Metal Coating Patents (Class 427/241)
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Patent number: 11471910Abstract: A coating method for coating parts in a dip-spin process is provided. The parts to be coated are dipped into a coating liquid and then centrifuged in at least one planetary basket arrangement in a planetary centrifuge. The planetary centrifuge includes a main rotor rotating about a main rotor axis of rotation and at least one planetary basket arrangement rotates about its planetary axis of rotation. Also, the planetary axis of rotation is arranged eccentrically on the main rotor. The at least one planetary basket arrangement can include a plurality of planetary baskets rotatably arranged about the planetary rotation axis of the at least one planetary basket arrangement and the planetary basket arrangement is rotated during a centrifuging operation.Type: GrantFiled: November 4, 2020Date of Patent: October 18, 2022Assignee: EJOT GmbH & Co. KGInventor: Fabian Simonsen
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Patent number: 11319626Abstract: A vacuum deposition facility is provided for continuously depositing on a running substrate coatings formed from metal alloys including a main element and at least one additional element. The facility includes a vacuum deposition chamber and a substrate running through the chamber. The facility also includes a vapor jet coater, an evaporation crucible for feeding the vapor jet coater with a vapor having the main element and the at least one additional element, a recharging furnace for feeding the evaporation crucible with the main element in molten state and maintaining a constant level of liquid in the evaporation crucible, and a feeding unit being fed with the at least one additional element in solid state for feeding the evaporation crucible with the at least one additional element either in molten state, in solid state or partially in solid state. A process is also provided.Type: GrantFiled: July 27, 2017Date of Patent: May 3, 2022Assignee: ArcelorMittalInventors: Sergio Pace, Eric Silberberg, Dimitri Wilders, Rémy Bonnemann, Lucie Gaouyat
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Patent number: 10121919Abstract: The physical and chemical properties of surfaces can be controlled by bonding nanoparticles, microspheres, or nanotextures to the surface via inorganic precursors. Surfaces can acquire a variety of desirable properties such as antireflection or reflection, antifogging, antifrosting, UV blocking, and IR absorption, while maintaining transparency to visible light. Micro or nanomaterials can also be used as etching masks to texture a surface and control its physical and chemical properties via its micro or nanotexture.Type: GrantFiled: August 3, 2017Date of Patent: November 6, 2018Assignee: NANOCLEAR TECHNOLOGIES INC.Inventors: Harold Frank Greer, Scott S. Harried, Ryan Morrow Briggs, Tony Lee
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Publication number: 20140287424Abstract: The present invention relates to a slide chip for a sensor for detection of food-borne bacteria and a fabrication method thereof. More particularly, the invention relates to a slide chip for a sensor for detection of food-borne bacteria and a fabrication method thereof, the slide chip comprising: a substrate coated with a metal; a linker having a substituent which may be bonded to the metal and is located at the 5? end of deoxythymidine (dT); and a food-borne bacterium-derived RNA aptamer that is bound to the linker by the 3?-end poly A tail. The slide chip makes it possible to detect food-borne bacteria in a rapid and accurate manner.Type: ApplicationFiled: February 22, 2012Publication date: September 25, 2014Applicant: KOREA FOOD RESEARCH INSTITUTEInventors: Young Jin Cho, Chul Jin Kim, Nam Soo Kim, Chong Tai Kim, Jin Soo Maeng, Tae Eun Kim, Myung Hyun Lee
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Patent number: 8802008Abstract: An automatic analyzer for analyzing samples, such as urine and blood, is adapted so that analysis measured values are not affected by carry over by a repeatedly used dispensing nozzle. Coating the surface of the dispensing nozzle with a chemisorbed polyethylene glycol derivative forms a molecular layer that inhibits the adsorption of biopolymers, to reduce carry over by the dispensing nozzle.Type: GrantFiled: November 26, 2010Date of Patent: August 12, 2014Assignee: Hitachi High-Technologies CorporationInventors: Shinichi Taniguchi, Akihiro Nojima
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Publication number: 20140141164Abstract: Systems and methods in accordance with embodiments of the invention implement layers of metallic glass-based materials. In one embodiment, a method of fabricating a layer of metallic glass includes: applying a coating layer of liquid phase metallic glass to an object, the coating layer being applied in a sufficient quantity such that the surface tension of the liquid phase metallic glass causes the coating layer to have a smooth surface; where the metallic glass has a critical cooling rate less than 1000 K/s; and cooling the coating layer of liquid phase metallic glass to form a layer of solid phase metallic glass.Type: ApplicationFiled: October 22, 2013Publication date: May 22, 2014Applicant: California Institute of TechnologyInventor: Douglas Hofmann
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Patent number: 8591985Abstract: A method is provided which includes dispensing a deposition solution at a plurality of locations extending different distances from a center of a microelectronic topography each at different moments in time during an electroless plating process. An electroless plating apparatus used for the method includes a substrate holder, a moveable dispense arm, and a storage medium comprising program instructions executable by a processor for positioning the moveable dispense arm. Another method and accompanying electroless deposition chamber are configured to introduce a gas into an electroless plating chamber above a plate which is suspended above a microelectronic topography and distribute the gas to regions extending above one or more discrete portions of the microelectronic topography.Type: GrantFiled: July 19, 2010Date of Patent: November 26, 2013Assignee: Lam Research CorporationInventor: Igor C. Ivanov
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Patent number: 8455048Abstract: A method of making a nanostructure by preparing a face centered cubic-ordered metal nanoparticle film from metal nanoparticles, such as gold and silver nanoparticles, exerting a hydrostatic pressure upon the film at pressures of several gigapascals, followed by applying a non-hydrostatic stress perpendicularly at a pressure greater than approximately 10 GPA to form an array of nanowires with individual nanowires having a relatively uniform length, average diameter and density.Type: GrantFiled: September 13, 2010Date of Patent: June 4, 2013Assignee: Sandia CorporationInventors: Hongyou Fan, Huimeng Wu
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Publication number: 20130108810Abstract: A method of coating a surface, preparing a doped metal-ion precursor solution for coating, and an article including a component coated by the described method are disclosed. The method of coating includes applying a fluoro-silane doped metal-ion precursor solution on the surface to form a coated surface. The metal-ion precursor solution includes greater than about 0.6 molar percent concentration of a metal-ion precursor in a solvent comprising an alcohol. The method of preparing the doped metal-ion precursor solution includes dissolving a metal-ion precursor in a solvent comprising an alcohol at a temperature greater than about 100° C. and refluxing at a temperature greater than about 150° C. such that the concentration of metal-ion precursor in the solution is greater than 0.6 molar percent of the solution, and adding a fluoro-silane to the metal-ion precursor solution.Type: ApplicationFiled: October 27, 2011Publication date: May 2, 2013Applicant: GENERAL ELECTRIC COMPANYInventors: Kevin Paul McEvoy, Ambarish Jayant Kulkarni, James Anthony Ruud
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Publication number: 20130022756Abstract: The adhesion of metal thin films onto polymeric substrates can be significantly enhanced by contacting the surface of the polymeric substrate with a non-complexing solvent before or after depositing the metal film.Type: ApplicationFiled: July 19, 2012Publication date: January 24, 2013Inventors: BRIAN HOWARD AUGUSTINE, WILLIAM CHRISTOPHER HUGHES, ALAN KOON-KEE MO, THOMAS CARROLL DEVORE
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Publication number: 20130022761Abstract: The present invention relates to a silver complex obtained by reacting at least one silver compound represented by the formula 2 below with at least one ammonium carbamate compound or ammonium carbonate compound represented by the formula 3, 4 or 5 below:Type: ApplicationFiled: May 11, 2012Publication date: January 24, 2013Applicant: Inktec Co., Ltd.Inventors: Kwang-Choon Chung, Hyun-Nam Cho, Myoung-Seon Gong, Yi-Sup Han, Jeong-Bin Park, Dong-Hun Nam, Seong-Yong Uhm, Young-Kwan Seo
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Publication number: 20120304889Abstract: Low temperature processes for converting mixtures of metal inks into alloys. The alloys can be dealloyed by etching. A method comprising: depositing at least one precursor composition on at least one substrate to form at least one deposited structure, wherein the precursor composition comprises at least two metal complexes, including at least one first metal complex comprising at least one first metal and at least one second metal complex different from the first metal complex and comprising at least one second metal different from the first metal, treating the deposited structure so that the first metal and the second metal form elemental forms of the first metal and the second metal in a treated structure. Further, one can remove at least some of the first metal to leave a nanoporous material comprising at least the second metal. Precursor compositions can be formulated to be homogeneous compositions.Type: ApplicationFiled: May 4, 2012Publication date: December 6, 2012Inventors: Richard D. MCCULLOUGH, John BELOT, Rebecca POTASH
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Publication number: 20110165348Abstract: A method of coating a surface comprising providing a source of amorphous metal that contains manganese (1 to 3 atomic %), yttrium (0.1 to 10 atomic %), and silicon (0.3 to 3.1 atomic %) in the range of composition given in parentheses; and that contains the following elements in the specified range of composition given in parentheses: chromium (15 to 20 atomic %), molybdenum (2 to 15 atomic %), tungsten (1 to 3 atomic %), boron (5 to 16 atomic %), carbon (3 to 16 atomic %), and the balance iron; and applying said amorphous metal to the surface by a spray.Type: ApplicationFiled: February 14, 2011Publication date: July 7, 2011Applicant: Lawrence Livermore National Security, LLCInventors: Joseph C. Farmer, Frank M.G. Wong, Jeffery J. Haslam, Xiaoyan (Jane) Ji, Sumner D. Day, Craig A. Blue, John D.K. Rivard, Louis F. Aprigliano, Leslie K. Kohler, Robert Bayles, Edward J. Lemieux, Nancy Yang, John H. Perepezko, Larry Kaufman, Arthur Heuer, Enrique J. Lavernia
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Publication number: 20100304037Abstract: A gas turbine engine component has a metallic substrate. A coating is on the substrate. A barrier coat is applied while varying a speed of the component rotation so as to provide a corresponding microstructure to the barrier coat.Type: ApplicationFiled: June 1, 2009Publication date: December 2, 2010Applicant: UNITED TECHNOLOGIES CORPORATIONInventors: Benjamin J. Zimmerman, David A. Litton, John F. Blondin
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Patent number: 7780059Abstract: A method of forming a structure by a material additive process, the method comprising the steps: providing a substrate having a surface, providing an interlayer on the surface which conforms to the surface of the substrate, forming a melt pool in the interlayer, the depth of the melt pool being less than the depth of the interlayer, selectively depositing a material within the melt pool, allowing the material to solidify, and applying heat and pressure to diffusion bond the material to the substrate.Type: GrantFiled: August 10, 2007Date of Patent: August 24, 2010Assignee: Rolls-Royce plcInventor: Daniel Clark
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Publication number: 20100183866Abstract: The present invention provides a method for easily producing a particle-arranged structure. In the structure produced by the method, particles are regularly arranged. The method of the present invention comprises: preparing a dispersion comprising a solvent, a polymerizable compound dissolved in the solvent and particles insoluble and dispersed uniformly in the solvent; spin-coating the dispersion on a substrate so as to arrange the particles in the liquid phase of the dispersion; and then curing the polymerizable compound.Type: ApplicationFiled: January 14, 2010Publication date: July 22, 2010Inventors: Akira FUJIMOTO, Tsutomu Nakanishi, Shigeru Matake, Koji Asakawa
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Publication number: 20100104749Abstract: Substrates having nanostructures disposed thereon and methods of forming nanostructures on the substrates are disclosed.Type: ApplicationFiled: November 20, 2009Publication date: April 29, 2010Inventors: Yiping Zhao, Jianguo Fan
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Publication number: 20100062203Abstract: The optical storage medium, in particular a read-only optical disc, comprises a substrate layer, a read only data layer comprising a pit structure and being arranged on the substrate layer, a mask layer comprising nanoparticles for providing a super resolution near field effect, and a dielectric layer arranged between the data layer and the mask layer. The dielectric layer has a thickness, which changes in dependency of the pit structure and is for example a plastic layer having a completely flat surface for providing a uniform arrangement of the nanoparticles. For the manufacturing of a respective optical storage medium, the dielectric layer is arranged on the data layer advantageously by means of spin coating.Type: ApplicationFiled: January 21, 2008Publication date: March 11, 2010Applicant: THOMSON LICENSINGInventor: Joachim Knittel
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Patent number: 7635741Abstract: This invention is a monomer comprising at least two dienophile groups and at least two ring structures which ring structures are characterized by the presence of two conjugated carbon-to-carbon double bonds and the presence of a leaving group L, wherein L is characterized that when the ring structure reacts with a dienophile in the presence of heat or other energy sources, L is removed to form an aromatic ring structure. This invention is also curable oligomers and polymers and highly cross-linked polymers made with such monomers. Moreover, this invention is a method of making porous films by combining such monomers or their oligomers with a porogen, curing the polymer and removing the porogen.Type: GrantFiled: February 12, 2003Date of Patent: December 22, 2009Inventors: Q. Jason Niu, Robert E. Hefner, Jr., James P. Godschalx, James T. Pechacek, Kim E. Arndt
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Publication number: 20090202719Abstract: The present invention provides microwave attenuating, filled composite materials which contain a polymer or ceramic matrix and metallic tubules and processes for making the same and devices which contain such materials.Type: ApplicationFiled: March 13, 2009Publication date: August 13, 2009Applicants: Science Applications International Corporation, Department of the NavyInventors: Paul E. SCHOEN, Ronald R. Price, Joel M. Schnur, Daniel Zabetakis, Robert F. Brady, JR., Ann Mera, Dana Leamann, Bor-Sen Chiou, Walter J. Dressick
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Patent number: 7563623Abstract: It is an object of the present invention to provide a biosensor on which a large amount of protein can be immobilized and nonspecific adsorption is less likely to occur with the use of a SAM compound having high water solubility and good performance in terms of supply. The present invention provides a biosensor comprising a substrate on which a hydrophilic polymer having a reactive group capable of binding to a physiologically active substance is immobilized via a compound represented by the following formula (1), said compound at a concentration of 1 mM being dissolved in water at 25° C.: X-L-Y??(1) wherein X represents a group capable of binding to metal, L represents a linking group, and Y represents a functional group to which the hydrophilic polymer is bound.Type: GrantFiled: February 21, 2007Date of Patent: July 21, 2009Assignee: FUJIFILM CorporationInventors: Toshihide Ezoe, Taisei Nishimi, Yukou Saito
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Publication number: 20090169741Abstract: A method of forming a water vapor barrier layer to a core of a golf ball is provided. The method includes placing the core of the golf ball into a vapor barrier composition, withdrawing the lifting device, and spinning and optionally oscillating the core within the composition for a time sufficient for the composition to form a layer on the core. The present invention also provides an apparatus that can be used to form a water vapor barrier layer.Type: ApplicationFiled: February 4, 2009Publication date: July 2, 2009Inventors: Matthew F. Hogge, Christopher Cavallaro, Richard Foukes, Michael J. Sullivan, William E. Morgan, Kevin M. Harris
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Publication number: 20080268280Abstract: Disclosed herein is a method of preparing a low resistance metal line, in which a wet plating technique is used instead of a vacuum film forming process in order to simplify the process and decrease the manufacturing cost. In addition, a self-assembled monolayer is formed that facilitates the increased adsorption density and strength of the metal catalyst resulting in the formation of a high-density metal catalyst layer, thereby obtaining a high-quality metal line. Also disclosed herein, are a patterned metal line structure, and a display device using the same.Type: ApplicationFiled: January 23, 2008Publication date: October 30, 2008Applicant: SAMSUNG ELECTRONICS CO., LTD.Inventors: Sung Hen CHO, Ki Yong SONG, Sang Eun PARK
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Publication number: 20080175982Abstract: Methods and devices are provided for forming thin-films from solid group IIIA-based particles. In one embodiment, a method is provided for creating solid alloy particles. The method may include providing a first material containing at least one alloy comprising of: a) a group IIIA element, b) at least one group IB, IIIA, and/or VIA element different from the group IIIA element of a), and c) a group IA-based material. The group IA-based material may be included in an amount sufficient so that no liquid phase of the alloy is present in a temperature range between room temperature and a deposition temperature higher than room temperature, wherein the group IIIA element is otherwise liquid in that temperature range.Type: ApplicationFiled: June 12, 2007Publication date: July 24, 2008Inventors: Matthew R. Robinson, Chris Eberspacher, Jeroen K. J. Van Duren
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Patent number: 7378230Abstract: The present invention relates to a photoresist composition for an MMN (multi-micro nozzle) head coater, more particularly to a photoresist composition comprising a novolak resin with a molecular weight ranging from 2000 to 12,000, a diazide photoactive compound, an organic solvent, and a Si-based surfactant for use in liquid crystal display circuits. The photoresist composition for liquid crystal display circuits of the present invention solves the stain problem, which occurs in MMN head coaters used for large-scale substrate glass, and improves coating characteristics, so that it can be utilized industrially and is expected to significantly improve productivity.Type: GrantFiled: January 5, 2004Date of Patent: May 27, 2008Assignee: Samsung Electronics Co., Ltd.Inventors: Sung-Chul Kang, Jin-Ho Ju, You-Kyoung Lee, Dong-Ki Lee, Hyo-Youl Kim, Hoon Kang, Seung-Uk Lee, Byung-Uk Kim
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Publication number: 20080102201Abstract: Methods for producing nanoparticle thin films are disclosed. According to one of the methods, a nanoparticle thin film is produced by modifying the surface of nanoparticles to allow the nanoparticles to be charged, controlling an electrostatic attractive force between the charged nanoparticles and a substrate and a repulsive force between the individual nanoparticles by a variation in pH to control the number density of the nanoparticles arranged on the substrate.Type: ApplicationFiled: April 4, 2007Publication date: May 1, 2008Applicant: SAMSUNG ELECTRONICS CO., LTD.Inventors: Seong Jae CHOI, Jae Young CHOI, Eun Joo JANG, Bulliard Xavier, Yu Jin KANG, Wan Ki BAE, Kook Heon CHAR
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Patent number: 7332198Abstract: There is provided a plating apparatus and method which can control the temperature of a plating solution during plating more uniformly and easily form a uniform plated film on the to-be-plated surface of a workpiece, and which can simplify the device and decrease the footprint. The plating apparatus includes a plating bath having a double bath structure including an inner bath for holding a plating solution and carrying out plating, and an outer bath which surrounds the inner bath and is in fluid communication therewith. A heating device is disposed in the outer bath. The plating apparatus may further include means for circulating or stirring the plating solution in the plating bath.Type: GrantFiled: October 28, 2002Date of Patent: February 19, 2008Assignee: Ebara CorporationInventors: Xinming Wang, Kenichi Abe, Koji Mishima
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Patent number: 7029721Abstract: A method for applying a bond coat on a metal-based substrate is described. A slurry which contains braze material and a volatile component is deposited on the substrate. The slurry can also include bond coat material. Alternatively, the bond coat material can be applied afterward, in solid form or in the form of a second slurry. The slurry and bond coat are then dried and fused to the substrate. A repair technique using this slurry is also described, along with related compositions and articles.Type: GrantFiled: December 23, 2003Date of Patent: April 18, 2006Assignee: General Electric CompanyInventors: Wayne Charles Hasz, D Sangeeta
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Patent number: 6720084Abstract: A heat-resistant resin film having a metallic thin film accumulated thereon or an endless belt having a metallic thin film accumulated thereon having good mechanical characteristics is produced in a simple process. A metallic thin film is formed on an inner surface of a cylindrical substrate, and a layer of a heat-resistant resin is formed thereon. An accumulated body of the heat-resistant resin and the metallic thin film is peeled off from the substrate. The metallic thin film may be formed by electroplating, electroless plating or vapor deposition, or may also be formed by attaching a metallic foil having been prepared on an inner surface of the substrate. The heat-resistant resin layer is formed by injecting a polyamide acid solution in a rotational drum, and then formed by centrifugal forming by rotating the rotational drum on rollers under heating. After forming, imidization is conducted by heating and baking to form a film member of a thermosetting polyimide.Type: GrantFiled: May 30, 2001Date of Patent: April 13, 2004Assignee: Fuji Xerox Co., Ltd.Inventors: Ryuichiro Maeyama, Yasuhiro Uehara, Michiaki Yasuno, Makoto Omata
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Patent number: 6716488Abstract: A ferrite layer formation process that may be performed at a lower temperature than conventional ferrite formation processes. The formation process may produce highly anisotropic structures. A ferrite layer is deposited on a substrate while the substrate is exposed to a magnetic field. An intermediate layer may be positioned between the substrate and the ferrite to promote bonding of the ferrite to the substrate. The process may be performed at temperatures less than 300° C. Ferrite film anisotropy may be achieved by embodiments of the invention in the range of about 1000 dyn-cm/cm3 to about 2×106 dyn-cm/cm3.Type: GrantFiled: June 22, 2001Date of Patent: April 6, 2004Assignee: Agere Systems Inc.Inventors: Debra Anne Fleming, Gideon S. Grader, David Wilfred Johnson, Jr., John Thomson, Jr., Robert Bruce Van Dover
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Patent number: 6635317Abstract: A method for coating an interior surface of a metallic tube with a corrosion-resistant and/or an abrasion-resistant alloy. The method includes placing an alloy within a tube, enclosing the open ends of the tube with end caps, at least one of which is vented, heating the tube by applying current across the tube sufficient to heat the tube and melt the alloy, and spinning tube by the longitudinal axis of the tube to distribute the molten alloy along the interior surface of the tube using the centrifugal forces created by the spinning. An apparatus suitable for carrying out the above method is also disclosed.Type: GrantFiled: July 2, 2002Date of Patent: October 21, 2003Inventor: Kenneth Casner, Jr.
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Patent number: 6548685Abstract: The invention relates to a process for preparing niobium(V) alkoxides and tantalum(V) alkoxides, in particular niobium(V) ethoxide and tantalum(V) ethoxide, by reacting NbCl5 or TaCl5 with an appropriate alcohol in the presence of ammonia, wherein NbCl5 or TaCl5 is dissolved at a temperature of from about 0° C. to −50° C. in the alcohol containing from about 5 to about 7 mol of ammonia per mol of NbCl5 or TaCl5 to be reacted.Type: GrantFiled: March 15, 2002Date of Patent: April 15, 2003Assignee: H.C. Starck GmbHInventor: Friedrich Zell
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Patent number: 6548104Abstract: A physical vapor deposition apparatus and process are provided for providing a highly smooth shiny coating to a substrate. The apparatus includes a chamber with a fixture for mounting the components to be coated. The fixture is arranged such that the surfaces to be coated define a “dark side” that faces away from the source of ion bombardment. With this arrangement, heavier multiple ions will travel past the surface to be coated. Lighter single ions will be drawn more readily to the oppositely charged surface to be coated, and hence will undergo a non-linear travel path for deposition onto the component.Type: GrantFiled: March 12, 2001Date of Patent: April 15, 2003Inventor: Michael J. Pappas
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Patent number: 6506509Abstract: The present invention relates to composite electroless coatings with varying densities of codeposited particles in the plated layer along the surface of the substrate where said variation of densities is directed by the angle of rotation of the substrate during the coating process.Type: GrantFiled: August 5, 1999Date of Patent: January 14, 2003Assignee: Surface Technology, Inc.Inventors: Michael David Feldstein, Thomas Stephen Lancsek
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Patent number: 6419992Abstract: A zinc coating directly covers a bare ferrous base of parking meter housing parts. A non-epoxy thermosetting electrically insulating organic non-epoxy powder coating directly covers the zinc coating. The organic coating is directly applied to the zinc coating by electrostatically charging the powder and parts with opposite d.c. voltage polarities and by heating the powder so it adheres to and covers the zinc coating. Alternatively, the base is zinc, directly covered by the organic powder coating.Type: GrantFiled: June 14, 2000Date of Patent: July 16, 2002Inventor: Scott Jay Lewin
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Patent number: 6406740Abstract: Disclosed is a method of manufacturing a liquid jet recording head by which a thin film composed of an inorganic material can be formed by a conventionally used method such as a printing method and coating method executed in the atmosphere, the method being able to be relatively easily achieved, a head made by the manufacturing method, and a liquid jet recording apparatus including the head and a member for mounting the head. According to this invention, there is provided a liquid jet recording apparatus including a heat acting portion communicating with a liquid jetting orifice for applying thermal energy to a liquid to form a bubble, an electrothermal converter for generating the thermal energy, a heat generating resistance layer contained in the electrothermal converter, and electrode layers for imposing a voltage to the heat generating resistance layer contained in the electrothermal converter, wherein the heat generating resistance layer is composed mainly of an organic resinate.Type: GrantFiled: November 8, 1995Date of Patent: June 18, 2002Assignee: Canon Kabushiki KaishaInventor: Hirokazu Komuro
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Patent number: 6399201Abstract: A powder comprising a blowing agent powder core which is coated with at least one oil-like substance on its surface, and a process for producing a powder comprising a blowing agent powder core which is coated with at least one oil-like substance on its surface, comprising the following steps (a) and (b): (a) adding at least one oil-like substance in the form of a mist to a blowing agent powder; and (b) mixing the oil-like substance with the blowing agent powder under such mixing conditions that the blowing agent powder is less susceptible to pulverization.Type: GrantFiled: July 10, 1998Date of Patent: June 4, 2002Assignee: Otsuka Chemical Co., Ltd.Inventors: Tsukasa Maekawa, Toshinori Takao, Sadafumi Shono, Chiaki Yasumaru, Shigeru Sumitomo, Nobuyuki Ueda, Yoshifumi Tachi
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Publication number: 20020000383Abstract: The invention discloses a method of electroplating a material onto a semiconductor substrate. A substrate is placed in a cylindrical processing chamber enclosure. A nozzle for spraying a liquid electroplating solution opposes the top surface of the substrate. The electroplating solution flows through the nozzle and outward angularly from the tip of the nozzle, so that the solution flows rotationally on the surface of the substrate.Type: ApplicationFiled: December 30, 1998Publication date: January 3, 2002Inventor: KEVIN J. LEE
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Patent number: 6263586Abstract: A device and method for planarizing a film layer device on a silicon wafer. The device has a circular track whose surface faces the track center, a carrier capable of moving along the track and carrying wafers around with their front surfaces facing the center, and a set of heating elements for heating the film layers on the wafers to make them fluid. Utilizing the centrifugal force on the film layer generated by the circular movement and the fluidity of the film layer provided by heating, planarization of the film layer is achieved.Type: GrantFiled: July 9, 1999Date of Patent: July 24, 2001Assignee: Taiwan Semiconductor Manufacturing Co., Ltd.Inventor: Kung Linliu
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Patent number: 6255228Abstract: A method for removing contaminants from a semiconductor wafer having a spin on coating of material. Contaminants are removed by applying a cleaning solution to the periphery, and preferably, the exposed backside of the wafer after the edge bead has been dissolved and removed. The cleaning solution is formulated to react chemically with unwanted coating material residue to form a compound that may be ejected from the periphery of the spinning wafer. Any residual solution or precipitate that is not ejected from the wafer may be rinsed away with water, preferably deoinized water. One exemplary use of this method is the removal of metallic contaminants that may be left on the periphery and backside of a wafer after the formation of ferroelectric film coatings. A cleaning solution comprising a mixture of hydrochloric acid HCl and water H2O or ammonium hydroxide NH4OH and water H2O is applied to the periphery of the spinning wafer.Type: GrantFiled: May 30, 2000Date of Patent: July 3, 2001Assignee: Micron Technology, Inc.Inventor: J. Brett Rolfson
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Patent number: 6197437Abstract: A composite barrel for use in extrusion or injection molding is disclosed. The composite barrel includes an outer housing having a cylindrical bore that extends throughout the length of the outer housing. A wear-resistant lining is disposed on an interior surface that defines the cylindrical bore. The lining is fabricated from an alloy that includes a base metal and phosphorus and the lining may contain hard abrasion-resistant particulate, such as tungsten carbide. The base metal is nickel or cobalt or a mixture of nickel and cobalt. The alloy is typically applied by centrifugal casting and can be cast in a nitrogen-rich atmosphere without creating undesirable lining porosity. Such linings can be made for a fraction of the cost of comparable linings that must be cast under vacuum or in an atmosphere of argon.Type: GrantFiled: February 22, 1999Date of Patent: March 6, 2001Assignee: Wall Colmonoy CorporationInventors: David Martin Bielec, Samuel Conrad DuBois, Subramaniam Rangaswamy
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Patent number: 6123989Abstract: A spinning rotor (1) with a spinning cup (2) has an interior surface coated with a nickel dispersion layer (6) of an essentially even layer thickness having a concentration of hard material grains (7) embedded therein which is clearly less at the surface of the fiber slide face (9) than in the rotor groove. The coating is produced by bathing the spinning cup in a nickel dispersion bath during the final stage of which the concentration of the hard material grains in the bath is reduced at least in the bathing area, while the spinning cup is moved in this bath and rotated around its longitudinal axis while maintaining the spinning cup in a spatial orientation relative to the bath wherein an imaginary plane passing through the rotor groove is at least approximately perpendicular to the surface of the nickel dispersion bath.Type: GrantFiled: July 28, 1999Date of Patent: September 26, 2000Assignee: W. Schlafhorst AG & Co.Inventors: Gottfried Schurmann, Bert Schlomer, Harald Schneider
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Patent number: 6114254Abstract: A method for removing contaminants from a semiconductor wafer having a spin on coating of material. Contaminants are removed by applying a cleaning solution to the periphery, and preferably, the exposed backside of the wafer after the edge bead has been dissolved and removed. The cleaning solution is formulated to react chemically with unwanted coating material residue to form a compound that may be ejected from the periphery of the spinning wafer. Any residual solution or precipitate that is not ejected from the wafer may be rinsed away with water, preferably deionized water. One exemplary use of this method is the removal of metallic contaminants that may be left on the periphery and backside of a wafer after the formation of ferroelectric film coatings. A cleaning solution comprising a mixture of hydrochloric acid HCl and water H.sub.2 O or ammonium hydroxide NH.sub.4 OH and water H.sub.2 O is applied to the periphery of the spinning wafer.Type: GrantFiled: October 15, 1996Date of Patent: September 5, 2000Assignee: Micron Technology, Inc.Inventor: J. Brett Rolfson
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Patent number: 6040009Abstract: The present invention is to provide a low solvent content type-coating composition by which the resultant coatings with good scuff resistance or water resistance as well as good chipping resistance are produced, while the content of an organic solvent to be used can be much reduced. The low solvent content type-coating composition comprises a polyester oligomer having a hydroxyl group in an amount of 2.0 to 10.0 moles/Kg-resin, a number average molecular weight (Mn) of 300 to 1500, a weight average molecular weight (Mw) of 300 to 3000, and a ratio of a weight average molecular weight/a number average molecular weight (Mw/Mn) of 1 to 2.0, an amount of a modifying lactone being 31 to 85%, and an aliphatic hydrocarbon group of C4-22 which is not derived from lactones. The present invention is also to provide a process for coating a low solvent content type-coating composition on, for example, a base coating composition by a wet-on-wet coating.Type: GrantFiled: June 19, 1995Date of Patent: March 21, 2000Assignee: Mazda Motor CorporationInventors: Yoshiaki Marutani, Takashi Tomita, Tadamitsu Nakahama, Hiroyuki Uemura, Kazuhi Koga, Mika Ohsawa
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Patent number: 5985365Abstract: An automated method and apparatus for galvanizing threaded rods, comprising conveying threaded rods while horizontally oriented through a bath of molten zinc, then simultaneously spinning the threaded rods in horizontal orientation at sufficient rotational velocity to remove excess molten zinc therefrom by centrifugal force and conveying the threaded rods to a cooling bath. The automated apparatus then conveys the zinc coated threaded rods through a cooling bath to solidify the molten zinc coating and then collects cooled zinc coated threaded rods to permit efficient removal thereof from the apparatus. A rotary conveyor mechanism of the automated apparatus conveys the threaded rods through a molten zinc bath and removes excess molten zinc therefrom by rolling the coated threaded rods down an inclined zinc removal platform.Type: GrantFiled: October 16, 1998Date of Patent: November 16, 1999Assignee: Galvanizing Services Co., Inc.Inventor: W. David Jaye
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Patent number: 5738787Abstract: The present invention features a filtration plate for use in a filter pan comprising a corrugated sheet having a series of alternately upwardly and downwardly opening channels and a reinforcing material bonded to surfaces of the downwardly opening channels. The reinforcing material is effective for strengthening the sheet and retaining heat in a manner effective to slow cooling of the filtration plate during washing and to reduce heat losses from the filtration plate during filtering. According to a preferred aspect of the invention, the corrugated sheet is a monolithic sheet of structural metal having a smooth upper filtration surface. The invention also provides a filter pan configured for use in filtration of a filtrate from solid particles. The filter pan comprises a filtration plate including a corrugated, monolithic sheet of structural metal having a series of alternately upwardly and downwardly opening channels.Type: GrantFiled: October 30, 1995Date of Patent: April 14, 1998Assignee: IMC-Agrico CompanyInventors: John Alexander, William A. Marrone, Miguel A. DeJesus
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Patent number: 5728626Abstract: A method of planarizing a non-planar substrate, such as filling vias and contact holes, spreads a suspension of a conducting material suspended in a liquid on a substrate. The suspension includes an organometallic material, preferably with particles of a polymerized tin or indium alkoxide. The material is spread by spinning the substrate after applying the suspension. The carrier liquid and organic groups are removed by baking and curing at elevated temperatures, thereby depositing the conductive material on the substrate in a layer which is more planar than the substrate and which has regions of greater and lesser thickness. A relatively brief etch step removes conductive material from regions of lesser thickness, leaving material filling vias or contact holes.Type: GrantFiled: October 23, 1995Date of Patent: March 17, 1998Assignees: AT&T Global Information Solutions Company, Hyundai Electronics America, Symbios Logic Inc.Inventors: Derryl D. J. Allman, Steven S. Lee
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Patent number: 5723403Abstract: A production process for supported catalysts is described comprising:(a) preparing a coating suspension containing at least one refractory inorganic oxide and at least some of the elements intended to constitute catalytically active phase (A);(b) filling at least part of the open porosity of a support with this suspension;(c) drying the filled support by centrifuging;(d) a thermal treatment of the support to obtain a support coated by a wash coat;(e) optionally impregnating the coated support with a solution containing the rest of, or elements of, catalytically active phase (A); and(f) thermally activating the catalyst.This preparation process is of particular interest in the production of catalysts for treating exhaust gases of internal combustion engines, where the wash coat deposited on a support comprises in particular a refractory inorganic oxide, iron oxide and cerium oxide and, by way of a catalytically active element, at least one noble metal such as platinum, rhodium or palladium.Type: GrantFiled: July 29, 1994Date of Patent: March 3, 1998Assignee: Institut Francais Du PetroleInventors: Daniel Durand, Gil Mabilon, Isabelle Guibard
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Patent number: 5702763Abstract: A process for the selective variation in density of particulate matter codeposited within metallic matrices deposited onto articles utilizing increased levels of rotation of said articles during plating cycle to attain said selective codeposition density. The attainment of varying densities of codeposited particulate matter in the plated layer along the surface of the substrate is particularly useful in cost reduction and improved product performance.Type: GrantFiled: February 15, 1995Date of Patent: December 30, 1997Assignee: Surface Technology, Inc.Inventor: Nathan Feldstein
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Patent number: 5550063Abstract: Method for producing an optical assay device having a substrate and one or more optical layers, an attachment layer and a receptive layer, including the step of spin coating an anti-reflective layer or an attachment layer.Type: GrantFiled: June 10, 1993Date of Patent: August 27, 1996Assignee: Biostar, Inc.Inventor: Gregory R. Bogart