Rolling Patents (Class 419/43)
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Patent number: 10431807Abstract: The present invention discloses a method of manufacturing a lithium-ion secondary battery electrode. The method includes the steps of: supplying composite particles (1), each containing an active material (2) and a binder (4), onto a sheet collector (42); and rolling the composite particles (1) supplied onto the collector (42), thus forming an active material layer (44). The rolling step includes a first rolling sub-step involving first rolling, and a second rolling sub-step to be performed after the first rolling sub-step. Rubber rolls (R1) are preferably used in the first rolling sub-step.Type: GrantFiled: September 8, 2015Date of Patent: October 1, 2019Assignees: TOYOTA JIDOSHA KABUSHIKI KAISHA, Zeon CorporationInventors: Kazuhiro Suzuki, Yasuhiro Sakashita, Yuji Shibata, Takahiro Ogawa
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Patent number: 8790572Abstract: Titanium flat product is produced by passing a titanium powder green flat material through a pre-heating station and heated under a protective atmosphere to a temperature at least sufficient for hot rolling. The pre-heated flat material then is passed through a rolling station while still under a protective atmosphere and hot rolled to produce a hot rolled flat product of a required level of hot densification. The hot rolled flat product is passed through a cooling station while still under a protective atmosphere, and cooled to a temperature at which it can be passed out of a protective atmosphere. In the process, the hot rolling provides the predominant hot densification mechanism involved.Type: GrantFiled: April 4, 2008Date of Patent: July 29, 2014Assignee: Commonwealth Scientific and Industrial Research OrganisationInventors: Nigel Austin Stone, Robert Wilson, Merchant Yousuff, Mark Gibson
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Patent number: 8293377Abstract: An object of this invention is to provide a case for rolling powder alloy without failures at the time of rolling. The case for rolling powder alloy (1) is formed like a shape of box and comprises a side constituent member (10) forming like a rectangular frame in a combination of two members (10a, 10a) and surrounding a side surface of metal powder, an upper lid constituent member (11) mounting on one opening of the side constituent member (10) and covering an upper surface of the metal powder, and a lower lid constituent member (12) mounting on the other opening of the side constituent member (10) and covering a lower surface of the metal powder. The peripheral edges of the upper lid constituent member (11) and the lower lid constituent member (12) are, respectively, provided with a peripheral wall (11b, 12b) standing upright along an outer peripheral surface of the side constituent member, and the side constituent member (10) is inserted into a space surrounded by the peripheral wall (11b, 12b).Type: GrantFiled: March 11, 2008Date of Patent: October 23, 2012Assignee: Nikkeikin Aluminum Core Technology Company Ltd.Inventors: Toshimasa Nishiyama, Hideki Hommo, Tsutomu Komata
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Patent number: 8231827Abstract: A method of manufacturing powder metal plates comprising feeding a predetermined mass of metal powder onto a moving tape (101), restricting the metal powder by surrounding the metal powder with vibrating boundary walls (201, 202) extending parallel to the direction of movement of the tape, rolling the metal powder at an ambient temperature to form a green compact strip (GS), continuously sintering the green compact strip in a furnace (400), forming the green compact strip to a net shape part (NS) while in the furnace, and cooling the net shape part in a non-oxidizing environment (404) at a temperature in excess of 1000 degrees Celsius.Type: GrantFiled: June 17, 2009Date of Patent: July 31, 2012Assignee: The Gates CorporationInventors: Yahya Hodjat, Roger Lawcock, Rohith Shivanath
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Publication number: 20110286873Abstract: The composition includes the iron as the main particulate metallic material; at least one particulate alloy element, with the function of hardening the ferrous structural matrix; and a precursor non-metallic particulate compound, generally a carbide or a carbonate, which is capable of generating, upon its dissociation during the sintering, graphite nodules, whose formation is facilitated: by the precursor compound itself when it includes a chemical element which stabilizes the iron alpha phase of the ferrous structural matrix; or by an additional alloy element included in the composition and which is defined by a chemical element that stabilizes the iron alpha phase during the sintering. The composition can be conformed by compaction or by powder injection molding. The process of the invention leads to obtaining products in self-lubricating sintered steel from said composition.Type: ApplicationFiled: December 9, 2009Publication date: November 24, 2011Inventors: Roberto Binder, Aloisio Nelmo Klein, Cristiano Binder, Waldyr Ristow Junior
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Patent number: 7854887Abstract: A method of producing an aluminum matrix composite material is described that comprises the steps of: mixing an aluminum powder and a ceramic powder to prepare a mixed powder; providing a lower casing made of aluminum and formed in a hollow rectangular parallelepiped shape having an open top, and a closing member made of aluminum and formed in a shape adapted to hermetically close the open top of the lower casing; packing the mixed powder into the lower casing; closing the open top of the lower casing filled with the mixed powder, by the closing member, to prepare a pre-rolling assembly having the mixed powder hermetically sealed therein; preheating the pre-rolling assembly; and rolling the preheated assembly to obtain the aluminum matrix composite material, where the aluminum matrix composite material includes a pair of metal plates having the mixed powder therebetween.Type: GrantFiled: October 23, 2007Date of Patent: December 21, 2010Assignees: Nippon Light Metal Co., Ltd., Nikkeikin Aluminum Core Technology Co., Ltd.Inventors: Toshimasa Nishiyama, Kazuto Sanada, Hideki Honmou
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Patent number: 7854886Abstract: A method of producing an aluminum matrix composite material is described that comprises the steps of: mixing an aluminum powder and a ceramic powder to prepare a mixed powder; providing a lower casing made of aluminum and formed in a hollow rectangular parallelepiped shape having an open top, and a closing member made of aluminum and formed in a shape adapted to hermetically close the open top of the lower casing; packing the mixed powder into the lower casing; closing the open top of the lower casing filled with the mixed powder, by the closing member, to prepare a pre-rolling assembly having the mixed powder hermetically sealed therein; preheating the pre-rolling assembly; and rolling the preheated assembly to obtain the aluminum matrix composite material, where the aluminum matrix composite material includes a pair of metal plates having the mixed powder therebetween.Type: GrantFiled: October 23, 2007Date of Patent: December 21, 2010Assignees: Nippon Light Metal Co., Ltd., Nikkeikin Aluminum Core Technology Co., Ltd.Inventors: Yuichi Tamaki, Kazuto Sanada, Toshimasa Nishiyama
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Patent number: 7641850Abstract: A technique for net shaping gear teeth of a high performance power transmission gear from a powder metal workpiece includes heating a powder metal workpiece in the form of a near net shaped gear blank having gear teeth surfaces above its critical temperature to obtain an austenitic structure throughout its surfaces, isothermally quenching the workpiece at a rate greater than the critical cooling rate of its surfaces to a uniform metastable austenitic temperature just above the martensitic transformation temperature, rolling the gear teeth surfaces of the workpiece to a desired outer peripheral profiled shape between opposed dies, each die having an outer peripheral profiled surface, while holding the workpiece at the uniform metastable austenitic temperature, the gear teeth surfaces undergoing densification, plastic deformation, and strengthening as a result of the rolling operation, and cooling the workpiece through the martensitic range to thereby harden the surfaces of the gear teeth.Type: GrantFiled: March 17, 2004Date of Patent: January 5, 2010Assignee: The Penn State Research FoundationInventors: Nagesh Sontti, Maurice F. Amateau, Suren B. Rao
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Patent number: 7560066Abstract: A composite article that can be used as a substrate for coated conductors is disclosed. The composite substrate has at least three layers in which one or more inner layers of Ni—W alloys with 9 at. %-13 at. % W and two outer layers of Ni—W alloys with 3 at. %-9 at. % W. The content of W element gradually decreases from the inner layers to the outer layers. The composite substrate can be prepared using a process of designing and sintering composite ingot, rolling composite ingot and then annealing composite substrate. The composite substrate have a dominant cube texture on the outer layer of the whole substrate which have a weaker magnetism and higher strength than that of a single Ni-5 at. % W alloy substrate.Type: GrantFiled: December 7, 2006Date of Patent: July 14, 2009Assignee: Beijing University of TechnologyInventors: Meiling Zhou, Hongli Suo, Min Liu, Yue Zhao, Dong He, Yingxiao Zhang, Lin Ma, Yaming Li, Jie Zhou, Yonghua Zhu, Shuai Ye, Lingji Ma, Zili Zhang, Tieyong Zuo
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Publication number: 20080181805Abstract: A nanocomposite comprising a plurality of nanoparticles dispersed in a molybdenum-based matrix, and an x-ray tube component formed from such a nanocomposite. The nanocomposite contains volume fraction of nanoparticle dispersoids in a range from about 2 volume percent to about 20 volume percent. A method of making such molybdenum-based nanocomposites is also disclosed.Type: ApplicationFiled: June 28, 2007Publication date: July 31, 2008Applicant: GENERAL ELECTRIC COMPANYInventors: Pazhayannur Ramanathan Subramanian, Judson Sloan Marte, Paul Leonard Dupree
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Publication number: 20080166579Abstract: A method for producing an at least partially surface-densified metallic toothed element comprising a densified sintering material, in order to improve a strength profile, a preform of the toothed element being produced with a locally selective oversize profile relative to a final size of the toothed element and being rolled to the final size by means of at least one rolling die, the toothed element being densified in locally varied manner at least in the region of at least one flank and/or one root of a tooth of the toothed element to produce a densified outer layer.Type: ApplicationFiled: December 10, 2007Publication date: July 10, 2008Inventor: Gerhard Kotthoff
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Patent number: 7387230Abstract: In order to provide a brazing sheet having excellent workability, a powder of a brazing filler metal composition is obtained from a single type of powder or by mixing two or more powders to form the brazing filler metal composition. By powder roll compaction of the powder, the powder is formed into a sheet shape.Type: GrantFiled: December 26, 2003Date of Patent: June 17, 2008Assignee: Ishikawajima-Harima Heavy Industries Co., Ltd.Inventors: Chitoshi Mochizuki, Takayuki Iwasaki, Hiroki Yoshizawa
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Patent number: 7311873Abstract: The invention relates to manufacturing of fully dense strips, plates, sheets, and foils from titanium alloys, titanium metal matrix composites, titanium aluminides, and flat multilayer composites of said materials by direct powder rolling of blended powders followed by sintering. The resulting titanium alloy flat products have properties that meet or exceed the conventional ingot metallurgy alloys and are suitable for aerospace, automotive, sporting goods, and other applications. The process includes: (a) providing C.P.Type: GrantFiled: December 30, 2004Date of Patent: December 25, 2007Assignee: ADMA Products, Inc.Inventors: Vladimir S. Moxson, Volodymyr A. Duz
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Patent number: 7297271Abstract: Provided are a porous sintered compact suitable for a filter, a power feeder in a polymer electrolyte membrane type water electrolyzer, a current collector in a solid polymer fuel cell and in addition a liquid dispersion plate, especially an ink dispersion plate for an ink jet printer ink and the like. A titanium powder sintered compact made of a plate-like porous compact is obtained by sintering spherical powder made of titanium or a titanium alloy produced by means of a gas atomization method. A void ratio in the range of from 35 to 55% is realized by filling without applying a pressure and sintering without applying a pressure.Type: GrantFiled: August 10, 2006Date of Patent: November 20, 2007Assignee: Sumitomo Titanium CorporationInventors: Takashi Onishi, Tadashi Ogasawara, Munetoshi Watanabe, Masamichi Kato
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Patent number: 6767416Abstract: A corrosion resistant, high strength austenitic stainless steel consisting of 1.0% or less of Si, 2.0% or less of Mn, 0.5% or less of O, 7 to 30% of Ni, 14 to 26% of Cr, 0.3% or less of combination of C and N, at least one element selected from the group consisting of 1.0% or less of Ti, 2.0% or less of Zr and 2.0% or less of Nb, and the balance consisting of Fe and unavoidable impurities, the percentage being given in weight basis; said steel containing carbonitride with a grain size of several to 100 nm dispersed therein; said steel having an average crystal grain size of 1 &mgr;m or less; and said steel containing 90% by volume or more of austenite phase; is excellent in strength and corrosion resistance.Type: GrantFiled: February 27, 2002Date of Patent: July 27, 2004Assignee: Hitachi, Ltd.Inventors: Ryo Ishibashi, Yasuhisa Aono
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Patent number: 6696168Abstract: A composite strip of compacted powders, which has a three layers structure, is continuously obtained by means of a rolling machine for powder compacting. The composite strip is sintered at a temperature of 460° C. to 550° C. to form a sintered composite strip. The sintered composite strip is continuously bonded by rolling to a steel strip. The bonded composite strip is optionally subjected to a heat treatment of heating at a temperature of 250° C. to 400° C. followed by heating to a temperature of 400° C. to 510° C., holding the strip under the temperature for not less than 30 seconds, and rapidly cooling down to 300° C. at a cooling rate of not lower than 50° C./minute, whereby obtaining a multi-layered composite material consisting of the steel strip, a sintered bonding layer, a sintered sliding layer and a sintered sacrificial layer.Type: GrantFiled: April 29, 2002Date of Patent: February 24, 2004Assignee: NDC Company Ltd.Inventors: Yasukuni Hasegawa, Koue Ohkawa, Hiroyuki Sugawara
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Patent number: 6679745Abstract: An improved method is described for the manufacture of mercury dispenser devices to be used in fluorescent lamps, of the type wherein the dispenser material (2) is contained inside a metal tube (1), these dispensers providing a more uniform distribution of mercury, with lower fluctuations from one device to the other.Type: GrantFiled: October 25, 2001Date of Patent: January 20, 2004Assignee: SAES Getters S.p.A.Inventors: Gianni Santella, Ausonio Tuissi
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Patent number: 6660109Abstract: A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as ≦1% Cr, ≧0.05% Zr ≦2% Ti, ≦2% Mo, ≦1% Ni, ≦0.75% C, ≦0.1% B, ≦1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, ≦1% rare earth metal, and/or ≦3% Cu.Type: GrantFiled: October 31, 2001Date of Patent: December 9, 2003Assignee: Chrysalis Technologies IncorporatedInventors: Mohammad R. Hajaligol, Clive Scorey, Vinod K. Sikka, Seetharama C. Deevi, Grier Fleishhauer, A. Clifton Lilly, Jr., Randall M. German
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Patent number: 6372362Abstract: A method for forming a composite vapor-deposited film one side of which suitable for vapor-deposition on a phosphor surface of a CRT, such as a color television picture tube, has high light reflectivity, and the other side of which has a property to absorb radiant heat, and a composite vapor-deposition material suitable for vacuum deposition are disclosed. The composite vapor-deposition material has a high vapor-pressure metal envelope and a low vapor-pressure metal in the core region of the envelope. Low vapor-pressure metal powder should preferably be dispersed and held by high vapor-pressure metal powder in the core region. Vacuum deposition using this composite vapor-deposition material yields a composite deposited film having a composition comprising almost 100% of the high vapor-pressure metal formed in the initial stage of evaporation, and a composition comprising 100% of the low vapor-pressure metal formed in the final stage of evaporation.Type: GrantFiled: March 24, 2000Date of Patent: April 16, 2002Assignee: Hitachi Metals, Ltd.Inventors: Shinji Furuichi, Shigetoshi Takashima
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Patent number: 6332936Abstract: A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as ≦1% Cr, ≧0.05% Zr ≦2% Ti, ≦2% Mo, ≦1% Ni, ≦0.75% C, ≦0.1% B, ≦1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, ≦1% rare earth metal, and/or ≦3% Cu.Type: GrantFiled: September 20, 1999Date of Patent: December 25, 2001Assignee: Chrysalis Technologies IncorporatedInventors: Mohammad R. Hajaligol, Clive Scorey, Vinod K. Sikka, Seetharama C. Deevi, Grier Fleischhauer, A. Clifton Lilly, Jr., Randall M. German
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Patent number: 6294130Abstract: A metallic alloy composition is manufactured into products such as press formed or stamped products or rolled products such as sheet, strip, rod, wire or band by one or more cold working steps with intermediate or final flash annealing. The method can include cold rolling an iron, nickel or titanium aluminide alloy and annealing the cold worked product in a furnace by infrared heating. The flash annealing is preferably carried out by rapidly heating the cold worked product to an elevated temperature for less than one minute. The flash annealing is effective to reduce surface hardness of the cold worked product sufficiently to allow further cold working. The product to be cold worked can be prepared by casting the alloy or by a powder metallurgical technique such as tape casting a mixture of metal powder and a binder, roll compacting a mixture of the powder and a binder or plasma spraying the powder onto a substrate.Type: GrantFiled: March 24, 2000Date of Patent: September 25, 2001Assignee: Chrysalis Technologies IncorporatedInventors: Mohammad R. Hajaligol, Vinod K. Sikka
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Patent number: 6143241Abstract: A metallic alloy composition is manufactured into products such as press formed or stamped products or rolled products such as sheet, strip, rod, wire or band by one or more cold working steps with intermediate or final flash annealing. The method can include cold rolling an iron, nickel or titanium aluminide alloy and annealing the cold worked product in a furnace by infrared heating. The flash annealing is preferably carried out by rapidly heating the cold worked product to an elevated temperature for less than one minute. The flash annealing is effective to reduce surface hardness of the cold worked product sufficiently to allow further cold working. The product to be cold worked can be prepared by casting the alloy or by a powder metallurgical technique such as tape casting a mixture of metal powder and a binder, roll compacting a mixture of the powder and a binder or plasma spraying the powder onto a substrate.Type: GrantFiled: February 9, 1999Date of Patent: November 7, 2000Assignee: Chrysalis Technologies, IncorporatedInventors: Mohammad R. Hajaligol, Vinod K. Sikka
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Patent number: 6063332Abstract: The method of making the metal fiber sintered body includes making a coiled material by coiling a thin sheet of Fe--Cr--Al--La, Fe--Cr--Al--Y or Fe--Cr--Al--Ce stainless steel; making a tow of Fe--Cr--Al--La, Fe--Cr--Al--Y or Fe--Cr--Al--Ce continuous fibers by lathe turning an end face of the coiled material at a tool feed speed of from 5 to 40 .mu.m/rev; extending the tow in a width direction and cutting the tow with a roller type cutting assembly to form Fe--Cr--Al--La, Fe--Cr--Al--Y or Fe--Cr--Al--Ce stainless steel fibers having a fiber length of 20 to 200 mm; feeding the Fe--Cr--Al--La, Fe--Cr--Al--Y or Fe--Cr--Al--Ce stainless steel fibers having the fiber length of 20 to 200 mm to a conveyor; dropping the stainless steel fibers onto the conveyor and dispersing the stainless steel fibers by making an air current act on the stainless steel fibers; transporting the resulting sheet-shaped accumulation on the conveyor and compressing it to form a web and sintering the web.Type: GrantFiled: September 25, 1996Date of Patent: May 16, 2000Assignee: Sintokogio, Ltd.Inventors: Masato Imamura, Kiichi Nakajima, Akira Yanagisawa, Masao Kaneko
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Patent number: 6033623Abstract: A powder metallurgical process of preparing iron aluminide useful as electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 20 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.05% Zr or ZrO.sub.2 stringers extending perpendicular to an exposed surface of the heating element, .ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Zr, .ltoreq.1% C, .ltoreq.0.1% B, .ltoreq.30% oxide dispersoid and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1 % rare earth metal, .ltoreq.1% oxygen, and/or .ltoreq.3% Cu.Type: GrantFiled: July 11, 1996Date of Patent: March 7, 2000Assignee: Philip Morris IncorporatedInventors: Seetharama C. Deevi, A. Clifton Lilly, Jr., Vinod K. Sikka, Mohammed R. Hajaligol
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Patent number: 6030472Abstract: A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.0.05% Zr.ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Ni, .ltoreq.0.75% C, .ltoreq.0.1% B, .ltoreq.1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, and/or .ltoreq.3% Cu.Type: GrantFiled: December 4, 1997Date of Patent: February 29, 2000Assignee: Philip Morris IncorporatedInventors: Mohammad R. Hajaligol, Clive Scorey, Vinod K. Sikka, Seetharama C. Deevi, Grier Fleischhauer, A. Clifton Lilly, Jr., Randall M. German
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Patent number: 5902942Abstract: There is now provided a roll for hot rolling comprising 70-95 weight %, preferably 85-94 weight %, WC in a binder phase consisting of only cobalt or alternatively a Co--Ni--Cr alloy containing 20-35 weight % Ni and up to 10 weight % Cr, possibly with small additions of molybdenum. The WC grains are rounded with an average grain size between 3-10 .mu.m, preferably 4-8 .mu.m. The maximum grain size should not exceed 2 times the average grain size and no more than 2% of the grains be less than half of the average grain size.Type: GrantFiled: June 30, 1997Date of Patent: May 11, 1999Assignee: Sandvik ABInventors: Carl-Johan Maderud, Thomas Ericson, Udo Fischer
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Patent number: 5850591Abstract: A method of manufacturing a porous metal sheet having pores forming a pattern, comprising the steps of supplying metal powders to a peripheral surface, of at least one pattern roller of a pair of rollers, on which a pattern including a large number of concaves is formed; dropping metal powders to the concaves and accumulating metal powders on the peripheral surface of the pattern roller except the concaves; and rolling directly the metal powders accumulated on the peripheral surface of the pattern roller by rotating a pair of the rollers. It is preferable to laminate porous metal sheets or solid metal sheets manufactured by a method other than the above-described method on the metal sheet manufactured by the above-described method.Type: GrantFiled: April 18, 1997Date of Patent: December 15, 1998Assignee: Katayama Special Industries, Ltd.Inventor: Hirofumi Sugikawa
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Patent number: 5849238Abstract: A method for forming a tool such as a mold includes the steps of initially selecting a cooling channel configuration for the mold. The initial selected cooling channel is evaluated utilizing a computer program. The program analyzes whether there would be local hot or cool spots in the mold with the initially selected channel. The channel is then modified based upon this evaluation. The modified channel is again subjected to the evaluation. This iterative process continues until an acceptable cooling channel configuration is achieved. The invention utilizes a generally helical cooling channel.Type: GrantFiled: June 26, 1997Date of Patent: December 15, 1998Assignee: UT Automotive Dearborn, Inc.Inventors: Wayde Schmidt, Joseph V. Bak, Ronald D. White, Umesh R. Wamorkar
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Patent number: 5766394Abstract: A polycrystalline diamond layer is bonded to a cemented metal carbide substrate by this process. A layer of dense high shear compaction material including diamond or cubic boron nitride particles is placed adjacent to a metal carbide substrate. The particles of diamond have become rounded instead of angular due to high shear compaction in a multiple roller process. The volatiles in the high shear compaction material are removed and binder decomposed at high temperature, for example, 950.degree. C., leaving residual amorphous carbon or graphite in a layer of ultra hard material particles on the carbide substrate. The substrate and layer assembly is then subjected to a high pressure, high temperature process, thereby sintering the ultra hard particles to each other to form a polycrystalline ultra hard layer bonded to the metal carbide substrate.Type: GrantFiled: December 6, 1995Date of Patent: June 16, 1998Assignee: Smith International, Inc.Inventors: Nathan R. Anderson, Ronald K. Eyre, Madapusi K. Keshavan, Ghanshyam Rai
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Patent number: 5564063Abstract: A method for manufacture of at least one micronozzle in an aerostatic bearing, wherein at least one hole is placed into a compacted bearing surface from porous sintered material by means of a laser beam and disposed so as to be distributed across the surface. The holes distributed across the compacted bearing surface constitute micronozzles of an aerostatic bearing.Type: GrantFiled: February 2, 1995Date of Patent: October 8, 1996Assignee: Joachim HeinzlInventors: Joachim Heinzl, Michael Muth, Bernd Schulz
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Patent number: 5540883Abstract: A method of producing bearing surfaces from powder metal blanks comprising: blending carbon and ferro alloys and lubricant with compressible elemental iron powder, pressing the blending mixture to form the powder metal blank, high temperature sintering the blank in a reducing atmosphere, compressing the powder metal blanks so as to produce a densified layer having a bearing surface, and then heat treating the densified layer.Type: GrantFiled: May 31, 1994Date of Patent: July 30, 1996Assignee: Stackpole LimitedInventors: Peter Jones, Keith Buckley-Golder
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Patent number: 5489411Abstract: A high strength titanium alloy or titanium aluminide metal foil having improved strength and density is produced, preferably in coilable strip form, by plasma-depositing the selected titanium-based material on a receiving surface, separating the deposited material from the receiving surface to provide two metal foil preforms each having a relatively smooth side as cast against the receiving surface and a relatively rough, opposite side as deposited from the plasma, disposing the two metal preforms together with the relatively rough sides of the two metal preforms in facing engagement with each other, and squeezing the two preforms together between pressure bonding rolls to metallurgically bond the preforms to each other and to consolidate the materials of the preforms to form a fully dense metal foil.Type: GrantFiled: September 23, 1991Date of Patent: February 6, 1996Assignee: Texas Instruments IncorporatedInventors: Sunil C. Jha, James A. Forster, Robert W. Howard
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Patent number: 5453243Abstract: A process for producing titanium aluminide weld rod comprising: attaching one end of a metal tube to a vacuum line; placing a means between said vacuum line and a junction of the metal tube to prevent powder from entering the vacuum line; inducing a vacuum within the tube; placing a mixture of titanium and aluminum powder in the tube and employing means to impact the powder in the tube to a filled tube; heating the tube in the vacuum at a temperature sufficient to initiate a high-temperature synthesis (SHS) reaction between the titanium and aluminum; and lowering the temperature to ambient temperature to obtain a intermetallic titanium aluminide alloy weld rod.Type: GrantFiled: August 17, 1994Date of Patent: September 26, 1995Assignee: The United States of America as represented by the Secretary of the InteriorInventors: Jeffrey S. Hansen, Paul C. Turner, Edward R. Argetsinger
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Patent number: 5447800Abstract: A martensitic hot work tool steel die block for use in the manufacture of die casting die components and other hot work tooling components and a method for manufacturing the same. The article has a hardness within the range of 35 to 50 HRC and a minimum transverse Charpy V-notch impact toughness of 5 foot pounds when heat treated to a hardness of 44 to 46 HRC and when tested at both 72.degree. F. and 600.degree. F. The article is a hot worked, heat treated and fully dense consolidated mass of prealloyed particles of the composition, in weight percent, 0.32 to 0.45 carbon, 0.20 to 2.00 manganese, 0.05 to 0.30 sulfur, up to 0.03 phosphorous, 0.80 to 1.20 silicon, 4.75 to 5.70 chromium, 1.10 to 1.75 molybdenum, 0.80 to 1.20 vanadium, and balance iron. The alloy may be any conventional wrought AISI hot work tool steel or wrought maraging or precipitation-hardening steel having 0.05 to 0.30 percent sulfur, and having sulfide particles which exhibit a maximum size of 50 microns in their longest dimension.Type: GrantFiled: September 27, 1993Date of Patent: September 5, 1995Assignee: Crucible Materials CorporationInventors: Carl J. Dorsch, Kenneth E. Pinnow, William Stasko
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Patent number: 5445790Abstract: A process for densifying a powder metallurgical product comprising steps of preparing a powdery starting material, pre-sintering the powdery starting material at a relatively low temperature, executing a pore-eliminating process for eliminating pores resulting from the preceding step on the powdery starting material, and sintering the powdery starting material at a relatively high temperature. It is beneficial to produce a product having a large dimension, a desired shape, and excellent mechanical properties, and being appropriate for or capable of suffering any post-treatment.Type: GrantFiled: May 5, 1994Date of Patent: August 29, 1995Assignee: National Science CouncilInventors: Chen-Ti Hu, Wen-Chih Chiou
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Patent number: 5399312Abstract: A process for fabricating Thallium-based superconducting tapes comprising the steps of: (1) preparing a powder mixture having a nominal composition of (Tl.sub.1-x-y Bi.sub.y Pb.sub.z)(Ba.sub.2-z Sr.sub.z)Ca.sub.2 Cu.sub.3 O.sub.9 ; (2) placing the powder mixture into a silver tube and drawing and/or swaging the silver tube containing the powder mixture into a wire having a pre-determined diameter, wherein x and y are real numbers between 0.2 and 0.4, and z is a real number between 0 and 2; (3) rolling the wire into a tape having a pre-determined thickness; and (4) subjecting the tape to a two-stage single-sintering process at two respective sintering temperatures. The two-stage single-sintering process of the present invention allows Thallium-based superconducting tapes to be fabricated which exhibit substantially increased critical current density, without causing a substantially increased cost and complexity, as do other prior art processes, such as the double-sintering process.Type: GrantFiled: October 4, 1993Date of Patent: March 21, 1995Assignee: Industrial Technology Research InstituteInventors: Ru-Shi Liu, Sheng-Feng Wu, Chung-Ho Tai, Der-Shiuh Shy
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Patent number: 5384087Abstract: The present invention relates to a process for making an aluminum silicon carbide composite material in strip form. The process comprises blending a powdered aluminum matrix material and a powdered silicon carbide material, roll compacting the blended powdered materials in an inert atmosphere to form a green strip having a first thickness, and directly hot working the blended and roll compacted materials to bond the aluminum matrix material particles and the silicon carbide particles and to form a thin strip material having a desired thickness.Type: GrantFiled: April 6, 1992Date of Patent: January 24, 1995Assignee: Ametek, Specialty Metal Products DivisionInventor: Clive Scorey
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Patent number: 5364586Abstract: A filter membrane and a process for making the filter membrane are provided. The filter membrane comprises a metal substrate having a filtering layer thereon comprising sintered ultra-fine particles of metal or ceramic compounds. The filtering layer preferably has an average pore size of from about 30 nanometers to about 200 nanometers. The filter membranes can withstand pressure drops of up to about 0.6 MPa and are useful for a variety of filtering applications.Type: GrantFiled: August 17, 1993Date of Patent: November 15, 1994Assignee: Ultram International L.L.C.Inventors: Lev I. Trusov, Vladimir N. Lapovok, Victor I. Novikov
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Patent number: 5360673Abstract: A semifinished product for electric contact made from a composite material based on silver-tin oxide is described as well as a powder-metallurgical process of making said product. The structure of the semifinished products contains regions which contain no metal oxide or very little metal oxide in alternation with regions which contain the entire metal oxide component or a greatly predominating/share thereof in a fine division.Type: GrantFiled: September 17, 1990Date of Patent: November 1, 1994Assignee: Doduco GmbH + Co. Dr. Eugen DurrwachterInventors: Ursula Mayer, Roland Michal, Karl E. Saeger
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Patent number: 5328772Abstract: A multilayer sliding material for high-speed engine, comprising a steel back metal, a Cu or Cu-base alloy plating layer, a Cu-Pb bearing alloy layer, and an overlay, said steel back metal having 155 or more of Vickers hardness and 42 kgf/mm.sup.2 or more of 0.2% yield strength, a Cu-Pb bearing alloy layer containing 15-30 wt % of Pb and 0.5-2.0 wt % of Sn and having 0.25 cal/cm.s..degree. C. or more of thermal conductivity, 75 or more of Vickers hardness and 18 kgf/mm.sup.2 or more of tensile strength, said overlay of a lead base alloy containing 2-8 wt % of Sn and 3-11 wt % of In and having more than 250.degree. C. of melting start temperature. The material has a superior antiseizure property at high speed of engine. In particular, the rising of the melting start temperature of the metal of the overlay and the thermal conductivity of the bearing alloy provides a superior sliding property of plain bearing at high speed of engine.Type: GrantFiled: February 12, 1992Date of Patent: July 12, 1994Assignee: Daido Metal CompanyInventors: Tadashi Tanaka, Masaaki Sakamoto, Motomu Wada, Koichi Yamamoto, Hideo Ishikawa, Youji Nagai, Kenji Sakai
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Patent number: 5242654Abstract: A process for producing strip products which comprises forming an aqueous slurry of a suspension of metallic particles in a film forming cellulose derivative, depositing a quantity of the slurry onto a support surface, drying the slurry to form a self supporting flat product, removing the dried product from the support surface and roll compacting the same to produce a green strip. The green strip is supported on a moving surface as it travels to and enters a heater in which it is heated in an oxidising atmosphere to a temperature at which substantially all traces of the cellulose derivative are removed. The heated strip is fed while still on the moving support surface to and through a sinter furnace to form a coherent strip of the required composition.Type: GrantFiled: January 27, 1992Date of Patent: September 7, 1993Assignee: Mixalloy LimitedInventors: Robert F. Ward, Nigel J. Brooks
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Patent number: 5230138Abstract: This invention relates to a method of producing a metal-contained composite material from a metal and a sinterable material such as a ceramic material, and to a metal-contained composite material produced by the method. Conventional composite materials consisting of metal and ceramic material do not have sufficient mechanical and electrical properties, under some conditions in use, and are too expensive to be applied extensively. To solve this problem, the invention provides a manufacturing method comprising a process of fabricating a roll of a laminate consisting of a metal strip and a sinterable material, by winding up the laminate, and a process of subjecting the roll to plastic working; a manufacturing method including a heat treatment process carried out at a predetermined temperature, in addition to the above processes; and metal-contained composite materials produced by these methods.Type: GrantFiled: March 22, 1991Date of Patent: July 27, 1993Assignee: Furukawa Electric Co., Ltd.Inventors: Shoji Shiga, Minoru Suzuki, Masanori Ozaki
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Patent number: 5039476Abstract: A method for the production of a metallic powder molding material is disclosed which comprises a step of imparting mechanical energy due to at least one of such physical actions as vibration, pulverization, attrition, rolling, shocks, agitation, and mixing a metallic particles in a vessel whose interior is held under vacuumized atmosphere or an atmosphere of inert gas thereby enabling the metallic particles to contact each other and acquire improvement in surface quality and a step of hot molding the metallic particles thereby producing a molding material.Type: GrantFiled: July 19, 1990Date of Patent: August 13, 1991Assignee: Ube Industries, Ltd.Inventors: Mitsuru Adachi, Akio Okamoto, Hideki Iwai, Yoshiharu Waku
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Patent number: 5028386Abstract: In a process for making tools from medium and high alloy steels or stellites by superplastic precision forming a powder metallurgically produced starting material with an equiaxed structure and more than 30% by volume of carbidic and/or boridic precipitated phase of particle size 1 to 0.2 .mu.m is given a matrix grain size of 1 to 3 .mu.m by thermomechanical processing (hot forming) and formed in the superplastic state.Type: GrantFiled: October 17, 1990Date of Patent: July 2, 1991Assignee: Robert Zapp Werkstofftechnik GmbH & Co. KGInventor: Georg Frommeyer
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Patent number: 5011654Abstract: A continuous process for producing strip products which comprises forming an aqueous slurry of a mixture of a metal powder and a film-forming cellulose derivative and producing from this slurry a self-supporting strip. This self-supporting strip is fed onto an endless moving belt by which the strip is transported into and through a sinter furnace. A tensile force is applied to the sintered strip in the direction of travel of the strip, and this tensile force is controlled such that the speed at which the strip leaves the furnace is greater than the speed at which the strip enters the furnace by an amount related to the expected or actual increase in strip length occasioned by expansion of the strip during the sintering process.Type: GrantFiled: July 25, 1990Date of Patent: April 30, 1991Inventor: Roy Mathers
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Patent number: 5009706Abstract: Rare-earth alloy anisotropic powders consist of, in atomic percent, over 12 percent and not more than 20 percent of R (R is at least one on neodymium and praseodymium or at least one of them and or more rare-earth elements), not less than 4 percent and not more than 10 percent of boron, not less than 0.05 percent and not more than 5 percent of copper and the rest that consists of iron and unavoidable impurities. Up to 20 percent of the iron contained is replaceable with cobalt. The alloy powders are made up of flat crystal grains having mean thickness h (the shortest measure), d not smaller than 0.01 .mu.m and not larger than 0.5 .mu.m and ratio d/h not smaller than 2, where d is the means measure of the grains taken at right angles to the widthwide direction thereof, and the alloy powders are magnetically anisotropic.Type: GrantFiled: July 18, 1990Date of Patent: April 23, 1991Assignee: Nippon Steel CorporationInventors: Hiroaki Sakamoto, Masahiro Fujikura, Toshio Mukai
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Patent number: 5010050Abstract: In a process of producing composite materials consisting of sheet metal plates, metal strips and foils and provided with a skeleton surface structure, a layer of a metal powder which is difficultly flowable and consists of irregularly shaped particles is applied to a continuously moved metallic carrier layer and is bonded to said carrier layer by cold roll cladding and is sintered in a reducing atmosphere at temperatures of 600.degree. to 1000.degree. C. In order to produce composite materials in which the skeleton structure constitutes a layer that is of uniform thickness throughout the surface and is firmly bonded to the carrier layer, the metal powder is uniformly distributed and applied as regards its bulk volume using a distributing roller, which rotates opposite to the main direction of movement of the carrier layer, whereby a uniform thickness is obtained.Type: GrantFiled: April 18, 1989Date of Patent: April 23, 1991Assignee: Metallgesellschaft AGInventors: Heinz Wullenweber, Peter Kohl, Herbert Jung, Jurgen Borchardt, Wolfgang Bickle, Jurgen Braus
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Patent number: 4976915Abstract: A method in which various kinds of powdered or granular materials such as metal, ceramic and the like are put into a metal cylindrical container which can be plastically-deformed, or in the space between a container and a core or a substrate, the surroundings are sealed so that the powdered or granular materials do not leak out, the container is locally pressed by a small roller, and the locally pressed treatment is provided to the whole container region. Therefore, the internal powdered or granular materials are pressurized to a uniform density without regard to selective parts, and the materials are formed to various shapes by means of the local pressing.Type: GrantFiled: August 1, 1988Date of Patent: December 11, 1990Assignee: Kuroki Kogyosho Co., Ltd.Inventor: Takanori Kuroki
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Patent number: 4971754Abstract: The method concerns preparing a contact material constituted by silver and tin oxide.According to the invention the method comprises the following steps:preparing an aqueous solution containing dissolved silver nitrate and tin oxide particles in suspension, with the size of said particles measured in terms of specific surface area using the BET method lying between about 2 m.sup.2 /g and 6 m.sup.2 /g;causing silver nitrate to precipitate in silver hydroxide by rapidly adding a strong base and stirring, with silver hydroxide being unstable and transforming progressively into silver oxide;eliminating the ions from the solution and then the water in order to obtain a dry product; andheating the dry product to a temperature of about 200.degree. C. to 500.degree. C. in order to reduce the silver oxide to metallic silver.The invention is applicable to manufacturing electrical contacts for opening and closing in electromechanical apparatuses.Type: GrantFiled: November 22, 1989Date of Patent: November 20, 1990Assignee: TelemecaniqueInventors: Gerard Fontet, Michel Leclercq, Jacques Muniesa, Thierry Pagnier, Tretarre Rene
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Patent number: 4961901Abstract: In a process of manufacturing diaphragms, a layer of a difficulty flowable metal powder is applied to a support, a wire net is rolled onto the powder layer and the latter is compacted at the same time and the metal powder is fired at 800.degree. to 1500.degree. C. in an oxidizing atmosphere. In order to impart to the diaphragms a constant thickness, strength and density, the metal powder is uniformly distributed and applied as regards its bulk volume to the support and the powder layer is moved under a distributing roller rotating opposite to the direction in which the powder is fed.Type: GrantFiled: April 18, 1989Date of Patent: October 9, 1990Assignee: Metallgesellschaft AGInventors: Heinz Wullenweber, Peter Kohl, Herbert Jung, Jorgen Borchardt, Wolfgang Bickle, Jurgen Braus, Hans-Joachim Hiedemann