Hot Rolling Patents (Class 419/50)
  • Patent number: 7993577
    Abstract: The invention relates to manufacture of titanium articles from sintered powders. The cost-effective initial powder: 10-50 wt % of titanium powder having ?500 microns in particle size manufactured from underseparated titanium sponge comprising ?2 wt % of chlorine and ?2 wt % of magnesium; 10-90 wt % of a mixture of two hydrogenated powders A and B containing different amount of hydrogen; 0-90 wt % of standard grade refined titanium powder, and/or 5-50 wt % of alloying metal powders. The method includes: mixing powders, compacting the blend to density at least 60% of the theoretical density, crushing titanium hydride powders into fine fragments at pressure of 400-960 MPa, chemical cleaning and refining titanium powders by heating to 300-900° C. and holding for ?30 minutes, heating in vacuum at 1000-1350° C., holding for ?30 minutes, and cooling.
    Type: Grant
    Filed: June 11, 2007
    Date of Patent: August 9, 2011
    Assignee: Advance Materials Products, Inc.
    Inventors: Volodymyr A. Duz, Orest M. Ivasishin, Vladimir S. Moxson, Dmitro G. Savvakin, Vladislav V. Telin
  • Patent number: 7854886
    Abstract: A method of producing an aluminum matrix composite material is described that comprises the steps of: mixing an aluminum powder and a ceramic powder to prepare a mixed powder; providing a lower casing made of aluminum and formed in a hollow rectangular parallelepiped shape having an open top, and a closing member made of aluminum and formed in a shape adapted to hermetically close the open top of the lower casing; packing the mixed powder into the lower casing; closing the open top of the lower casing filled with the mixed powder, by the closing member, to prepare a pre-rolling assembly having the mixed powder hermetically sealed therein; preheating the pre-rolling assembly; and rolling the preheated assembly to obtain the aluminum matrix composite material, where the aluminum matrix composite material includes a pair of metal plates having the mixed powder therebetween.
    Type: Grant
    Filed: October 23, 2007
    Date of Patent: December 21, 2010
    Assignees: Nippon Light Metal Co., Ltd., Nikkeikin Aluminum Core Technology Co., Ltd.
    Inventors: Yuichi Tamaki, Kazuto Sanada, Toshimasa Nishiyama
  • Patent number: 7854887
    Abstract: A method of producing an aluminum matrix composite material is described that comprises the steps of: mixing an aluminum powder and a ceramic powder to prepare a mixed powder; providing a lower casing made of aluminum and formed in a hollow rectangular parallelepiped shape having an open top, and a closing member made of aluminum and formed in a shape adapted to hermetically close the open top of the lower casing; packing the mixed powder into the lower casing; closing the open top of the lower casing filled with the mixed powder, by the closing member, to prepare a pre-rolling assembly having the mixed powder hermetically sealed therein; preheating the pre-rolling assembly; and rolling the preheated assembly to obtain the aluminum matrix composite material, where the aluminum matrix composite material includes a pair of metal plates having the mixed powder therebetween.
    Type: Grant
    Filed: October 23, 2007
    Date of Patent: December 21, 2010
    Assignees: Nippon Light Metal Co., Ltd., Nikkeikin Aluminum Core Technology Co., Ltd.
    Inventors: Toshimasa Nishiyama, Kazuto Sanada, Hideki Honmou
  • Publication number: 20090277301
    Abstract: The invention relates to mixtures of metal, alloy or composite powders which have a mean particle diameter D50 of not more than 75 ?m, preferably not more than 25 ?m, and are produced in a process in which a starting powder is firstly deformed to give platelet-like particles and these are then comminuted in the presence of milling aids together with further additives and also the use of these powder mixtures and shaped articles produced therefrom.
    Type: Application
    Filed: July 9, 2007
    Publication date: November 12, 2009
    Applicant: H.C. Starck GmbH
    Inventors: Roland Scholl, Ulf Waag, Aloys Eiling
  • Patent number: 6767416
    Abstract: A corrosion resistant, high strength austenitic stainless steel consisting of 1.0% or less of Si, 2.0% or less of Mn, 0.5% or less of O, 7 to 30% of Ni, 14 to 26% of Cr, 0.3% or less of combination of C and N, at least one element selected from the group consisting of 1.0% or less of Ti, 2.0% or less of Zr and 2.0% or less of Nb, and the balance consisting of Fe and unavoidable impurities, the percentage being given in weight basis; said steel containing carbonitride with a grain size of several to 100 nm dispersed therein; said steel having an average crystal grain size of 1 &mgr;m or less; and said steel containing 90% by volume or more of austenite phase; is excellent in strength and corrosion resistance.
    Type: Grant
    Filed: February 27, 2002
    Date of Patent: July 27, 2004
    Assignee: Hitachi, Ltd.
    Inventors: Ryo Ishibashi, Yasuhisa Aono
  • Patent number: 6696168
    Abstract: A composite strip of compacted powders, which has a three layers structure, is continuously obtained by means of a rolling machine for powder compacting. The composite strip is sintered at a temperature of 460° C. to 550° C. to form a sintered composite strip. The sintered composite strip is continuously bonded by rolling to a steel strip. The bonded composite strip is optionally subjected to a heat treatment of heating at a temperature of 250° C. to 400° C. followed by heating to a temperature of 400° C. to 510° C., holding the strip under the temperature for not less than 30 seconds, and rapidly cooling down to 300° C. at a cooling rate of not lower than 50° C./minute, whereby obtaining a multi-layered composite material consisting of the steel strip, a sintered bonding layer, a sintered sliding layer and a sintered sacrificial layer.
    Type: Grant
    Filed: April 29, 2002
    Date of Patent: February 24, 2004
    Assignee: NDC Company Ltd.
    Inventors: Yasukuni Hasegawa, Koue Ohkawa, Hiroyuki Sugawara
  • Patent number: 6660109
    Abstract: A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as ≦1% Cr, ≧0.05% Zr ≦2% Ti, ≦2% Mo, ≦1% Ni, ≦0.75% C, ≦0.1% B, ≦1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, ≦1% rare earth metal, and/or ≦3% Cu.
    Type: Grant
    Filed: October 31, 2001
    Date of Patent: December 9, 2003
    Assignee: Chrysalis Technologies Incorporated
    Inventors: Mohammad R. Hajaligol, Clive Scorey, Vinod K. Sikka, Seetharama C. Deevi, Grier Fleishhauer, A. Clifton Lilly, Jr., Randall M. German
  • Patent number: 6602314
    Abstract: The present invention provides an aluminum composite material having neutron absorbing power that improves the ability to absorb neutrons by increasing the content of B, while also being superior to materials of the prior art in terms of mechanical properties and workability. The aluminum composite material having neutron absorbing power contains in Al or an Al alloy matrix phase B or a B compound having neutron absorbing power in an amount such that the proportion of B is 1.5% by weight or more to 9% by weight or less, and the aluminum composite material has been pressure sintered.
    Type: Grant
    Filed: March 30, 2001
    Date of Patent: August 5, 2003
    Assignee: Mitsubishi Heavy Industries, Ltd.
    Inventors: Yasuhiro Sakaguchi, Tomikane Saida, Kazuo Murakami, Kazuhisa Shibue, Naoki Tokizane, Tatsumi Takahashi
  • Patent number: 6500385
    Abstract: Process for working up powder coating waste to yield reusable powder coatings by compacting the powder coating waste without complete melting to yield a sintered product, in which process powder coating residues arising during powder coating production are continuously separated, continuously compacted and the compacted product is continuously ground together with fresh material to be ground of the same batch of powder coating without extrusion to yield a powder coating.
    Type: Grant
    Filed: April 19, 2000
    Date of Patent: December 31, 2002
    Assignee: E. I. du Pont de Nemours and Company
    Inventors: Karsten Blatter, David Montgomery, Heléne Bolm
  • Publication number: 20020124914
    Abstract: A method of manufacturing an amorphous alloy core including the steps of mixing an amorphous alloy powder with a solution made by dissolving a polyimide/phenolic resin binder in an organic solvent, evenly coating the binder in liquid phase on the surface of the alloy powder to make a powder of composite particles, molding the power of composite particles, and performing a heating treatment thereon.
    Type: Application
    Filed: January 7, 2002
    Publication date: September 12, 2002
    Inventor: Kyu-Jin Kim
  • Patent number: 6332936
    Abstract: A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as ≦1% Cr, ≧0.05% Zr ≦2% Ti, ≦2% Mo, ≦1% Ni, ≦0.75% C, ≦0.1% B, ≦1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, ≦1% rare earth metal, and/or ≦3% Cu.
    Type: Grant
    Filed: September 20, 1999
    Date of Patent: December 25, 2001
    Assignee: Chrysalis Technologies Incorporated
    Inventors: Mohammad R. Hajaligol, Clive Scorey, Vinod K. Sikka, Seetharama C. Deevi, Grier Fleischhauer, A. Clifton Lilly, Jr., Randall M. German
  • Patent number: 6030472
    Abstract: A powder metallurgical process of preparing a sheet from a powder having an intermetallic alloy composition such as an iron, nickel or titanium aluminide. The sheet can be manufactured into electrical resistance heating elements having improved room temperature ductility, electrical resistivity, cyclic fatigue resistance, high temperature oxidation resistance, low and high temperature strength, and/or resistance to high temperature sagging. The iron aluminide has an entirely ferritic microstructure which is free of austenite and can include, in weight %, 4 to 32% Al, and optional additions such as .ltoreq.1% Cr, .gtoreq.0.05% Zr.ltoreq.2% Ti, .ltoreq.2% Mo, .ltoreq.1% Ni, .ltoreq.0.75% C, .ltoreq.0.1% B, .ltoreq.1% submicron oxide particles and/or electrically insulating or electrically conductive covalent ceramic particles, .ltoreq.1% rare earth metal, and/or .ltoreq.3% Cu.
    Type: Grant
    Filed: December 4, 1997
    Date of Patent: February 29, 2000
    Assignee: Philip Morris Incorporated
    Inventors: Mohammad R. Hajaligol, Clive Scorey, Vinod K. Sikka, Seetharama C. Deevi, Grier Fleischhauer, A. Clifton Lilly, Jr., Randall M. German
  • Patent number: 5799238
    Abstract: A method making a titanium ceramic composite involves forming a hot pressed powder body having a microstructure comprising at least one titanium metal or alloy layer and at least one ceramic particulate reinforced titanium metal or alloy layer and hot forging the hot pressed body follwed by hot rolling to substantially reduce a thickness dimension and substantially increase a lateral dimension thereof to form a composite plate or sheet that retains in the microstructure at least one titanium based layer and at least one ceramic reinforced titanium based layer in the thickness direction of the composite plate or sheet.
    Type: Grant
    Filed: June 14, 1995
    Date of Patent: August 25, 1998
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventors: George T. Fisher, II, Jeffrey S. Hansen, Laurance L. Oden, Paul C. Turner, Thomas L. Ochs
  • Patent number: 5722037
    Abstract: There is provided a process for producing titanium composite, comprising the steps of: molding titanium powder, titanium alloy powder, or powder comprising titanium into a certain shape by a cold isostatic press or cold press; reacting the shape with hydrocarbon gas at its decomposition temperature or higher, to form TiC therein; and providing the shape with high density by vacuum sintering, hot isostatic pressing, hot forging, hot rolling and/or the combinations thereof. TiC a reinforcing material, is in-situ formed by reacting a cold-pressed body of the powder with hydrocarbon gas and cleaner than the externally added one and distributed more uniformly and finely in the Ti matrix, leading to a significant improvement in wear resistance and high temperature property.
    Type: Grant
    Filed: May 9, 1996
    Date of Patent: February 24, 1998
    Assignee: Korea Institute of Machinery & Materials
    Inventors: Hyung-Sik Chung, Yong-Jin Kim, Byung-Kee Kim, Jian-Qing Jiang
  • Patent number: 5614684
    Abstract: A method for the production of a superplastic Mg-based composite material comprises preparing a composite material consisting of ceramic particles formed of at least one compound selected from among TiC, AlN, Si.sub.3 N.sub.4, and TiB.sub.2 and a matrix formed of a magnesium alloy, dispersing the ceramic particles in the matrix, hot extruding the composite material, and then hot rolling the resultant extrudate; and a superplastic Mg-based composite material produced by the method.
    Type: Grant
    Filed: October 3, 1995
    Date of Patent: March 25, 1997
    Assignee: Agency of Industrial Science and Technology, Ministry of International Trade & Industry
    Inventors: Suk-Won Lim, Tsunemichi Imai, Yoshinori Nishida, Takao Choh
  • Patent number: 5564064
    Abstract: A method for forming a gas-filled consolidated metal billet, involving preparing a metallic shell container, filling the shell with a metal core material and pressurized gas, and consolidating the shell and its contents to form the billet. The consolidated billet is further formed in the same manner as solid metal components by conventional wrought mill working technologies. After thus forming a shaped billet having a predetermined, desired geometry, it is subjected to a heat treatment that expands the gas trapped within the core, to produce in situ a metal body having an integral sandwich-type structure with a solid metal facing and a porous metal core.
    Type: Grant
    Filed: February 3, 1995
    Date of Patent: October 8, 1996
    Assignee: McDonnell Douglas Corporation
    Inventor: Ricky L. Martin
  • Patent number: 5489411
    Abstract: A high strength titanium alloy or titanium aluminide metal foil having improved strength and density is produced, preferably in coilable strip form, by plasma-depositing the selected titanium-based material on a receiving surface, separating the deposited material from the receiving surface to provide two metal foil preforms each having a relatively smooth side as cast against the receiving surface and a relatively rough, opposite side as deposited from the plasma, disposing the two metal preforms together with the relatively rough sides of the two metal preforms in facing engagement with each other, and squeezing the two preforms together between pressure bonding rolls to metallurgically bond the preforms to each other and to consolidate the materials of the preforms to form a fully dense metal foil.
    Type: Grant
    Filed: September 23, 1991
    Date of Patent: February 6, 1996
    Assignee: Texas Instruments Incorporated
    Inventors: Sunil C. Jha, James A. Forster, Robert W. Howard
  • Patent number: 5384087
    Abstract: The present invention relates to a process for making an aluminum silicon carbide composite material in strip form. The process comprises blending a powdered aluminum matrix material and a powdered silicon carbide material, roll compacting the blended powdered materials in an inert atmosphere to form a green strip having a first thickness, and directly hot working the blended and roll compacted materials to bond the aluminum matrix material particles and the silicon carbide particles and to form a thin strip material having a desired thickness.
    Type: Grant
    Filed: April 6, 1992
    Date of Patent: January 24, 1995
    Assignee: Ametek, Specialty Metal Products Division
    Inventor: Clive Scorey
  • Patent number: 5306463
    Abstract: A process for producing a structural member of an amorphous alloy, which includes the steps of subjecting a material formed from an amorphous alloy having a glass transition temperature Tg and a crystallization temperature Tx, which is higher than the glass transition temperature Tg, to a thermal treatment in which the material is kept at a heating temperature equal to or lower than the glass transition temperature Tg, thereby generating a structure relaxation phenomenon in the material, and subjecting the material to a hot plastic working while setting the hot working start temperature of the green compact at a level equal to or lower than the crystallization temperature Tx. In this process, the workability of the material can be improved to produce a high strength amorphous alloy structural member that has an increased volume fraction of an amorphous phase. Furthermore the generation of any defect due to gas inclusion is suppressed.
    Type: Grant
    Filed: April 19, 1991
    Date of Patent: April 26, 1994
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventor: Hiroyuki Horimura
  • Patent number: 5290508
    Abstract: The present invention relates to a manufacturing process for ring-shaped parts having high wear resistance and mechanical strength. Raw material powder containing (weight %) C at 0.4-0.9%, Ni at 1.5-4.0%, Mo 0.2-0.6%, and a remainder consisting of Fe and unavoidable impurities, is compacted and shaped, thereafter sintered and forged; obtained sintered body is hardened by heating at a temperature within a range of 800.degree.-950.degree. C., thereafter high temperature tempering is carried out for 20-60 minutes at a temperature within a range of 570.degree.-700.degree. C.; then the surface layer of the inner periphery and/or outer periphery of said sintering body is heated; then if required, low temperature tempering (temper process) is carried out at a temperature within a range of 160.degree.-220.degree. C.
    Type: Grant
    Filed: April 7, 1992
    Date of Patent: March 1, 1994
    Assignee: Mitsubishi Materials Corporation
    Inventors: Kazuya Kobayashi, Shigeyoshi Nagahara, Hikaru Hosono
  • Patent number: 5151246
    Abstract: A method is described for manufacturing foamable metal bodies in which a ture (17) of a metal powder (15) and a gas-splitting propellent powder (16) is hot-compacted to a semifinished product (19) at a temperature at which the joining of the metal powder particles takes place primarily by diffusion and at a pressure which is sufficiently high to hinder the decomposition of the propellent in such fashion that the metal particles form a solid bond with one another and constitute a gas-tight seal for the gas particles of the propellant. The foamable metal body can also be produced by rolling. In addition, a use of the foamable metal body (19) thus produced for manufacturing a porous metal body (21) is proposed.
    Type: Grant
    Filed: May 31, 1991
    Date of Patent: September 29, 1992
    Assignee: Fraunhofer-Gesellschaft zur Forderung der angewandten Forschung e.V.
    Inventors: Joachim Baumeister, Hartmut Schrader
  • Patent number: 5069868
    Abstract: Thermoelectric elements with excellent thermoelectric characteristics such as Seebeck coefficient thermoelectromotive force and thermal conductivity can be produced by molding a powder of metal or metal alloy as the raw material and then sintering; by using as such raw material, ultra fine powders containing Fe and Si as main components and having a mean particle diameter of 50 to 5,000.ANG..
    Type: Grant
    Filed: November 29, 1990
    Date of Patent: December 3, 1991
    Assignee: Idemitsu Petrolchemical Co., Ltd.
    Inventors: Takeo Tokiai, Takashi Uesugi
  • Patent number: 5041339
    Abstract: A multilayered sliding material of lead bronze containing graphite in the form of a bimetal, comprising a steel plate or a steel plate having a copper plating coating and a sintered copper alloy bonded to the steel plate, the sintered copper alloy having a composition consisting of 5 to 16 wt % Sn, 2 to 20 wt % Pb, 0.03 to 1 wt % P, 0.5 to 3.9 wt % graphite, and the balance Cu, wherein hardness of the alloy exceeds Hv 100.
    Type: Grant
    Filed: August 21, 1989
    Date of Patent: August 20, 1991
    Assignee: Daido Metal Company
    Inventors: Sanae Mori, Masaaki Sakamoto, Koichi Yamamoto, Kenji Sakai
  • Patent number: 5034187
    Abstract: A composition containing 30 to 70% chromium carbide, 5 to 20% soft noble metal, 5 to 20% metal fluorides, and 20 to 60% metal binder is used in a powdered metallurgy process for the production of self-lubricating components, such as bearings. The use of the material allows the self-lubricating bearing to maintain its low friction properties over an extended range of operating temperatures.
    Type: Grant
    Filed: August 23, 1990
    Date of Patent: July 23, 1991
    Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space Administration
    Inventors: Harold E. Sliney, Christopher Dellacorte
  • Patent number: 5010050
    Abstract: In a process of producing composite materials consisting of sheet metal plates, metal strips and foils and provided with a skeleton surface structure, a layer of a metal powder which is difficultly flowable and consists of irregularly shaped particles is applied to a continuously moved metallic carrier layer and is bonded to said carrier layer by cold roll cladding and is sintered in a reducing atmosphere at temperatures of 600.degree. to 1000.degree. C. In order to produce composite materials in which the skeleton structure constitutes a layer that is of uniform thickness throughout the surface and is firmly bonded to the carrier layer, the metal powder is uniformly distributed and applied as regards its bulk volume using a distributing roller, which rotates opposite to the main direction of movement of the carrier layer, whereby a uniform thickness is obtained.
    Type: Grant
    Filed: April 18, 1989
    Date of Patent: April 23, 1991
    Assignee: Metallgesellschaft AG
    Inventors: Heinz Wullenweber, Peter Kohl, Herbert Jung, Jurgen Borchardt, Wolfgang Bickle, Jurgen Braus
  • Patent number: 4832734
    Abstract: Discloses hot working by rolling or forging of mechanically alloyed aluminum-base alloys containing 5 to 35 volume percent of an aluminum transition metal intermetallic phase, e.g. Al.sub.3 Ti which is insoluble in the solid aluminum matrix. Hot working is carried out at a temperature above about 370.degree. C.
    Type: Grant
    Filed: May 6, 1988
    Date of Patent: May 23, 1989
    Assignee: Inco Alloys International, Inc.
    Inventors: Raymond C. Benn, Prakash K. Mirchandani, Walter E. Mattson
  • Patent number: 4820141
    Abstract: A method for forming non-equilibrium and/or metastable metallic or non-metallic powder, foil or fine wire material into a solid body comprises charging the material into a metal container, subjecting the metal container containing the material to rolling at a temperature at which the inherent properties of the material are maintained, and thereafter removing the metal container.
    Type: Grant
    Filed: December 11, 1987
    Date of Patent: April 11, 1989
    Assignee: Nippon Steel Corporation
    Inventors: Hideo Shingu, Mitsunobu Abe, Takashi Sato, Toshio Yamada
  • Patent number: 4705466
    Abstract: A method and apparatus for continuous processing of metal between molten and bright hot rolled stages includes the production of uniform liquid metal droplets at the top of a shot tower containing inert gas, forming and maintaining columns of closely spaced but separate metal droplets, retarding the flow of said droplets to a slow, substantially constant, velocity and cooling the droplets principally by radiation to at least partial solidification, collecting the at least partially solidified droplets in a bottomless receptacle in a weakly cohesive column, passing said column into the bite of a pair of mill rolls, rolling the said column into a rolled product, and cooling the rolled product by arc contact with off-set colling/flatening rolls and by radiation and convection cooling in an inert gas.
    Type: Grant
    Filed: December 16, 1985
    Date of Patent: November 10, 1987
    Inventor: Oscar Balassa
  • Patent number: 4666665
    Abstract: An apparatus and method of hot-forging in a forging press a cylindrical powdered metal preform to substantially full theoretical density to thereby produce a powdered metal part having a small inner bore wherein the core rod defining such bore is constructed so as to allow a continuous flow of a highly vaporizable liquid coolant such as nitrogen to the metal forming portion of the core rod and to thermally insulate the incoming coolant to assure its being maintained substantially unvaporized until being expelled to the core rod cooling chamber.
    Type: Grant
    Filed: January 30, 1986
    Date of Patent: May 19, 1987
    Assignee: Federal-Mogul Corporation
    Inventors: William S. Hornsby, Joseph C. Skurka, Hayward P. Summers
  • Patent number: 4644171
    Abstract: A panel of neutron shielding material comprises outer sheathing layers of aluminum having therebetween alternate thin layers or plies of aluminum and metallurgically bonded uniform mixtures of aluminum particles and particles of a neutron absorbing material, preferably boron carbide (B.sub.4 C) in which the layers have their major dimensions extending substantially parallel to the outer aluminum layers. In a modified construction, the alternate layers or plies may extend perpendicular to the outer aluminum layers or plies. The assembly is hot rolled to a final thickness, usually about one quarter or one eighth inch, metallurgically bonding the aluminum sheets, strips, and/or particles and the aluminum and boron carbide particles into a continuous mass.
    Type: Grant
    Filed: April 1, 1985
    Date of Patent: February 17, 1987
    Assignee: AAR Corporation
    Inventor: Leslie Mollon
  • Patent number: 4642218
    Abstract: A method for producing high technology ceramics with minimal porosity comsing the steps of filling a can with a constituent powder of a ceramic, creating a vacuum in the can and maintaining the vacuum throughout the entire process; outgassing the powder in the can by placing a furnace around the area of the can that encloses the powder and heating the furnace to at least 100.degree. C.; removing the furnace after a minimum of five minutes of heating; cold rolling the can in a rolling system; igniting the powder so a localized propagation reaction front is created; and hot rolling the can in the rolling system so the propagation reaction front is maintained between the rolls of the rolling system.
    Type: Grant
    Filed: October 19, 1984
    Date of Patent: February 10, 1987
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: Roy W. Rice
  • Patent number: 4620872
    Abstract: A novel composite target material that is composed of a rare earth metal and a transition metal (iron-group metal) and which is used in the formation of a thin magnetooptical recording film by sputtering is disclosed. Also disclosed is a process for producing such composite target material.The process comprises the steps of providing a rare earth metal and an iron-group transition metal as separate entities, mixing these metals without alloying, and hot-forming the mixture at a temperature lower than the eutectic point of the system of metallic components in the mixture, thereby forming an intermetallic compound at the interface between the rare earth metal and the transition metal while causing said metals to be bonded together.The target material produced by this process contains 30-50 wt % of the rare earth metal, with the balance being made of the iron-group transition metal and incidental impurities.
    Type: Grant
    Filed: October 15, 1985
    Date of Patent: November 4, 1986
    Assignee: Mitsubishi Kinzoku Kabushiki Kaisha
    Inventors: Kenichi Hijikata, Katsuyuki Sato, Hitoshi Maruyama, Ryoko Furuhashi
  • Patent number: 4613364
    Abstract: A method and a means for continuously producing a preformed metal product through direct reduction of a material containing ferric oxide in a shaft furnace and feeding the product manufactured in the shaft furnace via a gas lock into a hot preforming machine, the hot product obtained from the shaft furnace being kept at the temperature required for the subsequent hot preforming process, preferably at least about 550.degree. C., by means of hot, non-combustible gas consisting primarily of N.sub.2 and/or CO.sub.2 which has been heated by excess heat from the shaft furnace.
    Type: Grant
    Filed: February 11, 1985
    Date of Patent: September 23, 1986
    Assignee: SKF Steel Engineering, A.B.
    Inventor: Bjorn Hammarskog
  • Patent number: 4588552
    Abstract: Manufacture of a workpiece from a creep-resistant nickel superalloy which is hardened by means of an oxide dispersion, by a powder-metallurgical process in which the mechanically alloyed powder is subjected to an isothermal or quasi-isothermal hot-rolling operation, in the course of which the powder particles are converted into a flake-shaped form with a pronounced longitudinal axes, and the rolled powder is introduced into a steel container and is compressed by isostatic hot-pressing. The workpiece is afterwards subjected to an annealing treatment which is designed to develop a coarse grain size. A preferred embodiment comprises the introduction of the powder into the mold or container in an oriented manner, in order to obtain a stratified packing of the powder, and an annealing treatment which is designed to develop a coarse grain size and is performed as a zone-annealing treatment.
    Type: Grant
    Filed: November 1, 1984
    Date of Patent: May 13, 1986
    Assignee: BBC Brown, Boveri & Co., Ltd.
    Inventors: Gunther Schroder, Robert Singer
  • Patent number: 4582536
    Abstract: The present invention provides a method for consolidating rapidly solidified, transition metal alloys which includes the step of compacting a plurality of alloy bodies at a temperature ranging from about 0.90-0.99 Tm (melting temperature in .degree.C.) for a time period ranging from about 1 min to 24 hours. The alloy bodies contain at least two transition metal elements and consist essentially of the formula (Fe,Co and/or Ni).sub.bal (W, Mo, Nb and/or Ta).sub.a (Al and/or Ti).sub.b (Cr).sub.c (B and/or C).sub.d (Si and/or P).sub.e, wherein "a" ranges from about 0-40 at. %, "b" ranges from about 0-40 at. %, "c" ranges from about 0-40 at. %, "d" ranges from about 5-25 at. %, and "e" ranges from about 0-15 at. %. The alloy bodies also have a substantially homogeneous and optically featureless structure.
    Type: Grant
    Filed: December 7, 1984
    Date of Patent: April 15, 1986
    Assignee: Allied Corporation
    Inventor: Derek Raybould
  • Patent number: 4492671
    Abstract: A powder metallurgical method of consolidating iron-based alloy powder, particularly white cast iron, to form a body of high density in which the powder is thermally cycled above and below the alpha-gamma transformation temperature of below 800.degree. C., and a stress of between 1.7 MPa and 34.5 MPa is simultaneously applied to the powder to form a high density consolidated body.
    Type: Grant
    Filed: March 15, 1982
    Date of Patent: January 8, 1985
    Assignee: Leland Stanford Junior University
    Inventors: Oscar Ruano, Jeffrey Wadsworth, Oleg D. Sherby
  • Patent number: 4478787
    Abstract: A process and a product produced thereby, for forming rod or bar or tube stock or strip, comprising a sheath and a densified dispersion strengthened metal core. Powdered dispersion strengthened copper is put into a metal can and compressively reduced to size and density. The relationship between the tensile strength of the core when fully densified and the cold worked tensile strength of the can is important to the nature of the product.
    Type: Grant
    Filed: December 14, 1983
    Date of Patent: October 23, 1984
    Assignee: SCM Corporation
    Inventors: Anil V. Nadkarni, Prasanna K. Samal, James C. Wang, James E. Sunk
  • Patent number: 4435213
    Abstract: Aluminum alloy atomized or other powder is compacted and shaped into a useful article including heating the compact rapidly by induction heating techniques. Such rapid induction heating results in improved strength or toughness properties without substantial penalty in elongation, thereby rendering the product so produced more useful in high strength applications. The product so produced may be subsequently shaped by forging, extruding or rolling processes.
    Type: Grant
    Filed: September 13, 1982
    Date of Patent: March 6, 1984
    Assignee: Aluminum Company of America
    Inventors: Gregory J. Hildeman, John C. Kuli, Jr., Leo A. Vivola
  • Patent number: 4405295
    Abstract: The present invention provides a method for manufacturing complex metallic plates. A hollow metal piece, which will form the outer layer, is first made. A powder which will form the inner layer is then filled within the hollow metal piece. The multi-layer plate is then manufactured by hot-rolling the metal piece.
    Type: Grant
    Filed: March 1, 1982
    Date of Patent: September 20, 1983
    Assignee: AMSTED Industries Incorporated
    Inventors: Tetsuya Fujii, Yukio Oguchi, Norio Sumita, Isamu Goto
  • Patent number: 4393563
    Abstract: A method and material for the manufacture of improved bearing elements such as annular inner and outer bearing ring blanks for ball, roller and needle bearing assemblies comprising the steps of mixing a powder consisting substantially of iron with ferro-alloy powders of substantially smaller size, each ferro-alloy containing at least 80% iron and the balance being an alloying element, together with graphite powder and a lubricant, compacting the resulting mixture to form a preform, pre-sintering the preform, and then coating the sintered preform with a stop-off and lubricant. The preform is subjected to a plastic deformation of at least 50% in a cold (room temperature) forging operation to produce an article which is at least 98% dense and has approximately the shape of the finished article. This cold forged shape is resintered and annealed, after which the annealed and resintered shape is roll formed into substantially final dimensions.
    Type: Grant
    Filed: May 26, 1981
    Date of Patent: July 19, 1983
    Inventor: David T. Smith