Post Sintering Operation Patents (Class 419/26)
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Patent number: 5940675Abstract: Powder metallurgy production of T222 alloy affording properties comparable to melt derived T222, but at higher yields and lower costs, is enabled by blending component powders of minus 325 mesh and sintering at 2,400.degree. C. in three sinter steps and utilizing a slow ramp up in the first sinter step and cold isostatic pressing prior to the first sinter step and isostatic press densification in conjunction with at least the first sinter step.Type: GrantFiled: December 24, 1997Date of Patent: August 17, 1999Assignee: H. C. Starck, Inc.Inventors: Robert W. Balliett, Trung Luong
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Patent number: 5930581Abstract: The invention is a complex-shaped article, comprising an article prepared by joining at least one multi-phase ceramic-metal part and at least one shaped part of another material, wherein the theoretical density of the at least one ceramic-metal part is greater than 80 percent.In another aspect, the invention is a process for preparing complex-shaped articles, comprising:(a) forming at least one ceramic-metal part;(b) forming at least one shaped part of another material; and(c) joining the at least one shaped ceramic-metal part with the at least one shaped part of another material such that a complex-shaped article is formed.The invention is a less costly and time-consuming process for preparing complex-shaped composite articles wherein the articles are formed of two or more selected materials wherein one of the materials is a ceramic-metal composite.Type: GrantFiled: December 24, 1996Date of Patent: July 27, 1999Assignee: The Dow Chemical CompanyInventors: David W. Born, Richard T. Fox, Donald J. Perettie
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Patent number: 5925837Abstract: A manufacturing method and products of metallic friction materials includes processes of 1. preparing powder materials, 2. mixing copper as a base, proper proportion of iron powder or steel wool, aluminum powder, zinc or tin or lead powder, graphite powder and alumina or silicon dioxide powder, 3. pressing mixed materials into green bodies under 375.about.625 MPa at room temperature, 4. pre-heat treating the green bodies in an air furnace with temperature raised to 100.about.300.degree. C. for 1.about.3 hours, 5. sintering the green bodies into test samples under 350.about.750 MPa for 24.about.60 hours to gain sintered friction materials having an oxidized layer of less than 1 mm thick, 6. processing and grinding the sintered test samples with grinders to remove the oxidized layer, 7. washing the outer surface of the sintered test samples ground into finished products. The method of the invention may reduce largely difficulty in manufacturing processes, the investment and productive cost.Type: GrantFiled: September 16, 1998Date of Patent: July 20, 1999Assignees: Chien-Ping Ju, Jiin-Huey Chen LinInventors: Chien-Ping Ju, Jiin-Huey Chen Lin, Sun-Zen Chen
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Patent number: 5897830Abstract: A consumable billet for melting and casting a metal matrix composite component is made of a consolidated powder metal matrix composite having a titanium or titanium alloy matrix reinforced with particles. The preferred billet is a blended and sintered powder metal composite billet incorporating titanium carbide or titanium boride into a Ti--6Al--4V alloy.Type: GrantFiled: December 6, 1996Date of Patent: April 27, 1999Assignee: Dynamet TechnologyInventors: Stanley Abkowitz, Susan M. Abkowitz, Paul F. Weihrauch, Harold L. Heussi, Walter Zimmer
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Patent number: 5856032Abstract: A cermet including a cermet core zone in which the content of a binder amounts to at most 90% by mass in relationship to a cermet hard phase is formed with a 0.01 to 3 um deep surface layer having an increased resistance to wear compare to the cermet core zone.Type: GrantFiled: September 30, 1996Date of Patent: January 5, 1999Assignee: Widia GmbHInventors: Hans Werner Daub, Klaus Dreyer
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Patent number: 5841041Abstract: A porous mold material is provided that contains pores for ventilation in a metal casting, which pores range from 20 to 50 microns, and wherein the porosity value of the porous mold material ranges from 25 to 35% by volume. A method is further provided of producing a porous mold material that contains pores ranging from 20 to 50 microns for ventilation in casting, which method is characterized in that the mixing ratio of stainless steel particles to stainless steel short fibers is from 40 wt %:60 wt % to 65 wt %:35 wt %. The porous mold material of this invention does not have defects such as the inferior fluidity of a molten metal in the mold, or the shrinkage and blowholes in cast products.Type: GrantFiled: September 18, 1996Date of Patent: November 24, 1998Assignee: Sintokogio, Ltd.Inventors: Norihiro Asano, Tatsuhiko Kato
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Patent number: 5814272Abstract: A method for forming dendritic metal powders, comprising the steps of: (1) heating a powder comprising non-dendritic particles, under conditions suitable for initial stage sintering, to form a lightly sintered material; and (2) breaking the lightly sintered material to form a powder comprising dendritic particles. In one embodiment, the lightly sintered material is broken by brushing the material through a screen. Another aspect of the present invention comprises the dendritic particles that are produced by the method described above. These particles can comprise any suitable metal, such as transition metals, rare earth metals, main group metals or metalloids or an alloy of two or more such metals. The particles can also comprise a ceramic material, such as a metal oxide. These particles are characterized by a dendritic, highly anisotropic, morphology arising from the fusion of substantially non-dendritic particles, and by a low apparent density relative to the substantially non-dendritic starting material.Type: GrantFiled: February 21, 1996Date of Patent: September 29, 1998Assignee: Millipore CorporationInventors: Robert S. Zeller, Christopher J. Vroman
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Patent number: 5815790Abstract: The invention relates to a method for the manufacturing of a composite metal product. More particularly, the invention relates to a method for the manufacturing of a composite product consisting of at least two stainless steel materials having different chemical compositions, particularly a composite stainless product on which decorative patterns can or has been produced by etching.It is significant feature of the invention that at least two stainless steel materials having different chemical compositions are bonded together through hot isostatic compaction at a pressure exceeding 600 bar and a temperature exceeding 1000.degree. C., at least one of said materials consisting of powder, for the achievement of a consolidated body.Type: GrantFiled: December 4, 1996Date of Patent: September 29, 1998Assignee: Soderfors Powder AktiebolagInventors: Per Billgren, Kaj Embretsen
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Patent number: 5808213Abstract: Silver-iron materials for electrical switching contacts with properties which come very close to those of silver-nickel materials formed of 4.6 to 15% by weight iron and 0.05 to 5% by weight of one or more of the oxides magnesium oxide, calcium oxide, yttrium oxide, lanthanum oxide, cerium oxide, chromium oxide, iron oxide, aluminum oxide, indium oxide, silicon oxide, and tin oxide, the balance being silver.Type: GrantFiled: November 19, 1996Date of Patent: September 15, 1998Assignee: Degussa AktiengesellschaftInventors: Wolfgang Weise, Willi Malikowski, Roger Wolmer, Peter Braumann, Andreas Koffler
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Patent number: 5758253Abstract: A process for producing sintered titanium-graphite having improved wear resistance and low frictional characteristics is described. The said process which produces titanium-graphite composites having a triphasic structure with controlled porosity and a graphite lubricating film, comprises sintering a mixture of titanium and graphite powders in which the percentage of graphite may vary from 4 to 8 percent at temperatures from about 800.degree. C. to 1600.degree. C., for about 1/2 to 2 hours, under a compaction pressure of 0.17 to 0.62 MPa. The composites have applications in biomedical engineering and other fields of engineering due to their biocompatibility, strength and improved wear resistance.Type: GrantFiled: October 7, 1996Date of Patent: May 26, 1998Assignee: National University of SingaporeInventors: Swee Hin Teoh, Rajendran Thampuran, James Cho Hong Goh, Winston Kar Heng Seah
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Patent number: 5752155Abstract: A method of producing a cutting insert which includes the steps of: providing a generally homogeneous powder blend of powder components; forming the powder blend into a green body wherein the green body includes a rake face and a flank face with a cutting edge at the juncture of the rake face and the flank face; honing the cutting edge of the green body; and consolidating the green body with the honed cutting edge so as to form a consolidated body with a honed cutting edge.Type: GrantFiled: October 21, 1996Date of Patent: May 12, 1998Assignee: Kennametal Inc.Inventors: Alfred S. Gates, Jr., Bernard North, William R. Shaffer
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Patent number: 5729823Abstract: The present invention relates to a cemented carbide insert, comprising a cemented carbide substrate and a coating. The substrate contains WC and cubic carbonitride phase in a binder phase based of Co and/or Ni and has a binder phase enriched surface zone essentially free of cubic phase. The binder phase enriched surface zone prevails over the edge. As a result, an insert according to the invention has improved edge toughness and resistance against plastic deformation and is particularly useful for machining of sticky work piece materials such as stainless steel.Type: GrantFiled: March 14, 1996Date of Patent: March 17, 1998Assignee: Sandvik ABInventors: Per Gustafson, Leif kesson
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Patent number: 5728194Abstract: Silver-iron materials for electrical switching contacts with properties which come very close to those of silver-nickel materials formed of 0.5 to 20% by weight iron 0.5 to 5% by one or more of the elements rhenium, iridium, and ruthenium, and 0.05 to 2% by weight of one or more of the oxides magnesium oxide, calcium oxide, yttrium oxide, lanthanum oxide, titanium oxide, zirconium oxide, hafnium oxide, cerium oxide, niobium oxide, tantalum oxide, chromium oxide, manganese oxide, iron oxide, zinc oxide, copper oxide, aluminum oxide, indium oxide, silicon oxide, and tin oxide, the balance being silver.Type: GrantFiled: November 19, 1996Date of Patent: March 17, 1998Assignee: Degussa AktiengesellschaftInventors: Wolfgang Weise, Willi Malikowski, Roger Wolmer, Peter Braumann, Andreas Koffler
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Patent number: 5722034Abstract: A method of manufacturing a high-purity refractory metal or a an alloy based thereon, said refractory metal being selected from the group consisting of niobium, rhenium, tantalum, molybdenum, and tungsten, comprising the steps of compacting a mixed material, in the form of powders or small lumps, of a refractory metal or alloy to be refined together with one or two or more additive elements selected from the group of transition metal elements consisting of vanadium, chromium, manganese, iron, cobalt and nickel, and from the group of rare earth elements, sintering the resulting compact at a high temperature of at least 1000.degree. C. and a high pressure of at least 100 MPa, thereby forming a lower compound or nonstoichiometric compound between at least a part of the additive element or elements and the impurity gas ingredient element such as O, N, C, and H, contained in the refractory metal or alloy to be refined, and thereafter electron-beam melting the sintered body.Type: GrantFiled: December 5, 1995Date of Patent: February 24, 1998Assignee: Japan Energy CorporationInventor: Syozo Kambara
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Patent number: 5701575Abstract: An article essentially consisting of one or more of Ti--Al intermetallic compounds is fabricated so as to have a volume ratio of voids no more than 3.5%, by preparing a mixture of materials selected from a group consisting of Ti, Ti alloys, Al, Al alloys, and Ti--Al compounds, having a composition suitable for forming a desired Ti--Al intermetallic compound, and heating said mixture so that said mixture may be sintered. Typically, the temperature and pressure for the heating or sintering process is appropriately selected so that the desired porosity may be obtained. The mechanical strength of an article according to the present invention is not only improved but is highly predictable, or, in other word, highly reliable. The fabrication costs can be reduced because the fabrication process involves only relatively low temperatures when pressing and heating the work at the same time.Type: GrantFiled: January 11, 1996Date of Patent: December 23, 1997Assignee: NHK Spring Co., Ltd.Inventors: Kohei Taguchi, Michihiko Ayada, Hideo Shingu
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Patent number: 5701574Abstract: A method of producing a sliding sleeve for a synchronizer of a speed-changing gear, the sliding sleeve being comprised of a sintered powder metal compact having a claw extending along an inner periphery of the sleeve, and the claw consisting of teeth having opposite end faces and a cross-section between the end faces which is reduced relative to an undercut portion at at least one of the end faces, which method comprises the steps of sintering the powder metal compact having the claw consisting of the teeth having the opposite end faces and the reduced cross-section extending between the end faces, and then applying solely an axial upsetting force to the one end face to form the undercut portion thereat while leaving the reduced cross-section unchanged.Type: GrantFiled: February 6, 1996Date of Patent: December 23, 1997Assignee: Miba Sintermetall AktiengesellschaftInventors: Karl Derflinger, Herbert Schmid, Johann Dickinger
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Patent number: 5698008Abstract: A contact material for a vacuum valve including, a conductive constituent including at least copper, an arc-proof constituent including at least chromium and an auxiliary constituent including at least one selected from the group consisting of tungsten, molybdenum, tantalum and niobium. The contact material is manufactured by quench solidification of a composite body of the conductive constituent, the arc-proof constituent and the auxiliary constituent.Type: GrantFiled: February 21, 1995Date of Patent: December 16, 1997Assignee: Kabushiki Kaisha ToshibaInventors: Tsuneyo Seki, Tsutomu Okutomi, Atsushi Yamamoto, Takashi Kusano
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Patent number: 5678163Abstract: The present invention relates to an improved method of manufacturing an airbag initiator. Currently, an airbag initiator is comprised of three parts made out of two dissimilar materials plus a glass to metal seal. The present method builds the same airbag initiator with the body and the pins in one piece via a process called metal injection molding. The part is then placed in a furnace to remove a wax binder, then the temperature is ramped up slowly to remove a thermoplastic layer, and the temperature is further ramped up to form a sintered part. The sintered part being equal to or better than standards of wrought material. The initiator is then removed from the furnace and a glass bead is placed in a void area in the body of the initiator. The glass is melted forming a glass to metal seal between a first pin and the body of the initiator. A top portion of the initiator is then lapped off isolating the first pin from the body of the initiator.Type: GrantFiled: August 10, 1995Date of Patent: October 14, 1997Inventor: Eldon D. Rice
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Patent number: 5666634Abstract: The invention has for its object the provision alloy steel powders for Cr-based high strength sintered bodies having high tensile strength, fatigue strength and toughness which are adapted for use in parts for motor vehicles and parts for OA apparatus.The composition of the alloy steel powder comprises, by wt %, not larger than 0.1% of C, not larger than 0.08% of Mn, 0.5-3% of Cr, 0.1-2% of Mo, not larger than 0.01% of S, not larger than 0.01% of P, not larger than 0.2% of O, optionally one or more of 0.2.about.2.5% Ni, 0.5.about.2.5% Cu and the balance being inevitable impurities and Fe. The sintered body has substantially the same composition provided that the content of C alone is limited to 0.2-1.2%.The manufacturing method comprises molding the above alloy steel powder, sintering the resulting green compact at a temperature of 1100.degree.-1300.degree. C. and immediately cooling at a cooling rate of 10.degree.-200.degree. C./minute.Type: GrantFiled: December 23, 1994Date of Patent: September 9, 1997Assignee: Kawasaki Steel CorporationInventors: Shigeru Unami, Osamu Furukimi
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Patent number: 5618397Abstract: Metal silicide targets are provided for sputtering which have a density of at least 99%, no more than one coarse silicon phase 10 .mu.m or larger in size that appears, per square millimeter, on the sputter surface, and an oxygen content of at most 150 ppm. They are made by a method which comprises finely grinding a synthesized silicide powder, vacuum annealing the finely ground powder in a hot press die without the application of pressure, and thereafter compacting and sintering the compact to a density of at least 99% by hot pressing. Alternatively, the finely ground powder is vacuum annealed as a presintered body at a density ratio of 50 to 75%, and thereafter is compacted and sintered.Type: GrantFiled: April 17, 1995Date of Patent: April 8, 1997Assignee: Japan Energy CorporationInventors: Osamu Kano, Yasuhiro Yamakoshi, Junichi Anan, Koichi Yasui
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Patent number: 5536485Abstract: A powder of diamond or high-pressure phase boron nitride core particles charged into a coating space as it is dispersed, and a precursor of a coat forming substance allowed to contact and/or impinge against the particles in the powder of core particles so that their surfaces are covered with the coat forming substance, thereby preparing coated diamond or high-pressure phase boron nitride particles which are subsequently sintered. The thusly produced diamond of high-pressure phase boron nitride sinter is composed of coated core particles of high performance that are superhard, uniform, dense and sintered firmly, and which have a controlled microstructure.Type: GrantFiled: August 11, 1994Date of Patent: July 16, 1996Assignees: Agency of Industrial Science & Technology, Nisshin Flour Milling Co., Ltd., Reed Co., LtdInventors: Shoichi Kume, Haruo Yoshida, Yukiyoshi Yamada, Tadashi Fuyuki, Satoshi Akiyama, Yoshiaki Hamada, Eisuke Kuroda, Tadakatsu Nabeya, Yukio Sumita, Kenichi Kimura
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Patent number: 5478522Abstract: The present invention relates to a method for manufacturing a heating element, the method including the steps of: a) providing powders of two metals; b) mixing the powders; c) grinding the mixed powders; d) compacting the mixed powders to form a green compact; e) sintering the green compact in a first atmosphere; f) plastically working and process annealing the green compact; g) etching a surface of the green compact to cause pores thereon; and h) sintering the etched green compact in an oxidizing atmosphere. A Ni-Cr heating element manufactured by the present method has improved high temperature properties and a fusion temperature 300.degree. C. greater than those of conventional Ni-Cr heating elements.Type: GrantFiled: November 15, 1994Date of Patent: December 26, 1995Assignee: National Science CouncilInventor: S. Wang
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Patent number: 5476632Abstract: A process of forming a sintered article of powder metal comprising: selecting elemental iron powder; determining the desired properties of said sintered article and selecting, a quantity of carbon, and ferro alloy from the group of ferro manganese, ferro chromium, ferro molybdenum, ferro vanadium, ferro silicon and ferro boron; grinding said ferro alloy to a mean particle size of approximately 8 to 12 microns; introducing a lubricant while blending the carbon, ferro alloy, with said elemental iron powder; pressing the mixture to form the article; and then high temperature sintering the article at a temperature between 1,250.degree. C. and 1,350.degree. C. in a neutral or reducing atmosphere; so as to produce the sintered article of powdered metal; and includes the product formed thereby.Type: GrantFiled: January 14, 1994Date of Patent: December 19, 1995Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones
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Patent number: 5472662Abstract: A method for manufacturing a stator for an ultrasonic motor, wherein the stator includes a circular land portion, a plurality of teeth secured to the land portion by a plurality of radial slits, the method comprising the steps of: compressing fine metal particle to form a pre-compression body having a predetermined shape, whereby said pre-compression body is provided with a plurality of projections for forming a plurality of teeth of the stator; baking said pre-compression body, for producing a sintered body; applying a densification process on the teeth of said sintered body produced in said baking step, whereby each of said teeth is provided with a high dense portion having a density ratio of at least 90%; and applying a sizing process to said sintered body produced in said baking step.Type: GrantFiled: May 17, 1994Date of Patent: December 5, 1995Assignee: Asmo Co., Ltd.Inventors: Motoyasu Yano, Yoshinori Takemura, Takao Suzuki
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Patent number: 5466276Abstract: A secondary hardening type high temperature wear-resistant sintered alloy body comprising 0.4 to 15 wt. % of at least one species of metal carbide forming element which is selected from the group consisting of W, Mo, V, Ti, Nb, Ta and B; 5 to 35 wt. % of at least one species of austenite forming element which is selected from the group consisting of Ni, Co, Cu, and Cr; 0.2 to 1.2 wt. % of C; and 0.04 to 0.2 wt. % of Al consisting essentially the remainder of Fe, wherein the alloy body contains an austenite phase which is capable of martensitic transformation.Type: GrantFiled: July 7, 1993Date of Patent: November 14, 1995Assignees: Honda Giken Kogyo Kabushiki Kaisha, Nippon Piston Ring Co., Ltd.Inventors: Katsuaki Sato, Katsuhiko Tominaga, Tsutomu Saka, Osamu Kawamura, Teruo Takahashi, Arata Kakiuchi
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Patent number: 5464520Abstract: Silicide targets for sputtering which have an area ratio of silicon phases that appear on the sputter surface of no more than 23%, and a density of at least 99%, with a deformed layer partly removed from the surface to attain a surface roughness of from more than 0.05 .mu.m to 1 .mu.m, preferably with the number of coarse silicon phases at least 10 .mu.m in diameter that appear on the sputter surface being at most 10/mm.sup.2. The reduction of early-stage particle generation, in turn, reduces secondary particle generation, thus realizing the reduction of particle generation at both early stage and stabilized stage. A Si powder having a maximum particle diameter of no more than 20 .mu.m is mixed with a metal powder having a maximum particle diameter of no more than 60 .mu.m, in a rather Si-lower mixing ratio. A silicide powder is synthesized from the mixture and hot pressed, the sintered compact being machined and surface treated for the removal of the deformed layer.Type: GrantFiled: July 19, 1993Date of Patent: November 7, 1995Assignee: Japan Energy CorporationInventors: Osamu Kano, Koichi Yasui, Yasuyuki Sato, Yasuhiro Yamakoshi, Junichi Anan, Hironori Wada, Akio Yasuoka
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Patent number: 5460776Abstract: The invention relates to a method of producing connected sintered articles obtained by breaking a unitary preform.It is characterized in that:a) a preform is pressed from powdered metals while imprinting in it a superficial groove (3) located in a plane for the purpose of subsequent breakage,b) this preform is presintered in order to consolidate it mechanically, the preform however remaining brittle,c) it is optionally compacted by recompression,d) recesses for the members for the mechanical connection of the final parts are optionally machined in this preform,e) this preform is broken into at least two parts,f) final sintering is carried out,g) the articles are cooled.The invention is applicable in particular to the production of connecting rods and connecting rod covers or of annular articles with or without an undercut (broken in the axial plane).Type: GrantFiled: October 26, 1994Date of Patent: October 24, 1995Assignee: SintertechInventors: Luc Ackermann, Henri Gueydan
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Patent number: 5455001Abstract: A method for manufacturing an intermetallic compound comprises (a) preparing a powder, (b) canning said powder in a tube, (c) executing a first heat treatment to said tube-canned powder, and (d) treating said tube-canned powder for obtaining an intermetallic compound. This invention offers a simple, efficient, and inexpensive method for producing an intermetallic compound possessing excellent mechanical properties.Type: GrantFiled: July 7, 1994Date of Patent: October 3, 1995Assignee: National Science CouncilInventor: Chen-Ti Hu
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Patent number: 5445787Abstract: The process of forming an extruded product of tantalum or niobium requires a cold isostatic pressing of a charge of the powder to a density sufficient to form a green compact which is then placed in a capsule. The capsule is then sealed and heated to a temperature and for a time sufficient to anneal the green compact. Thereafter, the capsule and encapsulated compact are subjected to a cold isostatic pressing to achieve a density of from 70% to 85%. This is followed by subsequent heating and extrusion of the heated capsule and encapsulated compact to form the extruded product. The outer layer on the capsule which has been formed by the capsule material can be removed, as by pickling, in the case of the capsule being a carbon steel.Type: GrantFiled: November 2, 1993Date of Patent: August 29, 1995Inventors: Ira Friedman, Christer Aslund
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Patent number: 5439499Abstract: A cermet useful in the fabrication of metal cutting, rockdrilling and mineral tools, as well as wear parts. The cermet comprises (i) a hard phase of a simple boride of a transition metal, a mixture of simple borides of transition metals, or a mixed boride of transition metals; (ii) a binder phase of Fe, Ni, Co, Cr, or alloys thereof; (iii) a dispersion of particles of oxides of transition metals in which the oxygen can be replaced by nitrogen and/or carbon; and (iv) a dispersion of oxides of metals chosen from aluminum and Group IIA and IIIA metals.Type: GrantFiled: February 26, 1993Date of Patent: August 8, 1995Assignee: Sandvik ABInventors: Henri Pastor, Colette Allibert, Laurent Ottavi, Manuel Albajar, Francisco Castro-Fernandez
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Patent number: 5439637Abstract: Brazed structures are disassembled with little or no physical damage to the components by coating the brazed joints with a powdered wicking agent, preferably mixed with a fugitive liquid binder to form an adherent slurry, then heating the joint to allow the brazing alloy to melt and be drawn into the powdered wicking agent by capillary action. After cooling, the powder and braze alloy are mixed together to form a loosely consolidated mass which can be readily removed by mechanical and/or chemical means so that the components can then be separated for repair or reuse.Type: GrantFiled: July 20, 1994Date of Patent: August 8, 1995Assignee: Pyromet Group, Inc.Inventor: Craig R. Moyer
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Patent number: 5427734Abstract: The object of the invention is to provide a manufacturing method of a complex shaped R--Fe--B type sintered anisotropic magnet improved the moldability of injection molding and preventing the reaction between R ingredients and binder and controlled the degradation of magnetic characteristics due to residual carbon and oxygen. Utilizing the R--Fe--B type alloy powder or the resin coated said alloy powder, and methylcellulose and/or agar and water, instead of the usual thermoplastic binder, it is mixed and injection molded. The molded body is dehydrated by the freeze vacuum dry method to control the reaction between R ingredients and of the R--Fe--B alloy powder and water; furthermore, by administering the de-binder treatment in the hydrogen atmosphere, and sintering it after the dehydrogen treatment, residual oxygen and carbon in the R--Fe--B sintered body is drastically reduced, improving the moldability during the injection molding to obtain a three dimensionally complex shape sintered magnet.Type: GrantFiled: June 24, 1993Date of Patent: June 27, 1995Assignee: Sumitomo Special Metals Co., Ltd.Inventors: Osamu Yamashita, Masahiro Asano, Tsunekazu Saigo
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Patent number: 5358684Abstract: The friction lining for disk brakes comprises a carrier plate (10) and a block (16) of a compressed friction material secured to the latter, wherein the carrier plate, on the side bearing the block of friction material, is provided with a sinter-fused mounting bed (12) for the block of friction material of individual shaped members (13) forming frictional and positive connections with the block of friction material, in which, prior to the block of friction material is pressed onto the carrier plate (10) with the mounting bed sinter-fused thereupon, a galvanically, thermally or in some other suitable way produced metallic coating (50) is applied to the carrier plate as a corrosion protection.Type: GrantFiled: August 19, 1992Date of Patent: October 25, 1994Assignee: Jurid Werke GmbHInventor: Wolfgang Valentin
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Patent number: 5310520Abstract: Discrete powder particles of copper 14 and INVAR 12 are mixed together in a container 16 and packed into a powder metal article. This article is hot vacuum degassed and vacuum sealed and then heated to temperature well below the sintering temperature of copper or INVAR. Immediately after heating the article, it is subjected to a high pressure, high strain force such as extrusion through a die thereby yielding a fully dense, strong composite material 10 with excellent combined thermal expansion and conductivity properties.Type: GrantFiled: January 29, 1993Date of Patent: May 10, 1994Assignee: Texas Instruments IncorporatedInventors: Sunil C. Jha, James A. Forster, Henry F. Breit
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Patent number: 5298052Abstract: An Ni-based bearing alloy consisting, by weight, of 9-30% Cr, 5-19% Fe, 0.1-1.5% Si, 2-22% Co, 1.4-11.0% Mo, and the balance Ni and incidental impurities, said alloy having a matrix in which hard particles of a Co-Mo-Cr-Si alloy and/or BN are uniformly dispersed in weight ratios of 5 to 35% and not more than 5.0, respectively. The Ni-based alloy matrix provides superior heat resistance. Hard particles of Co-Mo-Cr-Si alloy uniformly dispersed in the matrix improve sliding characteristic with or without uniform dispersion of Bn as a solid lubricant, whereby the bearing alloy exhibits superior heat resistance and sliding characteristic when used in high temperature oxidizing atmosphere.Type: GrantFiled: June 11, 1992Date of Patent: March 29, 1994Assignee: Daido Metal Company, Ltd.Inventors: Tadashi Tanaka, Masaaki Sakamoto, Koichi Yamamoto, Kenji Sakai
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Patent number: 5286323Abstract: An dome-shaped extrusion die for use in forming honeycomb monolith structures is disclosed. The die is formed by deforming an extrusion die having a flat cross section to obtain a dome-shaped cross section. Alternatively, the die may be fabricated from sinterable ceramic or metal powders in which case the holes and slots may be formed either in the green state, or in a chalk-hard state after partial densification.Type: GrantFiled: February 23, 1993Date of Patent: February 15, 1994Assignee: Corning IncorporatedInventor: Rodney D. Bagley
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Patent number: 5252288Abstract: Method for producing an elongated sintered article, characterized by the steps including filling powder material in a pipe, carrying out plastic deformation of the pipe filled with the powder material, and heating the pipe filled with the powder material to burn and/or sinter the powder material.The method of the present invention is advantageously applicable to production of wire or rod of ceramics, particularly so called new ceramics or fine ceramics, sintered alloys or their combination, which are difficult to shape or mold by conventional process such as wire-drawing, rolling or extrusion of powder material which is difficult to mold and machine after the powder material is sintered.Type: GrantFiled: May 15, 1992Date of Patent: October 12, 1993Assignee: Sumitomo Electric Industries, Inc.Inventors: Susumu Yamamoto, Teruyuki Murai, Nozomu Kawabe, Masaaki Tobioka
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Patent number: 5207821Abstract: Disclosed is a sintered alloy composition and method of manufacturing the same, the sintered alloy composition having a multi-phase structure, comprising: a first phase composed of aluminum and copper; and a second phase being dispersed in the first phase and composed of molybdenum, chromium, silicon and cobalt. This alloy composition has excellent abrasion and corrosion resistance, preferably to be used for making machine parts such as valve seats for engines.Type: GrantFiled: July 9, 1991Date of Patent: May 4, 1993Assignees: Hitachi Powdered Metals Co., Ltd., Honda Giken Kogyo Kabushiki KaishaInventors: Yutaka Ikenoue, Keitaro Suzuki, Yoshimasa Aoki, Hideo Urata, Koji Koishikawa, Makoto Tsuji
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Patent number: 5194219Abstract: Very good masking of pack diffusion aluminizing or chromizing on any metal to keep portions from being diffusion coated, is effected by localized coating the lowest layer of which is depletion-reducing masking powder the metal portion of which can have same composition as substrates, mixed with inert refractory diluent and non-contaminating film-former such as acrylic resin. The upper coating layer can be of non-contaminating particles like nickel or Cr.sub.2 O.sub.3 that upon aluminizing or chromizing become coherently held together to form a secure sheath. Such sheath can also be used for holding localized diffusion-coating layer in place. Film-former can be dissolved in volatile solvent, preferably methyl chloroform, in which masking powder or sheath-forming powder is suspended. Chromizing can be performed before aluminizing for greater effects. Aluminizing of metals like iron and nickel followed by leaching out much of the diffused-in aluminum, gives these substrates a pyrophoric and catalytic surface.Type: GrantFiled: July 7, 1992Date of Patent: March 16, 1993Assignee: Alloy Surfaces Company, Inc.Inventor: Alfonso L. Baldi
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Patent number: 5182078Abstract: Diffusion coating can be speeded by high heat input. Diffusion coating packs can be made with chemically reduced metal content of sludges. Diffusion aluminizing followed by caustic leaching to remove much of the diffused-in aluminum, yields catalytically and pyrophorically active porous surface that also accepts top coatings. Mixtures of aluminum powder with nickel and/or iron powders react when heated to form Raney-like product that can be leached to become pyrophoric, and when held on a metal foil or gauze web will adhere to the web so that leached product can be used as pyrophoric foil for decoying heat-seeking missiles. Such adhesion is improved by addition of small amount of copper.Type: GrantFiled: June 6, 1990Date of Patent: January 26, 1993Assignee: Alloy Surfaces Company, Inc.Inventor: Alfonso L. Baldi
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Patent number: 5152828Abstract: The present invention relates to a method of producing a mold material used for obtaining a mold for casting metals such as Zn, Al and the like or molding resins. In the method, the short fibers having an aspect ratio of 30 to 300 and obtained by cutting ferritic stainless steel long fibers having a width of 100 .mu.m or less, ferritic stainless steel powder and at least one of Cu powder and Cu alloy powder are used as raw materials. The raw materials are blended to obtain a material mixture which is then compressed under pressure in a Cold Isostatic Press process. The thus obtained compressed product is sintered in a vacuum atmosphere. The sintered material is held in an atmosphere of nitrogen gas or decomposed ammonia gas so that 0.3 to 1.2 wt % of nitrogen is added to the stainless steel in the sintered material. The thus obtained mold material has a hardness of HMV 250 to 500.Type: GrantFiled: October 8, 1991Date of Patent: October 6, 1992Assignee: Sintokogio Ltd.Inventor: Tatsuhiko Katoh
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Patent number: 5130084Abstract: A method and apparatus are disclosed for fabrication of hollow articles by hot consolidation of metal alloy powder between a hollow core and a fluid pressure resistant outer shell. The hollow core is formed, a disposable layer is applied to define the object contour, a fluid pressure resistant metallic layer is formed over the disposable layer, which is then melted, removed and replaced by the metal alloy powder, and this assembly is hot isostatically pressed. The powder and core materials are preferably selected to be metallurgically compatible, so the core becomes an integral part of the finished article. The hollow article is inflated in a form die to establish the finished article contour.Type: GrantFiled: December 24, 1990Date of Patent: July 14, 1992Assignee: United Technologies CorporationInventors: A. Paul Matheny, Paul M. Buxe
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Patent number: 5126104Abstract: A method is disclosed for preparing an intimate mixture of powders of nickel-chromium-boron-silicon alloy, molybdenum metal powder, and Cr.sub.3 C.sub.2 /NiCr alloy suitable for thermal spray coatings which comprises milling a starting mixture of the above two alloys with molybdenum powder to produce a milled mixture wherein the average particle size is less than about 10 micrometers in diameter, forming an aqueous slurry of the resulting milled mixture and a binder which can be an ammoniacal molybdate compound or polyvinyl alcohol, and agglomerating the milled mixture and binder. The intimate mixture and binder may be sintered in a reducing atmosphere at a temperature of about 800.degree. C. to 950.degree. C. for a sufficient time to form a sintered partially alloyed mixture wherein the bulk density is greater than about 1.2 g/cc.Type: GrantFiled: June 6, 1991Date of Patent: June 30, 1992Assignee: GTE Products CorporationInventors: Vidhu Anand, Sanjay Sampath, David L. Houck, Jack E. Vanderpool
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Patent number: 5110543Abstract: A blade member for cutting-tools includes a cermet substrate which contains, apart from unavoidable impurities, a binder phase and a hard dispersed phase. The binder phase contains 5% to 30% by weight of cobalt and/or nickel. The hard dispersed phase contains a balance composite carbonitride of titanium and one or more of the elements tungsten, molybdenum, tantalum, niobium, hafnium and zirconium. The composite carbo-nitride satisfies the relationship 0.2.ltoreq.b/(a+b).ltoreq.0.7, where a and b denote atomic ratios of carbon and nitrogen, respectively. The substrate includes a hard surface layer in which the maximum hardness is present at a depth between 5 .mu.m and 50 .mu.m from a substrate surface thereof. The substrate surface has a hardness of 20% to 90% of the maximum hardness.Type: GrantFiled: July 19, 1991Date of Patent: May 5, 1992Assignee: Mitsubishi Metal CorporationInventors: Niro Odani, Kazuyoshi Yoshioka, Sinichi Sekiya
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Patent number: 5082433Abstract: Molded articles, particularly cams for camshafts of internal combustion engines, are subjected to high wear conditions. In order to make them resistant to wear, they are produced from a sintered alloy, which has been fabricated by powder metallurgical means. The alloy has a hardened matrix with interstitial copper and consists of 0.5 to 16% by weight of molybdenum, 1 to 20% by weight of copper, 0.1 to 1.5% by weight of carbon and, optionally, of admixtures of chromium, manganese, silicon and nickel totalling, at most, 5% by weight, the remainder being iron.Type: GrantFiled: December 17, 1990Date of Patent: January 21, 1992Assignee: Etablissement SupervisInventor: Karl Leithner
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Patent number: 5063021Abstract: A method is disclosed for preparing an intimate mixture of powders of nickel-boron-silicon alloy and molybdenum metal powder suitable for thermal spray coatings which comprises milling a starting mixture of the alloy and molybdenum powder to produce a milled mixture wherein the average particle size is less than about 10 micrometers in diameter, forming an aqueous slurry of the resulting milled mixture and a binder which can be an ammoniacal molybdate compound or polyvinyl alcohol, and agglomerating the milled mixture and binder. The intimate mixture and binder are preferably sintered in a reducing atmosphere at a temperature of about 800.degree. C. to about 950.degree. C. for a sufficient time to form a sintered partially alloyed mixture wherein the bulk density is greater than about 1.2 g/cc.Type: GrantFiled: May 23, 1990Date of Patent: November 5, 1991Assignee: GTE Products CorporationInventors: Vidhu Anand, Sanjay Sampath, Clarke D. Davis, David L. Houck
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Patent number: 5059489Abstract: A structure comprising a mixture of metals and metal alloys which are sintered into a hard porous body is presented. The structure can be useful for many different chemical and physical purposes, such as for catalysis, desorption and absorption, and selective leaching of the structure components into solutions.Type: GrantFiled: July 15, 1988Date of Patent: October 22, 1991Assignee: Corning IncorporatedInventors: Charles Q. Buckwalter, Jr., Irwin M. Lachman, Mallanagouda D. Patil, Jimmie L. Williams
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Patent number: 5045276Abstract: An injection molded powder metallurgy product of highly satisfactory quality is obtained by a method which comprises injection molding mixture obtained by kneading a metal powder with a binder, depriving the molded mass of the binder while keeping the molded mass at least in contact with ceramic powder, projecting beads on the molded mass free from the binder, and thereafter sintering the molded mass studded with the beads.Type: GrantFiled: October 11, 1990Date of Patent: September 3, 1991Assignee: Sumitomo Metal Mining Company LimitedInventor: Yoshio Kijima
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Patent number: 5032353Abstract: Structural components of at least one intermetallc compound and having complicated contours, are made by the steps of preparing a powder mixture of elemental metal powders including at least one powder of a low melting metal element or component and one powder of a high melting metal element or component that subsequently are to form the intermetallic compound. The powder mixture is then sintered to form a sintered body which is machined to a contour close to the finished contour and to dimensions close to the final dimensions. The so machined and shaped part is enveloped with an envelope of the high melting metal element or component. The enveloped part is subjected to a hot isostatic reaction pressing whereby the intermetallic compound is formed.Type: GrantFiled: October 26, 1990Date of Patent: July 16, 1991Assignee: MTU Motoren-und Turbinen-Union Muenchen GmbHInventors: Wilfried Smarsly, Raimund Lackermeier
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Patent number: 5015440Abstract: Light weight refractory aluminides, such as Al.sub.3 Nb and related aluminides may be produced from metallic powders by a high temperature exothermic reaction of refractory metals with molten aluminum. Mixtures of refractory metals and aluminum may be prepared and densified by powder metalurgy techniques. Applicant's process permits near net formations of stock shapes and parts by conducting the reaction in situ in a die.Type: GrantFiled: September 1, 1989Date of Patent: May 14, 1991Assignee: McDonnell Douglas CorporationInventor: David M. Bowden