Mechanical Blending Patents (Class 419/32)
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Patent number: 5561832Abstract: A tool steel powder added with a vanadium carbide powder by a milling process, and a method for manufacturing parts therewith are disclosed. Particularly, a method for adding a vanadium carbide (VC) powder to a tool steel powder by a ball milling or an attrition milling, and a method for manufacturing a part by using the milled tool steel powder are disclosed. The method for manufacturing a vanadium carbide added tool steel powder and for manufacturing parts using the powder, includes the steps of: mixing a tool steel powder with vanadium carbide powder in an amount of 5.about.15 wt %; ball-milling the mixture powder under wet atmosphere; carrying out an annealing in a vacuum; carrying out a cold die compaction or cold isostatic pressing to near net dimension and carrying out a vacuum sintering and then a hot isotropic pressing without canning.Type: GrantFiled: June 29, 1995Date of Patent: October 1, 1996Assignee: Korea Institute of Machinery & MetalsInventors: Chung Hyung-Sik, Bae Jong-Su, Kim Young-Jin
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Patent number: 5554338Abstract: The invention relates to a method of preparing a composite sintered body having inner and outer portions fitted with each other. The method includes the steps of: (a) preparing an inner powder compact; (b) preparing an outer powder compact; (c) fitting the inner and outer powder compacts with each other so as to prepare a composite powder compact; and (d) sintering the composite powder compact so as to prepare the composite sintered body. The inner and outer powder compacts are respectively selected such that, during the step (d), the amount of growth of the inner powder compact becomes greater than that of the outer powder compact. Each of the inner and outer composite powder compacts is made of one member selected from the group consisting of a wax-type segregation prevention powder mixture and a metal-soap-type segregation prevention powder mixture. At least one of the inner and outer composite powder compacts is made of the wax-type segregation prevention powder.Type: GrantFiled: April 18, 1995Date of Patent: September 10, 1996Assignees: Nissan Motor Co., Ltd., Hitachi Powdered Metals Co., Ltd.Inventors: Hiroshi Sugihara, Hiroyuki Ishikawa, Tsutomu Uemura, Akira Fujiki, Hiromasa Imazato, Shinichi Umino
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Patent number: 5552109Abstract: This invention relates to a process of forming a sintered article of powder metal comprising blending graphite and lubricant with a pre-alloyed iron based powder, pressing said blended mixture to shape in a single compaction stage sintering said article, and then high temperature sintering said article in a reducing atmosphere to produce a sintered article having a density greater than 7.4 g/cc.Type: GrantFiled: June 29, 1995Date of Patent: September 3, 1996Inventors: Rohith Shivanath, Peter Jones, Danny T. D. Thieu
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Patent number: 5540883Abstract: A method of producing bearing surfaces from powder metal blanks comprising: blending carbon and ferro alloys and lubricant with compressible elemental iron powder, pressing the blending mixture to form the powder metal blank, high temperature sintering the blank in a reducing atmosphere, compressing the powder metal blanks so as to produce a densified layer having a bearing surface, and then heat treating the densified layer.Type: GrantFiled: May 31, 1994Date of Patent: July 30, 1996Assignee: Stackpole LimitedInventors: Peter Jones, Keith Buckley-Golder
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Patent number: 5534220Abstract: A method is described for the manufacture of a sintered ferrous-based material having improved machinability, the method comprises the steps of making a mixture of a ferrous-based powder, the mixture including a compound containing at least one metal from the group comprising manganese and the alkaline-earth series of metals; at least one sulphur donating material; pressing the powder mixture and sintering the pressed mixture so as to cause the formation by reaction during sintering of at least one stable metal sulphide within the sintered material. Materials and articles made by the method are also described.Type: GrantFiled: September 30, 1994Date of Patent: July 9, 1996Assignee: Brico Engineering LimitedInventors: Charles G. Purnell, Mohammad S. Mahmoud, Helen A. Brownlie
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Patent number: 5529745Abstract: By compacting in a magnetic field a mixture containing powder raw material A having a composition represented by (Tb.sub.x Dy.sub.1-x)T.sub.y wherein T is at least one metal of Fe, Co, and Ni and 0.30<x.ltoreq.x 0.50 and 1.70.ltoreq.y.ltoreq.2.00, powder raw material B having a composition represented by (Dy.sub.1-t Tb.sub.t).sub.z T.sub.1-z wherein 0.ltoreq.t.ltoreq.0.30 and 0.40.ltoreq.z.ltoreq.0.80 and optionally, powder raw material C consisting essentially of element T, and sintering the compact, there is prepared a magnetostrictive material having a composition represented by (Tb.sub.v Dy.sub.1-v)T.sub.w wherein 0.27.ltoreq.v<0.50 and 1.70.ltoreq.w.ltoreq.2.00, with grains oriented along [111] axis. The material having minimal crystalline magnetic anisotropy at room temperature and large magnetostrains is obtained at low cost by powder metallurgy.Type: GrantFiled: April 18, 1995Date of Patent: June 25, 1996Assignee: TDK CorporationInventors: Teruo Mori, Tomoko Nakamura
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Patent number: 5520878Abstract: An unsintered aluminum nitride body including:(a) 1 to 5 weight percent of a vitreous solid of boria, alumina, and calcia in the proportions of (1) boria between 3 and 25 weight percent, (2) alumina between 10 and 50 weight percent, and (3) calcia between 40 and 80 weight percent; and(b) aluminum nitride powder as the balance of the aluminum nitride body.The invention further relates to a method of forming the unsintered aluminum nitride body and then sintering it at a temperature between 1550 and 1650 degrees Centrigrade so as to form a dense, thermally conductive aluminum nitride body.Type: GrantFiled: May 10, 1995Date of Patent: May 28, 1996Assignee: International Business Machines CorporationInventors: Peter R. Duncombe, Subhash L. Shinde, Takeshi Takamori
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Patent number: 5512236Abstract: A process of coining sintered articles of powder metal comprising: blending carbon, ferro manganese, and lubricant with compressible elemental iron powder, pressing the blended mixture to form the articles, high temperature sintering of the articles in a reducing atmosphere and then coining the sintered articles to final shape so as to narrow the tolerance variability of coined articles and substantially eliminate secondary operations.Type: GrantFiled: August 25, 1994Date of Patent: April 30, 1996Assignee: Stackpole LimitedInventors: Peter Jones, Roger Lawcock
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Patent number: 5508116Abstract: A metal matrix composite reinforced with shape memory alloy is disclosed ch is formed by blending metal particles and shape memory alloy particles to form a homogeneous powder blend, and consolidating the powder blend to form a unitary mass. The unitary mass is then plastically deformed such as by extrusion in the presence of heat so as to cause an elongation thereof, whereby the metal particles form a matrix and the shape memory alloy partices align in the direction of elongation of the unitary mass. The composite can be used in structural applications and will exhibit shape memory characteristics.Type: GrantFiled: April 28, 1995Date of Patent: April 16, 1996Assignee: The United States of America as represented by the Secretary of the NavyInventor: David J. Barrett
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Patent number: 5498393Abstract: An aluminum alloy powder or a green compact thereof is prepared, wherein: (1) the composition formula is Al.sub.100-a-b Fe.sub.a X.sub.b where a and b in atomic % are 4.0.ltoreq.a.ltoreq.6.0, 1.0.ltoreq.b.ltoreq.4.0, and where X is at least one alloy element selected from Y and Mm (mish metal); or (2) the composition formula is Al.sub.100-a-b-c Fe.sub.a Si.sub.b X.sub.c, where a, b and c in atomic % are 3.0.ltoreq.a.ltoreq.6.0, 0.5.ltoreq.b.ltoreq.3.0, and 0.5.ltoreq.c.ltoreq.3.0, and where X is at least one alloy element selected from Ti, Co, Ni, Mn and Cr, and wherein both (1) and (2) include an amorphous phase of at least 1% by volume. The aluminum alloy powder or the green compact thereof is heated at a temperature increasing at a rate of at least 80.degree. C./min. to a predetermined temperature of at least 560.degree. C. and not more than a temperature at which 10% by volume of a liquid phase is contained in the alloy powder or green compact.Type: GrantFiled: July 26, 1994Date of Patent: March 12, 1996Assignees: Honda Giken Kogyo Kabushiki Kaisha, Sumitomo Electric Industries, Ltd.Inventors: Hiroyuki Horimura, Kenji Okamoto, Masahiko Minemi, Toshihiko Kaji, Yoshishige Takano, Yoshinobu Takeda
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Patent number: 5476633Abstract: An INVAR 36 material having long-term dimensional stability is produced by sintering a blend of powders of nickel and iron under pressure in an inert atmosphere to form an alloy containing less than 0.01 parts of carbon and less than 0.1 part aggregate and preferably 0.01 part individually of Mn, Si, P, S, and Al impurities. The sintered alloy is heat treated and slowly and uniformly cooled to form a material having a coefficient of thermal expansion of less than 1 ppm/.degree.C. and a temporal stability of less than 1 ppm/year.Type: GrantFiled: July 6, 1994Date of Patent: December 19, 1995Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space AdministrationInventors: Witold M. Sokolowski, Marc S. Lane, Cheng H. Hsieh, Timothy P. O'Donnell
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Patent number: 5470527Abstract: A sputtering target that consists essentially of a continuous matrix of Ti-W phase, Ti phase having a particle diameter of 50 .mu.m or less distributed in the matrix, and a W phase having a particle diameter of 20 .mu.m or less also distributed in the matrix. Preferably the target contains aluminum in the range of 1 ppm or less. The target has high density and a low impurity content, which reduces the generation of particles from the target when it is used for sputtering. A method of manufacturing the sputtering target is also disclosed.Type: GrantFiled: September 12, 1994Date of Patent: November 28, 1995Assignee: Kabushiki Kaisha ToshibaInventors: Takashi Yamanobe, Michio Satou, Takashi Ishigami, Minoru Obata, Mituo Kawai, Noriaki Yagi, Toshihiro Maki, Shigeru Ando
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Patent number: 5466277Abstract: A sintered Al-alloy, which has a composition of 0.2 to 2.0% of Mg, 10.0 to 35.0% of Si, from 0.2 to 4.0% of Cu, and Al and unavoidable impurities in balance, is produced by using a mixture of the main powder (10.0-35.0% of Si, 0.2-2.0% of Cu, and Al and unavoidable impurities in balance) and at least one metal or mother-alloy powder selected from (a)-(i): (a) Mg powder; (b) Al--Mg powder; (c) Al--Cu powder; (d) Al--Mg--Si powder; (e) Al--Cu--Si powder; (f) Al--Mg--Cu powder; (g) Al--Mg--Cu--Si powder; (h) Mg--Cu powder; and, (i) Mg--Cu--Si powder.Type: GrantFiled: March 30, 1994Date of Patent: November 14, 1995Assignee: Showa Denko K.K.Inventors: Shin Miura, Youichi Hirose, Mitsuaki Sato
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Patent number: 5454999Abstract: A method of producing a composite powder by providing particles of, e.g., molybdenum, silicon and carbon, in a proportion relative to each other so as to possess an overall chemical composition in that segment of the ternary diagram of FIG. 1 designated A, and subjecting the particles to a mechanical alloying process under conditions and for a time sufficient to produce the composite powder. Also disclosed is a method of forming a substantially silica-free composition of matter comprising a matrix substance of MoSi.sub.2 having SiC dispersed therein, the method comprising consolidating the above-described composite powder. Also disclosed is a method of forming oxidation- and wear-resistant coatings by subjecting the composite powder whose composition lies in segment A to a metallurgical process such as plasma spraying. A method of forming a composite material of uniformly dispersed particles of silicon carbide in a silicide or an alloy silicide matrix, particularly molybdenum disilicide, is also disclosed.Type: GrantFiled: June 1, 1993Date of Patent: October 3, 1995Assignee: University of FloridaInventors: S. Jayashankar, Michael J. Kaufman
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Patent number: 5445790Abstract: A process for densifying a powder metallurgical product comprising steps of preparing a powdery starting material, pre-sintering the powdery starting material at a relatively low temperature, executing a pore-eliminating process for eliminating pores resulting from the preceding step on the powdery starting material, and sintering the powdery starting material at a relatively high temperature. It is beneficial to produce a product having a large dimension, a desired shape, and excellent mechanical properties, and being appropriate for or capable of suffering any post-treatment.Type: GrantFiled: May 5, 1994Date of Patent: August 29, 1995Assignee: National Science CouncilInventors: Chen-Ti Hu, Wen-Chih Chiou
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Patent number: 5445788Abstract: Complex-shaped parts can be produced from powders, for example metal-matrix composites, by injection molding using a mixture of the powders with a suitable binder. The binder must be removed from the powder mixture before the final thermal treatment of the so-called green part. The present invention proposes to remove the binder by surrounding a cast part with a layer of a particulate material and to subject the cast part to isostatic pressure through the surrounding layer which can thus act as an absorbent. The surrounding layer is removed after the isostatic pressing and the part can be subjected to sintering. The method is suitable for example for aluminum-ceramic powder mixtures.Type: GrantFiled: December 1, 1993Date of Patent: August 29, 1995Assignee: National Research Council of CanadaInventors: Sylvain Turenne, Paul-Emile Mongeon
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Patent number: 5443787Abstract: An iron system soft magnetic sintered body is prepared by blending an iron powder with a powder of a metal or ferroalloy so as to give a desired chemical composition and subjecting the blend to mechanical alloying, thereby alloying at least a portion of the metal or ferroalloy with iron, followed by shaping and firing. Alternatively, the same is prepared by treating an iron system alloy powder of a desired chemical composition by a mechanical grinding process, followed by shaping and firing. Even when starting with relatively large mean particle size powder, the resulting sintered body has a high density and improved magnetic properties.Type: GrantFiled: July 13, 1994Date of Patent: August 22, 1995Assignee: TDK CorporationInventors: Teruo Mori, Norishige Yamaguchi, Katsuhiko Wakayama
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Patent number: 5439500Abstract: A magneto-optical sputter target having a composition comprising at least one rare earth element and at least one transition metal, with a structure which includes a transition metal constituent and a finely mixed alloy constituent of a rare earth phase and a rare earth/transition metal intermetallic compound. The structure of the present target contains a minimum of the intermetallic compound. A method of producing the present sputter target includes mixing particles of the transition metal constituent (preferably only alloyed transition metals) with particles of the finely mixed alloy to produce a powder blend and subjecting the powder blend to a pressing operation in an oxidizing inhibiting environment for a time and at a temperature and pressure which minimizes the rare earth/transition metal intermetallic compound content of the target.Type: GrantFiled: December 2, 1993Date of Patent: August 8, 1995Assignee: Materials Research CorporationInventor: Daniel R. Marx
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Patent number: 5439499Abstract: A cermet useful in the fabrication of metal cutting, rockdrilling and mineral tools, as well as wear parts. The cermet comprises (i) a hard phase of a simple boride of a transition metal, a mixture of simple borides of transition metals, or a mixed boride of transition metals; (ii) a binder phase of Fe, Ni, Co, Cr, or alloys thereof; (iii) a dispersion of particles of oxides of transition metals in which the oxygen can be replaced by nitrogen and/or carbon; and (iv) a dispersion of oxides of metals chosen from aluminum and Group IIA and IIIA metals.Type: GrantFiled: February 26, 1993Date of Patent: August 8, 1995Assignee: Sandvik ABInventors: Henri Pastor, Colette Allibert, Laurent Ottavi, Manuel Albajar, Francisco Castro-Fernandez
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Patent number: 5433917Abstract: Process for producing novel fluxed PZT dielectric ceramic compositions having sintering temperatures below about 1000.degree., so as to be non-reactive with electrode layers when co-fired therewith. The PZT is sintered with an effective amount of an eutectic mixture of CuO and an oxide of an alkaline earth metal, preferably barium oxide and/or strontium oxide, to reduce the sintering temperature of the PZT composition below about 1000.degree. C. Dopant such as manganese oxide may be added to reduce the dielectric losses.Type: GrantFiled: September 16, 1993Date of Patent: July 18, 1995Assignee: The Penn State Research FoundationInventors: Ashvin Srivastava, Amar Bhalla, L. Eric Cross
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Patent number: 5427600Abstract: A low alloy sintered steel contains at least 0.15 percent by weight and less than 0.8 percent by weight of carbon. Its matrix is formed by a tempered martensite containing prior austenite crystal grains of not more than 15 .mu.m in mean grain size. Pores and nonmetallic inclusions contained in the matrix are not more than 50 .mu.m in maximum diameter, and the density of the low alloy sintered steel is at least 96 percent of theoretical density. A raw material powder for forming the low alloy sintered steel includes iron alloy powder which is prepared by an atomizing process, and is treated with a dry mill in an inert gas atmosphere or in the atmospheric air. Thus, dislocations are introduced into the raw material powder, and nonmetallic inclusions contained in the raw material powder are pulverized to be not more than 50 .mu.m in maximum diameter. Not only static characteristics but also dynamic characteristics, such as fatigue strength, of the low alloy sintered steel are improved.Type: GrantFiled: November 30, 1993Date of Patent: June 27, 1995Assignee: Sumitomo Electric Industries, Ltd.Inventors: Yoshiaki Itoh, Kozo Ito, Yoshinobu Takeda
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Patent number: 5421851Abstract: The present invention relates to a sintered titanium-based carbonitride alloy for milling and turning where the hard constituents are based on Ti, Zr, Hf, V, Nb, Ta, Cr, Mo and/or W and the binder phase based on Co and/or Ni. The structure comprises 10-50% by volume hard constituent grains with core-rim-structure with a mean grain size for the cores of 2-8 .mu.m in a more fine-grained matrix with a mean grain size of the hard constituents of <1 .mu.m and where said mean grain size of the coarse hard constituents grains is >1.5 .mu.m, preferably >2 .mu.m, larger than the mean grain size for the grains in the matrix. The coarse grains can be Ti(C,N), (Ti,Ta)C, (Ti,Ta)(C,N) and/or (Ti,Ta,V)(C,N).Type: GrantFiled: May 6, 1992Date of Patent: June 6, 1995Assignee: Sandvik ABInventors: Rolf G. Oskarsson, Gerold Weinl, Ake Ostlund
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Patent number: 5418071Abstract: In the present invention, metal silicide grains form an interlinked structure of a metal silicide phase, and Si grains which form a Si phase are discontinuously dispersed between the metal silicide phase to provide a sputtering target having a high density two-phased structure and having an aluminum content of 1 ppm or less. Because of the high density and high strength of the target, the generation of particles from the target during sputtering is reduced, and due to the reduced carbon content of the target, the mixing of carbon into the thin film during sputtering can be prevented.Type: GrantFiled: February 4, 1993Date of Patent: May 23, 1995Assignee: Kabushiki Kaisha ToshibaInventors: Michio Satou, Takashi Yamanobe, Takashi Ishigami, Mituo Kawai, Noriaki Yagi, Toshihiro Maki, Minoru Obata, Shigeru Ando
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Patent number: 5415829Abstract: A method of manufacturing metal silicide targets or alloy targets for sputtering use comprises the steps of (a) mechanically alloying silicon and a metal to provide a metal silicide powder or mechanically alloying silicon and a plurality of metal powders to provide an alloy powder, (b) and then pressing the metal silicide powder or alloy powder. The invention also relates to the metal silicide targets or alloy targets so manufactured. In the mechanical alloying step, rapid and fine division and agglomeration of the mixed powder is repeated until the particles of the material powders are finely divided to a submicron level. They form aggregates tens of microns in diameter. The aggregates gradually take an equi-axed shape. Homogenization of the material powder mixture progresses to mixing on the atomic level, until alloying takes place.Type: GrantFiled: December 22, 1993Date of Patent: May 16, 1995Assignee: Nikko Kyodo Co., Ltd.Inventors: Tateo Ohhashi, Takakazu Seki, Takeo Okabe, Koichi Yasui, Hideaki Fukuyo
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Patent number: 5415831Abstract: The method serves to produce a material based on a doped intermetallic compound. In carrying out the method, at least two differently doped powders each based on the intermetallic compound are selected. One of the two powders predominantly has coarse-grained particles. On the other hand, another powder is formed from comparatively fine-grained particles composed of a material having a lower creep strength but a higher ductility than the material of the coarse-grained powder. The at least two powders are mixed with one another in a ratio serving to establish a desired mixed microstructure and then hot-compacted and heat-treated to form the material.Material produced by this method is suitable for components which are exposed to high mechanical loads at high temperatures, such as, in particular, gas-turbine blades or turbine wheels of turbo chargers.Type: GrantFiled: December 13, 1993Date of Patent: May 16, 1995Assignee: ABB Research Ltd.Inventors: Robert Baumann, Joachim Rosler, Christoph Tonnes
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Patent number: 5413753Abstract: Methods of forming composite articles of superconducting materials and metal at ambient temperature by applying a mixture of metal and binder to a ceramic oxide preform to yield a coated preform which is then heat treated to provide composite articles of superconducting ceramic and metal.Type: GrantFiled: September 17, 1993Date of Patent: May 9, 1995Assignee: E. I. Du Pont de Nemours and CompanyInventor: George E. Zahr
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Patent number: 5407633Abstract: Method of manufacturing a dispenser cathode, in which method tungsten and a scandium-containing material are mechanically alloyed and the product thus formed is pressed into a cathode body. The cathode body is further provided with a barium-containing component. In the mechanical alloying process the tungsten is highly deformed and the scandium-containing material is mixed with the tungsten so as to be very finely distributed therein, so that an improved dispensation of scandium and hence an improved recovery after ion bombardment of the final cathode is attained.Type: GrantFiled: March 15, 1994Date of Patent: April 18, 1995Assignee: U.S. Philips CorporationInventors: Jan Hasker, Robert H. Kane, Paul D. Goodell, Jacobus A. J. M. Deckers
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Patent number: 5384087Abstract: The present invention relates to a process for making an aluminum silicon carbide composite material in strip form. The process comprises blending a powdered aluminum matrix material and a powdered silicon carbide material, roll compacting the blended powdered materials in an inert atmosphere to form a green strip having a first thickness, and directly hot working the blended and roll compacted materials to bond the aluminum matrix material particles and the silicon carbide particles and to form a thin strip material having a desired thickness.Type: GrantFiled: April 6, 1992Date of Patent: January 24, 1995Assignee: Ametek, Specialty Metal Products DivisionInventor: Clive Scorey
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Patent number: 5382405Abstract: A method of manufacturing a shaped article from a powdered precursor, wherein the components of the powdered precursor are subjected to a self-propagating high-temperature synthesis (SHS) reaction and are consolidated essentially simultaneously. The shaped article requires essentially no machining after manufacture.Type: GrantFiled: September 3, 1993Date of Patent: January 17, 1995Assignee: Inland Steel CompanyInventors: Kenneth F. Lowrance, II, Eric C. Knorr, William M. Goldberger, Daniel Boss, Doreen Edwards
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Patent number: 5368812Abstract: Metal carbides may be formed by mixing metal powder with a stoichiometric amount of graphite, compressing the same in a mould/die and then sintering. High temperatures (and maybe a bonding agent) are required to effect the final step and finished product. These disadvantages are overcome by exploiting dry high energy milling to bring the starting materials into a very finely divided and reactive state, with regions of metal, carbon and metal based solid solution ranging from 3 to 100 nanometers in diameter. As an alternative source of carbon, cationic organic surfactants may be used instead of graphite in the appropriate proportion. Compacting the milled mixture, followed by sintering at lower temperatures by a margin of at least 400.degree. C., will produce very strong dense carbides at low cost. The method may be extended to include metal based composites, which also includes cermets, by incorporating an appropriate excess of metal powder(s) in the starting materials.Type: GrantFiled: December 10, 1992Date of Patent: November 29, 1994Assignee: Australian National UniversityInventors: Andrzej Calka, Barry W. Ninham
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Patent number: 5364587Abstract: Master alloys and methods of producing same are disclosed, wherein an intermetallic compound is first prepared via thermite processing, then size reduced, then mixed with other components in amounts yielding a mixture in the desired proportion for the master alloy. The mixture is compacted, then heated to produce the master alloy, which is used for making Nickel-based alloys used, (for example), in hydrogen battery electrodes.Type: GrantFiled: July 23, 1992Date of Patent: November 15, 1994Assignee: Reading Alloys, Inc.Inventor: Frederick H. Perfect, deceased
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Patent number: 5358685Abstract: A new silicon carbide material is made following a procedure including hot pressing to provide a finished product having a microstructure with an optimal grain size of less than 7 micrometers. The material exhibits a dominant failure mode of intergranular fracture requiring significant energy for crack propagation. The method of manufacturing is cost-effective by allowing the use of "dirty" raw materials since the process causes impurities to segregate at multi-grain boundary junctions to form isolated pockets of impurities which do not affect the structural integrity of the material. End uses include use as optical and electronic substrate materials.Type: GrantFiled: September 3, 1993Date of Patent: October 25, 1994Assignee: Cercom Inc.Inventor: Andre Ezis
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Patent number: 5342573Abstract: A method of producing a tungsten heavy alloy product according to a powder metallurgical procedure utilizing the injection molding technique which enables production of tungsten heavy alloy products having high dimensional accuracy and complex configuration and yet having high physical strength and toughness in high productivity and at low cost. A powder mixture of tungsten powder and nickel powder, iron powder or copper powder is mixed with an organic binder and they are kneaded together. The kneaded mixture is injection molded into a predetermined shape, and thereafter the binder is removed from the molded product. Subsequently, the molded product is sintered in a temperature range of from the melting point of the bond phase of nickel, iron or copper to +50.degree. C. relative to the melting point.Type: GrantFiled: August 20, 1992Date of Patent: August 30, 1994Assignee: Sumitomo Electric Industries, Ltd.Inventors: Yoshinari Amano, Masahiro Omati, Junzo Matsumura
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Patent number: 5326526Abstract: Sintered iron alloy composition and method of manufacturing the same, the sintered alloy composition comprising: about 1.5 to about 2.5% carbon by weight; about 0.5 to about 0.9% manganese by weight; about 0.1 to about 0.2% sulfur by weight; about 1.9 to about 2.5% chromium by weight; about 0.15 to about 0.3% molybdenum by weight; about 2 to about 6% copper by weight; not more than about 0.3% by weight of a metal element material comprising at least one member selected from the group consisting of tungsten and vanadium; an effective content of a first solid lubricant material comprising at least one member selected from the group consisting of magnesium metasilicate minerals and magnesium orthosilicate minerals; and balance iron. This alloy composition is preferably used for making machine parts, such as slide members of valve operating systems for internal combustion engines.Type: GrantFiled: September 30, 1991Date of Patent: July 5, 1994Assignees: Hitachi Powdered Metals Co., Ltd., Nissan Motor Co., Ltd.Inventors: Yutaka Ikenoue, Koichiro Hayashi, Makoto Kano, Akira Fujiki
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Patent number: 5322666Abstract: The invention provides a method of mechanical alloying a titanium-base metal powder. Titanium-base metal powder is provided in a mechanical alloying apparatus. The mechanical alloying apparatus has a controlled atmosphere to prevent excessive oxidation of the titanium-base metal powder. An effective amount of tin process control agent is added to the mechanical alloying apparatus. The mechanical alloying apparatus is operated to weld and fracture the titanium-base metal powder in a manner controlled by the tin process control agent. The controlled welding and fracturing ultimately forms a titanium-base mechanically alloyed powder.Type: GrantFiled: March 24, 1992Date of Patent: June 21, 1994Assignee: Inco Alloys International, Inc.Inventor: Arunkumar S. Watwe
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Patent number: 5314656Abstract: Transition metal carbonitrides (in particular, titanium carbonitride, TiC.sub.0.5 N.sub.0.5) are synthesized by a self-propagating reaction between the metal (e.g., titanium) and carbon in a nitrogen atmosphere. Complete conversion to the carbonitride phase is achieved with the addition of TiN as diluent and with a nitrogen pressure .gtoreq.0.6 MPa. Thermodynamic phase-stability calculations and experimental characterizations of quenched samples provided revealed that the mechanism of formation of the carbonitride is a two-step process. The first step involves the formation of the nonstoichiometric carbide, TiC.sub.0.5, and is followed by the formation of the product by the incorporation of nitrogen in the defect-structure carbide.Type: GrantFiled: November 20, 1992Date of Patent: May 24, 1994Assignee: The Regents of the University of CaliforniaInventors: Zuhair A. R. Munir, Maryam Eslamloo-Grami
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Patent number: 5302181Abstract: An oxide-dispersion-strengthened sintered alloy improved in oxidation resistance and compressive strength for use at high temperatures of at least 1350.degree. C. The alloy includes a matrix of a metal consisting substantially or predominantly of Cr, and 0.2 to 2.0% by weight of Y.sub.2 O.sub.3 uniformly dispersed in the matrix. The Y.sub.2 O.sub.3 as uniformly dispersed is up to 0.1 .mu.m in mean particle size.Type: GrantFiled: April 14, 1992Date of Patent: April 12, 1994Assignee: Kubota CorporationInventors: Toshiaki Morichika, Takashi Onishi, Hiroshi Yamamoto, Koichi Yanai, Hiroyuki Araragi
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Patent number: 5296189Abstract: Methods of fabricating powders of metal particles containing grain growth control additives are described. A powder, metal particles, e.g., copper particles, are mixed with a powder of additive particles, e.g., alumina particles. The mixture is milled in a high energy ball mill to provide metal particles having substantially uniformly distributed therein of additive particles. The ball milled powder contains elongated high aspect ratio particles. The high aspect ratio particles are reduced in size by jet impact milling. The jet impact milled powder can be used to form a conductor forming paste in the fabrication of a metallized ceramic substrate for semiconductor chip packaging application. The jet impact milled powder has particles of sufficiently small in size to fill vias between metallization layers in the green ceramic precursor to the ceramic substrate.Type: GrantFiled: April 28, 1992Date of Patent: March 22, 1994Assignee: International Business Machines CorporationInventors: Sung K. Kang, Sampath Purushothaman, John J. Ritsko, Jane M. Shaw, Subhash L. Shinde
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Patent number: 5284615Abstract: The present invention presents a method of processing ferrous powder materials to produce small component parts exhibiting excellent soft magnetic properties, in particular, residual magnetic flux density. The processing steps involve, in part, mixing with a binder, dewaxing or presintering at a temperature higher than in the conventional dewaxing process, followed by final sintering and a further conversion sintering, at a temperature lower than in the conventional sintering process, to produce parts having density values of over 96% theoretical density and excellent soft magnetic properties. The invented method is suitable for producing small component parts having sufficient strength and excellent soft magnetic properties to make them suitable for miniaturized electrical and electronic equipment.Type: GrantFiled: July 15, 1992Date of Patent: February 8, 1994Assignee: Mitsubishi Materials CorporationInventors: Koshiro Ueda, Mutsumi Moribayashi, Tohru Kohno
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Patent number: 5279786Abstract: Multi-layer, porous material and process of manufacturing same produced from aluminum scrap powder by means of a centrifugal atomizer for use in noise absorbing devices and filter elements. The multi-layers are arranged according to increasing particle size so that a first layer contains the largest particle size and a last layer contains the smallest particle size. Arranging the layer sin this manner produces a multilayer porous material having a shell configuration of a conch which effectively absorbs noise.Type: GrantFiled: October 13, 1992Date of Patent: January 18, 1994Assignee: Jae Chang ByunInventor: Seong S. Cho
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Patent number: 5173107Abstract: The invention relates to a composite hard metal body of hard material, a binder and embedded reinforcing material, as well as to a process for the production of the composite hard metal body by methods of powder metallurgy.In order to create a composite hard metal body with improved toughness under load, improved hardness and a lower fracture susceptibility, the invention proposes to build in monocrystalline, preferably needle-shaped and/or platelet-shaped reinforcing materials, coated with an inert layer with respect to the binder metal phase and consisting of borides and/or carbides, and/or nitrides and/or carbonitrides of the elements of Groups IVa or Va or mixtures thereof and/or coated monocrystalline reinforcing material of SiC, Si.sub.3 N.sub.4, Si.sub.2 N.sub.2 O, Al.sub.2 O.sub.3, ZrO.sub.2, AlN and/or BN.Type: GrantFiled: June 10, 1991Date of Patent: December 22, 1992Assignee: Krupp Widia GmbHInventors: Klaus Dreyer, Hans Kolaska
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Patent number: 5167697Abstract: A substrate material for mounting a semiconductor device thereon, comprises a skeleton prepared by liquid-phase presintering the composition of W and/or Mo powder in which Cu and/or Ag powder is uniformly dispersed, and a Cu and/or Ag phase infiltrated into the pores of the skeleton. The total amount of Cu and/or Ag in the product is adjusted to 10-50 vol. %. The substrate material is manufactured by two steps of: presintering the Cu and/or Ag-contng. powdery composition to form a porous skeleton, and infiltrating Cu and/or Ag into the pores of the skeleton. Since the skeleton contng. Cu and/or Ag exhibits an excellent affinity to molten Cu and/or Ag, the infiltration of molten Cu and/or Ag is performed uniformly into every nook and corner of the skeleton. Consequently, the obtained product is free from pores which would deteriorate a junction plane between the substrate and a semiconductor device mounted thereon.Type: GrantFiled: April 17, 1991Date of Patent: December 1, 1992Assignee: Nippon Tungsten Co., Ltd.Inventors: Takeshie Koumura, Yoshihiro Umeda, Jitsuo Matsumoto
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Patent number: 5160534Abstract: Ti-W target material for sputtering includes a structure composed of a W phase, a Ti phase, and a Ti-W alloy phase of which 20% or more consist of the area ratio of a micro structure covering the cross section of the Ti-W target material. The Wi-W target material further includes dispersed tungsten particles, the Ti-W alloy phases substantially surrounding the W grains, and the Ti phases dispersed adjacent to the Ti-W alloy phase or the W grains. The formation of the Ti-W alloy phases is capable of reducing a substantial amount of the Ti phase in the target material. It is thus possible to prevent the generation of particles attributable to a difference between sputtering speeds of Ti and Ti-W.Type: GrantFiled: May 31, 1991Date of Patent: November 3, 1992Assignee: Hitachi Metals Ltd.Inventor: Akitoshi Hiraki
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Patent number: 5149496Abstract: A magnesium based metal matrix composite is made from rapidly solidified magnesium alloy powder and SiC particulate using liquid suspension coprocessing or mechanical alloying. The composite is suitable for consolidation into bulk shapes having, in combination, high strength, high stiffness, low density, low coefficient of thermal expansion, and high hardness. The composite is suited for uses in such applications as space and missile guidance and navigation and control system precision components where low density, very high specific stiffness and long term dimensional and environmental stability are principal performance criteria.Type: GrantFiled: January 27, 1992Date of Patent: September 22, 1992Assignee: Allied-Signal Inc.Inventors: Santosh K. Das, Chin-Fong Chang, Derek Raybould
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Patent number: 5145513Abstract: A process for the preparation of composite materials consisting essentially of an oxide phase and a metal phase is effected by grinding a mixture of at least one oxide precursor of the metal phase of the composite with at least one reducing agent, the reducing agent being a precursor of the oxide phase. The grinding being performed in a high energy mechanical grinder for a sufficient length of time so that at least 80 percent of the oxide precursor is reduced to metal or to a metal alloy. The process is particularly valuable for the preparation of oxide/metal composite materials which have improved mechanical, electrical or radiation absorption properties.Type: GrantFiled: April 12, 1991Date of Patent: September 8, 1992Assignee: Centre National de le Recherche ScientifiqueInventors: Paolo Matteazzi, Gerard Le Caer, Elizabeth Grosse-Bauer
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Patent number: 5120351Abstract: This invention is a ferrite molding made by a manufacturing method of molding and sintering ferrite particles, which are made by pre-sintering of magnetic materials including iron oxide, together with metallic particles mixed therein by a hydrostatic pressing at extra-high pressure, whereby metal fills in between the ferrite particles. The ferrite molding has improved ductility so as to resist chipping and breaking and has extremely low hydroscopicity so as to maintain its characteristics.Type: GrantFiled: April 9, 1991Date of Patent: June 9, 1992Assignee: Kitagawa Industries Co., Ltd.Inventor: Hiroji Kitagawa
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Patent number: 5118341Abstract: The invention provides a sinterable brass powder blend, comprising about 90% to about 99% by weight of brass powder, about 0.2% to about 6.0% by weight manganese sulfide, and 0% to about 5.0% by weight of lubricants, binders, graphite, sintering enhancing additives and mixtures thereof.The invention also provides methods for making lead-free but machinable sintered brass powder metal parts.Type: GrantFiled: March 28, 1991Date of Patent: June 2, 1992Assignee: Alcan Aluminum CorporationInventors: Edul M. Daver, Krishnakant B. Patel
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Patent number: 5110349Abstract: A cutting insert of a sintered carbonitride alloy and with a complicated geometry, the insert having improved efficiency. This is obtained by giving the powder non-uniform compaction during pressing of the powder into a press-body so that the ultimate working edges will have a higher relative density than the surrounding, more "supporting" material in the press-body. By these means are often obtained surface defects in the form of cracks because of dissolved strains during the sintering.Type: GrantFiled: November 14, 1990Date of Patent: May 5, 1992Assignee: Sandvik ABInventors: Kenneth Westergren, Gerold Weinl, Rolf Oskarsson
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Patent number: 5098469Abstract: A powder metallurgy process for producing near-net shape, near-theoretical density structures of multiphase nickel, aluminum and/or titanium intermetallic alloys is provided by employing pressureless sintering techniques. The process consists of blending a brittle aluminide master alloy powder with ductile nickel powder, so as to achieve the desired composition. Then, after cold compaction of the powdered mixture, the compact is liquid phase sintered. The four step liquid phase sintering process is intended to ensure maximum degassing, eliminate surface nickel oxide, homogenize the alloy, and complete densification of the alloy by liquid phase sintering.Type: GrantFiled: September 12, 1991Date of Patent: March 24, 1992Assignee: General Motors CorporationInventor: Vadim Rezhets
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Patent number: H1411Abstract: Magnesium lithium based alloys prepared by mechanical alloying are disclosed.Type: GrantFiled: November 12, 1992Date of Patent: February 7, 1995Inventor: Uday V. Deshmukh