Post Sintering Operation Patents (Class 419/26)
  • Patent number: 5940675
    Abstract: Powder metallurgy production of T222 alloy affording properties comparable to melt derived T222, but at higher yields and lower costs, is enabled by blending component powders of minus 325 mesh and sintering at 2,400.degree. C. in three sinter steps and utilizing a slow ramp up in the first sinter step and cold isostatic pressing prior to the first sinter step and isostatic press densification in conjunction with at least the first sinter step.
    Type: Grant
    Filed: December 24, 1997
    Date of Patent: August 17, 1999
    Assignee: H. C. Starck, Inc.
    Inventors: Robert W. Balliett, Trung Luong
  • Patent number: 5930581
    Abstract: The invention is a complex-shaped article, comprising an article prepared by joining at least one multi-phase ceramic-metal part and at least one shaped part of another material, wherein the theoretical density of the at least one ceramic-metal part is greater than 80 percent.In another aspect, the invention is a process for preparing complex-shaped articles, comprising:(a) forming at least one ceramic-metal part;(b) forming at least one shaped part of another material; and(c) joining the at least one shaped ceramic-metal part with the at least one shaped part of another material such that a complex-shaped article is formed.The invention is a less costly and time-consuming process for preparing complex-shaped composite articles wherein the articles are formed of two or more selected materials wherein one of the materials is a ceramic-metal composite.
    Type: Grant
    Filed: December 24, 1996
    Date of Patent: July 27, 1999
    Assignee: The Dow Chemical Company
    Inventors: David W. Born, Richard T. Fox, Donald J. Perettie
  • Patent number: 5925837
    Abstract: A manufacturing method and products of metallic friction materials includes processes of 1. preparing powder materials, 2. mixing copper as a base, proper proportion of iron powder or steel wool, aluminum powder, zinc or tin or lead powder, graphite powder and alumina or silicon dioxide powder, 3. pressing mixed materials into green bodies under 375.about.625 MPa at room temperature, 4. pre-heat treating the green bodies in an air furnace with temperature raised to 100.about.300.degree. C. for 1.about.3 hours, 5. sintering the green bodies into test samples under 350.about.750 MPa for 24.about.60 hours to gain sintered friction materials having an oxidized layer of less than 1 mm thick, 6. processing and grinding the sintered test samples with grinders to remove the oxidized layer, 7. washing the outer surface of the sintered test samples ground into finished products. The method of the invention may reduce largely difficulty in manufacturing processes, the investment and productive cost.
    Type: Grant
    Filed: September 16, 1998
    Date of Patent: July 20, 1999
    Assignees: Chien-Ping Ju, Jiin-Huey Chen Lin
    Inventors: Chien-Ping Ju, Jiin-Huey Chen Lin, Sun-Zen Chen
  • Patent number: 5897830
    Abstract: A consumable billet for melting and casting a metal matrix composite component is made of a consolidated powder metal matrix composite having a titanium or titanium alloy matrix reinforced with particles. The preferred billet is a blended and sintered powder metal composite billet incorporating titanium carbide or titanium boride into a Ti--6Al--4V alloy.
    Type: Grant
    Filed: December 6, 1996
    Date of Patent: April 27, 1999
    Assignee: Dynamet Technology
    Inventors: Stanley Abkowitz, Susan M. Abkowitz, Paul F. Weihrauch, Harold L. Heussi, Walter Zimmer
  • Patent number: 5856032
    Abstract: A cermet including a cermet core zone in which the content of a binder amounts to at most 90% by mass in relationship to a cermet hard phase is formed with a 0.01 to 3 um deep surface layer having an increased resistance to wear compare to the cermet core zone.
    Type: Grant
    Filed: September 30, 1996
    Date of Patent: January 5, 1999
    Assignee: Widia GmbH
    Inventors: Hans Werner Daub, Klaus Dreyer
  • Patent number: 5841041
    Abstract: A porous mold material is provided that contains pores for ventilation in a metal casting, which pores range from 20 to 50 microns, and wherein the porosity value of the porous mold material ranges from 25 to 35% by volume. A method is further provided of producing a porous mold material that contains pores ranging from 20 to 50 microns for ventilation in casting, which method is characterized in that the mixing ratio of stainless steel particles to stainless steel short fibers is from 40 wt %:60 wt % to 65 wt %:35 wt %. The porous mold material of this invention does not have defects such as the inferior fluidity of a molten metal in the mold, or the shrinkage and blowholes in cast products.
    Type: Grant
    Filed: September 18, 1996
    Date of Patent: November 24, 1998
    Assignee: Sintokogio, Ltd.
    Inventors: Norihiro Asano, Tatsuhiko Kato
  • Patent number: 5814272
    Abstract: A method for forming dendritic metal powders, comprising the steps of: (1) heating a powder comprising non-dendritic particles, under conditions suitable for initial stage sintering, to form a lightly sintered material; and (2) breaking the lightly sintered material to form a powder comprising dendritic particles. In one embodiment, the lightly sintered material is broken by brushing the material through a screen. Another aspect of the present invention comprises the dendritic particles that are produced by the method described above. These particles can comprise any suitable metal, such as transition metals, rare earth metals, main group metals or metalloids or an alloy of two or more such metals. The particles can also comprise a ceramic material, such as a metal oxide. These particles are characterized by a dendritic, highly anisotropic, morphology arising from the fusion of substantially non-dendritic particles, and by a low apparent density relative to the substantially non-dendritic starting material.
    Type: Grant
    Filed: February 21, 1996
    Date of Patent: September 29, 1998
    Assignee: Millipore Corporation
    Inventors: Robert S. Zeller, Christopher J. Vroman
  • Patent number: 5815790
    Abstract: The invention relates to a method for the manufacturing of a composite metal product. More particularly, the invention relates to a method for the manufacturing of a composite product consisting of at least two stainless steel materials having different chemical compositions, particularly a composite stainless product on which decorative patterns can or has been produced by etching.It is significant feature of the invention that at least two stainless steel materials having different chemical compositions are bonded together through hot isostatic compaction at a pressure exceeding 600 bar and a temperature exceeding 1000.degree. C., at least one of said materials consisting of powder, for the achievement of a consolidated body.
    Type: Grant
    Filed: December 4, 1996
    Date of Patent: September 29, 1998
    Assignee: Soderfors Powder Aktiebolag
    Inventors: Per Billgren, Kaj Embretsen
  • Patent number: 5808213
    Abstract: Silver-iron materials for electrical switching contacts with properties which come very close to those of silver-nickel materials formed of 4.6 to 15% by weight iron and 0.05 to 5% by weight of one or more of the oxides magnesium oxide, calcium oxide, yttrium oxide, lanthanum oxide, cerium oxide, chromium oxide, iron oxide, aluminum oxide, indium oxide, silicon oxide, and tin oxide, the balance being silver.
    Type: Grant
    Filed: November 19, 1996
    Date of Patent: September 15, 1998
    Assignee: Degussa Aktiengesellschaft
    Inventors: Wolfgang Weise, Willi Malikowski, Roger Wolmer, Peter Braumann, Andreas Koffler
  • Patent number: 5758253
    Abstract: A process for producing sintered titanium-graphite having improved wear resistance and low frictional characteristics is described. The said process which produces titanium-graphite composites having a triphasic structure with controlled porosity and a graphite lubricating film, comprises sintering a mixture of titanium and graphite powders in which the percentage of graphite may vary from 4 to 8 percent at temperatures from about 800.degree. C. to 1600.degree. C., for about 1/2 to 2 hours, under a compaction pressure of 0.17 to 0.62 MPa. The composites have applications in biomedical engineering and other fields of engineering due to their biocompatibility, strength and improved wear resistance.
    Type: Grant
    Filed: October 7, 1996
    Date of Patent: May 26, 1998
    Assignee: National University of Singapore
    Inventors: Swee Hin Teoh, Rajendran Thampuran, James Cho Hong Goh, Winston Kar Heng Seah
  • Patent number: 5752155
    Abstract: A method of producing a cutting insert which includes the steps of: providing a generally homogeneous powder blend of powder components; forming the powder blend into a green body wherein the green body includes a rake face and a flank face with a cutting edge at the juncture of the rake face and the flank face; honing the cutting edge of the green body; and consolidating the green body with the honed cutting edge so as to form a consolidated body with a honed cutting edge.
    Type: Grant
    Filed: October 21, 1996
    Date of Patent: May 12, 1998
    Assignee: Kennametal Inc.
    Inventors: Alfred S. Gates, Jr., Bernard North, William R. Shaffer
  • Patent number: 5729823
    Abstract: The present invention relates to a cemented carbide insert, comprising a cemented carbide substrate and a coating. The substrate contains WC and cubic carbonitride phase in a binder phase based of Co and/or Ni and has a binder phase enriched surface zone essentially free of cubic phase. The binder phase enriched surface zone prevails over the edge. As a result, an insert according to the invention has improved edge toughness and resistance against plastic deformation and is particularly useful for machining of sticky work piece materials such as stainless steel.
    Type: Grant
    Filed: March 14, 1996
    Date of Patent: March 17, 1998
    Assignee: Sandvik AB
    Inventors: Per Gustafson, Leif kesson
  • Patent number: 5728194
    Abstract: Silver-iron materials for electrical switching contacts with properties which come very close to those of silver-nickel materials formed of 0.5 to 20% by weight iron 0.5 to 5% by one or more of the elements rhenium, iridium, and ruthenium, and 0.05 to 2% by weight of one or more of the oxides magnesium oxide, calcium oxide, yttrium oxide, lanthanum oxide, titanium oxide, zirconium oxide, hafnium oxide, cerium oxide, niobium oxide, tantalum oxide, chromium oxide, manganese oxide, iron oxide, zinc oxide, copper oxide, aluminum oxide, indium oxide, silicon oxide, and tin oxide, the balance being silver.
    Type: Grant
    Filed: November 19, 1996
    Date of Patent: March 17, 1998
    Assignee: Degussa Aktiengesellschaft
    Inventors: Wolfgang Weise, Willi Malikowski, Roger Wolmer, Peter Braumann, Andreas Koffler
  • Patent number: 5722034
    Abstract: A method of manufacturing a high-purity refractory metal or a an alloy based thereon, said refractory metal being selected from the group consisting of niobium, rhenium, tantalum, molybdenum, and tungsten, comprising the steps of compacting a mixed material, in the form of powders or small lumps, of a refractory metal or alloy to be refined together with one or two or more additive elements selected from the group of transition metal elements consisting of vanadium, chromium, manganese, iron, cobalt and nickel, and from the group of rare earth elements, sintering the resulting compact at a high temperature of at least 1000.degree. C. and a high pressure of at least 100 MPa, thereby forming a lower compound or nonstoichiometric compound between at least a part of the additive element or elements and the impurity gas ingredient element such as O, N, C, and H, contained in the refractory metal or alloy to be refined, and thereafter electron-beam melting the sintered body.
    Type: Grant
    Filed: December 5, 1995
    Date of Patent: February 24, 1998
    Assignee: Japan Energy Corporation
    Inventor: Syozo Kambara
  • Patent number: 5701575
    Abstract: An article essentially consisting of one or more of Ti--Al intermetallic compounds is fabricated so as to have a volume ratio of voids no more than 3.5%, by preparing a mixture of materials selected from a group consisting of Ti, Ti alloys, Al, Al alloys, and Ti--Al compounds, having a composition suitable for forming a desired Ti--Al intermetallic compound, and heating said mixture so that said mixture may be sintered. Typically, the temperature and pressure for the heating or sintering process is appropriately selected so that the desired porosity may be obtained. The mechanical strength of an article according to the present invention is not only improved but is highly predictable, or, in other word, highly reliable. The fabrication costs can be reduced because the fabrication process involves only relatively low temperatures when pressing and heating the work at the same time.
    Type: Grant
    Filed: January 11, 1996
    Date of Patent: December 23, 1997
    Assignee: NHK Spring Co., Ltd.
    Inventors: Kohei Taguchi, Michihiko Ayada, Hideo Shingu
  • Patent number: 5701574
    Abstract: A method of producing a sliding sleeve for a synchronizer of a speed-changing gear, the sliding sleeve being comprised of a sintered powder metal compact having a claw extending along an inner periphery of the sleeve, and the claw consisting of teeth having opposite end faces and a cross-section between the end faces which is reduced relative to an undercut portion at at least one of the end faces, which method comprises the steps of sintering the powder metal compact having the claw consisting of the teeth having the opposite end faces and the reduced cross-section extending between the end faces, and then applying solely an axial upsetting force to the one end face to form the undercut portion thereat while leaving the reduced cross-section unchanged.
    Type: Grant
    Filed: February 6, 1996
    Date of Patent: December 23, 1997
    Assignee: Miba Sintermetall Aktiengesellschaft
    Inventors: Karl Derflinger, Herbert Schmid, Johann Dickinger
  • Patent number: 5698008
    Abstract: A contact material for a vacuum valve including, a conductive constituent including at least copper, an arc-proof constituent including at least chromium and an auxiliary constituent including at least one selected from the group consisting of tungsten, molybdenum, tantalum and niobium. The contact material is manufactured by quench solidification of a composite body of the conductive constituent, the arc-proof constituent and the auxiliary constituent.
    Type: Grant
    Filed: February 21, 1995
    Date of Patent: December 16, 1997
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Tsuneyo Seki, Tsutomu Okutomi, Atsushi Yamamoto, Takashi Kusano
  • Patent number: 5678163
    Abstract: The present invention relates to an improved method of manufacturing an airbag initiator. Currently, an airbag initiator is comprised of three parts made out of two dissimilar materials plus a glass to metal seal. The present method builds the same airbag initiator with the body and the pins in one piece via a process called metal injection molding. The part is then placed in a furnace to remove a wax binder, then the temperature is ramped up slowly to remove a thermoplastic layer, and the temperature is further ramped up to form a sintered part. The sintered part being equal to or better than standards of wrought material. The initiator is then removed from the furnace and a glass bead is placed in a void area in the body of the initiator. The glass is melted forming a glass to metal seal between a first pin and the body of the initiator. A top portion of the initiator is then lapped off isolating the first pin from the body of the initiator.
    Type: Grant
    Filed: August 10, 1995
    Date of Patent: October 14, 1997
    Inventor: Eldon D. Rice
  • Patent number: 5666634
    Abstract: The invention has for its object the provision alloy steel powders for Cr-based high strength sintered bodies having high tensile strength, fatigue strength and toughness which are adapted for use in parts for motor vehicles and parts for OA apparatus.The composition of the alloy steel powder comprises, by wt %, not larger than 0.1% of C, not larger than 0.08% of Mn, 0.5-3% of Cr, 0.1-2% of Mo, not larger than 0.01% of S, not larger than 0.01% of P, not larger than 0.2% of O, optionally one or more of 0.2.about.2.5% Ni, 0.5.about.2.5% Cu and the balance being inevitable impurities and Fe. The sintered body has substantially the same composition provided that the content of C alone is limited to 0.2-1.2%.The manufacturing method comprises molding the above alloy steel powder, sintering the resulting green compact at a temperature of 1100.degree.-1300.degree. C. and immediately cooling at a cooling rate of 10.degree.-200.degree. C./minute.
    Type: Grant
    Filed: December 23, 1994
    Date of Patent: September 9, 1997
    Assignee: Kawasaki Steel Corporation
    Inventors: Shigeru Unami, Osamu Furukimi
  • Patent number: 5618397
    Abstract: Metal silicide targets are provided for sputtering which have a density of at least 99%, no more than one coarse silicon phase 10 .mu.m or larger in size that appears, per square millimeter, on the sputter surface, and an oxygen content of at most 150 ppm. They are made by a method which comprises finely grinding a synthesized silicide powder, vacuum annealing the finely ground powder in a hot press die without the application of pressure, and thereafter compacting and sintering the compact to a density of at least 99% by hot pressing. Alternatively, the finely ground powder is vacuum annealed as a presintered body at a density ratio of 50 to 75%, and thereafter is compacted and sintered.
    Type: Grant
    Filed: April 17, 1995
    Date of Patent: April 8, 1997
    Assignee: Japan Energy Corporation
    Inventors: Osamu Kano, Yasuhiro Yamakoshi, Junichi Anan, Koichi Yasui
  • Patent number: 5536485
    Abstract: A powder of diamond or high-pressure phase boron nitride core particles charged into a coating space as it is dispersed, and a precursor of a coat forming substance allowed to contact and/or impinge against the particles in the powder of core particles so that their surfaces are covered with the coat forming substance, thereby preparing coated diamond or high-pressure phase boron nitride particles which are subsequently sintered. The thusly produced diamond of high-pressure phase boron nitride sinter is composed of coated core particles of high performance that are superhard, uniform, dense and sintered firmly, and which have a controlled microstructure.
    Type: Grant
    Filed: August 11, 1994
    Date of Patent: July 16, 1996
    Assignees: Agency of Industrial Science & Technology, Nisshin Flour Milling Co., Ltd., Reed Co., Ltd
    Inventors: Shoichi Kume, Haruo Yoshida, Yukiyoshi Yamada, Tadashi Fuyuki, Satoshi Akiyama, Yoshiaki Hamada, Eisuke Kuroda, Tadakatsu Nabeya, Yukio Sumita, Kenichi Kimura
  • Patent number: 5478522
    Abstract: The present invention relates to a method for manufacturing a heating element, the method including the steps of: a) providing powders of two metals; b) mixing the powders; c) grinding the mixed powders; d) compacting the mixed powders to form a green compact; e) sintering the green compact in a first atmosphere; f) plastically working and process annealing the green compact; g) etching a surface of the green compact to cause pores thereon; and h) sintering the etched green compact in an oxidizing atmosphere. A Ni-Cr heating element manufactured by the present method has improved high temperature properties and a fusion temperature 300.degree. C. greater than those of conventional Ni-Cr heating elements.
    Type: Grant
    Filed: November 15, 1994
    Date of Patent: December 26, 1995
    Assignee: National Science Council
    Inventor: S. Wang
  • Patent number: 5476632
    Abstract: A process of forming a sintered article of powder metal comprising: selecting elemental iron powder; determining the desired properties of said sintered article and selecting, a quantity of carbon, and ferro alloy from the group of ferro manganese, ferro chromium, ferro molybdenum, ferro vanadium, ferro silicon and ferro boron; grinding said ferro alloy to a mean particle size of approximately 8 to 12 microns; introducing a lubricant while blending the carbon, ferro alloy, with said elemental iron powder; pressing the mixture to form the article; and then high temperature sintering the article at a temperature between 1,250.degree. C. and 1,350.degree. C. in a neutral or reducing atmosphere; so as to produce the sintered article of powdered metal; and includes the product formed thereby.
    Type: Grant
    Filed: January 14, 1994
    Date of Patent: December 19, 1995
    Assignee: Stackpole Limited
    Inventors: Rohith Shivanath, Peter Jones
  • Patent number: 5472662
    Abstract: A method for manufacturing a stator for an ultrasonic motor, wherein the stator includes a circular land portion, a plurality of teeth secured to the land portion by a plurality of radial slits, the method comprising the steps of: compressing fine metal particle to form a pre-compression body having a predetermined shape, whereby said pre-compression body is provided with a plurality of projections for forming a plurality of teeth of the stator; baking said pre-compression body, for producing a sintered body; applying a densification process on the teeth of said sintered body produced in said baking step, whereby each of said teeth is provided with a high dense portion having a density ratio of at least 90%; and applying a sizing process to said sintered body produced in said baking step.
    Type: Grant
    Filed: May 17, 1994
    Date of Patent: December 5, 1995
    Assignee: Asmo Co., Ltd.
    Inventors: Motoyasu Yano, Yoshinori Takemura, Takao Suzuki
  • Patent number: 5466276
    Abstract: A secondary hardening type high temperature wear-resistant sintered alloy body comprising 0.4 to 15 wt. % of at least one species of metal carbide forming element which is selected from the group consisting of W, Mo, V, Ti, Nb, Ta and B; 5 to 35 wt. % of at least one species of austenite forming element which is selected from the group consisting of Ni, Co, Cu, and Cr; 0.2 to 1.2 wt. % of C; and 0.04 to 0.2 wt. % of Al consisting essentially the remainder of Fe, wherein the alloy body contains an austenite phase which is capable of martensitic transformation.
    Type: Grant
    Filed: July 7, 1993
    Date of Patent: November 14, 1995
    Assignees: Honda Giken Kogyo Kabushiki Kaisha, Nippon Piston Ring Co., Ltd.
    Inventors: Katsuaki Sato, Katsuhiko Tominaga, Tsutomu Saka, Osamu Kawamura, Teruo Takahashi, Arata Kakiuchi
  • Patent number: 5464520
    Abstract: Silicide targets for sputtering which have an area ratio of silicon phases that appear on the sputter surface of no more than 23%, and a density of at least 99%, with a deformed layer partly removed from the surface to attain a surface roughness of from more than 0.05 .mu.m to 1 .mu.m, preferably with the number of coarse silicon phases at least 10 .mu.m in diameter that appear on the sputter surface being at most 10/mm.sup.2. The reduction of early-stage particle generation, in turn, reduces secondary particle generation, thus realizing the reduction of particle generation at both early stage and stabilized stage. A Si powder having a maximum particle diameter of no more than 20 .mu.m is mixed with a metal powder having a maximum particle diameter of no more than 60 .mu.m, in a rather Si-lower mixing ratio. A silicide powder is synthesized from the mixture and hot pressed, the sintered compact being machined and surface treated for the removal of the deformed layer.
    Type: Grant
    Filed: July 19, 1993
    Date of Patent: November 7, 1995
    Assignee: Japan Energy Corporation
    Inventors: Osamu Kano, Koichi Yasui, Yasuyuki Sato, Yasuhiro Yamakoshi, Junichi Anan, Hironori Wada, Akio Yasuoka
  • Patent number: 5460776
    Abstract: The invention relates to a method of producing connected sintered articles obtained by breaking a unitary preform.It is characterized in that:a) a preform is pressed from powdered metals while imprinting in it a superficial groove (3) located in a plane for the purpose of subsequent breakage,b) this preform is presintered in order to consolidate it mechanically, the preform however remaining brittle,c) it is optionally compacted by recompression,d) recesses for the members for the mechanical connection of the final parts are optionally machined in this preform,e) this preform is broken into at least two parts,f) final sintering is carried out,g) the articles are cooled.The invention is applicable in particular to the production of connecting rods and connecting rod covers or of annular articles with or without an undercut (broken in the axial plane).
    Type: Grant
    Filed: October 26, 1994
    Date of Patent: October 24, 1995
    Assignee: Sintertech
    Inventors: Luc Ackermann, Henri Gueydan
  • Patent number: 5455001
    Abstract: A method for manufacturing an intermetallic compound comprises (a) preparing a powder, (b) canning said powder in a tube, (c) executing a first heat treatment to said tube-canned powder, and (d) treating said tube-canned powder for obtaining an intermetallic compound. This invention offers a simple, efficient, and inexpensive method for producing an intermetallic compound possessing excellent mechanical properties.
    Type: Grant
    Filed: July 7, 1994
    Date of Patent: October 3, 1995
    Assignee: National Science Council
    Inventor: Chen-Ti Hu
  • Patent number: 5445787
    Abstract: The process of forming an extruded product of tantalum or niobium requires a cold isostatic pressing of a charge of the powder to a density sufficient to form a green compact which is then placed in a capsule. The capsule is then sealed and heated to a temperature and for a time sufficient to anneal the green compact. Thereafter, the capsule and encapsulated compact are subjected to a cold isostatic pressing to achieve a density of from 70% to 85%. This is followed by subsequent heating and extrusion of the heated capsule and encapsulated compact to form the extruded product. The outer layer on the capsule which has been formed by the capsule material can be removed, as by pickling, in the case of the capsule being a carbon steel.
    Type: Grant
    Filed: November 2, 1993
    Date of Patent: August 29, 1995
    Inventors: Ira Friedman, Christer Aslund
  • Patent number: 5439499
    Abstract: A cermet useful in the fabrication of metal cutting, rockdrilling and mineral tools, as well as wear parts. The cermet comprises (i) a hard phase of a simple boride of a transition metal, a mixture of simple borides of transition metals, or a mixed boride of transition metals; (ii) a binder phase of Fe, Ni, Co, Cr, or alloys thereof; (iii) a dispersion of particles of oxides of transition metals in which the oxygen can be replaced by nitrogen and/or carbon; and (iv) a dispersion of oxides of metals chosen from aluminum and Group IIA and IIIA metals.
    Type: Grant
    Filed: February 26, 1993
    Date of Patent: August 8, 1995
    Assignee: Sandvik AB
    Inventors: Henri Pastor, Colette Allibert, Laurent Ottavi, Manuel Albajar, Francisco Castro-Fernandez
  • Patent number: 5439637
    Abstract: Brazed structures are disassembled with little or no physical damage to the components by coating the brazed joints with a powdered wicking agent, preferably mixed with a fugitive liquid binder to form an adherent slurry, then heating the joint to allow the brazing alloy to melt and be drawn into the powdered wicking agent by capillary action. After cooling, the powder and braze alloy are mixed together to form a loosely consolidated mass which can be readily removed by mechanical and/or chemical means so that the components can then be separated for repair or reuse.
    Type: Grant
    Filed: July 20, 1994
    Date of Patent: August 8, 1995
    Assignee: Pyromet Group, Inc.
    Inventor: Craig R. Moyer
  • Patent number: 5427734
    Abstract: The object of the invention is to provide a manufacturing method of a complex shaped R--Fe--B type sintered anisotropic magnet improved the moldability of injection molding and preventing the reaction between R ingredients and binder and controlled the degradation of magnetic characteristics due to residual carbon and oxygen. Utilizing the R--Fe--B type alloy powder or the resin coated said alloy powder, and methylcellulose and/or agar and water, instead of the usual thermoplastic binder, it is mixed and injection molded. The molded body is dehydrated by the freeze vacuum dry method to control the reaction between R ingredients and of the R--Fe--B alloy powder and water; furthermore, by administering the de-binder treatment in the hydrogen atmosphere, and sintering it after the dehydrogen treatment, residual oxygen and carbon in the R--Fe--B sintered body is drastically reduced, improving the moldability during the injection molding to obtain a three dimensionally complex shape sintered magnet.
    Type: Grant
    Filed: June 24, 1993
    Date of Patent: June 27, 1995
    Assignee: Sumitomo Special Metals Co., Ltd.
    Inventors: Osamu Yamashita, Masahiro Asano, Tsunekazu Saigo
  • Patent number: 5358684
    Abstract: The friction lining for disk brakes comprises a carrier plate (10) and a block (16) of a compressed friction material secured to the latter, wherein the carrier plate, on the side bearing the block of friction material, is provided with a sinter-fused mounting bed (12) for the block of friction material of individual shaped members (13) forming frictional and positive connections with the block of friction material, in which, prior to the block of friction material is pressed onto the carrier plate (10) with the mounting bed sinter-fused thereupon, a galvanically, thermally or in some other suitable way produced metallic coating (50) is applied to the carrier plate as a corrosion protection.
    Type: Grant
    Filed: August 19, 1992
    Date of Patent: October 25, 1994
    Assignee: Jurid Werke GmbH
    Inventor: Wolfgang Valentin
  • Patent number: 5310520
    Abstract: Discrete powder particles of copper 14 and INVAR 12 are mixed together in a container 16 and packed into a powder metal article. This article is hot vacuum degassed and vacuum sealed and then heated to temperature well below the sintering temperature of copper or INVAR. Immediately after heating the article, it is subjected to a high pressure, high strain force such as extrusion through a die thereby yielding a fully dense, strong composite material 10 with excellent combined thermal expansion and conductivity properties.
    Type: Grant
    Filed: January 29, 1993
    Date of Patent: May 10, 1994
    Assignee: Texas Instruments Incorporated
    Inventors: Sunil C. Jha, James A. Forster, Henry F. Breit
  • Patent number: 5298052
    Abstract: An Ni-based bearing alloy consisting, by weight, of 9-30% Cr, 5-19% Fe, 0.1-1.5% Si, 2-22% Co, 1.4-11.0% Mo, and the balance Ni and incidental impurities, said alloy having a matrix in which hard particles of a Co-Mo-Cr-Si alloy and/or BN are uniformly dispersed in weight ratios of 5 to 35% and not more than 5.0, respectively. The Ni-based alloy matrix provides superior heat resistance. Hard particles of Co-Mo-Cr-Si alloy uniformly dispersed in the matrix improve sliding characteristic with or without uniform dispersion of Bn as a solid lubricant, whereby the bearing alloy exhibits superior heat resistance and sliding characteristic when used in high temperature oxidizing atmosphere.
    Type: Grant
    Filed: June 11, 1992
    Date of Patent: March 29, 1994
    Assignee: Daido Metal Company, Ltd.
    Inventors: Tadashi Tanaka, Masaaki Sakamoto, Koichi Yamamoto, Kenji Sakai
  • Patent number: 5286323
    Abstract: An dome-shaped extrusion die for use in forming honeycomb monolith structures is disclosed. The die is formed by deforming an extrusion die having a flat cross section to obtain a dome-shaped cross section. Alternatively, the die may be fabricated from sinterable ceramic or metal powders in which case the holes and slots may be formed either in the green state, or in a chalk-hard state after partial densification.
    Type: Grant
    Filed: February 23, 1993
    Date of Patent: February 15, 1994
    Assignee: Corning Incorporated
    Inventor: Rodney D. Bagley
  • Patent number: 5252288
    Abstract: Method for producing an elongated sintered article, characterized by the steps including filling powder material in a pipe, carrying out plastic deformation of the pipe filled with the powder material, and heating the pipe filled with the powder material to burn and/or sinter the powder material.The method of the present invention is advantageously applicable to production of wire or rod of ceramics, particularly so called new ceramics or fine ceramics, sintered alloys or their combination, which are difficult to shape or mold by conventional process such as wire-drawing, rolling or extrusion of powder material which is difficult to mold and machine after the powder material is sintered.
    Type: Grant
    Filed: May 15, 1992
    Date of Patent: October 12, 1993
    Assignee: Sumitomo Electric Industries, Inc.
    Inventors: Susumu Yamamoto, Teruyuki Murai, Nozomu Kawabe, Masaaki Tobioka
  • Patent number: 5207821
    Abstract: Disclosed is a sintered alloy composition and method of manufacturing the same, the sintered alloy composition having a multi-phase structure, comprising: a first phase composed of aluminum and copper; and a second phase being dispersed in the first phase and composed of molybdenum, chromium, silicon and cobalt. This alloy composition has excellent abrasion and corrosion resistance, preferably to be used for making machine parts such as valve seats for engines.
    Type: Grant
    Filed: July 9, 1991
    Date of Patent: May 4, 1993
    Assignees: Hitachi Powdered Metals Co., Ltd., Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Yutaka Ikenoue, Keitaro Suzuki, Yoshimasa Aoki, Hideo Urata, Koji Koishikawa, Makoto Tsuji
  • Patent number: 5194219
    Abstract: Very good masking of pack diffusion aluminizing or chromizing on any metal to keep portions from being diffusion coated, is effected by localized coating the lowest layer of which is depletion-reducing masking powder the metal portion of which can have same composition as substrates, mixed with inert refractory diluent and non-contaminating film-former such as acrylic resin. The upper coating layer can be of non-contaminating particles like nickel or Cr.sub.2 O.sub.3 that upon aluminizing or chromizing become coherently held together to form a secure sheath. Such sheath can also be used for holding localized diffusion-coating layer in place. Film-former can be dissolved in volatile solvent, preferably methyl chloroform, in which masking powder or sheath-forming powder is suspended. Chromizing can be performed before aluminizing for greater effects. Aluminizing of metals like iron and nickel followed by leaching out much of the diffused-in aluminum, gives these substrates a pyrophoric and catalytic surface.
    Type: Grant
    Filed: July 7, 1992
    Date of Patent: March 16, 1993
    Assignee: Alloy Surfaces Company, Inc.
    Inventor: Alfonso L. Baldi
  • Patent number: 5182078
    Abstract: Diffusion coating can be speeded by high heat input. Diffusion coating packs can be made with chemically reduced metal content of sludges. Diffusion aluminizing followed by caustic leaching to remove much of the diffused-in aluminum, yields catalytically and pyrophorically active porous surface that also accepts top coatings. Mixtures of aluminum powder with nickel and/or iron powders react when heated to form Raney-like product that can be leached to become pyrophoric, and when held on a metal foil or gauze web will adhere to the web so that leached product can be used as pyrophoric foil for decoying heat-seeking missiles. Such adhesion is improved by addition of small amount of copper.
    Type: Grant
    Filed: June 6, 1990
    Date of Patent: January 26, 1993
    Assignee: Alloy Surfaces Company, Inc.
    Inventor: Alfonso L. Baldi
  • Patent number: 5152828
    Abstract: The present invention relates to a method of producing a mold material used for obtaining a mold for casting metals such as Zn, Al and the like or molding resins. In the method, the short fibers having an aspect ratio of 30 to 300 and obtained by cutting ferritic stainless steel long fibers having a width of 100 .mu.m or less, ferritic stainless steel powder and at least one of Cu powder and Cu alloy powder are used as raw materials. The raw materials are blended to obtain a material mixture which is then compressed under pressure in a Cold Isostatic Press process. The thus obtained compressed product is sintered in a vacuum atmosphere. The sintered material is held in an atmosphere of nitrogen gas or decomposed ammonia gas so that 0.3 to 1.2 wt % of nitrogen is added to the stainless steel in the sintered material. The thus obtained mold material has a hardness of HMV 250 to 500.
    Type: Grant
    Filed: October 8, 1991
    Date of Patent: October 6, 1992
    Assignee: Sintokogio Ltd.
    Inventor: Tatsuhiko Katoh
  • Patent number: 5130084
    Abstract: A method and apparatus are disclosed for fabrication of hollow articles by hot consolidation of metal alloy powder between a hollow core and a fluid pressure resistant outer shell. The hollow core is formed, a disposable layer is applied to define the object contour, a fluid pressure resistant metallic layer is formed over the disposable layer, which is then melted, removed and replaced by the metal alloy powder, and this assembly is hot isostatically pressed. The powder and core materials are preferably selected to be metallurgically compatible, so the core becomes an integral part of the finished article. The hollow article is inflated in a form die to establish the finished article contour.
    Type: Grant
    Filed: December 24, 1990
    Date of Patent: July 14, 1992
    Assignee: United Technologies Corporation
    Inventors: A. Paul Matheny, Paul M. Buxe
  • Patent number: 5126104
    Abstract: A method is disclosed for preparing an intimate mixture of powders of nickel-chromium-boron-silicon alloy, molybdenum metal powder, and Cr.sub.3 C.sub.2 /NiCr alloy suitable for thermal spray coatings which comprises milling a starting mixture of the above two alloys with molybdenum powder to produce a milled mixture wherein the average particle size is less than about 10 micrometers in diameter, forming an aqueous slurry of the resulting milled mixture and a binder which can be an ammoniacal molybdate compound or polyvinyl alcohol, and agglomerating the milled mixture and binder. The intimate mixture and binder may be sintered in a reducing atmosphere at a temperature of about 800.degree. C. to 950.degree. C. for a sufficient time to form a sintered partially alloyed mixture wherein the bulk density is greater than about 1.2 g/cc.
    Type: Grant
    Filed: June 6, 1991
    Date of Patent: June 30, 1992
    Assignee: GTE Products Corporation
    Inventors: Vidhu Anand, Sanjay Sampath, David L. Houck, Jack E. Vanderpool
  • Patent number: 5110543
    Abstract: A blade member for cutting-tools includes a cermet substrate which contains, apart from unavoidable impurities, a binder phase and a hard dispersed phase. The binder phase contains 5% to 30% by weight of cobalt and/or nickel. The hard dispersed phase contains a balance composite carbonitride of titanium and one or more of the elements tungsten, molybdenum, tantalum, niobium, hafnium and zirconium. The composite carbo-nitride satisfies the relationship 0.2.ltoreq.b/(a+b).ltoreq.0.7, where a and b denote atomic ratios of carbon and nitrogen, respectively. The substrate includes a hard surface layer in which the maximum hardness is present at a depth between 5 .mu.m and 50 .mu.m from a substrate surface thereof. The substrate surface has a hardness of 20% to 90% of the maximum hardness.
    Type: Grant
    Filed: July 19, 1991
    Date of Patent: May 5, 1992
    Assignee: Mitsubishi Metal Corporation
    Inventors: Niro Odani, Kazuyoshi Yoshioka, Sinichi Sekiya
  • Patent number: 5082433
    Abstract: Molded articles, particularly cams for camshafts of internal combustion engines, are subjected to high wear conditions. In order to make them resistant to wear, they are produced from a sintered alloy, which has been fabricated by powder metallurgical means. The alloy has a hardened matrix with interstitial copper and consists of 0.5 to 16% by weight of molybdenum, 1 to 20% by weight of copper, 0.1 to 1.5% by weight of carbon and, optionally, of admixtures of chromium, manganese, silicon and nickel totalling, at most, 5% by weight, the remainder being iron.
    Type: Grant
    Filed: December 17, 1990
    Date of Patent: January 21, 1992
    Assignee: Etablissement Supervis
    Inventor: Karl Leithner
  • Patent number: 5063021
    Abstract: A method is disclosed for preparing an intimate mixture of powders of nickel-boron-silicon alloy and molybdenum metal powder suitable for thermal spray coatings which comprises milling a starting mixture of the alloy and molybdenum powder to produce a milled mixture wherein the average particle size is less than about 10 micrometers in diameter, forming an aqueous slurry of the resulting milled mixture and a binder which can be an ammoniacal molybdate compound or polyvinyl alcohol, and agglomerating the milled mixture and binder. The intimate mixture and binder are preferably sintered in a reducing atmosphere at a temperature of about 800.degree. C. to about 950.degree. C. for a sufficient time to form a sintered partially alloyed mixture wherein the bulk density is greater than about 1.2 g/cc.
    Type: Grant
    Filed: May 23, 1990
    Date of Patent: November 5, 1991
    Assignee: GTE Products Corporation
    Inventors: Vidhu Anand, Sanjay Sampath, Clarke D. Davis, David L. Houck
  • Patent number: 5059489
    Abstract: A structure comprising a mixture of metals and metal alloys which are sintered into a hard porous body is presented. The structure can be useful for many different chemical and physical purposes, such as for catalysis, desorption and absorption, and selective leaching of the structure components into solutions.
    Type: Grant
    Filed: July 15, 1988
    Date of Patent: October 22, 1991
    Assignee: Corning Incorporated
    Inventors: Charles Q. Buckwalter, Jr., Irwin M. Lachman, Mallanagouda D. Patil, Jimmie L. Williams
  • Patent number: 5045276
    Abstract: An injection molded powder metallurgy product of highly satisfactory quality is obtained by a method which comprises injection molding mixture obtained by kneading a metal powder with a binder, depriving the molded mass of the binder while keeping the molded mass at least in contact with ceramic powder, projecting beads on the molded mass free from the binder, and thereafter sintering the molded mass studded with the beads.
    Type: Grant
    Filed: October 11, 1990
    Date of Patent: September 3, 1991
    Assignee: Sumitomo Metal Mining Company Limited
    Inventor: Yoshio Kijima
  • Patent number: 5032353
    Abstract: Structural components of at least one intermetallc compound and having complicated contours, are made by the steps of preparing a powder mixture of elemental metal powders including at least one powder of a low melting metal element or component and one powder of a high melting metal element or component that subsequently are to form the intermetallic compound. The powder mixture is then sintered to form a sintered body which is machined to a contour close to the finished contour and to dimensions close to the final dimensions. The so machined and shaped part is enveloped with an envelope of the high melting metal element or component. The enveloped part is subjected to a hot isostatic reaction pressing whereby the intermetallic compound is formed.
    Type: Grant
    Filed: October 26, 1990
    Date of Patent: July 16, 1991
    Assignee: MTU Motoren-und Turbinen-Union Muenchen GmbH
    Inventors: Wilfried Smarsly, Raimund Lackermeier
  • Patent number: 5015440
    Abstract: Light weight refractory aluminides, such as Al.sub.3 Nb and related aluminides may be produced from metallic powders by a high temperature exothermic reaction of refractory metals with molten aluminum. Mixtures of refractory metals and aluminum may be prepared and densified by powder metalurgy techniques. Applicant's process permits near net formations of stock shapes and parts by conducting the reaction in situ in a die.
    Type: Grant
    Filed: September 1, 1989
    Date of Patent: May 14, 1991
    Assignee: McDonnell Douglas Corporation
    Inventor: David M. Bowden