Abstract: A robotic arm assembly includes a robotic arm, a base, and a utility member, the robotic arm extending between a root end attached to the base and a distal end including the utility member. A method for controlling the robotic arm assembly includes: determining a position of the base, the root end, or both relative to the environment; determining a task position and orientation for the utility member within the environment; determining a three-dimensional constraint of the environment; and determining a path for the robotic arm through the environment based on each of the position of the base, the root end, or both relative to the environment, the task position and orientation for the utility member within the environment, and the three-dimensional constraint of the environment.

Abstract: An inspection system comprises a crane system, a six axis, one hundred and fifty degree articulating robotic arm, a laser inspection system, and a communications system. The robotic arm is connected to a base of the crane system. The laser inspection system is connected to the robotic arm. The communications system is configured to send and receive instructions for the crane system, the robotic arm, and the laser inspection system.

Abstract: The present invention relates to a method of treating lead anode slime having high fluorine and arsenic content, in particular to a method comprising smelting of the lead anode slime and cleaning the produced off gases in a one or more wet gas cleaning stages.

Abstract: Extracting gallium and/or arsenic from materials comprising gallium arsenide is generally disclosed. In some example embodiments, a material comprising gallium arsenide may be exposed to a first heating condition to form a first exhaust. The first exhaust may be directed to an arsenic collection bed including aluminum, which may form aluminum arsenide. The material including gallium arsenide may be exposed to a second heating condition and/or a vacuum may be applied, which may form a second exhaust. The second exhaust may be directed to a gallium collection bed including aluminum, which may form gallium alloys of aluminum.

Abstract: A warpage test system uses a calibration block to calibrate the warpage test system over a temperature profile. The calibration block includes a first metal block bonded to a second metal block. The first metal block includes a first metal and a second different metal. The first metal block includes a CTE different than a CTE of the second metal block. The calibration block is disposed in the warpage test system. A warpage of the calibration block is measured over a temperature profile ranging from 28° C. to 260° C. A deviation between the measured warpage of the calibration block and a known thermal expansion of the calibration block over the temperature profile is recorded. The warpage measurement in a semiconductor package is compensated by the deviation between the measured warpage of the calibration block and the known thermal expansion or warpage of the calibration block over the temperature profile.

Abstract: Process for degrading organic substances in an aqueous composition comprising a step (a) wherein, in a liquid reaction medium, said aqueous composition is reacted with at least one composition comprising hydroxide ions (OH?) and hypochlorite in a molar ratio between hydroxide and hypochlorite higher than or equal to 0.001 and lower than 1.5, in order to oxidize said organic substances.

Abstract: A method of removing lead sulfide contained in refined molybdenite powder concentrates (major component; MoS2) is provided. More specifically, in order to solve the problems associated with a leaching method using a leaching agent that is employed for conventional hydrometallurgical process, oxygen-free inert gas is circulated in a furnace for pyrometallurgical treatment to evaporate lead sulfide at high temperature, followed by condensing process to recover lead sulfide at low temperature. The method is characterized in that, it can reduce environmental contamination and can easily recover sulfides of valuable metals such as lead, indium, zinc and the like.

Abstract: A method of extracting gold from arsenic gold ore concentrate, wherein increase the temperature of smelting chamber to 100-300° C. and then hold the temperature to remove the vapor and small quantity of dust in the arsenic gold ore concentrate; Under residual pressure?50 Pa, increase the temperature of smelting chamber and crystallization chamber to 300-500° C. and then hold the temperature to remove the volatilized arsenic sulfides; Hold the temperature of crystallization chamber, increase the temperature of smelting chamber to 500-600° C. and then hold the temperature to remove the gaseous element sulfur decomposed; Increase the temperature of smelting chamber to 600-760° C. and then hold the temperature, lower the crystallization chamber temperature to 270-370° C. and then hold the temperature to get element arsenic; shutdown, lower the temperature, charge the air, take out the gold-rich slag after dearsenization, and extract fine gold using conventional method.

Abstract: This invention pertains to a chalcogenide glass of low optical loss that can be on the order of 30 dB/km or lower, and to a process for preparing the chalcogenide glass.

Abstract: A process for preparing As4O6 comprises successively heating and cooling a mixture of natural Sinsuk and 40% alcohol in a ratio of about 1: about 1 for about 1 to about 2 hour(s) resulting in a product, successively washing the product with distilled water thereby forming washed precipitates, maintaining the washed precipitates at about ?40° C. for 24 hours, defrosting, filtering, and drying the precipitates, and successively heating and cooling the precipitates to obtain the final As4O6 product.

Abstract: A process for the recovery of arsenic trioxide from acid solutions, particularly the aqueous acid effluent produced by a gas-washing process in the pyrometallurgy of copper sulfide ores is provided. Generally, the process comprises concentrating the acid solution in one or more evaporators in series; crystallizing arsenic contained in the concentrated solution as arsenic trioxide crystals; filtering the crystallized solution to obtain a solid phase comprising impure arsenic trioxide crystals; and purifying the solid phase to obtain a purified crystal product comprising arsenic trioxide. The process produces a commercially salable arsenic trioxide product without producing any solid or liquid residues subject to special handling or treatment regulations.

Abstract: In a process for separating tin as well as, if required, copper from scrap melts, in particular, tinplate melts or metallic melts as formed in the working up of waste or metal-oxide-containing combustion residues, the carbon content of the melt is adjusted to 3 to 4.2% by weight and hot wind, oxygen or air enriched with oxygen is locally blown on partial regions of the surface of the melt bath, whereby SnO is discharged, via the gaseous phase, from the redox-gradient-exhibiting zone formed between the carbon-rich bath and the iron oxides produced by top-blowing.

Abstract: A method is described which allows two hazardous waste products, namely PVC and electric arc furnace dust, both of which have negative commercial value, to be combined to produce an iron oxide suitable for steel making and making pure cadmium lead and zinc and chlorine, all of which can be sold. The heat generated during the exothermic reaction may be used to generate electricity which may be sold or used in plants where the reaction is carded out. The method can also be used for metal scraps.

Abstract: A process for the removal of volatilizable inorganic contaminants from solid waste is provided. The process comprises the steps of: (a) providing solid waste containing volatilizable inorganic contaminants; (b) heating the waste to a temperature sufficiently high for the volatilization of the inorganic contaminants and sufficiently low so as to prevent slag formation of the solid waste, thereby producing a contaminant-rich vapor phase and a contaminant-poor solid phase; and (c) separating the solid phase and the vapor phase.

Abstract: The present invention provides a process for recovering arsenic acid from a starting mixture comprising sulfuric and arsenic acids and water. In step (a), the starting mixture is treated with a sulfur (IV) compound which will reduce the arsenic acid to arsenic (III) compound under conditions sufficient to substantially convert the arsenic acid to arsenic (III) wherein the resulting mixture comprises arsenic (III) compound, the sulfur (IV) compound, sulfuric acid, and water. In step (b), the resulting mixture is purged with gas to substantially remove the sulfur (IV) compound from the mixture wherein the purged mixture comprises the arsenic (III) compounds, sulfuric acid, and water. In step (c), the purged mixture is treated under conditions sufficient to substantially separate the arsenic (III) compounds from the purged mixture.

Abstract: This invention relates to a novel method of, and means for, directing energy through Si.sub.2 HSb.sub.2 in such a manner that normal energy parameters can be exceeded. The principal object of the invention is to provide the means for more efficient radiant energy power systems to be constructed. For example, this invention can be applied to construct more efficient rocket propulsion systems.Si.sub.2 HSb.sub.2 has a crystalline structure with a regular pattern of electron deficiencies which physicists call "holes" in the lattice. Energy can be radiated at the top of the compound and be accelerated as it passes through to a new higher velocity as it expelled out the bottom of the compound. This is accomplished by applying electrical potentials to the sides of the compound which rectify the "holes" in the lattice. The electrical potentials applied to the sides of the compound can be varied to allow the radiated energy output to be directed in the x,y plane.

Abstract: To recover the antimony contained in a solution of use antimony-containing catalyst, emananting from units for the fluorination or chlorofluorination of halogenated hydrocarbons comprising at least two carbon atoms, the solution is concentrated to the limit of distillation of antimony trichloride, an excess of chlorine is then added to convert SbCl.sub.3 to SbCl.sub.5, and SbCl.sub.5 is distilled under reduced pressure without exceeding 120.degree. C.The recoverd antimony pentachloride is sufficiently pure to be able to be recycled directly to the fluorination reactor.

Abstract: Fume generated by roasting speiss is contacted with an oxygen-containing gas at an elevated temperature for a sufficient time to product arsenic and antimony products which may be separated from each other by means such as condensation. Further, in the roasting of antimony-containing phases (such as speiss) the presence of arsenic can enhance the volatility of the antimony.

Abstract: This invention relates to the metallurgy of iron and particularly to the separation and recovery of metals from electric arc furnace (EAF) dusts. While the invention discloses a process for the separation and recovery applicable to zinc, lead, cadmium and antimony contained in such EAF dusts, the invention is particularly applicable to the separation and recovery of zinc. This invention describes a method for reducing the zinc contained in an EAF dust, volatilizing the metallic zinc so produced from the mass of the dust, and reoxidizing the metallic zinc to zinc oxide along with the simultaneous regeneration of hydrogen which can be recycled to treat additional EAF dust.

Abstract: Method and apparatus for producing matte and/or metal from sulphidic fine-grained ore or ore concentrate. The ore or ore concentrate is smelted in a flame chamber in such a way that at least part of the solid material in the flame chamber melts and flows downward into a smelt bath furnace, on top of which the flame chamber is disposed. Volatile metallic and sulphuric components are conducted upward from the flame chamber to a fluidized bed reactor to be utilized as fluidizing gas, the gases being rapidly cooled down in the fluidized bed.

Abstract: An exhaust processing apparatus comprises a cracking furnace for cracking and solidifying exhaust discharged from a reactor for forming crystals on a semiconductor substrate, a first collecting device for collecting relatively large components solidified in the cracking furnace, a second collecting device for collecting relatively small solidified components passed through the first collecting device, and a chemical or a physical adsorbing member for chemically or physically adsorbing the exhaust passed through the first and second collecting devices.The apparatus may be provided with bypass piping for bypassing a particular section of the apparatus, a shutoff member for opening and closing the bypass piping and a control device for controlling the shutoff member.

Abstract: Arsenic and antimony are separated from speiss by a roasting operation employing pyrite and coke and the arsenic is separated from the resultant product by a water pressure leaching operation.

Abstract: A method for preparing compounds of sulfur, selenium, and tellurium includes the formation of the compound from the elements in a closed environment which excludes oxygen, and then the purification of the compound by contacting it with carbon or carbon monoxide. Oxygen, the principal contaminant in conventionally prepared compounds of this group, is excluded from the formation of the compound in the formation step by using a closed reactor, preferably made of vitreous silica. Oxygen in the initial elemental reactants remains in the compound made in this way, and the purification step eliminates the oxygen originally present in the elemental reactants from the compound. Arsenic triselenide made by this approach, glassy and of high purity, is suitable for use in applications requiring infrared transparency.

Abstract: Ultra-fine spherical particles of a metal oxide having an average particle diameter of 40 nm or smaller can be prepared by a method in which a vaporizable metal compound is vaporized and decomposed under heating to give ultra-fine particles of a metal oxide followed by immediate cooling down to a temperature at which coalescence of the fine particles are prevented from coalescence. The fine particles have characteristics such as an excellent power of ultraviolet scattering.

Abstract: Fume generated by roasting speiss is contacted with an oxygen-containing gas at an elevated temperature for a sufficient time to produce arsenic and antimony products which may be separated from each other by means such as condensation. Further, in the roasting of antimony-containing phases (such as speiss) the presence of arsenic can enhance the volatility of the antimony.

Abstract: A process is disclosed for producing a powdered antimony pentoxide composition that rapidly disperses on contact with water. The process comprises spray drying the antimony sol at a temperature of from 180.degree. to 210.degree. F.

Abstract: Hazardous waste containing inorganic compounds which contain heavy metals or particular hazardous anionic groups or which are hazardous halides or non-metal oxides or sulfides is contacted with molten aluminum to provide reduction to lower less hazardous oxidation state.

Abstract: A method is disclosed for recovering gallium and/or germanium from fly ash which comprises pelletizing the fly ash, treating the pellets in the presence of an oxidizing gas at a temperature of from about 900.degree. C. to just below the fusion temperature of the pellets, treating the pellets in the presence of a reducing gas at the same temperature range, and recovering gallium and/or germanium suboxides from the gas.

Abstract: Scrap containing gallium and arsenic is treated with chlorine gas to form a crude gallium and arsenic chloride mixture. Arsenic chloride and impurities having a lower boiling point than that of arsenic chloride are removed from the mixture by vaporization so that crude gallium chloride may be obtained. The crude gallium chloride is purified by distillation. The purified gallium chloride is electrolyzed to yield metallic gallium. If the scrap has a molar gallium/arsenic ratio exceeding 1, arsenic chloride or metallic arsenic or both are added to the scrap before it if treated with chlorine gas.

Abstract: The invention relates to a method for preparing a sulphidic concentrate which is intended for further processing to copper and/or precious metals and which contains high percentages of arsenic and/or antimony, and possibly also bismuth in quantities likely to disturb subsequent processing stages, by partially roasting the concentrate in a fluidized bed, so as to eliminate substantially all the arsenic present and a major part of the antimony and/or bismuth. According to the invention, the concentrate and gas are supplied to a fluidized-bed reactor, and are there heated to a minimum temperature above the splitting or decomposition temperatures of the complex minerals containing arsenic and/or antimony and bismuth present in the concentrate. The oxygen potential in the reactor is regulated, so as to prevent the formation of non-volatile compounds of said impurities. The residence time of the concentrate in the reactor is controlled in a manner to ensure a given minimum elimination of the impurities.

Abstract: The invention relates to an improvement in a method for recovering metal values from copper-containing and/or precious-metal containing materials which also contain antimony and/or bismuth in such high quantities as to render working-up of the materials with conventional metallurgical processes difficult or impossible. In accordance with the improvement, the material is subjected to a chlorination volatilization process in a manner to bring the antimony and/or bismuth content of the material to a predetermined low level acceptable for the continued working-up of the material in conventional process stages, while maintaining the metal values of the material in a substantially unaffected form. The volatilization process is best carried out at temperatures of between 450.degree. C. and 750.degree. C., preferably between 550.degree. C. and 650.degree. C.

Abstract: The invention relates to a process for the refining of sulfidic concentrates which contain arsenic, antimony and bismuth, wherein a suspension of the sulfidic concentrate and oxygen or oxygen-enriched air is introduced into the upper part of a reaction zone, in the lower part of which the direction of the gases is deflected sidewards in order to cause the molten and solid particles traveling along with the gases to impinge against the surface of the melt below the reaction zone. In order to form a molten or semi-solid phase, concentrate, oxygen or oxygen-enriched air, and a carbon- or sulfur-containing fuel are introduced into the reaction zone in such proportions that in the upper part of the reaction zone there is formed an atmosphere containing sulfur and sulfur dioxide and having a temperture above 900.degree. C. and a maximum oxygen pressure of 10.sup.-6 atm in order to volatilize the arsenic, antimony and bismuth, and possibly the lead and zinc.

Abstract: Method and apparatus for the removal of arsenic compounds from an arsenic-containing material wherein the material is reacted with an oxygen carrier and a sulfur carrier under temperature conditions sufficiently high to convert the arsenic compounds to sulfides and the arsenic sulfides are thereupon condensed and deposited in solid form.

Abstract: A method is disclosed for converting an arsenic-containing waste product to a depositable, substantially arsenic-free form by fuming-off the arsenic content thereof. The method comprises melting the waste product under oxidizing conditions in a furnace to form an oxidic slag melt; causing turbulence of the melt, while maintaining a reducing atmosphere supporting the formation of arsenic (III) oxide at the furnace temperature driving-off arsenic content of the waste product substantially in the form of gaseous arsenic (III) oxide; separating the formed oxide by condensation and recovering the same and removing from said furnace a substantially arsenic-free depositable slag.

Abstract: Bromide ions when used as the redox intermediates in the oxidation of arsenic (III) oxide to arsenic (V) acid can be removed from a solution having a major proportion of arsenic acid by treatment with an oxidant selected from H.sub.2 O.sub.2, O.sub.3 or Cr(VI) to oxidize the bromide to bromine followed by purging with air, nitrogen or other inert gas to sweep out the resultant bromine. The bromine can be recovered and recycled to a fresh batch of arsenic (III) oxide.

Abstract: The present invention relates to a process for the separation of gold and silver from complex sulfide ores and concentrates which, in addition to the primary metals, contain constituents having an adverse effect on the separation of the noble metals, by heating the sulfide ore or concentrate at a temperature of 600.degree.-900.degree. C. and a sulfur pressure of 0.2-1 atm in order to bring the complex metal compounds to a suitable form for subsequent alkalic cyanide leaching, and by separating the gold- and silver-bearing cyanide solution from the undissolved residue.

Abstract: Uranium ores, concentrates, calcines or tailings are processed to remove radium and thorium as well as uranium. Selected ores, concentrates or tailings, or if more appropriate, chlorination calcines thereof, are leached by selected aqueous chlorine-containing media (preferably in two stages) until uranium, radium and thorium are substantially all dissolved, with the insoluble residual solids being suitable for disposal. The leach solution is treated to recover sequentially uranium, usually thorium, and radium by selected techniques. The radium recovered can be disposed of in any environmentally-acceptable manner. The amount of iron in the residual leach liquor should be controlled to avoid iron build-up, with the barren leach solution being suitable for recycle.

Abstract: A tellurium component is separated from a tellurium-antimony-containing metal oxide catalyst by heating the catalyst at a temperature of about 900.degree. C. to about 1,000.degree. C. in a non-reducing atmosphere.

Abstract: The invention comprises a process for the manufacture of metal chlorides by the double-decomposition reaction between a metal chlorinating agent and a metal oxide having greater affinity for chlorine than does the oxide of the metal chloride, and in the presence of small amounts of boron chloride or functionally equivalent boron compounds that increase the rate and degree of completion of the reaction.A major application of this invention is for the making by the chlorination of clay of aluminum chloride and alumina intermediates for the manufacture of aluminum metal.SiCl.sub.4 is formed in the carbo-chlorination of clay or other aluminous-siliceous ores. The SiCl.sub.4 by this invention is catalyzed with BCl.sub.3 and reacted with calcined clay to produce AlCl.sub.3 and SiO.sub.2. The practical use of SiCl.sub.4 to make AlCl.sub.3 thus eliminates the previous costly burden of waste SiCl.sub.4 production.

Abstract: Titanium disulphide particles comprising orthogonally intersecting plates, and having a relatively high surface area, e.g. above 4 m.sup.2 /g, in relation to its size, e.g. average largest diameter 2-16 microns, and a method for its preparation by the vapor phase reaction between titanium tetrachloride and hydrogen sulphide is provided. This material is susceptible to intercalation by, for example, lithium and may be used as an active cathodic material in electrochemical cells such as secondary batteries.

Abstract: Purified lead and antimony oxide are produced from antimonial lead alloys by oxidation of the molten alloy to form purified metallic lead and a slag of lead oxides and antimony oxides, separation of the metal and slag, and subsequent partial reduction and fuming of the slag to produce pure antimony oxide.

Abstract: A method for removing sulfur and arsenic from cobaltiferous ores and recovering an enriched cobalt product is described. The procedure involves the steps of(a) oxidizing said ore at a temperature of at least about 700.degree. C. to reduce the sulfur content of the ore to the desired level,(b) heating said oxidized ore with a reducing agent at a temperature of at least about 700.degree. C. to remove arsenic from the ore, and(c) recovering an enriched cobalt containing solid as the product of the process.

Abstract: A process for treatment of antimony-containing materials in a fluidized bed by way of calcination of the materials at a temperature within the range of from 800.degree. to 1,100.degree. C. obtained by combusting a mixture of a fuel gas and an oxygen-containing gas in said fluidized bed. Said mixture of the gases is formed directly in said fluidized bed by supplying, thereinto, the fuel gas and oxygen-containing gas in separated streams uniformly distributed over the bottom cross-section of said fluidized bed so that the fuel gas stream is surrounded over the entire perimeter by the oxygen-containing gas streams.The process according to the present invention makes it possible to treat antimony-containing materials with a content of antimony ranging from 0.3 to 15% by weight and to obtain antimony-rich sublimates with a content of antimony as high as 40 to 75% by weight.

Abstract: A method of preparing a colloidal aqueous dispersion of antimony pentoxide from substantially water-insoluble metal antimonate is described. The method comprises contacting an aqueous slurry of the metal antimonate with a cation exchange resin whereby the metal antimonate is converted to the colloidal antimony pentoxide. A preferred method involves passing the slurry of metal antimonate through a fluidized bed containing a cation exchange resin. The colloidal sols obtained in the prescribed manner are useful as flame retardants when combined with halogen compounds.

Abstract: A process for thermally treating fine-grained solids with high-oxygen gases at temperatures at which the solids can form molten and gaseous reaction products comprises carrying out the thermal treatment at least in part in a cyclone chamber. The solids, high-oxygen gases and, if desired, an energy carrier (usually a carbon-containing solid, liquid or gas) are mixed to form a suspension at a temperature below the reaction temperature. The suspension is fed to a vertical combustion path (tube) and reacts therein to form another suspension of primarily molten particles which is admitted to the cyclone chamber. Reactants are added to the gas phase within a core-flow region of the cyclone chamber and/or immediately after the discharge of gas therefrom to a cooling chamber.

Abstract: A process for substantially reducing the presence of impurities from a sulfur-containing feed material such as dust and hydrometallurgical wastes that result from smelting and refining operations. Pelletized feed materials are heated to 800.degree. to 1150.degree. C and reacted with a gas stream containing chlorine and oxygen. In the presence of sulfur dioxide formed in situ and due to the presence of residual sulfur, the order of volatilization of the elements contained in the feed material is changed from that known for conventional chloridization processes to a more advantageous order. The elements Cd, Bi, Re, Pb, Mo, Sn, Sb, Zn, and As are volatilized and thereby separated from the solid feed material which is consequently enriched in Cu, Ag, Co, Fe, Ni, Au, and precious metals. The feed material is subsequently refined conventionally.

Abstract: This invention relates to refining platinum group metal concentrates and the separation therefrom of silver and of the majority of base metals with which they naturally occur. In more detail the process comprises the steps of:(a) contacting a solid particulate mixture of base, silver and precious metal components, any of which components may be in metallic or chemically combined form, with a halogen-containing gas at a temperature which is sufficiently high for the base metal and silver components to form their halides and for the said halides substantially to volatilize from the said solid mixture, and(b) removing the said volatilized halides from the solid precious metal-containing component which remains.

Abstract: A method of regenerating used particulate contaminant-removing material, such as iron oxide or iron sulfide, that has been used to remove a contaminant, such as arsenic, from a synthetic hydrocarbonaceous feed and effect deposition of the contaminant within the material, characterized by a multi-step process as follows: (1) the used, or spent, contaminant-removing material is intimately contacted with a sulfur-containing material, such as hydrogen sulfide or sulfur, in an inert atmosphere of non-oxidizing fluid and at elevated temperature; (2) the contaminant deposited in the contaminant-removing material is reacted with the sulfur in the sulfur-containing material at the elevated temperature and the resulting sulfides of the contaminant; for example, arsenic sulfides; are converted to gaseous form to separate them from the regenerated contaminant-removing material; and (3) the sulfides of the contaminant are condensed and oxidized to form the oxides of the contaminant; for example, arsenic oxides.

Abstract: Antimony pentachloride is recovered from a spent antimony catalyst mixture in a simple manner by bubbling through the spent catalyst mixture an inactive gas such as trichlorotrifluoroethane at an elevated temperature to convert and to remove high melting point or high sublimating point substances as lower boiling point substances; converting fluorinated antimony into chlorinated antimony by means of a chlorinating agent such as carbon tetrachloride; converting antimony (III) into antimony (V) by oxidation with chlorine; and recovering antimony pentachloride by distillation. The antimony pentachloride thus recovered may readily be used as a catalyst for fluorination of a chlorinated hydrocarbon by reaction with hydrogen fluoride.

Abstract: Disclosed is a process for the recovery of antimony pentachloride from catalyst solutions used in the fluorination of chlorinated hydrocarbons characterized in that the exhausted catalyst solution containing antimony ions and high boiling halogenated hydrocarbons is chlorinated to convert the Sb.sup.3.sup.+ to Sb.sup.5.sup.+ followed by treatment of the solution with hydrogen fluoride to give SbCl.sub.x F.sub.y compounds, wherein x is 4-2 and y is 1-3, the sum of x+y being 5, and to convert the high boiling halogenated hydrocarbons to lower boiling halogenated hydrocarbons, thereafter removing the halogenated hydrocarbons having a lower boiling temperature than the boiling point of SbCl.sub.x F.sub.y and converting the remaining SbCl.sub.x F.sub.y compound with carbon tetrachloride to form antimony pentachloride which is thereafter separated from the remaining organic compounds and inorganic residue.