paint from the conduit. The nozzle has an outlet configured to dispense the paint. The at least one first transducer is disposed in the housing at a location downstream of the nozzle outlet in a flow direction of the paint.Type: GrantFiled: May 28, 2021Date of Patent: February 18, 2025Assignee: Nissan North America, Inc.Inventors: Sandeep Patil, Nanzhu Zhao
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Patent number: 12157260Abstract: A method of making thermoplastic polymer particles may include mixing in an extruder a mixture comprising a thermoplastic polymer and a carrier fluid that is immiscible with the thermoplastic polymer at a temperature greater than a melting point or softening temperature of the thermoplastic polymer and at a shear rate sufficiently high to disperse the thermoplastic polymer in the carrier fluid; cooling the mixture to below the melting point or softening temperature of the thermoplastic polymer to form solidified particles comprising thermoplastic polymer particles having a circularity of 0.90 or greater and that comprise the thermoplastic polymer; and separating the solidified particles from the carrier fluid.Type: GrantFiled: June 30, 2020Date of Patent: December 3, 2024Assignee: Xerox CorporationInventors: Valerie M. Farrugia, Michael S. Hawkins, David John William Lawton, Carolyn Patricia Moorlag
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Patent number: 12151006Abstract: Solid anhydrous cosmetic composition, preparation process, cosmetic treatment processes and associated kit The present invention relates to a solid anhydrous cosmetic composition, in particle form, and comprising at least 30% by weight of anionic surfactants, at least 5% by weight of amphoteric surfactants, and at least 10% by weight of fillers. The invention also relates to a process for preparing this composition by granulation on a fluidized air bed and also to a process for the cosmetic treatment, in particular the care and/or the cleaning, of keratin materials, in particular the hair, comprising the application of said solid anhydrous cosmetic composition, alone or in combination with a hair conditioning composition. The invention also relates to a kit comprising said solid anhydrous cosmetic composition and said conditioning composition.Type: GrantFiled: March 29, 2021Date of Patent: November 26, 2024Assignee: L'OREALInventors: Estelle Mathonneau, Gregory Plos, Emmanuelle Lebon-Hipolite, Marie-Florence D'Arras, Rafik Kerboussa
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Patent number: 12083556Abstract: An acoustic force assisted painting system has a housing, at least one nozzle and at least one acoustic emitter. The housing has a conduit for receiving paint from an external source into the housing. The at least one nozzle is disposed in the housing. The at least one nozzle has an inlet that is fluidly connected to the conduit to receive paint from the conduit. The at least one nozzle has an outlet that dispenses paint. The least one acoustic emitter is disposed in the housing at a location downstream of the inlet with respect to the conduit.Type: GrantFiled: December 21, 2020Date of Patent: September 10, 2024Assignee: Nissan North America, Inc.Inventors: Sandeep Patil, Nanzhu Zhao
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Patent number: 11897169Abstract: A process for producing particles of a thermoplastic polymer in spherical form involves providing at least one thermoplastic polymer in a molten state and providing an aqueous solution of at least one surface-active substance. The aqueous solution is in a temperature range from 100 to 300° C. The process also involves dispersing the thermoplastic polymer in the aqueous solution to obtain an aqueous solution containing dispersed thermoplastic polymer, which is cooled down to a temperature below the solidification point of the thermoplastic polymer to obtain a suspension containing an aqueous solution and particles of the thermoplastic polymer suspended in a solid state and in spherical form. The particles can be separated from the suspension and, optionally, dried. The particles obtained from the process have a particle size distribution having a d[4,3] value of more than 10 ?m and a d90.3 value of more than 20 ?m.Type: GrantFiled: June 18, 2020Date of Patent: February 13, 2024Assignee: BASF SEInventors: Andreas Bauder, Kerstin Muelheims, Michael Freese, Achim Stammer
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Patent number: 11850770Abstract: A process for producing particles of a thermoplastic polymer in spherical form involves providing at least one thermoplastic polymer in a molten state and providing an aqueous solution of at least one surface-active substance. The aqueous solution is in a temperature range from 100 to 300° C. The process also involves dispersing the thermoplastic polymer in the aqueous solution to obtain an aqueous solution containing dispersed thermoplastic polymer, which is cooled down to a temperature below the solidification point of the thermoplastic polymer to obtain a suspension containing an aqueous solution and particles of the thermoplastic polymer suspended in a solid state and in spherical form. The particles can be separated from the suspension and, optionally, dried. The particles obtained from the process have a particle size distribution having a d[4,3] value of more than 10 ?m and a d90.3 value of more than 20 ?m.Type: GrantFiled: June 18, 2020Date of Patent: December 26, 2023Assignee: BASF SEInventors: Andreas Bauder, Kerstin Muelheims, Michael Freese, Achim Stammer
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Patent number: 11801617Abstract: Optical absorber-containing thermoplastic polymer particles (OACTP particles) may be produced by methods that comprise: mixing a mixture comprising a thermoplastic polymer, a carrier fluid that is immiscible with the thermoplastic polymer, and optionally an emulsion stabilizer at a temperature greater than a melting point or softening temperature of the thermoplastic polymer and at a shear rate sufficiently high to disperse the thermoplastic polymer in the carrier fluid; cooling the mixture to below the melting point or softening temperature of the thermoplastic polymer to form solidified particles comprising the thermoplastic polymer; separating the solidified particles from the carrier fluid; and exposing the solidified particles to an optical absorber to produce the OACTP particles.Type: GrantFiled: June 30, 2020Date of Patent: October 31, 2023Assignee: Xerox CorporationInventors: Valerie M. Farrugia, Mihaela Maria Birau
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Patent number: 11794158Abstract: Provided is an apparatus for producing solid polymeric microparticles, the apparatus comprising a plurality of liquid droplet generators for forming liquid droplets of a first liquid, and a nozzle for forming a jet of a second liquid, wherein the plurality of liquid droplet generators and the nozzle are arranged relative to each other such that, in use, liquid droplets from the plurality of liquid droplet generators pass through a gas into said jet of second liquid.Type: GrantFiled: March 17, 2021Date of Patent: October 24, 2023Assignee: MIDATECH PHARMA (WALES) LIMITEDInventors: Paul Seaman, Huw Jones, Liam McAleer
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Patent number: 11745156Abstract: Method of producing prills includes providing a hollow body rotatable about a first axis, the body having a wall rotationally symmetrical around the first axis forming an interior space, the wall including nozzles; providing a second body disposed in the hollow body such that a gap exists between the hollow body and the second body; supplying liquid to the gap; generating jets of liquid from the nozzles radially outward by driving the rotational motion of the hollow body and/or second body around the first axis of rotation using a rotary drive unit; applying a reciprocal pressure excitation on the jets of liquid by moving the hollow body and/or second body along the first axis; and decoupling the rotations of the one of the hollow body and second body and a reciprocating drive-unit.Type: GrantFiled: February 5, 2021Date of Patent: September 5, 2023Assignee: MACHINEFABRIEK KREBER B.V.Inventors: Paulus Johannes Nicolaas Dits, Marcus Wilhelmus Maria Groenewegen
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Patent number: 11596603Abstract: A respirable dry powder including acetylsalicylic acid in particles has a mass median aerodynamic diameter (MMAD) within a range of about 0.5 ?m to about 10 ?m. The respirable dry powder may contain a pharmaceutically acceptable excipient, such as a phospholipid, in an amount ranging from about 0.1% (w/w) to about 10% (w/w) of the particles.Type: GrantFiled: August 7, 2020Date of Patent: March 7, 2023Assignee: Vectura Inc.Inventor: Kambiz Yadidi
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Patent number: 11136438Abstract: A process for producing polyolefin particles from a polyolefin composition, comprising the steps of: a) providing a melted composition of a polyolefin and b) providing particles from the melted composition by: b1) mixing a first flow of a supercritical fluid in the melted composition in a pressure vessel to obtain a solution saturated with the supercritical fluid and b2) passing the solution from the pressure vessel through a throttling device to a spraying tower to expand the solution to obtain the polyolefin particles in the spraying tower, wherein a second flow of a supercritical fluid is injected in the throttling device, wherein the supercritical fluid is a supercritical fluid of a substance selected from the group consisting of CO2, NH3, H2O, N2O, CH4, ethane, propane, propylene, n-butane, i-butane, n-pentane, benzene, methanol, ethanol, isopropanol, isobutanol, chlorotrifluoromethane, monofluoromethane, 1,1,1,2-Tetrafluoroethane, toluene, pyridine, cyclohexane, cyclohexanol, o-xylene, dimethyl ether anType: GrantFiled: June 30, 2016Date of Patent: October 5, 2021Assignee: SABIC GLOBAL TECHNOLOGIES B.V.Inventors: Diego Mauricio Castaneda Zuniga, Jan Nicolaas Eddy Duchateau, Peter Neuteboom, Zeljko Knez
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Patent number: 10948271Abstract: A cold spark fire electronic eruptive apparatus characterized in that the erupting apparatus is comprised of an ejecting unit, an activation unit, a power unit, and a storage unit, wherein, the storage unit stores a cold fireworks material for discharge, the power unit is connected to the storage unit and also is connected with a heating unit, the power unit transmitting the cold fireworks material in the storage unit to the heating unit, and the heating unit activating the cold fireworks raw material, sending it to the air removal unit for eruption.Type: GrantFiled: November 1, 2018Date of Patent: March 16, 2021Inventors: Zhou Xiaowen, Steve Bruce Freedman
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Patent number: 10852105Abstract: A cold spark waterfall machine, which comprises an accelerating unit, a heating unit, a power unit, and a storage unit. The storage unit stores a cold fireworks raw material for discharging. The power unit is connected to the storage unit wherein the storage unit is connected with the heating unit, and the power unit transmits the cold fireworks raw material in the storage unit to the heating unit. The heating unit activates the cold fireworks raw material and sends the cold fireworks raw material to the acceleration unit. The acceleration unit causes the activated material to accelerate in a downward eruption, thus forming a waterfall of low temperature sparks.Type: GrantFiled: November 23, 2018Date of Patent: December 1, 2020Inventors: Zhou Xiaowen, Steve Bruce Freedman
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Patent number: 9688781Abstract: Superabsorbent material, comprising clay-crosslinked superabsorbent polymers, obtainable by polymerizing in a spray-stream, polymerizable compounds in the presence of a polymerization initiator system, and nano-sized or individual clay particles, which are all introduced into a vessel by a spraying step in the form of a said spray-stream thereof, whereby said clay particles crosslink said polymers during polymerization. The invention also relates to such a process and absorbent articles comprising such superabsorbent material.Type: GrantFiled: July 19, 2010Date of Patent: June 27, 2017Assignee: The Procter & Gamble CompanyInventors: Axel Meyer, Torsten Lindner, Mattias Schmidt
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Patent number: 9321207Abstract: In a method and apparatus for micropelletization of a polymeric material, a melt thread of the polymeric material is formed by an extruder. A flowing gas is directed to the melt thread to form Rayleigh disturbances in the melt thread and break up the melt thread into discrete microdroplets. The discrete microdroplets are then solidified to form micropellets.Type: GrantFiled: March 6, 2013Date of Patent: April 26, 2016Assignee: Wisconsin Alumni Research FoundationInventors: Tim Osswald, Martin Launhardt
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Patent number: 9205590Abstract: Polymer pellets are formed using air to influence the separation of polymer from a polymer melt. In accordance with one or more embodiments, a polymer material is extruded through a nozzle to form a polymer melt extending from the nozzle. A non-uniform thickness is generated in the polymer melt using a gas or gasses to apply a drag force to the polymer melt. This drag force reduces a thickness of a portion of the polymer melt adjacent the nozzle, and the polymer melt is fractured into discrete droplets at the reduced thickness. The discrete droplets are then solidified to form pellets.Type: GrantFiled: March 6, 2013Date of Patent: December 8, 2015Assignee: Wisconsin Alumni Research FoundationInventors: Tim Andreas Osswald, William Mauricio Aquite
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Patent number: 9149433Abstract: A method for formation of micro-prilled poloxamer particles is disclosed. The particles find special use in pharmaceutical formulations. The process involves use of atomizing nozzles at higher than normal pressure atomizing gas, high atomizing gas temperature, use of high feed temperatures to reduce the viscosity of the poloxamer and optionally sieving after prill formation in prilling towers. The poloxamer particles are spherical and preferably have an average nominal diameter of less than or equal to 106 microns. The process is very cost effective and rapid.Type: GrantFiled: November 30, 2004Date of Patent: October 6, 2015Assignee: BASF CORPORATIONInventors: Rudolph Ernest Lisa, Anisul Quadir, Rebecca Ham Scheper, Peter Grzesowski
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Publication number: 20150114179Abstract: The problem addressed by the present invention is providing a method for producing microparticles. At least two fluids to be processed, a raw material fluid that contains a raw material and a processing fluid that contains a substance for processing the raw material are mixed in a thin film fluid formed between at least two surfaces for processing that are disposed so as to face each other, that can approach and separate from each other and at least one of which rotates relative to the other, and microparticles of the raw material that is processed are obtained. At this time, the proportion of the microparticles of the raw material which has been processed that coalesces with each other is controlled by controlling the circumferential speed of the rotation in a confluence section in which the raw material fluid and processing fluid flow together.Type: ApplicationFiled: May 1, 2012Publication date: April 30, 2015Applicant: M. TECHNIQUE CO., LTD.Inventor: Masakazu Enomura
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Publication number: 20150108671Abstract: A method for producing fine particles, including: discharging a fine particle material liquid, where solid materials to be formed into fine particles are dissolved or dispersed in a solvent or are melted, from two or more discharge holes in a downward vertical direction, to thereby form liquid droplets; and solidifying the liquid droplets discharged to form fine particles, wherein in the discharging a fine particle material liquid, gas flow is supplied at angle of greater than 0° but 90° or smaller to the downward vertical direction, and wherein an initial discharge velocity of the liquid droplets discharged from the discharge hole located at an upstream side of the gas flow in a flowing direction thereof is equal to or higher than an initial discharge velocity of the liquid droplets discharged from the discharge hole located at a downstream side of the gas flow in the flowing direction thereof.Type: ApplicationFiled: February 28, 2013Publication date: April 23, 2015Inventors: Yoshihiro Norikane, Satoshi Takahashi, Masaru Ohgaki, Andrew Mwaniki Mulwa
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Patent number: 8992196Abstract: A seamless capsule manufacturing apparatus (1) manufactures a seamless capsule by means of nozzles (2a-2d). A core liquid (5) and a coating liquid (6) are supplied to each of the nozzles (2a-2d) from pumps (16, 18) through distributors (21, 22). The distributors (21, 22) and the nozzles (2a-2d) are connected to each other by core liquid distributing tubes (23a-23d) and coating liquid distributing tubes (25a-25d), and each of the core liquid distributing tubes (23a-23d) and each of the coating liquid distributing tubes (25a-25d) have the same length. A vibrator (24) is mounted to the distributor (21), and the core liquid (5) is supplied to the nozzles (2a-2d) while being vibrated. Each of the distributors (21, 22) is provided with an air vent device (35), and air vent is performed appropriately.Type: GrantFiled: October 9, 2009Date of Patent: March 31, 2015Assignee: Freund CorporationInventors: Masayuki Ikeda, Hiroshi Nagao
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Publication number: 20150064468Abstract: The present invention provides a method for making uniform, spherical, acrylic polymeric beads by jetting, the beads produced, and ion exchange resins produced from functionalizing the uniform, spherical polymeric beads.Type: ApplicationFiled: March 27, 2013Publication date: March 5, 2015Inventors: John D. Finch, Thomas C. Kirk
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Publication number: 20140339078Abstract: Provided is a glucose sensor. The glucose sensor according to the present invention includes noble metal-graphene composites, and has high sensitivity and significantly excellent current flow as compared to titanium dioxide-graphene composites. In addition, the noble metal-graphene composite manufactured by aerosol spray pyrolysis serves as an improved glucose sensor having desirable sensitivity, stability, reproducibility, and selectivity.Type: ApplicationFiled: September 17, 2013Publication date: November 20, 2014Applicant: KOREA INSTITUTE OF GEOSCIENCE AND MINERAL RESOURCESInventors: Hee Dong JANG, Han Kwon CHANG, Sun Kyung KIM, Ki Min ROH
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Patent number: 8828285Abstract: A particulate production apparatus, including a droplet discharger to discharge a liquid including a particulate element which is solidified to become a particulate; and a pressure controller to feed the liquid including a particulate element to the droplet discharger at a pressure within a desired range.Type: GrantFiled: July 27, 2012Date of Patent: September 9, 2014Assignee: Ricoh Company, Ltd.Inventors: Kiyotada Katoh, Minoru Masuda, Yasutada Shitara, Yoshihiro Norikane, Satoshi Takahashi
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Patent number: 8784706Abstract: A spherical tungsten carbide powder is characterized by that the material has a microhardness higher than 3600 kgf/mm2, and that the powder has an apparent density from 9.80 to 11.56 g/cm3. A method for the manufacture of a powder comprises the steps: a) providing a chamber comprising a rotatable crucible, b) adding material into said rotatable crucible, c) melting the material using a plasma arc discharge, d) rotating the crucible to atomize the molten material to form liquid droplets, with subsequent cooling of the droplets to obtain a powder, wherein the material added into said rotatable crucible is heated to a temperature above 40% of the melting temperature of the material before it enters the crucible. It is possible to reduce the current required for melting the stock. Heat losses are decreased, and the spherical powder obtained during atomization becomes more homogeneous in its composition and structure. The cost is reduced.Type: GrantFiled: May 18, 2011Date of Patent: July 22, 2014Assignee: MetaSphere Technology ABInventors: Ruslan Alekseevich Shevchenko, Andrey Pavlovich Chukanov, Boris Vladimirovich Safronov, Yuri Gennadievich Nadezhdin, Alexander Yurievich Vakhrushin
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Patent number: 8778239Abstract: A method of producing particulate, including introducing an initial liquid including a particulate component in a lower concentration than that of a liquid including a particulate component or no concentration to a projection hole of a droplet projector so as to be projected at the start of the discharging; discharging a droplet of the liquid comprising a particulate component from the projection hole; and solidifying the droplet to form a particulate.Type: GrantFiled: August 17, 2012Date of Patent: July 15, 2014Assignee: Ricoh Company, Ltd.Inventors: Andrew Mwaniki Mulwa, Yoshihiro Norikane, Shinji Aoki, Masaru Ohgaki
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Publication number: 20140193489Abstract: The present invention provides a sonochemical irradiation-based method for the preparation of polydopamine (PDA) nanocapsules having reduced wall thickness and uniform size distribution, which may further comprise at least one payload; nanocapsules obtained by this method; and compositions thereof. Such compositions may be formulated for different purposes, e.g., as pharmaceutical compositions for various therapeutic or diagnostic purposes.Type: ApplicationFiled: January 7, 2014Publication date: July 10, 2014Applicant: BAR-ILAN UNIVERSITYInventors: Shai Rahimipour, Gil Yeroslavsky, Michal Richman
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Patent number: 8765349Abstract: A method of manufacturing toner is provided. In the method, toner constituents are dissolved or dispersed in an organic solvent to prepare a toner constituents liquid. The toner constituents liquid is degassed so that the toner constituents liquid includes dissolved oxygen in an amount of 3 mg/L or less. The toner constituents liquid is vibrated in a chamber having at least one nozzle to form a liquid column resonance standing wave in the toner constituents liquid. The toner constituents liquid is discharged from the nozzle disposed within an area including an antinode of the liquid column resonance standing wave to form the toner constituents liquid into liquid droplets. The liquid droplets are dried to solidify the liquid droplets into solid particles.Type: GrantFiled: July 25, 2012Date of Patent: July 1, 2014Assignee: Ricoh Company, Ltd.Inventors: Yoshihiro Norikane, Andrew Mwaniki Mulwa, Kiyotada Katoh, Yasutada Shitara
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Patent number: 8709379Abstract: Formulations of neutral retinoids, in particular fenretinide (HPR) in the form of lipid nanoparticles, solid dispersions and emulsions are disclosed. These compositions are used to treat diseases that are amenable to treatment by HPR, such as neoplastic diseases by achieving higher and more prolonged concentrations of HPR in the subject. The key steps for preparing lipid nanovesicles of HPR include mixing and sonication, sterile filtration, without or without lyophilization for long-term stable storage, and employ processes and materials that are scalable from the laboratory to the manufacturing level. The formulation are suitable for injection into human or animal patients without causing allergic or hypersensitivity responses by avoiding chemical surfactants and animal sources of phospholipids in their manufacture.Type: GrantFiled: March 29, 2007Date of Patent: April 29, 2014Assignee: Scitech Development, LLCInventors: Ralph E. Parchment, Bhaskara R. Jasti, Ramesh R. Boinpally, Stephen E. Rose, Earle T. Holsapple
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Patent number: 8603373Abstract: A method for producing particles, including: bringing a compressive fluid into contact with a pressure plastic material, so as to produce a melt of the pressure plastic material; and discharging the melt of the pressure plastic material by differential pressure to a space, so as to form particles, wherein the discharging includes at least one of (A) discharging the melt of the pressure plastic material while a compressive fluid is supplied to the melt of the pressure plastic material, and (B) discharging the melt of the pressure plastic material through one or more through-holes, to which vibration is applied, so as to change the shape of the melt of the pressure plastic material from a columnar shape, through the columnar shape with constrictions, into a particle shape.Type: GrantFiled: October 31, 2011Date of Patent: December 10, 2013Assignee: Ricoh Company, Ltd.Inventors: Shinji Ohtani, Chiaki Tanaka
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Publication number: 20130316018Abstract: The present invention relates to a new manufacture process for producing an iron containing phosphate adsorbent, in particular to a process for manufacturing and isolating an iron(III)-based phosphate adsorbent which exhibits valuable pharmacological properties.Type: ApplicationFiled: July 31, 2013Publication date: November 28, 2013Applicant: Novartis AGInventors: Daniel Kaufmann, Nicole Bieri, Ulrich Meier, Ranjit Thakur, Zdenek Zencak, Christa Hartmann, Andreas Meyer
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Publication number: 20130295181Abstract: A process for obtaining compositions constituted by propolis nanoparticles is disclosed. The nanoparticles are optionally associated to a substance of interest such as active ingredients, and, optionally, substances of secondary effect such as synergists and adjuvants. The process includes preparing a fraction A, which consists of propolis extract dissolved in an organic solvent, to which stabilizer and/or emulsifier may be added, and, optionally, substances of interest and/or of secondary effect; ii) preparing a fraction B, aqueous phase, constituted by: (ii.1) water; or (ii.2) an aqueous solution or dispersion, to which stabilizer and/or emulsifier may be added; (iii) dropping the fraction A onto the fraction B or vice versa; iv) homogenizing the mixture by stifling and spontaneous formation of nanoparticles with average size from 1 to 1000 nm in a dispersion; and v) optionally (v-1) removing organic solvent and/or (v-2) drying the nanodispersion.Type: ApplicationFiled: October 27, 2011Publication date: November 7, 2013Inventor: Humberto de Mello Brandão
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Publication number: 20130288050Abstract: Dissociation of a macroscale version of an aramid fiber leads to the nanofiber form of this polymer. Indefinitely stable dispersions of uniform high-aspect-ratio aramid nanofibers (ANFs) with diameters between 3 and 30 nm controlled by the media composition and up to 10 ?m in length are obtained. ANFs can be processed in transparent thin films using layer-by-layer assembly (LBL) with superior mechanical performance.Type: ApplicationFiled: April 26, 2013Publication date: October 31, 2013Inventors: Ellen M. Arruda, Keqin Cao, Carlos A. Pons Siepermann, Michael D. Thouless, Ryan M. Anderson, Nicholas A. Kotov, Ming Yang, Anthony M. Waas
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Patent number: 8551763Abstract: In a method and system for forming concentrated volumes of microbeads, a polymer solution and/or suspension includes a polymer dissolved and/or dispersed in a medium. Streams of a focusing fluid and of the polymer solution and/or suspension flow towards a fluid bath, and into intersection with one another, so &s to focus the polymer solution and/or suspension. The polymer solution and/or suspension stream forms microbeads in the fluid bath. Some of the focusing fluid is drawn from the fluid bath, so as to concentrate the microbeads in die fluid bath. The system includes a flow focusing apparatus and a liquid-containing cell. The focusing apparatus includes polymer and focusing nozzles. The cell contains the fluid bath and has an outlet port, through which the focusing fluid is drawn from the fluid bath.Type: GrantFiled: October 10, 2008Date of Patent: October 8, 2013Assignee: FIO CorporationInventors: Sebastien Fournier-Bidoz, Warren Che Wor Chan
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Patent number: 8545739Abstract: The present invention relates to a method for the production of micro-particles of polysaccharides. The method includes preparing a feeding solution and a gelifying liquid to collect nebulized jets of the feeding solution. The feeding solution contains at least one polymer capable of forming micro-particle structures and at least one biologically active substance. The feeding solution is pressurized inside an air-less nebulizing unit and then nebulized through the unit itself so as to generate nebulized jets impacting the surface of the gelifying liquid.Type: GrantFiled: September 2, 2010Date of Patent: October 1, 2013Inventors: Moreno Cocchietto, Dario Voinovich, Laura Zorzin, Gianni Sava
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Patent number: 8501055Abstract: A toner manufacturing method, a toner manufacturing apparatus, and a toner are disclosed. The toner manufacturing apparatus includes a droplet generating unit that includes a thin film in which plural nozzles are formed, and an annular vibrating unit that is arranged at a perimeter of a deformable domain of the thin film for vibrating the thin film; a storage unit for storing a toner-containing liquid that includes at least a resin and a colorant, and for supplying the toner-containing liquid 10 to the droplet generating unit; and a granulating unit for solidifying droplets that are periodically breathed out from the nozzles of the droplet generating unit to form toner particles.Type: GrantFiled: March 5, 2008Date of Patent: August 6, 2013Assignee: Ricoh Company, Ltd.Inventors: Shinji Ohtani, Yoshihiro Norikane, Seichin Kinuta
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Publication number: 20130140483Abstract: Disclosed is a micro particle for a thermal control material capable of being applied as a highly thermal conductive material for thermal control, and an apparatus and a method of producing the micro particle for the thermal control material by using an ultrasonic high-temperature vibration scheme. More specifically, a Boron Nitride (BN) particle having a plate shape and an excellent thermal conductivity is coated on a PCM having a shape of a micro bead, to increase the thermal conduction to the inside PCM, so that a phase change is easily generated, and which allows an easy treatment of the PCM in a liquid state at a temperature equal to or higher than a melting point of the PCM.Type: ApplicationFiled: February 27, 2012Publication date: June 6, 2013Applicant: HYUNDAI MOTOR COMPANYInventors: Han Saem Lee, Do Suck Han, Jin Woo Kwak, Chi Hoon Choi, Kyong Hwa Song, Byung Sam Choi
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Patent number: 8454866Abstract: The invention relates to a process for the preparation of particles based on a thermoplastic polymer with a mean diameter of less than 1 mm. The process of the invention comprises more particularly a stage of preparation of a composition comprising the thermoplastic polymer and an additive, in the molten state, of cooling the composition and of disintegration of the thermoplastic polymer dispersion.Type: GrantFiled: October 6, 2005Date of Patent: June 4, 2013Assignee: Rhodia ChimieInventors: Pascal Herve, Christophe Paulo, Eric Roche, Mare Labeille, Franck Touraud
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Patent number: 8444886Abstract: Controlled geometry particles of thermoplastic polymers are prepared from compositions containing the thermoplastic polymer and two additives, in the molten state, by cooling the molten composition and disintegrating the resulting dispersion of thermoplastic polymer; powders obtained therefrom advantageously have mean particle diameters ranging from 0.1 to 800 ?m and are useful additives in, e.g., paints and coatings.Type: GrantFiled: April 3, 2007Date of Patent: May 21, 2013Assignee: Rhodia OperationsInventor: Pascal Herve
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Patent number: 8409621Abstract: A method of forming particles, comprises accelerating a first stream comprising a first liquid, applying a charging voltage of at most 1.5 kV to the first stream, and vibrating the first stream, to form particles.Type: GrantFiled: November 13, 2007Date of Patent: April 2, 2013Assignee: The Board of Trustees of the University of IllinoisInventors: Kyekyoon Kim, Hyungsoo Choi, Young Bin Choy
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Publication number: 20130069263Abstract: A particulate production apparatus, including a droplet discharger to discharge a liquid including a particulate element which is solidified to become a particulate; and a pressure controller to feed the liquid including a particulate element to the droplet discharger at a pressure within a desired range.Type: ApplicationFiled: July 27, 2012Publication date: March 21, 2013Inventors: Kiyotada Katoh, Minoru Masuda, Yasutada Shitara, Yoshihiro Norikane, Satoshi Takahashi
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Publication number: 20130034810Abstract: A method of manufacturing toner is provided. In the method, toner constituents are dissolved or dispersed in an organic solvent to prepare a toner constituents liquid. The toner constituents liquid is degassed so that the toner constituents liquid includes dissolved oxygen in an amount of 3 mg/L or less. The toner constituents liquid is vibrated in a chamber having at least one nozzle to form a liquid column resonance standing wave in the toner constituents liquid. The toner constituents liquid is discharged from the nozzle disposed within an area including an antinode of the liquid column resonance standing wave to form the toner constituents liquid into liquid droplets. The liquid droplets are dried to solidify the liquid droplets into solid particles.Type: ApplicationFiled: July 25, 2012Publication date: February 7, 2013Inventors: Yoshihiro NORIKANE, Andrew Mwaniki MULWA, Kiyotada KATOH, Yasutada SHITARA
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Publication number: 20130025862Abstract: Proppant material for hydraulic fracturing is provided. The particles of the proppant are formed by drip casting. A slurry of finely divided ceramic particles is flowed through nozzles and formed into droplets under the influence of vibration. Uniform sized, smooth surface, spherical green particles are formed. The green particles are dried and sintered to form the proppant. The proppant is used in the process of hydraulic fracturing of wells.Type: ApplicationFiled: September 10, 2012Publication date: January 31, 2013Applicant: CARBO Ceramics, Inc.Inventors: Benjamin T. Eldred, Brett A. Wilson, Clayton F. Gardinier, Robert J. Duenckel
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Publication number: 20130026669Abstract: Methods and systems for preparing nanocrystalline compositions using focused acoustic processing to cause and/or enhance crystal growth. A flow through system may be employed to expose sample material having a volume of greater or less than 30 mL to focused acoustic energy while flowing through a process chamber at a rate of at least 0.1 mL/min. Sample material may be processed by a suitable focused acoustic field in a cyclic fashion and/or with adjustment of processing parameters based on monitored characteristics of the sample, such as level of crystallinity. Nanocrystalline particles within the sample may have a tight particle size distribution with an average particle size between 10 nm and 1 micron. Stable nanocrystalline compositions may be reproducibly prepared using focused acoustics to have controllable morphologies and dimensions.Type: ApplicationFiled: July 13, 2012Publication date: January 31, 2013Applicant: Covaris, INCInventors: Carl Beckett, James A. Laugharn, JR., Srikanth Kakumanu
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Publication number: 20130008348Abstract: A composition for pelletized bitumen and a method for preparing the same is disclosed. The composition is comprised of: between approximately 30% to approximately 40% by weight of bitumen; between approximately 15% to approximately 30% by weight of stiffening compound; between approximately 35% to approximately 45% by weight of setting compound; and approximately 0.05% by weight of water. The stiffening compound is comprised of between approximately 10% to approximately 20% by weight of ground asphalt shingles; between approximately 5% to approximately 10% by weight of vulcanized rubber; between approximately 1% to approximately 2% by weight of uintahite; and up to approximately 0.5% by weight of zeolite. And the stiffening compound may be Type II Portland cement.Type: ApplicationFiled: July 8, 2011Publication date: January 10, 2013Inventor: Kelly Sockwell
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Patent number: 8349229Abstract: A method for producing tables made of mixtures of a plurality of materials, and a method for producing a sulfurous fertilizer. A method for producing tablets made of mixtures of a plurality of materials, particularly urea mixtures, having the following steps:—producing a liquid melt of a first material,—adding at least one further material in solid or liquid form to the melt for producing a mixture,—output of drops of the mixture onto a steel belt by means of a drop former having a rotating, perforated outer drum,—solidification of the drops of the mixture on the steel belt into tablets, wherein the at least one additional material is mixed into the liquid melt in liquid form immediately before the drop former or into the liquid melt in solid. form upstream of a two-stage heated grinding and mixing unit.Type: GrantFiled: December 3, 2008Date of Patent: January 8, 2013Assignee: Sandvik Materials Technology Deutschland GmbHInventors: Hans-Kurt Schromm, Albert Baeder, Matthias Kleinhans
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Patent number: 8349230Abstract: The present invention provides spherical rubber chemicals and the method for preparing the same. The spherical rubber chemicals of the present invention include spherical antioxidants, spherical vulcanization agents, spherical processing aids, spherical reinforcing agents, or spherical adhesive agents. With the spherical rubber chemicals of the present invention, the shortcomings of powdery or semi-spherical rubber chemicals are overcome, including eliminating the dust pollution during granulation procedure and avoiding the raw material loss and the environmental pollution, while solving the quality problem of lower melting point of product caused by the presence of fine powder crystal. Furthermore, the resultant rubber chemicals has an improved smoothness of surface, which is helpful to improve the flowing and mixing behaviors of the rubber chemicals in mixing or open milling process with rubbers.Type: GrantFiled: November 28, 2011Date of Patent: January 8, 2013Assignee: Jiangsu Sinorgchem Technology Co., Ltd.Inventors: Nongyue Wang, Xiaohui Mao, Xiaogen Feng, Qianwen Cheng, Luxin Wang
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Publication number: 20120315308Abstract: Methods and apparatus for continuously preparing a particulate material are provided. One method of the invention includes mixing a first solution comprising a solute dissolved in a solvent, with a second solution, thereby providing a first solution-second solution mixture; and introducing the mixture into the high-energy zone of a high shear dispersion system and dispersing the first solution-second solution mixture prior to significant particulate growth, whereby the dispersed mixture forms a suspension of particles of the solute; and wherein significant particulate growth has occurred when the average equivalent spherical diameter of at least one particle in the solution is greater than 10 micrometer. Integrated apparatuses for performing methods of the invention are also provided.Type: ApplicationFiled: February 24, 2011Publication date: December 13, 2012Inventor: William A. Travers
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Publication number: 20120309250Abstract: Nanofibers are fabricated by introducing a mixture of a polymer solution and inorganic precursor into a dispersion medium and shearing the mixture. Liquid strands, streaks or droplets of the mixture are spun into elongated fibers that include inorganic fibrils. The resulting composite inorganic/polymer fibers may be provided as an end product. Alternatively, the polymer may be removed to liberate the inorganic fibrils, which may be of the same or smaller cross-section as the polymer fibers and may be provided as an end product.Type: ApplicationFiled: May 16, 2012Publication date: December 6, 2012Applicant: NORTH CAROLINA STATE UNIVERSITYInventors: ORLIN D. VELEV, STOYAN SMOUKOV
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Publication number: 20120251595Abstract: The present invention relates to methods and compositions to prepare small size particles of poorly water soluble agents or drugs with surface enriched hydrophilicity.Type: ApplicationFiled: November 9, 2010Publication date: October 4, 2012Applicant: BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEMInventors: Robert O. Williams, III, Keat Theng Chow
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Patent number: 8273274Abstract: The current invention relates to methods of making nano-particles of a material with a narrow polydispersity. The particle materials are active agents, organic compounds, polymers, and combinations thereof.Type: GrantFiled: March 18, 2010Date of Patent: September 25, 2012Assignee: Abbott Cardiovascular Systems Inc.Inventor: Dariush Davalian