And Additional Disinfecting Or Sterilizing Agent Patents (Class 422/27)
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Patent number: 5658529Abstract: A process for color anodizing and sterilizing aluminum surfaces on medical instruments without fading the anodized color comprises the steps of: anodizing an aluminum surface on a medical instrument to form an oxide film; immersing the surface in a salt bath of a coloring metal and electrolytically depositing the coloring metal onto the oxide film; and repeatedly sterilizing the medical instrument and its surface by exposing it to an oxidizing sterilant, whereby the electrolytically deposited coloring metal remains adhered to the surface and the color of the surface is not adversely affected by the repeated exposure to the oxidizing sterilant. Preferably, the sterilant comprises hydrogen peroxide, the coloring metal comprises tin and the surface remains non-cytotoxic after the anodizing, coloring steps and sterilizing steps.Type: GrantFiled: March 13, 1996Date of Patent: August 19, 1997Assignee: Johnson & Johnson Medical, Inc.Inventors: Leslie A. Feldman, Henry Hui
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Patent number: 5650693Abstract: An apparatus for plasma sterilization of articles is provided that comprises a plasma generator and a sterilizing chamber. The plasma generator has an inlet for receiving a premixed gas mixture from a pressurized source. The pressurized gas mixture source is a single container (or multiple containers with the same contents), having a noble gas and further having a non-flammable mixture of hydrogen and oxygen.Type: GrantFiled: June 5, 1995Date of Patent: July 22, 1997Assignee: Abtox, Inc.Inventors: Bryant A. Campbell, deceased, Kern A. Moulton, Jim Fisher
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Patent number: 5609830Abstract: A method and an apparatus for the sterilization of refuse, in particular hospital refuse, is described, according to which plastic containers filled with the refuse are first introduced into a lock chamber in which a preparatory conveyor belt is arranged and thereafter the entire charge of the lock chamber is transferred to a sterilization chamber in which a main conveyor belt is arranged. The sterilization chamber is then hermetically sealed and injection needles are stuck into the respective containers to inject water and/or disinfectant into the interior of the respective plastic containers. The refuse is then treated with microwave energy and subsequently the charge in the sterilization chamber discharged via the discharge opening. With the method and the apparatus according to the invention it is always ensured that the refuse in the interior of the plastic containers is impregnated in adequate manner with water or a disinfectant, this being done before or during the microwave irradiation.Type: GrantFiled: February 28, 1994Date of Patent: March 11, 1997Assignee: Nordpunkt AGInventor: Willi Maihofer
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Patent number: 5609821Abstract: A process for disinfecting or sterilizing an article comprising spraying on at least one surface of the article an aqueous hydrogen peroxide solution including an organic phosphonic acid in an amount effective to stabilize said hydrogen peroxide solution, said solution being free of other stabilizing agents.Type: GrantFiled: July 22, 1994Date of Patent: March 11, 1997Assignee: Chemoxal S.A.Inventors: Aur elie Grimberg, G erard DeClerck, Jean-Marc Rabillier, Raymond Soumarmon
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Patent number: 5587127Abstract: A method and apparatus for sterilizing preformed cartons prior to filling is disclosed. The interior of the cartons are first sprayed with a solution of hydrogen peroxide. The cartons are then treated with heated air to remove the hydrogen peroxide. The heated air is applied by means of a hollow mandrel having nozzles at one end. The mandrel corresponds generally to the shape of the carton. When the mandrel is inserted in the carton, air is directed against the interior side walls and bottom of the carton, and is exhausted from the carton by flowing upwardly between the side walls of the mandrel and the side walls of the carton.Type: GrantFiled: August 24, 1994Date of Patent: December 24, 1996Assignee: Tetra Laval Holdings & Finance SAInventor: Leonard A. Carlson
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Patent number: 5580521Abstract: A method and system of treating medical waste product materials that are contaminated with blood, urine and/or other bodily fluids is disclosed. Disinfecting and sterilizing such materials is accomplished through use of heat to deactivate catalase contained in the medical waste. The waste is then contacted with hydrogen peroxide to sterilize the waste.Type: GrantFiled: June 14, 1994Date of Patent: December 3, 1996Assignee: American Sterilizer CompanyInventor: Donald R. Gagne
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Patent number: 5570845Abstract: Containerized medical waste is treated by a process in which the materials are carried by a conveyor under a negative pressure to a multiple-stage shredder. Sodium hypochlorite is added at several points in the shredder section of the apparatus. The output of the shredder is compressed and the liquid component which is separated out is recirculated. The compressed solid is conveyed through a conveyor in which the temperature is maintained at a level just under 212.degree. F. by the introduction of steam. The pressure is maintained at or below atmospheric pressure at all points in the system to prevent release of contaminated materials into the atmosphere. By using the combination of sodium hypochlorite and steam, it is possible to eliminate live microorganisms entirely while still taking advantage of low pressure to avoid accidental release of contaminated materials.Type: GrantFiled: August 3, 1995Date of Patent: November 5, 1996Assignee: Sterile Technology Industries, Inc.Inventors: Robert W. Lewis, Randall G. McKee, William Jones
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Patent number: 5525295Abstract: A microbial barrier isolation system for enclosing and decontaminating equipment so that the equipment may be used in handling or otherwise contacting biologically-sensitive materials such as parenteral solutions and solids. The barrier system is formed with a lower cavity, an upper chamber separated from the inner cavity by filters, an air return conduit, means for supplying dry, heated air to heat the system and means for using steam and hydrogen peroxide to decontaminate the internal parts of the system. The decontamination process involves using dry air to heat the internal equipment of the system to reduce water condensation and then introducing saturated steam and peroxide at a positive pressure slightly above atmospheric pressure. The internal equipment, including all surfaces, is exposed to the steam and peroxide sterilant for a sufficient time to decontaminate the equipment and the system is cooled down with cool, sterile air.Type: GrantFiled: August 27, 1992Date of Patent: June 11, 1996Assignees: Despatch Industries Limited Partnership, TL Systems CorporationInventors: Irving J. Pflug, Allan B. Larson, Hans L. Melgaard
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Patent number: 5520882Abstract: About 1/2 cc of a sterile composition (5) dropped into the rotor drive air feed line (11) of a dental handpiece (10) while holding the handpiece upside down protects and lubricates the handpiece bearings and turbine during the subsequent auto-clave sterilization process. An additional dosage inserted into the bur hole after the auto-clave process further lubricates the handpiece and inhibits rust from forming on the handpiece bearings and turbine during use. The pre-sterilization dosage and post-sterilization dosage of measured amounts may be separately packaged in disposable capsules (20, 30). The composition (5) is made by heat mixing until sterile about 10% by volume of a sterile solution of Power-Up.TM. NNL-690, which is a liquid hydrocarbon boundary lubricant; and corrosion inhibitor, with 90% by volume of pharmaceutical grade mineral oil.Type: GrantFiled: August 1, 1994Date of Patent: May 28, 1996Inventor: Kenneth R. Brown
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Patent number: 5513662Abstract: A method of preparing bone for transplantation in which the internal matrix of the bone is contacted with an atmosphere at less than ambient pressure. The method may additionally, include a further step in which the bone is maintained in contact with a decontaminating agent or a detergent during the period of contact with the atmosphere.Type: GrantFiled: January 21, 1994Date of Patent: May 7, 1996Assignee: Osteotech, Inc.Inventors: Brenda S. Morse, Clement D. Dioh
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Patent number: 5480565Abstract: A method for reprocessing dialyzer cartridges used with kidney dialysis machines is provided. The method involves filling the blood and dialysate compartments of the dialyzer with an aqueous solution containing citric acid at a concentration of 1.0-5.0 wt. %, e.g., 1.5 wt. %, and then subjecting the dialyzer to an elevated temperature above 90.degree. C. and below 100.degree. C., e.g., 95.degree. C., for a period of at least 15 hours, e.g., 20 hours. Although citric acid is non-toxic and the temperature used is below the boiling point of water, the process has been found to produce a fully sterilized dialyzer. After reprocessing, the aqueous citric acid solution is preferably left in the dialyzer where it acts as a bacteriostatic agent during storage. Essentially no damage to the dialyzer and, in particular, to its semipermeable membrane results from either the reprocessing or storage procedures.Type: GrantFiled: October 8, 1993Date of Patent: January 2, 1996Inventors: Nathan Levin, Hans-Dietrich Polaschegg
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Patent number: 5472665Abstract: A method for removing impurities and potentially toxic substances from cellulose is disclosed. The method comprises the following steps: (a) immersing cellulose containing organic extractables in one or more acid baths so as to remove traces of organic extractables; (b) immersing the cellulose in a water bath; (c) immersing the compressed cellulose in an alkaline bath; and (d) sterilizing the treated cellulose using pressurized steam.Type: GrantFiled: January 21, 1993Date of Patent: December 5, 1995Inventors: Paul M. Rosofsky, Seymour Gilbert
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Patent number: 5472042Abstract: The invention provides a method and apparatus for managing retort over-pressure during pressure cooling. The invention allows the specification of an initial cooling temperature and a final cooling temperature and a final cooling pressure. Using these values the invention provides a pressure ramping to manage retort over-pressure.Type: GrantFiled: April 13, 1994Date of Patent: December 5, 1995Assignee: FMC CorporationInventors: Joost Veltman, Richard W. Ripley
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Patent number: 5456881Abstract: Organic and/or inorganic substances and water are thermally separated from contaminated materials, solid aggregates, the contaminated material is pretreated and is subsequently heated in a directly or indirectly heated furnace, which includes a rotary kiln, a fluidized bed furnace or a floating zone reactor, and during the heating the material is treated with recycled hot gases or recycled hot steam and with oxidizing agents. The exiting processing gases, which contain water vapor, are dedusted, and 80 to 90% by volume of the water vapor-containing processing gases are recycled to the furnace to act as entraining gas. The remaining water vapor-containing processing gases are condensed, the resulting liquid phase is withdrawn, and pollutants are removed from the withdrawn liquid phase by a wet chemical or physical processing.Type: GrantFiled: February 10, 1994Date of Patent: October 10, 1995Assignee: Metallgesellschaft AktiengesellschaftInventors: Gebhard Bandel, Stephan Becker, Dirk Hankel, Gurudas Samant, Erhard Weilandt, Johann Renner
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Patent number: 5443385Abstract: A method of disinfecting and lubricating a discrete dental-medical device which comprises immersing the device in a water-alcohol-glycerin-chlorhexidine solution which includes methylcellulouse as a lubrication-enhancing and film-forming agent and polyglycol as an antifoaming agent, followed by autoclaving the device.Type: GrantFiled: May 3, 1994Date of Patent: August 22, 1995Inventor: Thad J. Overmyer
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Patent number: 5422074Abstract: Waste materials containing pathogenic microorganisms may be processed by a method that includes granulating the waste material; treating the granulated waste material by heating at a temperature of about 160.degree. to about 200.degree. C. at a pressure of about 90 to about 226 psi in an atmosphere of the steam from a non-isotonic salt solution. The treatment is conducted for a period of time sufficient to substantially reduce the amount of pathogenic microorganisms present in the waste material. After treatment, the material is separated into useful solid and liquid phases.Type: GrantFiled: July 15, 1993Date of Patent: June 6, 1995Assignee: Envirotrust Technologies, Inc.Inventor: Erick Schmidt
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Patent number: 5364589Abstract: A method and apparatus are disclosed for sterilizing biological waste. The waste material is introduced into a shredder mechanism to chop the material into particles of reduced size, which are transmitted into a preheating chamber. Steam is introduced into the chamber to preheat the particles to at least 140 degrees Fahrenheit. A selected amount of the preheated particles are continuously transmitted into a sterilization chamber and steam is introduced into the sterilization chamber to heat the preheated particles to at least 248 degrees Fahrenheit for a sufficient duration such that the particles are sterilized.Type: GrantFiled: April 1, 1991Date of Patent: November 15, 1994Assignee: Sterile Systems, Inc.Inventors: James A. Buehler, Lynnford W. Claypoole
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Patent number: 5358030Abstract: The invention provides a method and apparatus for managing retort over-pressure during pressure cooling. The invention allows the specification of an initial cooling temperature and a final cooling temperature and a final cooling pressure. Using these values the invention provides a pressure ramping to manage retort over-pressure.Type: GrantFiled: May 8, 1992Date of Patent: October 25, 1994Assignee: FMC CorporationInventors: Joost Veltman, Richard W. Ripley
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Patent number: 5333626Abstract: The invention provides a simple, safe and effective method for treating bone and making it suitable for transplantation comprising: (a) contacting said bone with a global decontaminating agent effective to inactivate bacteria, fungi, virus and parasites; (b) cleaning said bone; and (c) terminally decontaminating said cleaned bone by contacting it with a global decontaminating agent effective to inactivate bacteria, fungi, virus and parasites. The invention also provides a method of cleaning bone which can be used in step (b) of the method described above and comprises contacting the bone with detergent under high pressure washing conditions at elevated temperatures.Type: GrantFiled: December 31, 1991Date of Patent: August 2, 1994Assignee: Cryolife, Inc.Inventors: Brenda S. Morse, Edward Shanbrom
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Patent number: 5314668Abstract: An automated method of disinfecting door handles of units such as disinfecting apparatus. Disinfecting occurs in response to a predetermined function or state, such as the termination of a cleansing operation in a disinfecting apparatus, established time intervals, or a set number of manipulations of the door handle. The door handle may be disinfected by physically moving the handle into the disinfecting apparatus chamber. Alternatively, the handle may be sprayed or impregnated with a disinfecting solution. As another alternative, the door handle may be covered with a sterile, protective film. As a final alternative, the door handle may be disinfected by thermal convection.Type: GrantFiled: March 19, 1993Date of Patent: May 24, 1994Inventor: Stephan Biermaier
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Patent number: 5283053Abstract: A contact lens treating vessel equipped with an electromagnetic induction coil and a rectifier for converting an alternating current into a direct current, and an apparatus for treating contact lenses comprising a treating apparatus body for supplying electric power and the vessel which can be attached to or detached from the apparatus body, wherein the apparatus body is equipped with a magnet-generating coil and the vessel is equipped with an electromagnetic induction coil.Type: GrantFiled: October 21, 1992Date of Patent: February 1, 1994Assignee: Tomei Sangyo Kabushiki KaishaInventors: Hideaki Kamiya, Makoto Nakagawa, Masashi Endo, Masakatsu Yamauchi
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Patent number: 5273714Abstract: The hydrogen peroxide gas supplying apparatus to be sterilized by the method of the invention comprises a hydrogen peroxide gas transport air pipe extending from an air source to the location of the article to be sterilized by way of a closed gasifying tank having a heater incorporated therein, and a microorganism removing filter provided on the air pipe and positioned upstream from the gasifying tank. The apparatus is sterilized by supplying an aqueous solution of hydrogen peroxide to the gasifying tank while supply of air from the air source to the air pipe is discontinued so that the solution is gasified by being heated with the heater.Type: GrantFiled: July 14, 1992Date of Patent: December 28, 1993Assignee: Shikoku Kakoki Co., Ltd.Inventors: Tadao Akai, Kazuo Abe, Hiromichi Nishino
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Patent number: 5268144Abstract: This invention relates to a method for sterilizing a medical unit having at least two connections for a fluid flow pathway where a sterilizing medium flows through the medical unit.Medical units of this type are e.g. medical filters, in particular dialyzers. A high degree of sterility is here required. This is accomplished through the steps of:(a) inserting the medical unit into a system under pressure-tight coupling of the at least two connections to a feed conduit and discharge conduit of the system under atmospheric conditions;(b) passing the sterilizing medium from the system through the medical unit for a given period of time;(c) closing the at least two connections in the coupled state and in a germproof manner, without the same being opened, on completion of the sterilization operation; and(d) removing said medical unit from said system as a sterile medical unit with closed connections.Type: GrantFiled: July 29, 1992Date of Patent: December 7, 1993Assignee: Fresenius AGInventors: Klaus Heilmann, Bernd Mathieu, Michael Rink, Wolfram Weber
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Patent number: 5248486Abstract: A heat generating agent for medical waste sterilization. The agent is at least one compound selected from calcium oxide, calcined dolomite, and magnesium oxide, and at least one compound selected from sulfamic acid, sodium bisulfate, and anhydrous phosphoric acid. The present invention also provides a method for sterilizing medical wastes. The method includes the steps of subjecting medical waste to exothermic reaction between water and a heat generating agent selected from calcium oxide and calcined dolomite or to exothermic reaction between iron powder and oxygen to generate reaction heat and/or alkalinity by the exothermic reaction. The present invention provides an aparatus to be used according to the method mentioned above.Type: GrantFiled: November 30, 1992Date of Patent: September 28, 1993Assignees: Akira Matsuoka, Nihon Health Science Ltd., Kawai Lime Industry Co., Ltd., Sumitomo Cement Co., Ltd.Inventors: Akira Matsuoka, Koichi Mimura, Masayuki Matsumoto, Masaru Matsunami, Kozo Mizutani, Minoru Okamura, Kazuomi Sakai, Toru Yamakawa
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Patent number: 5246674Abstract: A container for use in a microwave apparatus, in particular for heating, drying, disinfecting and/or sterilizing of materials, objects, liquids or the like, includes a lid securely attachable via a pressure lock to the container and including connections for allowing attachment of various valves, pumps etc. to monitor and influence conditions in the container. The connections are self-sealing plug connector pipes which are engageable with a complementary coupler piece of the microwave apparatus. The microwave apparatus includes an injector unit by which water or other liquid is introduced into the material to be treated, with the amount of injected water being dependent on the water content of the material. The injector unit includes a nozzle head which projects into the treatment chamber of the microwave apparatus and incorporates sensors for determining physical and/or chemical parameters.Type: GrantFiled: October 23, 1991Date of Patent: September 21, 1993Assignee: Helmut KatschnigInventors: Helmut Katschnig, Leonard Gage
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Patent number: 5213759Abstract: In a method of sterilizing micro-organisms, the micro-organisms are subjected to UV radiation, in a wavelength band which kills micro-organisms, while in an atmosphere of inert gas or of ozone.Type: GrantFiled: January 18, 1991Date of Patent: May 25, 1993Assignee: Elopak Systems A.G.Inventors: Helge B. Castberg, Nigel A. Chant
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Patent number: 5173258Abstract: A recirculation/drying unit is provided for connection to a sealable enclosure. The unit and the enclosure form a closed circuit through which the gaseous medium of the enclosure is circulated, filtered, dehumidified or optionally, humidified, and returned to the enclosure. A vapor decontaminant is carried into and through the enclosure by the gaseous medium for a predetermined period of time sufficient to sterilize, disinfect or sanitize the gaseous medium, the enclosure and its contents. The decontaminant is returned to the unit for conversion into a form suitable for release into the atmosphere. The unit preferably includes filters, an air pump, a drier, a reservoir of liquid decontaminant, a reservoir of water, an injection pump, at least one vaporizer and at least one converter.Type: GrantFiled: October 11, 1989Date of Patent: December 22, 1992Assignee: American Sterilizer CompanyInventor: Robert W. Childers
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Patent number: 5089228Abstract: A method for sterilizing infectious waste includes placing the waste in a disposal apparatus which has an isolated volume for holding the waste. A dry granulated medium which has a disinfectant constituent is also placed within the isolated volume along with the waste. When the disposal apparatus is activated, an atomized mist is introduced into the volume and the waste, the medium, and the moisture in the mist are thoroughly blended together. The resulting destroyed waste is thoroughly moistened with the disinfectant solution which is formed by the mist and the disinfectant constituents of the medium. Then, the moistened, destroyed waste is heated to a predetermined temperature for a predetermined time to ensure efficacious sterilization of the waste.Type: GrantFiled: April 19, 1990Date of Patent: February 18, 1992Assignee: Winfield CorporationInventor: Robert S. Meijer
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Patent number: 5043175Abstract: A method and apparatus for the sterilization of animal feed, wherein a bactericidal agent is mixed with steam for contacting and conditioning animal feed prior to a compaction process as, for instance, a pelletizing process. In one embodiment, chlorine gas is introduced in the burner of a direct fired steam generator to produce a mixture of steam, chlorine, and products of combustion which are introduced to a feed mixture in a blending unit prior to pelletizing, resulting in sterilization of the animal feed.Type: GrantFiled: October 1, 1990Date of Patent: August 27, 1991Assignee: California Pellet Mill CompanyInventors: Peter T. Bayley, Derek H. Shrimpton
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Patent number: 5035858Abstract: A method of disinfecting medical materials, which comprises heating medical materials and exposing the medical materials to gamma radiation, is provided. One method of heating is the application of radio-frequency waves. The medical materials are subjected to radio-frequency waves for at least approximately 5 minutes and to gamma radiation measuring at least approximately 0.25 Mrads. When the starting material consists of pre-sorted medical or veterinary waste, the method further comprises shredding the irradiated waste and recycling the shredded waste.Type: GrantFiled: June 1, 1990Date of Patent: July 30, 1991Assignee: Stericycle, Inc.Inventors: Jeffery S. Held, James W. Sharp
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Patent number: 4973449Abstract: Heat-labile articles are sterilized by subjecting them to pulses of sporicidal vapors and maintaining them for a holding period in contact with such vapors.Type: GrantFiled: March 10, 1986Date of Patent: November 27, 1990Assignee: MDT CorporationInventors: Robert A. Kolstad, Robert R. Runnells, John C. Schmoegner
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Patent number: 4952370Abstract: This process sterilizes the surfaces within a chamber wherein a first portion of the surfaces is at a temperature below 10.degree. C. and a second portion of the surfaces is at a temperature greater than 20.degree. C. The process includes the steps of introducing vapor phase hydrogen peroxide to the chamber, contacting the first portion with the vapor to effect condensation thereon, contacting the second portion with the vapor, applying a source of vacuum to the chamber and continuing to introduce vapor phase hydrogen peroxide into the chamber until the surfaces are sterile while preserving the temperature ranges of the first and second portions.Type: GrantFiled: May 6, 1988Date of Patent: August 28, 1990Assignee: American Sterilizer CompanyInventors: Arthur L. Cummings, Robert W. Childers
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Patent number: 4908188Abstract: A system for treating articles, preferably with a sterilizing, gas is disclosed. The system includes a chamber into which the articles are received and valves for supplying the sterilizing gas to the chamber and for removing the gas from the chamber after a predetermined time period. The sterilizing gas is generated on site from at least two components, thus minimizing problems in the transportation of the gas to the location. The sterilizing gas generated on site is preferably chlorine dioxide and the two components may be chlorine gas and sodium chlorite. The system includes a programmed microprocessor controller for controlling the valves executing a predetermined sequence of instructions. The predetermined sequence of instructions define a state diagram for the system having a plurality of successive states. In order to provide for system safety, the controller preferably employs a plurality of abort states to which the system returns in the event of a failure.Type: GrantFiled: April 14, 1988Date of Patent: March 13, 1990Assignee: The Scopas Technology Company, Inc.Inventors: Raymond P. Jefferis, III, Phillip V. Engler, Aaron A. Rosenblatt
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Patent number: 4770851Abstract: Methods for sterilization wherein air is purged from the load to be sterilized prior to the addition of the sterilant and wherein residue chemical sterilants, such as ethylene oxide, are purged post-sterilization by introducing air and steam at pressures which cause the steam to condense on the interstices of the load and then vaporize to provide a carrier for trapped air (prior to sterilization) and residue chemical sterilant (post-sterilization).Type: GrantFiled: July 7, 1986Date of Patent: September 13, 1988Assignee: Joslyn Valve Corp.Inventor: Larry Joslyn
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Patent number: 4764351Abstract: An apparatus for sterilization comprises a treatment chamber (1) with constant temperature control (3, 4, 5) connected to a source of vacuum (6, 7, 8, 9), and to a circuit for admitting a carrier gas comprising a means (10) for sterilizing a gas and a means (14) for heating the gas at constant temperature as well as a steam generator (16) connected to a water supply (19) and to a system (20) for controlling the temperature and/or pressure (20). In addition, a sterilizing gas generator (21) contains a solution of a sterilizing agent (22) and is equipped with means for heating and/or cooling and for temperature control (24, 25, 26, 27). Also, suitable means (33) for circulating the atmosphere in the chamber (1) in contact with the solution (22) are provided.Type: GrantFiled: November 27, 1984Date of Patent: August 16, 1988Assignees: Universite Catholique de Louvain, Manufacture Belge de Gemblous S.A.Inventors: Pierre Hennebert, Jean Gillard, Michel Roland
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Patent number: 4752445Abstract: A method for controlling air flow from an inlet to a chamber and from the chamber through the inlet to atmosphere wherein an ethylene oxide gas sterilization process is practiced in the chamber, which process includes conditions of controlled alternating vacuum and pressure. The method employs a diaphragm actuated two-way valve in the inlet line in combination with a remotely mounted three-way solenoid valve. The chamber is sealed against air flow during conditions of vacuum by spring biasing, and during conditions of pressure by spring and pressure biasing, a closure against an orifice in the two-way valve. The vacuum in the chamber is relieved at predetermined periods by selectively exerting sufficient fluid pressure against the diaphragm of the two-way valve to force the closure, which is operatively connected to the diaphragm, away from the orifice into an open position.Type: GrantFiled: August 20, 1985Date of Patent: June 21, 1988Assignee: American Sterilizer CompanyInventor: Peter E. Zell
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Patent number: 4744951Abstract: A process for concentrating hydrogen peroxide from a relatively dilute solution of hydrogen peroxide and water and supplying the concentrated hydrogen peroxide in vapor form to a sterilization chamber. The process includes vaporizing a major portion of the water from the solution and removing the water vapor thereby produced before injecting the concentrated hydrogen peroxide vapor into the sterilizing chamber.Type: GrantFiled: May 10, 1985Date of Patent: May 17, 1988Assignee: American Sterilizer CompanyInventors: Arthur L. Cummings, Jack H. Young, Ralph W. Makinen
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Patent number: 4732735Abstract: When sterilizing packing materials for the aseptic packaging of fruit juice and wine using sulfurous acid it is suggested that the packing material be treated with an aqueous solution of sulfurous acid and alcohol.Type: GrantFiled: March 31, 1987Date of Patent: March 22, 1988Assignee: Tetra Pak Developpement S.A.Inventors: Erwin W. Wartenberg, Hong-An Duong
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Patent number: 4704254Abstract: One or more ports (34) are formed in a bottom wall (18) of a housing (12) and/or a lid (14) of a medical instrument sterilization container (10). As formed in bottom wall (18), the port (34) includes a circumferential, downwardly tapering side member (42) that extends to a bottom member (40) having a plurality of orifices (44) to communicate a sealed interior (26) with the exterior. A filter cartridge (36) is provided for insertion in the port (34) and has a filter medium (60) that permits the passage of sterilizing gas or steam but does not permit the passage of contaminants. A side member (54) of the cartridge (36) tapers downwardly and inwardly from its perimeter to the filter medium (60) and is adapted to sealingly register with the port side member (42). A retainer (38) may be provided for keeping the cartridge side member (54) in sealing registration with the port side member (42).Type: GrantFiled: January 27, 1986Date of Patent: November 3, 1987Inventor: Robert L. Nichols
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Patent number: 4642165Abstract: A method of vaporizing a multicomponent liquid, such as a hydrogen peroxide and water solution, for injection into a vacuum chamber including the steps of metering successive predetermined increments of the liquid at a predetermined rate onto a heated surface in a vaporization chamber. Upon exposure to the heated surface, each liquid increment is substantially instantaneously vaporized before the next succeeding liquid increment is metered onto the heated surface to produce a multicomponent vapor increment having substantially the same weight percent composition as the multicomponent liquid increment. Each vapor increment is passed into the vacuum chamber.Type: GrantFiled: December 21, 1984Date of Patent: February 10, 1987Assignee: American Sterilizer CompanyInventor: Mark E. Bier
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Patent number: 4637916Abstract: A sterilization method comprising subjecting a sterilization chamber to an initial vacuum and then introducing steam to increase chamber pressure. The introduction of steam is interrupted and the chamber is brought into communication with a solution in a gaseous sterilant generator. The mixture of gaseous sterilant and chamber atmosphere are continuously circulated whereby equilibrium is established and the material to be sterilized is subject to constant temperature, pressure, sterilant concentration, and relative humidity for a period of time sufficient for sterilization. Also disclosed is an apparatus capable of performing the sterilization method comprising a sterilization chamber in combination with a gaseous sterilant generator. Formaldehyde is the preferred sterilizing agent.Type: GrantFiled: January 18, 1984Date of Patent: January 20, 1987Assignees: Universite Catholique de Louvain, Manufacture Belge de Gembloux S.A.Inventors: Pierre Hennebert, Jean Gillard, Michel Roland
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Patent number: 4585624Abstract: A gas generator to produce formaldehyde gas in enclosed spaces such as animal houses or for conveying such gas to inaccessible areas through a flexible hose which includes a base and hood mounted thereon. The base is in the form of an open topped container having a heating element oriented under the bottom wall thereof and in heat exchange relation to water and paraformaldehyde flakes or formalgen powder in shallow compartments interiorly of the container for producing formaldehyde gas and water vapor that is heated above ambient temperature. The container includes air inlet slots adjacent to but below the open top and below the lower edge of the hood which is supported on supporting ledge structures on the interior of the container whereby air is entrained into the upwardly moving gas and water vapor for mixing therewith and assisting in disseminating the gas into all areas of the enclosed space when the gas, moisture and air mixture is discharged from an opening in the upper end of the hood.Type: GrantFiled: November 19, 1984Date of Patent: April 29, 1986Inventors: Galen F. Young, Bernell E. Swords
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Patent number: 4576792Abstract: In a chamber (24) in a pressure vessel, e.g. an autoclave (10), articles (26) are heat-treated by water, which is sprayed over the articles through nozzles (20) and supplies heat to or removes heat from the articles. Simultaneously, a gaseous medium, e.g. a mixture of steam and air, is forced by an impeller (34) to flow through the articles in countercurrent to the water. By this a very even temperature distribution of the articles in the chamber (24) is obtained.Type: GrantFiled: September 17, 1984Date of Patent: March 18, 1986Assignee: Aktiebolaget ElectroluxInventor: Karl I. M. Martensson
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Patent number: 4447399Abstract: A combination unsaturated chemical vapor sterilization system and a steam sterilization system utilizing the same sterilizing chamber. It includes a pressure chamber in communication with a source of sterilizing chemicals and water, transport means to selectively deliver sterilizing chemicals or water into the chamber, a heating element to heat the interior of the chamber, and a microprocessor control panel operably associated with the heating element and transport means to control the sterilant composition, the temperature and the pressure within the chamber at any given time in accordance with a preselected setting.Type: GrantFiled: May 7, 1981Date of Patent: May 8, 1984Assignee: MDT Chemical CompanyInventors: Robert R. Runnells, Peter A. Haak, Rodney B. Larkin, C. Keith Vandervelden
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Patent number: 4447394Abstract: An apparatus and method for sterilizing particles in an autoclave with an atmosphere of formaldehyde and water vapor so that the sterilized articles have tolerable quantities of residue of formaldehyde and paraformaldehyde thereon. In the process, formalin is used which is transformed to a gaseous condition and supplied to the autoclave. The apparatus is provided with a vaporizer for formalin in which the vaporizer is provided with a liquid trap so that the formalin becomes said water vapor and formaldehyde.Type: GrantFiled: August 1, 1983Date of Patent: May 8, 1984Assignee: Aktiebolaget ElectroluxInventor: Jan K. Krouthen
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Patent number: 4424189Abstract: The sterilization of open-topped containers is accomplished by vaporizing a sterilizing agent in the vicinity of the container. The vaporization is preferably achieved by spraying the sterilizing agent on to a heating element positioned either in or immediately above the open top of the container.Type: GrantFiled: June 23, 1982Date of Patent: January 3, 1984Assignee: Hick & Co. GmbHInventor: Werner Hick
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Patent number: 4410492Abstract: A method for sterilizing medical devices is disclosed. The method comprises the circulation of a sterilant gas through a contaminated device bacteriologically to sterilize exposed surfaces, permitting the sterilant gas to remain within the lumen of the device for an effective period of time, and thereafter removing the sterilant gas by purging with sterile air or other inert gas.Type: GrantFiled: May 17, 1982Date of Patent: October 18, 1983Assignee: Ben Venue Laboratories, Inc.Inventor: Saul Kaye
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Patent number: 4397814Abstract: A conventional cooker or retort for heat processing sealed containers, such as sealed pouches, jars or cans, has an evaporator associated therewith. A source of water is coupled to the evaporator through a valve and a source of a liquid having a higher vapor pressure than water, such as ethyl alcohol, is connected to the evaporator through a metering pump. Pressure and temperature within the retort are monitored and signals indicative thereof are connected to controllers for metering the heat supplied to the evaporator and for metering the ethyl alcohol and water delivered to the evaporator. One controller is configured to operate so that as pressure rises, proportions of ethyl alcohol introduced into the evaporator is reduced while the proportion of water introduced is increased. Another controller functions to restrict the amount of heating medium, such as steam, delivered to the evaporator as the retort temperature increases.Type: GrantFiled: April 26, 1982Date of Patent: August 9, 1983Assignee: FMC CorporationInventor: Andrea Darecchio
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Patent number: 4366125Abstract: A long sheet material to be sterilized is passed through an atmosphere of H.sub.2 O.sub.2 mist of low concentration and of droplet particle size of approximately 10 microns at room temperature for approximately one second and is then irradiated for approximately one second with ultraviolet-ray lamps positioned to irradiate opposite surfaces of the sheet material each at a distance of approximately 20 mm therefrom, whereby the material is thoroughly sterilized as a result of the synergistic effect produced by the combination of these two sterilization steps.Type: GrantFiled: November 24, 1980Date of Patent: December 28, 1982Assignee: Dai Nippon Insatsu Kabushiki KaishaInventors: Tokio Kodera, Masaru Hoshino, Kimiaki Hyakutome
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Patent number: RE33007Abstract: A method of vaporizing a multicomponent liquid, such as a hydrogen peroxide and water solution, for injection into a vacuum chamber including the steps of metering successive predetermined increments of the liquid at a predetermined rate onto a heated surface in a vaporization chamber. Upon exposure to the heated surface, each liquid increment is substantially instantaneously vaporized before the next succeeding liquid increment is metered onto the heated surface to produce a multi-component vapor increment having substantially the same weight percent composition as the multicomponent liquid increment. Each vapor increment is passed into the vacuum chamber.Type: GrantFiled: February 9, 1988Date of Patent: August 1, 1989Assignee: American Sterilizer CompanyInventor: Mark E. Bier