Mechanical Blending Patents (Class 419/32)
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Publication number: 20080210555Abstract: A method of manufacturing sputtering targets from powder materials, comprising steps of: providing at least one raw powder material; forming the at least one raw powder material into a green body with density greater than about 40 % of theoretical maximum density; treating the green body with microwaves to form a sintered body with density greater than about 97% of theoretical maximum density; and forming a sputtering target from the sintered body. The methodology is especially useful in the fabrication of targets comprising dielectric and cermet materials.Type: ApplicationFiled: December 4, 2007Publication date: September 4, 2008Applicant: HERAEUS INC.Inventors: Fenglin Yang, Anirban Das, Carl Derrington, Bernd Kunkel
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Patent number: 7413703Abstract: Processes for making rigid, binder free agglomerates of powdered metal are disclosed. The agglomerates have a low tap density. Articles that contain binder free agglomerates made from electrochemically active powder are also disclosed.Type: GrantFiled: January 17, 2003Date of Patent: August 19, 2008Assignee: Eveready Battery Company, Inc.Inventors: Peter Ru-Feng Tsai, Ning Ciu
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Publication number: 20080159905Abstract: A controlled combustion synthesis apparatus comprises an ignition system, a pressure sensor for detecting internal pressure, a nitrogen supply, a gas pressure control valve for feeding nitrogen and exhausting reaction gas, means for detecting the internal temperature of the reaction container, a water cooled jacket, and a cooling plate. A temperature control system controls the temperature of the reaction container by controlling the flow of cooling water supplied to the jacket and the cooling plate in response to the detected temperature. By combustion synthesizing, while controlling the internal pressure and temperature, the apparatus can synthesize a silicon alloy including 30-70 wt. % silicon, 10-45 wt. % nitrogen, 1-40 wt. % aluminum, and 1-40 wt % oxygen.Type: ApplicationFiled: April 19, 2007Publication date: July 3, 2008Applicant: ISMAN J CorporationInventors: Toshiyuki Watanabe, Masafumi Matsushita, Toshitaka Sakurai, Kazuya Sato, Yoko Matsushita
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Patent number: 7378053Abstract: The invention proposes a copper-based material with low thermal expansion and high thermal conductivity having good machinability and adaptability to nickel plating and also proposes a method for producing the same. The copper-based material is prepared through the steps of: adding 5 to 60% of iron-based alloy power having a certain value in thermal expansion coefficient into a matrix powder of pure copper phase powder and/or a precipitation hardening copper alloy powder; mixing the powders together; compacting the obtained powder mixture into a green compact and sintering it at temperatures of 400 to 600° C.Type: GrantFiled: April 27, 2004Date of Patent: May 27, 2008Assignee: Hitachi Powered Metals Co., Ltd.Inventor: Zenzo Ishijima
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Publication number: 20080102303Abstract: A composite is produced by the steps of (a) blending a first mixture of metallic powders; (b) compacting the blended first mixture of metallic powders to a plurality of discretely shaped articles; (c) blending a second mixture of metallic powders; (d) mixing the plurality of discretely shaped articles with the blended second mixture of metallic powders to form a precursor blend; (e) compacting the precursor blend; and (f) sintering the precursor blend. The composite has a metallic matrix with embedded shapes dispersed throughout the matrix where the embedded shapes have an incipient liquid phase sintering temperature less than an incipient liquid phase sintering temperature of the matrix.Type: ApplicationFiled: June 12, 2007Publication date: May 1, 2008Inventors: Timothy J. Brent, Michael T. Stawovy
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Patent number: 7311874Abstract: A method of fabricating a sputter target comprises: homogenously blending a plurality of powders including at least a first powder and a second powder. The first powder is comprised of chromium (Cr), cobalt (Co), ruthenium (Ru), nickel (Ni), or iron (Fe). The second powder is comprised of boron (B), carbon (C), a nitrogen (N)-containing material, a boride, a carbide, a nitride, a silicide, an oxygen (O)-containing material or an oxide. The second powder has a particle size of between 0.01 microns and 50 microns. The method further comprises: canning the blended plurality of powders to form a substantially non-segregated encapsulated powdered material mix; pressing the encapsulated powdered material mix to form a billet; and machining the billet to form a sputter target.Type: GrantFiled: December 19, 2003Date of Patent: December 25, 2007Assignee: Heraeus Inc.Inventor: Wenjun Zhang
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Patent number: 7273584Abstract: An oxide dispersion strengthened martensitic steel excellent in high-temperature strength having residual ?-grains can be manufactured by a method comprising mixing either element powders or alloy powders and a Y2O3 powder; subjecting the resulting mixed powder to mechanical alloying treatment; solidifying the resulting alloyed powder by hot extrusion; and subjecting the resulting extruded solidified material to final heat treatment involving normalizing and tempering heat treatment to thereby manufacture an oxide dispersion strengthened martensitic steel in which Y2O3 particles are dispersed in the steel, wherein ?to ?transformation is not allowed to occur during the described hot extrusion and the proportion of residual ?-grains in which oxide particles are finely dispersed in high density is increased by controlling the mixture ratio of the powders for the mechanical alloying treatment.Type: GrantFiled: August 30, 2004Date of Patent: September 25, 2007Assignee: Japan Nuclear Cycle Development InstituteInventors: Satoshi Ohtsuka, Shigeharu Ukai, Takeji Kaito, Takeshi Narita, Masayuki Fujiwara
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Patent number: 7250134Abstract: A steel powder metal skeleton is infiltrated with an infiltrant composition similar to the skeleton, with an additional agent that depresses the melting point of the infiltrant relative to the skeleton. Infiltration is driven primarily by capillary pressure. The powder and infiltrant compositions differ primarily only in a higher concentration of a melting point depressant agent “MPD” in the infiltrant. Carbon (C) and silicon (Si) and several other elements can be elements in an MPD, either alone or in combination. Certain steel target compositions are such that a complementary infiltrant, and skeleton can be chosen such that a skeleton will remain solid at an infiltration temperature at which the infiltrant can be melted and fully infiltrated, and further where there is a persistent two phase field, with a liquid phase that is large enough (greater than 7% vol, and typically between 20 and 40 vol %) so that flow can be maintained without choke off from diffusional solidification.Type: GrantFiled: November 26, 2003Date of Patent: July 31, 2007Assignee: Massachusetts Institute of TechnologyInventors: Brian D. Kernan, Emanuel M. Sachs, Samuel M. Allen, Adam M. Lorenz
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Patent number: 7229588Abstract: A cobalt-chromium-boron-platinum sputtering target alloy having multiple phases. The alloy can include Cr, B, Ta, Nb, C, Mo, Ti, V, W, Zr, Zn, Cu, Hf, O, Si or N. The alloy is prepared by mixing Pt powder with a cobalt-chromium-boron master alloy, ball milling the powders and HIP'ing to densify the powder into the alloy.Type: GrantFiled: January 13, 2004Date of Patent: June 12, 2007Assignee: Heraeus, Inc.Inventors: Michael Sandlin, Bernd Kunkel, Willy Zhang, Phillip Corno
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Patent number: 7217388Abstract: The present invention provides a method in which a strengthened platinum material can be produced, in which no blisters occur on the surface of the material even after heat treatment of 1,400° C. or higher and a metal oxide such as zirconium oxide is finely dispersed, and which has excellent high-temperature creep properties, when the strengthened platinum material is produced using a melt-sprayed platinum alloy powder. The method for producing a strengthened platinum material includes oxidizing a platinum alloy powder obtained by melt-spray, wet-milling the platinum alloy powder by adding an organic solvent, sintering, and forging, wherein the wet-milled platinum alloy fine powder is charged into a heat resistant container and heated to 1,200 to 1,400° C. in a vacuum atmosphere to be subjected to degassing.Type: GrantFiled: April 12, 2002Date of Patent: May 15, 2007Assignee: Tanaka Kikinzoku Kogyo K.K.Inventor: Haruki Yamasaki
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Patent number: 7175802Abstract: Spent sputtering targets are refurbished by filling the depleted region of the target with new sputter material using a hot isostatic pressing or HIP'ing technique.Type: GrantFiled: September 16, 2002Date of Patent: February 13, 2007Assignee: Heraeus, Inc.Inventors: Michael Sandlin, Wenjun Zhang, Bernd Kunkel
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Patent number: 7175803Abstract: The present invention is directed to methods of manufacturing an x-ray tube component, such as an evacuated housing and the like. The component has a radiation shielding layer, which is comprised of a plurality of powder metals, at least one of which is comprised of powder metal component that is substantially non-transmissive to x-radiation. The powder metal includes, for example, tungsten.Type: GrantFiled: June 14, 2004Date of Patent: February 13, 2007Assignee: Varian Medical Systems Technologies, Inc.Inventors: Christopher F. Artig, Deborah L. Salmon
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Patent number: 7169208Abstract: A composition for use with alloys including extra-fine nickel powder dispersed with a hydrophobic inorganic dispersant which is preferably high-purity silica treated with hexamethyldisilazane (fumed silica). The composition breaks and prevents the agglomeration of the nickel powder, thereby preventing weaknesses in alloys, like steel for example, formed with the nickel powder. A method for making an alloy with the composition includes mixing the nickel powder with other metals and/or nonmetals and the hydrophobic fumed silica to form an alloy blend, pressing the alloy blend, and sintering the alloy blend.Type: GrantFiled: June 10, 2004Date of Patent: January 30, 2007Assignee: Inco LimitedInventors: Scott Thomas Campbell, Thomas Francis Stephenson, Tajpreet Singh
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Patent number: 7087202Abstract: This invention concerns particulate reinforced Al-based composites, and the near net shape forming process of their components. The average size of the reinforced particle in the invented composites is 0.1–3.5 ?m and the volume percentage is 10–40%, and a good interfacial bonding between the reinforced particulate and the matrix is formed with the reinforced particles uniformly distributed. The production method of its billet is to have the reinforced particles and Al-base alloy powder receive variable-speed high-energy ball-milling in the balling drum. Then, with addition of a liquid surfactant, the ball-mill proceeds to carry on ball-milling. After the ball-milling, the produced composite powder undergoes cold isostatic pressing and the subsequent vacuum sintering or vacuum hot-pressing to be shaped into a hot compressed billet, which in turn undergoes semisolid thixotropic forming and may be shaped into complex-shaped components. These components can be used in various fields.Type: GrantFiled: July 28, 2003Date of Patent: August 8, 2006Assignees: ASM Assembly Automation Ltd., General Research Institute for Non-Ferrous MetalsInventors: Deming Liu, Chou Kee Peter Liu, Jian Zhong Fan, Jun Xu, Tao Zuo, Zhao Zu Gao
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Patent number: 7052526Abstract: A magnesium base composite material is provided such that compound particles generated by a solid-phase reaction with magnesium are uniformly dispersed in a magnesium alloy body. The compound particles dispersed in the body comprise magnesium silicide (Mg2Si) and magnesium oxide (MgO) so that the magnesium base composite material may have excellent strength, hardness and abrasion resistance and tempered opponent aggression.Type: GrantFiled: February 14, 2003Date of Patent: May 30, 2006Assignee: Toudai TLO, Ltd.Inventor: Katsuyoshi Kondoh
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Patent number: 7037464Abstract: In an oxide dispersion strengthened martensitic steel which comprises, by % by weight, 0.05 to 0.25% C, 8.0 to 12.0% Cr, 0.1 to 4.0% W, 0.1 to 1.0% Ti, 0.1 to 0.5% Y2O3 with the balance being Fe and unavoidable impurities and in which Y2O3 particles are dispersed in the steel, by adjusting the Ti content within the range of 0.1 to 1.0% so that an excess oxygen content Ex.O in steel satisfies [0.22×Ti (% by weight)<Ex.O (% by weight)<0.46×Ti (% by weight)], the oxide particles are finely dispersed and highly densified to thereby obtain an oxide dispersion strengthened martensitic steel excellent in high-temperature strength. It is also possible to reduce the amount of oxygen contamination in steel during the mechanical alloying of raw material powders to provide Ex.O within a predetermined range, by carrying out the mechanical alloying in an Ar atmosphere having a super purity of not less than 99.Type: GrantFiled: August 7, 2003Date of Patent: May 2, 2006Assignee: Japan Nuclear Cycle Development InstituteInventors: Satoshi Ohtsuka, Shigeharu Ukai, Takeji Kaito, Takeshi Narita, Masayuki Fujiwara
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Patent number: 6960319Abstract: Disclosed is a flow-softening tungsten alloy having the general formula: W100-pAiBjCkDe wherein W is tungsten; A is one or more elements selected from the group consisting of nickel, iron, chromium and cobalt; B is in or more elements selected from the group consisting of molybdenum, niobium and tantalum; C is one or more of the elements selected from the groups consisting of titanium and aluminum; D is one or more elements selected from the group consisting of boron, carbon, and silicon; i is from about 5 to about 8 weight percent; j is from 0 to about 4 weight percent; k is from about 0.1 to about 4 weight percent; 1 is from 0 to about 0.1 weight percent; and p is greater than or equal to about 7 weight percent and less than or equal to about 20 weight percent. In this alloy p is approximately equal to the sum of i, j, k and 1. A method of preparing this alloy and a kinetic energy penetrator manufactured from it are also disclosed.Type: GrantFiled: October 27, 1995Date of Patent: November 1, 2005Assignee: The United States of America as represented by the Secretary of the ArmyInventor: Deepak Kapoor
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Patent number: 6905779Abstract: A copper-based sliding material comprising sintered copper or sintered copper alloy, and 0.1 to 5 vol. % hard substance particles harder in hardness than said copper or copper alloy, said hard substance particles being substantially evenly dispersed so that, when at least one, randomly selected surface portion or sectional portion of said sintered copper or sintered copper alloy is partitioned into squares each having a side of 20 ?m, at least one particle exists in each of squares not less than 80% of the whole squares. The copper-based sliding material has good anti-seizure property and superior resistance to fatigue without containing any lead.Type: GrantFiled: December 27, 2000Date of Patent: June 14, 2005Assignee: Daido Metal Company Ltd.Inventors: Kenji Sakai, Naohisa Kawakami, Satoru Kurimoto, Takashi Inaba, Koichi Yamamoto, Takayuki Shibayama
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Patent number: 6902697Abstract: An aluminum powder is mixed with a neutron absorber powder through cold isostatic press to form a preliminary molding. The preliminary molding is then subjected to sintering under no pressure in vacuum. After sintering, a billet is subjected to induction heating and hot extrusion to form a square pipe.Type: GrantFiled: April 19, 2002Date of Patent: June 7, 2005Assignee: Mitsubishi Heavy Industries, Ltd.Inventors: Katsunari Ohsono, Kazuo Murakami, Yasuhiro Sakaguchi, Toshiro Kobayashi, Toyoaki Yasui
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Patent number: 6902809Abstract: The present invention provides a method for preparing a rhenium-tantalum alloy with improved strength and ductility characteristics. The method includes mixing powders of rhenium and tantalum with a weight ration of approximately 97% rhenium to approximately 3% tantalum. The powdered blend is then compressed to a green state. The green compress of rhenium and tantalum is then sintered such that tantalum goes into solid solution with rhenium. The sintered material is then cold rolled. The cold rolling disperses oxides away from concentrations in the alloy grain boundaries. If desired, the alloy may then be annealed. The result is a rhenium-tantalum alloy that displays improved high temperature strength and ductility over pure rhenium materials. The present alloy is particularly suited to fabrication of rocketry components such as valve bodies, poppets, seats, and nozzles.Type: GrantFiled: June 29, 2004Date of Patent: June 7, 2005Assignee: Honeywell International, Inc.Inventor: Don L. Mittendorf
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Patent number: 6863862Abstract: Methods of producing atomized intermetallic aluminide powders with a controlled oxygen content, and articles made from the powders by powder metallurgical techniques are disclosed. Gas atomized intermetallic aluminide powders can be oxidized to increase their oxygen content. Water atomized intermetallic aluminide powders can be milled to change their size, shape and/or oxygen content. Blends or mixtures of modified gas and water atomized intermetallic aluminide powders can be processed into articles by powder metallurgical techniques.Type: GrantFiled: September 4, 2002Date of Patent: March 8, 2005Assignee: Philip Morris USA Inc.Inventors: Firooz Rasouli, Clive Scorey, John McKernan, John F. Cunningham
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Patent number: 6852274Abstract: A hard metal granulate is produced by wet milling and spray drying in a spray tower using pure water as the liquid phase. The spray tower is configured and operated in such a way that a ratio of the quantity of water added via the slurry (in liters per hour) to tower volume (in m3) is between 0.5 and 1.8 and in that a maximum of 0.17 kg of slurry is atomized per m3 of incoming drying gas. The slurry has a solid particle concentration within a range of 65-85% by weight. Under these conditions, the addition of a water-soluble, long-chain polyglycol to the slurry prior to spraying previously required in order to prevent oxidation of the hard metal granulate is no longer necessary.Type: GrantFiled: November 22, 2002Date of Patent: February 8, 2005Assignee: Ceratizit Austria Gesellschaft m.b.H.Inventors: Gerhard Knünz, Helmut Beirer, Andreas Lackner, Wolfgang Glätzle, Erwin Hartlmayr
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Publication number: 20040266605Abstract: This invention pertains to product and process. The product is a transparent product of a density in excess 99.5% comprising spinel and having uniform mechanical properties. The process pertains to fabrication of a transparent spinel product comprising the steps of dissolving a sintering aid in water to form a neutral sintering aid solution, adding a suitable additive to the sintering aid solution, applying the sintering aid solution to spinel particles to form a spinel dispersion, sub-dividing or atomizing the spinel dispersion to form droplets comprising one or more spinel particles coated with the final spinel solution, drying the droplets to form dried coated particles comprising one or more spinel particles coated with a dried layer of the sintering aid, and densifying the dried coated particles to form a transparent spinel product having uniform optical and mechanical properties in absence of grains of exaggerated size.Type: ApplicationFiled: June 24, 2003Publication date: December 30, 2004Inventors: Guillermo R. Villalobos, Jas S. Sanghera, Shyam S. Bayya, Ishwar D. Aggarwal
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Publication number: 20040247481Abstract: New alloys of the AB5 type are disclosed which are of the formula:Type: ApplicationFiled: February 3, 2004Publication date: December 9, 2004Applicant: HERA, Hydrogen Storage Systems, Inc.Inventors: Guoxian Liang, Robert Schulz
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Patent number: 6827755Abstract: A high-strength and high-toughness ferritic steel having a tensile strength of not less than 1,000 MPA and a Charpy impact value of not less than 1 MJ/m2 is provided. A ferritic steel comprising, by weight, not more than 1% Si, not more than 1.25% Mn, 8 to 30% Cr, not more than 0.2% C, not more than 0.2% N, not more than 0.4% O, a total amount of not more than 12% of at least one compound-forming element selected from the group of Ti, Zr, Hf, V and Nb in amounts of not more than 3% Ti, not more than 6% Zr, not more than 10% Hf, not more than 1.0% V and not more than 2.0% Nb, also containing where necessary not more than 0.3% Mo, not more than 4% W and not more than 1.6% Ni, and the balance consisting of Fe and unavoidable impurities, and having an average crystal grain size of not more than 1 &mgr;m, can be obtained by a method comprising encapsulating a steel powder produced by mechanical alloying, and subjecting the encapsulated steel powder to plastic deformation.Type: GrantFiled: July 2, 2002Date of Patent: December 7, 2004Assignee: Hitachi, Ltd.Inventors: Masami Taguchi, Ryo Ishibashi, Yasuhisa Aono, Hidehiko Sumitomo, Hiroki Masumoto, Masakuni Fujikura
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Publication number: 20040213692Abstract: The invention proposes a copper-based material with low thermal expansion and high thermal conductivity having good machinability and adaptability to nickel plating and also proposes a method for producing the same. The copper-based material is prepared through the steps of: adding 5 to 60% of iron-based alloy power having a certain value in thermal expansion coefficient into a matrix powder of pure copper phase powder and/or a precipitation hardening copper alloy powder; mixing the powders together; compacting the obtained powder mixture into a green compact and sintering it at temperatures of 400 to 600° C.Type: ApplicationFiled: April 27, 2004Publication date: October 28, 2004Inventor: Zenzo Ishijima
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Publication number: 20040180217Abstract: A sputtering target including indium oxide and tin oxide, the content by percentage of the tin atoms therein being from 3 to 20 atomic % of the total of the indium atoms and the tin atoms, and the maximum grain size of indium oxide crystal in the sputtering target being 5 &mgr;m or less. When a transparent conductive film is formed by sputtering, this sputtering target makes it possible to suppress the generation of nodules on the surface of the target and to conduct the sputtering stably.Type: ApplicationFiled: January 30, 2004Publication date: September 16, 2004Inventors: Kazuyoshi Inoue, Shigeo Matsuzaki
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Patent number: 6783568Abstract: A sintered steel and a method for the manufacture thereof are described, the sintered steel being made by a method comprising the steps of providing a first pre-alloyed steel powder having a composition comprising in weight %: C 0.5-2, Cr 3.5-6, (2 Mo+W) 12-22, V 0.5-5, Co 0-12, Mn 0.1-0.5, Si 0.1-0.6, Fe balance apart from incidental impurities; providing a second pre-alloyed steel powder having a composition comprising in weight %: C 0.3-0.7, Cr 3-5.5, Mo 1-2.5, V 0.3-1.5, W 0-2, Mn 0.1-0.6, Si 0.8-1.2. Fe balance apart from incidental impurities; mixing together from 2 to 50 weight % of the first pre-alloyed steel powder with 98 to 50 weight % of the second pre-alloyed steel powder optionally up to 60 weight % of an iron powder and with carbon powder such that the final carbon content of the matrix of the sintered steel powder is a maximum of 1.1 weight %1; compacting the mixture and sintering to form the sintered steel.Type: GrantFiled: January 24, 2002Date of Patent: August 31, 2004Assignee: Federal-Mogul Sintered Products LimitedInventors: Andrew Keith Bowskill, Charles Grant Pumell, Iain Robert Whitaker
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Publication number: 20040161625Abstract: A copper-based sliding material comprising sintered copper or sintered copper alloy, and 0.1 to 5 vol. % hard substance particles harder in hardness than said copper or copper alloy, said hard substance particles being substantially evenly dispersed so that, when at least one, randomly selected surface portion or sectional portion of said sintered copper or sintered copper alloy is partitioned into squares each having a side of 20 &mgr;m, at least one particle exists in each of squares not less than 80% of the whole squares. The copper-based sliding material has good anti-seizure property and superior resistance to fatigue without containing any lead.Type: ApplicationFiled: December 27, 2000Publication date: August 19, 2004Inventors: Kenji Sakai, Naohisa Kawakami, Satoru Kurimoto, Takashi Inaba, Koichi Yamamoto, Takayuki Shibayama
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Patent number: 6740288Abstract: The present invention relates to a process for preparing a powdered tungsten-aluminum alloy, in which the powdered tungsten and aluminum as starting materials is mechanical alloyed at normal temperature to provide the tungsten-aluminum alloy. The process of this present invention is simple and easy and the device used is simple to handle. The process is carried out at room temperature, and is suitable for preparing an alloy of metals wherein there is large disparity between melting points and densities of the metals, which alloy could not be prepared by the known smelting process.Type: GrantFiled: June 17, 2002Date of Patent: May 25, 2004Assignee: Changchun Institute of Applied Chemistry Chinese Academy of ScienceInventors: Xianfeng Ma, Xuewei Yan, Wei Zhao, Shixue Wu
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Patent number: 6723387Abstract: A thermal spray method for the fabrication of ceramic/metal and ceramic/ceramic hardcoating for wear applications. The method makes use of feedstock powder, composed of micron-scale aggregates of hard phase material particles that are either mixed or coated with a readily fusible nano-scale binder phase material. Thus, during thermal spraying, the nanostructured material undergoes rapid melting while the aggregated material is heated but not necessarily melted. A dense coating is formed when the molten nano-material fills the available pore spaces between the heated and softened aggregates, providing a strong and tough matrix for the consolidated material. Optimal wear properties are achieved when the volume fraction of aggregated particles is high, typically in the range of 0.5-0.9. Aggregated material may be composed of one, two or more particles of difference sizes and/or compositions, with particle size distribution that gives high packing density for the hard phase.Type: GrantFiled: September 19, 2002Date of Patent: April 20, 2004Assignee: Rutgers UniversityInventors: Bernard H. Kear, Ganesh Skandan
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Publication number: 20040050454Abstract: A blended powder including a first powder containing an R2T14B phase as a main phase, and a second powder containing an R2T17 phase at 25 wt % or more of the whole is prepared. Herein, R is at least one element selected from the group consisting of all rare-earth elements and Y (yttrium), T is at least one element selected from the group consisting of all transition elements, and Q is at least one element selected from the group consisting of B (boron) and C (carbon). The blended powder is sintered, so as to manufacture a permanent magnet having a structure in which a rare-earth element included in the second powder is concentrated in a grain surgace region of a main phase.Type: ApplicationFiled: July 30, 2003Publication date: March 18, 2004Inventors: Takao Sekino, Yuji Kaneko
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Versatile processes for preparing and using novel composite particles in powder coating compositions
Publication number: 20040018109Abstract: Methodology for constructing composite particles from ingredients comprising two or more particulate components. The resultant particles are usefully incorporated into powder coating compositions. The approach also finds utility in other applications, including but not limited to the food, drug, and cosmetics industry. Fluidized particles are subjected to an intense, but relatively brief heating event. This causes associated particles to fusingly assemble into fused composite clusters.Type: ApplicationFiled: July 26, 2002Publication date: January 29, 2004Inventors: Walter J. Blatter, James A. Heck, Lowell G. Lindquist -
Patent number: 6673307Abstract: The present invention relates to a method of making a cemented carbide by mixing powder of WC and possibly other powders forming hard constituents and binder phase and pressing agent, drying, pressing and sintering whereby; the mixing is wet mixing with no change in grain size or grain size distribution of the hard constituent powders; the WC grains are coated with binder metal and deagglomerated prior to the mixing. The sintering is made by microwave sintering at 1325-1410° C. with a holding time of 5-15 min. As a result a cemented carbide with improved properties is obtained.Type: GrantFiled: March 28, 2001Date of Patent: January 6, 2004Assignee: Sandvik ABInventors: Mikael Lindholm, Mats Waldenström, Mats Ahlgren
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Publication number: 20030231975Abstract: The present invention provides:Type: ApplicationFiled: May 20, 2003Publication date: December 18, 2003Applicants: SNECMA MOTEURS, SNECMA SERVICESInventors: Frederic Braillard, Claude Mons, Philippe Perruchaut, Didier Ribot, Joel Vigneau
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Publication number: 20030202898Abstract: A metal-made seamless pipe is provided, containing at least one metal selected from the group consisting of metals each having a melting point of 1,600° C. or more, and has a porosity of 0.3 to 25%. The porosity is defined as a ratio of the open pores present at the outer surface of the pipe to the total surface area of the outer surface of the pipe. The open pores do not include through-pores perforating to the inner surface of the pipe. A process for producing such a metal-made seamless pipe is also provided. The metal-made seamless pipe is low in processability but can be produced having a small thickness and a small inner diameter, having superior mechanical strength and gastightness, and can be suitably used as a sealing member of a translucent vessel of a high-pressure discharge lamp.Type: ApplicationFiled: April 25, 2003Publication date: October 30, 2003Applicant: NGK Insulators, Ltd.Inventor: Norikazu Niimi
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Patent number: 6630100Abstract: A rectangular pipe is molded by mixing aluminum powder with powder of a neutron absorbing material, molding a premolded body by means of cold isostatic pressing (CIP), canning the premolded body, sintering the premolded body by means of hot isostatic pressing (HIP), performing outer cutting and end face cutting on the can after the sintering, taking a billet out of the can, and extruding this billet.Type: GrantFiled: April 9, 2001Date of Patent: October 7, 2003Assignee: Mitsubishi Heavy Industries, Ltd.Inventors: Kazuo Murakami, Yasuhiro Sakaguchi, Toshiro Kobayashi, Toyoaki Yasui
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Patent number: 6626975Abstract: The invention relates to a method for producing a homogeneous mixture of hard material powders and binder metal powders without using grinding bodies, liquid grinding auxiliary agents and suspending media. According to the invention, the mixture components are mixed at close range while generating a high shearing collision velocity of the powder particles and are remotely mixed by rotating the mixing bed without resulting in a particle size reduction of the hard material powders.Type: GrantFiled: July 13, 2001Date of Patent: September 30, 2003Assignee: H. C. Starck GmbH & Co. KGInventors: Benno Gries, Jörg Bredthauer
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Patent number: 6627058Abstract: This invention is directed to a composition comprising: (a) platinum group metal powder, alloys, or mixtures thereof as a powder or deposited on graphite supports; (b) poly(glycol ether), derivatives, or mixtures thereof; (c) carbon-based electrically conductive filler; and (d) thermoplastic polymer or mixtures thereof. The invention is further directed to a process for dispersing platinum group metal powder, alloys, or mixtures thereof in poly(glycol ether), derivatives, or mixtures thereof. The invention is further directed to the above composition wherein the platinum group metal powder has been dispersed according to the above process.Type: GrantFiled: January 17, 2001Date of Patent: September 30, 2003Assignee: E. I. du Pont de Nemours and CompanyInventor: Man-Sheung Chan
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Patent number: 6613276Abstract: Alloys of transition metal suicides that contain one or more alloying elements are fabricated by a two-stage process involving mechanical activation as the first stage and densification and field-activated reaction as the second stage. Mechanical activation, preferably performed by high-energy planetary milling, results in the incorporation of atoms of the alloying element(s) into the crystal lattice of the transition metal, while the densification and field-activated reaction, preferably performed by spark plasma sintering, result in the formation of the alloyed transition metal silicide. Among the many advantages of the process are its ability to accommodate materials that are incompatible in other alloying methods.Type: GrantFiled: April 16, 2002Date of Patent: September 2, 2003Assignee: The Regents of the University of CaliforniaInventors: Zuhair A. Munir, Joseph N. Woolman, John J. Petrovic
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Patent number: 6596226Abstract: A process for producing a thermoelectric material based on two or more elements selected in the group constituted by Bi, Sb, Te and Se, which process comprises: i. an alloying step wherein determined amounts of the elements Bi, Sb, Te or Se are mixed until an homogenous powdered alloy is obtained; ii. an extrusion step of the powdered homogenous alloy obtained in the preceding step. The elements Bi, Sb, Te or Se being preferably mechanically mixed in an homogenous powdered alloy. The thermoelectric material, which are obtainable by this process, exhibits improved thermoelectric and mechanical properties and are therefore suitable, for example, as cooler, as temperature stabilizer in a electronic device or as power generator.Type: GrantFiled: August 24, 2000Date of Patent: July 22, 2003Assignee: 5NPLUS Inc.Inventors: Jean-Pierre Simard, Dmitri Vasilevskiy, Jacques L'Ecuyer
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Patent number: 6576038Abstract: A method to agglomerate metal particles such as tantalum and niobium powders is described which includes combining a volatilizable or vaporizable liquid with the particles to form wet particles; compacting the wet particles; drying the compacted wet particles to form a cake; and heat treating the cake to form the agglomerated particles. Also described are agglomerated particles obtained by this method and further, particles, preferably tantalum or niobium powder, having a flow rate of at least about 65 mg/sec and/or an improved pore size distribution, and/or a higher Scott Density. Capacitors made from tantalum powder and niobium powder are also described.Type: GrantFiled: May 19, 1999Date of Patent: June 10, 2003Assignee: Cabot CorporationInventor: Bhamidipaty K. D. P. Rao
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Patent number: 6527824Abstract: A method of producing a high-density article is presented comprising selecting one or more primary tungsten-containing constituents with densities greater than 10.0 g/cc and one or more secondary constituents with densities less than 10.0 g/cc, co-milling the mixture of constituents in a high-energy mill to obtain mechanical alloying effects, then processing the resulting powder product by conventional powder metallurgy to produce an article with bulk density greater than 9.0 g/cc.Type: GrantFiled: June 18, 2001Date of Patent: March 4, 2003Inventor: Darryl D. Amick
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Publication number: 20030010153Abstract: A ferrous sintered valve seat material is made of mixed powders comprising a sinter-hardenable phase and a finely dispersed carbide phase. The powder mixture comprises a sinter-hardening prealloyed powder forming 75 to 90 wt. % of the mixture and a tool steel powder with finely dispersed carbides forming 5 to 25% of the mixture. Machinability additives of MnS, CaF2 or MoS2types are added in an amount of 1 to 5 wt. %. Improved thermal conductivity is obtained by infiltrating the compact with Cu up to 25 wt. %.Type: ApplicationFiled: April 30, 2002Publication date: January 16, 2003Applicant: FEDERAL-MOGUL WORLD WIDE, INC.Inventors: Mark Birler, Salvator Nigarura, Juan Trasorras
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Publication number: 20020152841Abstract: An aluminum powder is mixed with a neutron absorber powder through cold isostatic press to form a preliminary molding. The preliminary molding is then subjected to sintering under no pressure in vacuum. After sintering, a billet is subjected to induction heating and hot extrusion to form a square pipe.Type: ApplicationFiled: April 19, 2002Publication date: October 24, 2002Applicant: MITSUBISHI HEAVY INDUSTRIES, LTD.Inventors: Katsunari Ohsono, Kazuo Murakami, Yasuhiro Sakaguchi, Toshiro Kobayashi, Toyoaki Yasui
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Patent number: 6454992Abstract: A bond coat composition for use in thermal barrier coatings comprises a NiAl—CoCrAlY matrix containing particles of AlN dispersed therein. The bond coat composition is prepared by croymilling NiAl and CoCrAlY in liquid nitrogen.Type: GrantFiled: September 29, 2000Date of Patent: September 24, 2002Assignee: Ohio Aerospace InstituteInventor: Mohan G. Hebsur
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Patent number: 6428596Abstract: A multiplex powder composite for use in a cored wire electrode to be deployed in a thermal spray or welding apparatus. The composite comprises micron-sized particles and sub-micron-sized particles, including nano-scale particles, the particles mechanically cooperating to promote smooth powder flow, which facilitates compaction of the cored wire electrode.Type: GrantFiled: November 13, 2000Date of Patent: August 6, 2002Assignee: Concept Alloys, L.L.C.Inventors: David John Urevich, Joseph Paul Hughes
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Patent number: 6398843Abstract: A dispersion-strengthened material is described which comprises aluminium or aluminium alloy containing a substantially uniform dispersion of ceramic particles to confer dispersion strengthening which is inherently stable at high working temperatures, the ceramic particles having a diameter of less than 400 nm, and preferably in the range 10 nm to 100 nm. Suitable ceramic dispersoids include Al2O3, TiO2, Al3C4, ZrO2, Si3N4, SiC, SiO2.Type: GrantFiled: May 4, 2000Date of Patent: June 4, 2002Assignee: Qinetiq LimitedInventor: Andrew Tarrant
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Patent number: 6375709Abstract: This invention concerns a lubricant for warm compaction of iron-based metallurgical powder compositions. 50 to 100% by weight of the lubricant is a polyester, aromatic or partly aromatic, which has a number-average molecular weight Mn of 5,000-50,000. This invention further concerns a metal powder composition containing the lubricant, a method for making sintered products by using the lubricant, and use of the same in warm compaction of metallurgical powders.Type: GrantFiled: March 23, 2000Date of Patent: April 23, 2002Assignee: Höganäs ABInventors: Helge Storström, Hilmar Vidarsson
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Patent number: 6368376Abstract: Disclosed is a process for making an oxide dispersion-strengthened tungsten heavy alloy by mechanical alloying that includes the steps of: adding 0.1 to 5 wt. % of Y2O3 powder to a mixed powder comprising more than 90 wt. % of tungsten powder, and nickel and iron powders for the rest; and subjecting the resulting mixture to a mechanical alloying to prepare an oxide dispersion-strengthened tungsten heavy alloy powder. The oxide dispersion-strengthened tungsten heavy alloy prepared by the mechanical alloying is characterized in that fine Y2O3 particles are uniformly dispersed in the matrix which are stable at high temperatures results in enhanced high-temperature strength and a reduction of the shearing strain of the fraction during high strain rate deformation.Type: GrantFiled: December 12, 2000Date of Patent: April 9, 2002Assignee: Korea Advanced Institute of Science and TechnologyInventors: Soon Hyung Hong, Ho Jin Ryu