Deforming The Base Or Coating Or Removing A Portion Of The Coating Patents (Class 427/264)
  • Patent number: 5643654
    Abstract: A pellicle structure comprises a frame having a vertical through opening and a pellicle film spread on the upper the upper end of the opening of the frame. The pellicle film has a coating layer comprising a coating agent formed at least on the inner surface thereof, and a bonding portion for bonding the end edge of the frame to the peripheral edge of the pellicle film through an adhesive layer. The coating agent, in the bonding portion, is dissolved or dispersed in the adhesive so that the pellicle substrate is directly contacted by and bonded to the adhesive.
    Type: Grant
    Filed: November 27, 1991
    Date of Patent: July 1, 1997
    Assignee: Mitsui Petrochemical Industries, Ltd.
    Inventors: Minoru Fujita, Hiroaki Nakagawa, Tsutomu Saito
  • Patent number: 5639509
    Abstract: A flux enhanced data transducer and method for producing the same in conjunction with shared shields on MR read heads in which substantially between 500-2500 .ANG. of a relatively higher magnetic moment material is added to the upper surface of the shared shield, or bottom write head pole, prior to a magnetic flux containment ion milling operation utilizing the upper pole as a mask. The relatively higher magnetic moment flux enhancement layer may comprise CoNiFe, FeN or similar material which is deposited prior to the formation of the dielectric gap layer. The flux enhancement layer may then be selectively removed substantially surrounding the upper pole by means of a relatively brief ion milling process in which only on the order of 1.0 k.ANG. of the layer need be removed and during which only an insignificant amount of the material removed might be re-deposited on the sides of the upper pole.
    Type: Grant
    Filed: July 22, 1996
    Date of Patent: June 17, 1997
    Assignee: Quantum Peripherals Colorado, Inc.
    Inventor: Terence D. Schemmel
  • Patent number: 5609914
    Abstract: A method for preparing high resolution wash-off polyimide images is described having the sequential steps of (a) providing a non-photosensitive layer containing a substantially non-crystalline poly(amic acid) polymer or salt thereof on a substrate; (b) applying an aqueous ink imagewise to the non-photosensitive layer to change the solubility in the ink-applied areas, the aqueous ink containing a solubility altering agent; (c) washing the non-photosensitive layer with an aqueous solution to remove the soluble areas; and (d) converting the poly(amic acid) polymer to a polyimide.
    Type: Grant
    Filed: May 2, 1995
    Date of Patent: March 11, 1997
    Assignee: E.I. Du Pont de Nemours and Company
    Inventors: Sheau-Hwa Ma, Walter R. Hertler, Howard E. Simmons, III
  • Patent number: 5607733
    Abstract: A process for preparing an X-ray mask structure comprises an X-ray transmissive film, an X-ray absorptive member held on the X-ray transmissive film and supporting frame for supporting the X-ray transmissive film. The X-ray absorptive member is constituted of crystalline grains having a grain boundary size of 1 .mu.m or larger, or has a density of 90% or more relative to the density of the bulk material.
    Type: Grant
    Filed: June 7, 1995
    Date of Patent: March 4, 1997
    Assignee: Canon Kabushiki Kaisha
    Inventors: Yasuaki Fukuda, Shigeyuki Matsumoto
  • Patent number: 5607534
    Abstract: A method of recycling a support material for supporting images thereon, at least part of the support material including a paper layer which contains cellulose fibers as the main component and bears thereon hydrophobic images having a coloring agent and a heat softening or thermofusible material, includes the steps of causing the support material to hold a water-containing image peeling liquid thereon; bringing an image peeling member into contact with the hydrophobic images while the image peeling liquid is held on the support material; and peeling the hydrophobic images off the paper layer, with the image peeling liquid being held in an amount of 1.0 g or more per A4-size paper layer, or with the rate of the penetration of the image peeling liquid into the paper layer of the support material being set at 12 ml/m.sup.2 or more for a contact time of 0.
    Type: Grant
    Filed: August 22, 1994
    Date of Patent: March 4, 1997
    Assignee: Ricoh Company, Ltd.
    Inventors: Toshiyuki Kawanishi, Masato Igarashi, Eiichi Kawamura, Tadashi Saitoh, Kiyoshi Tanikawa, Kakuji Murakami
  • Patent number: 5599580
    Abstract: A magnetic recording medium is constructed with a substrate made of glass, one or two underlayers, and a magnetic film. In order that the easy magnetization axis of the magnetic film is parallel to the magnetic film, an underlayer having an NaCl crystallographic structure is superposed on the substrate. A magnetic film made of a Co based alloy having a hexagonal close packed crystallographic structure is formed on this underlayer, putting an underlayer made of a material having a body centered cubic crystallographic structure therebetween at need. Magnetic anisotropy of the magnetic film is increased by forming grooves in a predetermined direction in a surface portion of the substrate. These grooves play a role also for defining the orientation of the underlayer made of the material having an NaCl crystallographic structure.
    Type: Grant
    Filed: April 10, 1996
    Date of Patent: February 4, 1997
    Assignee: Hitachi, Ltd.
    Inventors: Masaaki Futamoto, Atsushi Nakamura, Nobuyuki Inaba, Yoshiyuki Hirayama, Yoshibumi Matsuda, Mikio Suzuki, Yukio Honda
  • Patent number: 5599592
    Abstract: A positive metallization process for metallizing a plastic composite piece containing a polymer and grains of one or more oxides, includes three successive steps. The first step consists of irradiating the plastic piece surface to be metallized with a light beam emitted by an excimer laser. The second step consists of immersing the irradiated piece into at least one autocatalytic bath containing metal ions and without palladium. This immersion induces the deposit of the metal ions onto the irradiated surface to form a metal film onto the surface. The third step consists of thermally processing the metallized plastic piece to induce the diffusion of the deposited metal into the plastic piece.
    Type: Grant
    Filed: September 29, 1995
    Date of Patent: February 4, 1997
    Inventor: Lucien D. Laude
  • Patent number: 5597620
    Abstract: A semi-finished wood simulating product and method is disclosed. The product is manufactured by providing a substrate having at least one surface to be finished. A liquid basecoat is applied on the substrate and dried. A wood grain pattern is deposited, in liquid form, on the basecoat. Some of the pattern is transferred from the originally deposited position on the basecoat to a subsequent position. The pattern is then cured. A polymerizable protective coating is applied onto the substrate overlying the basecoat and the pattern. The protective coating seals the substrate and-is adapted for accepting a colorant to be applied by an end user. The protective coating is then polymerized. Additionally, if a porous substrate is provided, a sealer is applied prior to the liquid basecoat and is then cured.
    Type: Grant
    Filed: May 24, 1995
    Date of Patent: January 28, 1997
    Assignee: Premdor, Inc.
    Inventor: Ralph A. Martino
  • Patent number: 5595790
    Abstract: An effective non-specular reflector, for use in a Liquid Crystal Display, is formed by first coating a substrate with a two component solution. One component hardens when heated or when exposed to ultraviolet light (optionally through a mask) while the other component remains liquid. The result is a solid layer in which are dispersed multiple liquid regions, some of which break the surface where they are easily removed, leaving behind a roughened surface. Once a high reflectance metal has been deposited onto this surface it becomes an effective nonspecular reflector. Examples of materials for use as the two components are given.
    Type: Grant
    Filed: June 21, 1996
    Date of Patent: January 21, 1997
    Assignee: Industrial Technology Research Institute
    Inventor: Chung-Kuang Wei
  • Patent number: 5593937
    Abstract: An image-bearing member for supporting thereon images formed by a thermofusible or heat-softening ink containing a dye coloring component, at least part of the image-bearing member having a paper layer which contains cellulose fibers and a discoloring agent capable of discoloring the dye coloring component of the thermofusible or heat-softening ink. In addition, a method for recycling the above-mentioned image-bearing member is also disclosed.
    Type: Grant
    Filed: July 22, 1994
    Date of Patent: January 14, 1997
    Assignee: Ricoh Company, Ltd.
    Inventors: Tadashi Saito, Kiyoshi Tanikawa, Eiichi Kawamura, Toshiyuki Kawanishi
  • Patent number: 5593739
    Abstract: A method for patterned metallization of substrate surfaces, especially circuit boards, even three-dimensional ones, by using electromagnetic UV radiation, particularly from an excimer laser. In the method a primer layer is applied to the full substrate surface in the area of a metal layer that is subsequently applied; insulating channels then are made in the primer layer by complete removal of the primer in certain areas by the action of electromagnetic radiation in the UV range; and afterward the remaining patterned primer layer is provided with the metal layer to form conductor strips. The method makes it possible to create insulating channels with extremely sharp contours in the primer layer on the surface of even three-dimensional, electronic circuit media.
    Type: Grant
    Filed: February 14, 1996
    Date of Patent: January 14, 1997
    Assignee: LPKF CAD/CAM Systeme GmbH
    Inventor: Joerg Kickelhain
  • Patent number: 5589270
    Abstract: Electrification is suppressed with a water-soluble electrification-suppressing film having an electron conductivity and comprising a polymer resin. A high electrification-suppressing effect which is also high in vacuum can be easily obtained by using the electrification-suppressing film with less contamination.
    Type: Grant
    Filed: June 1, 1995
    Date of Patent: December 31, 1996
    Assignees: Hitachi, Ltd., Showa Denko K.K.
    Inventors: Fumio Murai, Yasunori Suzuki, Hideki Tomozawa, Ryuma Takashi, Yoshihiro Saida, Yoshiaki Ikenoue
  • Patent number: 5580615
    Abstract: A method of forming a conductive film on an insulating region of a substrate wherein a surface of the insulating region formed on the substrate is activated by irradiating the surface with electrons, ions or light. Next, a metal film pattern constituting, for example, an electrical interconnection, is deposited on the surface by applying a selective chemical vapor deposition process using a metal halide gas.
    Type: Grant
    Filed: April 7, 1994
    Date of Patent: December 3, 1996
    Assignee: Kabushiki Kaisha Toshiba
    Inventors: Hitoshi Itoh, Takahiko Moriya
  • Patent number: 5580604
    Abstract: A method of manufacturing a hot-stamped decal includes step A: preparing a metalized polyester film including a metalized layer disposed on a top surface thereof, a clear polyester sheet disposed to an under side of the metalized layer, an adhesive layer disposed to an under side of the clear polyester sheet and a release sheet disposed to an under side of the adhesive layer, step B: applying a printing process on the metalized layer to form a mark thereon composed of a printed ink layer, step C: preparing an alkaline corrosive solution, step D: flushing the top surface of the metalized layer with the alkaline solution composed of water and NaOH to the top surface of the metalized layer to corrode the metalized layer not covered by the printing ink layer, step E: flushing the top surface of the metalized layer with water and step F: drying the hot-stamped decal.
    Type: Grant
    Filed: March 6, 1995
    Date of Patent: December 3, 1996
    Inventor: Chih C. Chang
  • Patent number: 5573815
    Abstract: Polymeric ledges on a metal stencil screen are made using a polymeric layer which is partially removed by a developer solution.
    Type: Grant
    Filed: May 30, 1995
    Date of Patent: November 12, 1996
    Assignee: E. I. Du Pont de Nemours and Company
    Inventors: Allan Cairncross, Chester A. Thayer, II
  • Patent number: 5549928
    Abstract: A process for making an absorbent structure having a capillary substrate and regions of osmotic absorbent on the capillary substrate. The osmotic absorbent is cured from a liquid precursor applied to the capillary substrate. The capillary substrate has regions of topographically different elevations, taken normal to the plane of the capillary substrate. The capillary substrate is passed through a gap between a transfer roll and an anvil roll in a printing apparatus. The transfer roll has at liquid precursor on its periphery. The liquid precursor is applied to only the topographically elevated regions of the capillary substrate which contact the periphery of the transfer roll. By changing the topography of the capillary substrate, the liquid precursor can be applied to the capillary substrate in different pattern, without changing the transfer roll.
    Type: Grant
    Filed: May 15, 1995
    Date of Patent: August 27, 1996
    Assignee: The Procter & Gamble Company
    Inventors: Paul D. Trokhan, Dean V. Phan
  • Patent number: 5545220
    Abstract: A method for forming an open cell texturized surface in a silicone elastomer layer of a breast implant, or other medical implant, is created by forming a layer of uncured silicone elastomer, applying a coating of particles to the surface thereof, and curing the layer by heating it at an elevated temperature which also volatilizes the particles such that their constituent gases boil through the surface of the layer and create the texturing.
    Type: Grant
    Filed: November 4, 1993
    Date of Patent: August 13, 1996
    Assignee: Lipomatrix Incorporated
    Inventors: Winston A. Andrews, David Nelson, Richard W. Novy
  • Patent number: 5538753
    Abstract: A security element for the authentication of a substrate has a pattern comprising optical diffraction elements which are embossed in a carrier material of plastic material and unembossed neutral areas. On the embossing side of the carrier material a reflecting layer covers only surfaces with relief structures of the diffraction elements while the neutral areas which lie therebetween are free of the reflecting layer and are therefore non-reflecting. If the security element is stuck in the form of a stamp onto the substrate and the carrier metal is transparent, image portions, which are covered by the stamp, of a feature on the substrate can be discerned through the neutral areas.
    Type: Grant
    Filed: June 2, 1995
    Date of Patent: July 23, 1996
    Assignee: Landis & Gyr Betriebs AG
    Inventors: Gregor Antes, Walter Trachslin
  • Patent number: 5536530
    Abstract: A product having a textured surface thereon (and its process of manufacture) is disclosed wherein the textured surface is obtained by relieving the stress in pre-stressed polymeric chips that have been distributed as a single layer throughout a polymeric layer superimposed on a substrate.
    Type: Grant
    Filed: June 5, 1995
    Date of Patent: July 16, 1996
    Assignee: Armstrong World Industries, Inc.
    Inventors: Cheryl W. Landers, Ralph W. Wright, Jr.
  • Patent number: 5529812
    Abstract: The present invention concerns a method of manufacturing decorative board meeting exceptionally high standard concerning abrasion resistance, scratch resistance and impact resistance and which for this pruposes is varnished, electron-beam cured to 60-9.5%, is subjected to a pressing treatment and finally it is electron-beam cured to 100% to provide the disired abrasion resistance, gloss, and surface finish.
    Type: Grant
    Filed: February 21, 1995
    Date of Patent: June 25, 1996
    Inventor: Djorn Keding
  • Patent number: 5523125
    Abstract: A process for providing indicia to the surface of an article. The process comprising the steps of: providing an article having material initially forming at least a portion of its exterior surface; coating at least part of the material whereat indicia is to be provided to thereby form a film; contacting, with radiation from a radiation beam, indicia areas of the film intended to be provided with indicia, the radiation thereby removing the film and modifying the surface of the material of the indicia areas and also forming a mask in the non-indicia areas of the film; applying an ink to the indicia areas thereby forming the indicia on the surface; drying the ink; and removing the film.
    Type: Grant
    Filed: July 25, 1995
    Date of Patent: June 4, 1996
    Assignee: Lisco, Inc.
    Inventors: Thomas J. Kennedy, Mark L. Binette, Michael Konieczny
  • Patent number: 5512328
    Abstract: In forming a thin film pattern, first a seed material film is formed on a substrate and then exposed using electron beam lithography, for example, in the shape of the pattern. The latent image is then removed and an oriented material is deposited on one of the seed material and the substrtate, which have different hydrophilicity properties, to form the pattern. The oriented film is formed by an LB film forming method, in one example, and in another example the LB film material is a cresol novolak resin having a proportion of p-cresol novolak to m-cresol novolak of at least 20%.
    Type: Grant
    Filed: July 28, 1993
    Date of Patent: April 30, 1996
    Assignee: Hitachi, Ltd.
    Inventors: Toshiyuki Yoshimura, Naoko Miura, Shinji Okazaki, Minoru Toriumi, Hiroshi Shiraishi
  • Patent number: 5510156
    Abstract: A method for forming sub-micron sized bumps on the bottom surface of a suspended microstructure or the top surface of the underlying layer in order to reduce contact area and sticking between the two layers without the need for sub-micron standard photolithography capabilities and the thus-formed microstructure. The process involves the deposition of latex spheres on the sacrificial layer which will later temporarily support the microstructure, shrinking the spheres, depositing aluminum over the spheres, dissolving the spheres to leave openings in the metal layer, etching the sacrificial layer through the openings, removing the remaining metal and depositing the microstructure material over the now textured top surface of the sacrificial layer.
    Type: Grant
    Filed: August 23, 1994
    Date of Patent: April 23, 1996
    Assignee: Analog Devices, Inc.
    Inventor: Yang Zhao
  • Patent number: 5476690
    Abstract: Disclosed is a process for preparing a printed circuit board, which comprises the steps of:(1) forming, on the surface of an insulating substrate on a necessitate portion of which electrolessly plated copper is to be precipitated, a layer of a light-sensitive resin composition comprising (a) 40 to 80 parts by weight of a vinyl-polymerized high molecular weight binder having an acid value of 10 to 46 mgKOH/g, (b) 20 to 60 parts by weight of a compound having at least two polymerizable unsaturated double bonds in a molecule, with the total amount of Components (a) and (b) being 100 parts by weight, and (c) a photopolymerization initiator generating free radicals by irradiation of active light in an amount of 0.
    Type: Grant
    Filed: June 3, 1994
    Date of Patent: December 19, 1995
    Assignee: Hitachi Chemical Co., Ltd.
    Inventors: Fumihiko Ohta, Takeshi Nojiri, Shinji Tsuchikawa, Akio Nakano, Toshiaki Ishimaru, Hiroshi Yamazaki, Haruo Akahoshi, Mineo Kawamoto, Akio Takahashi
  • Patent number: 5476830
    Abstract: A latent image printing method and apparatus uses a substrate with one main surface having a covering comprising one of a first pair of a color developer and color former dye defining a background color in conjunction with the one main surface, wherein the color developer and the color former dye react when mixed to produce a first spectral response which is visible relative to the background color and a continuous coating over the covering which is non-porous with respect to the other of the pair and solvent-resistant to the other of the pair. The coating above selected portions of the covering corresponding to a desired latent image is removed.
    Type: Grant
    Filed: August 10, 1994
    Date of Patent: December 19, 1995
    Assignee: NOCOPI International, Inc.
    Inventor: Arshavir Gundjian
  • Patent number: 5474796
    Abstract: The invention provides apparatus and methods for making arrays of functionalized binding sites on a support surface. The invention further provides apparatus and methods for sequencing oligonucleotides and for identifying the amino acid sequence of peptides that bind to biologically active macromolecules, by specifically binding biologically active macromolecules to arrays of peptides or peptide mimetics.
    Type: Grant
    Filed: May 27, 1993
    Date of Patent: December 12, 1995
    Assignee: ProtoGene Laboratories, Inc.
    Inventor: Thomas M. Brennan
  • Patent number: 5474627
    Abstract: The present invention provides a method and a machine for marking an electric cable that comprises a conductive core, an insulating coating, and a varnish comprising an outer layer and an inner layer of contrasting colors, with the marking being performed by ablating the outer layer of said varnish with a laser, the outer layer of varnish being based on polytetrafluoroethylene and being 10 .mu.m to 20 .mu.m thick. According to the invention the machine comprises:a pulsed CO.sub.2 laser (2) whose power is adjusted to obtain an energy density lying in the range 8 J/cm.sup.2 to 15 J/cm.sup.2 at the outer layer of the cable varnish;drive means (9) for driving the cable (4) so as to cause it to run past the laser beam (5);guide means (13, 14, 15) for guiding the cable (4) in the vicinity of the point of impact of said beam (5) on the cable; andcomputerized control means (6).
    Type: Grant
    Filed: February 15, 1995
    Date of Patent: December 12, 1995
    Assignee: Aerospatiale Societe Nationale Industrielle
    Inventors: Pierre Carriere, Vincent Dabadie, Philippe Record, Jean-Luc Ballenghien
  • Patent number: 5470609
    Abstract: A process for repairing surface defects in plastic articles, especially plastic articles formed from fiber reinforced thermosetting resins, includes the steps of applying a powder coating composition to a defective area on the surface of a plastic article, curing the applied powder coating composition through the application of heat, and removing excess cured powder coating composition from the area of the defect to conform the area of the defect to the proper contours of the plastic article. The process can be utilized for repairing surface defects such as porosity, scratches, gouges and sand-through areas of cured thermoset substrates such as automotive body panels formed from sheet or bulk molding compounds.
    Type: Grant
    Filed: December 7, 1992
    Date of Patent: November 28, 1995
    Assignee: GenCorp Inc.
    Inventors: Burr L. Leach, David Hawkins
  • Patent number: 5466653
    Abstract: A method for preparing high resolution, negative-working, wash-off relief images, preferably using ink jet printing, comprising the sequential steps of: (a) providing a non-photosensitive layer comprising an acid-containing polymer; (b) applying an ink imagewise to the non-photosensitive layer to produce image areas and unimaged areas, said ink comprising an esterification agent which is capable of reacting with the acid groups in the polymer to form water-insoluble ester groups; (c) drying the non-photosensitive layer to induce or accelerate the esterification reaction between the acid groups and the esterification agent in the imaged areas; and (d) washing the non-photosensitive layer with an aqueous developer solution to remove the unimaged areas of the non-photosensitive layer is described.
    Type: Grant
    Filed: June 29, 1994
    Date of Patent: November 14, 1995
    Assignee: E. I. Du Pont de Nemours and Company
    Inventors: Sheau-Hwa Ma, Michael W. J. West
  • Patent number: 5464662
    Abstract: A fabrication method of a printed wiring board in which the halation effect of light irradiated to a solder resist film is utilized in a process of selectively removing the solder resist film. After a conductive layer is patterned to a given circuit pattern including soldering pads, the solder resist film is formed on the base material to cover the patterned conductive layer. The solder resist film is selectively exposed to light utilizing reflection of the irradiated light from the insulating base material and developed so that the solder resist film is selectively left in areas adjacent to the respective soldering pads. Then, an etching resist film is formed to cover the patterned conductive layer except for the soldering pads, and surface areas of the respective soldering pads are selectively etched using the etching resist film as a mask to produce solder resist dams made of the solder resist film left on the base material. Solder films are formed on the respective soldering pads thus selectively etched.
    Type: Grant
    Filed: September 2, 1994
    Date of Patent: November 7, 1995
    Assignee: NEC Corporation
    Inventors: Tomoo Murakami, Takanori Tsunoda
  • Patent number: 5460767
    Abstract: A method is provided for processing an electronic circuit assembly having surface mount integrated circuit packages mounted to its substrate, in which ingress of a conformal coating into a void present between the IC package and the substrate is prevented by a masking composition which forms a barrier around the IC package prior to the conformal coating process. The masking compositions are hot melt materials, in that each is initially a solid at roughly room temperature, melts to become a liquid at an elevated temperature at which the masking composition is applied to the electronic assembly, and forms a solid upon cooling to a temperature corresponding to a service temperature of the electronic assembly. As such, the masking compositions can be rapidly applied through various highly controllable techniques, and will quickly and sufficiently solidify upon cooling to allow handling of the electronic assembly.
    Type: Grant
    Filed: May 31, 1994
    Date of Patent: October 24, 1995
    Assignee: Delco Electronics Corporation
    Inventors: Henry M. Sanftleben, James M. Rosson
  • Patent number: 5460859
    Abstract: A method and system is disclosed in which an article, having large open areas or a multiplicity of apertures, is dip coated. The method and system is particularly adapted for use in coating a grid of a corona charging device utilized in the xerographic process. A transport system immerses and removes the article from a tank storing coating material. An unwanted coating material is created across the apertures of the article. Thereafter, the transport system moves the article past an ultrasonic wave source. The impact of the ultrasonic energy transmitted to the unwanted coating material across the apertures causes the removal thereof. The removed coating material is returned to the coating material in which the article was immersed.
    Type: Grant
    Filed: March 23, 1992
    Date of Patent: October 24, 1995
    Assignee: Xerox Corporation
    Inventor: Louis Reale
  • Patent number: 5458908
    Abstract: A magnetoresistive (MR) read transducer assembly having passive end regions separated by a central active region, and a method of fabricating it. Layers of a first biasing material and a nonmagnetic decoupling spacer material are deposited on a substrate, then covered by a mask only in the central region. By etching or ion milling, those parts of the layers not covered by the mask are removed to define a transverse biasing means in the central region and define the passive end regions. With the same mask remaining in place, a conductive material and exchange layer comprising a second biasing material are deposited over all regions. The mask is removed to define and provide conductor leads and longitudinal biasing means only in the end regions. MR material is thereafter deposited as a continuous thin film in direct contact with the central region containing the transverse biasing means and in direct contact with the end regions containing the longitudinal biasing means.
    Type: Grant
    Filed: September 21, 1994
    Date of Patent: October 17, 1995
    Assignee: International Business Machines Corporation
    Inventors: Mohamad T. Krounbi, Kenneth T. Kung, Ching H. Tsang
  • Patent number: 5451433
    Abstract: A method for producing polymeric diacetylene thin films having desirable nonlinear optical characteristics has been achieved by producing amorphous diacetylene polymeric films by simultaneous polymerization of diacetylene monomers in solution and deposition of polymerized diacetylenes on to the surface of a transparent substrate through which ultraviolet light has been transmitted. These amorphous polydiacetylene films produced by photo-deposition from solution possess very high optical quality and exhibit large third-order nonlinear optical susceptibilities, such properties being suitable for nonlinear optical devices such as waveguides and integrated optics.
    Type: Grant
    Filed: November 18, 1994
    Date of Patent: September 19, 1995
    Assignee: The United States of America as represented by the National Aeronautics and Space Administration
    Inventors: Donald O. Frazier, Samuel P. McManus, Mark S. Paley, David N. Donovan
  • Patent number: 5437893
    Abstract: Electrification is suppressed with a water-soluble electrification-suppressing film having an electron conductivity and comprising a polymer resin. A high electrification-suppressing effect which is also high in vacuum can be easily obtained by using the electrification-suppressing film with less contamination.
    Type: Grant
    Filed: April 26, 1993
    Date of Patent: August 1, 1995
    Assignees: Hitachi, Ltd, Showa Denko K. K.
    Inventors: Fumio Murai, Yasunori Suzuki, Hideki Tomozawa, Ryuma Takashi, Yoshihiro Saida, Yoshiaki Ikenoue
  • Patent number: 5436034
    Abstract: Electrolessly deposited metal films having improved adhesion can be obtained by coating the surface of the substrates to be metallized with a formulation consisting of UV-curable varnishes which contain noble metal compounds as activators and, in addition, either fillers or solvents or a combination of fillers and solvents, curing these varnishes by means of UV radiation, followed by electroless metallization of the substrates thus treated.
    Type: Grant
    Filed: December 19, 1994
    Date of Patent: July 25, 1995
    Assignee: Bayer Aktiengesellschaft
    Inventors: Henning Giesecke, Gerhard-Dieter Wolf, Wilfried Haese
  • Patent number: 5436027
    Abstract: A method and apparatus for applying a coating design to selected portions of a surface (13) of a structure (14) including the steps of applying a maskant (18) to the surface (13), positioning a plurality of sensors (20) on the structure (14) around the surface (13), positioning a laser (22) at a distance from the surface (13), directing a laser beam (32) from the laser (22) to each of the sensors (20) as input to the sensors, and using output from the sensors (20) based on the input to determine the position of the laser (22) relative to the surface (13), scanning the perimeter of the selected portions (36) with a laser beam (34), including using the determined relative positions of the laser and the surface to guide the laser beam, to cut into the maskant (18) around the perimeter, peeling the maskant (18) away from the selected portions (36), and applying the coating to the selected portions.
    Type: Grant
    Filed: December 23, 1993
    Date of Patent: July 25, 1995
    Assignee: The Boeing Company
    Inventor: Brad W. Offer
  • Patent number: 5427819
    Abstract: A repair and rehabilitation treatment process for reinforced concrete structures involves the removal of concrete from above rebar or other metal reinforcement material in the concrete structure. After removal of concrete, the metal reinforcement materials are saturated with corrosion inhibiting agents. Saturation is best achieved by multiple spray applications of the corrosion inhibitor. The cavity in the concrete structure with the treated rebar or other metal reinforcement materials is then backfilled and/or overlaid with repair concrete. Preferably, the repair concrete includes corrosion inhibitors which will diffuse to the rebar over time or is a low permeability concrete that reduces the rate of diffusion of chloride corrosion causing agents to the rebar. The repair and rehabilitation process significantly increases the concrete structure's service life.
    Type: Grant
    Filed: May 13, 1994
    Date of Patent: June 27, 1995
    Assignee: Virginia Tech Intellectual Properties, Inc.
    Inventors: Richard E. Weyers, Brian D. Prowell
  • Patent number: 5425848
    Abstract: A description is given of a method and a device (1) for providing (replicating) a patterned resyntetic resin relief (37) on the surface (25) of a glass substrate (27). For this purpose, a UV-curable acrylate lacquer (33) is applied to the surface (25), after which a transparent mould (3) having a relief (13) is rolled-off over the surface (25). By means of a UV light source (17) and an elliptic mirror (21), the lacquer is cured at the location of the focal line (23), thereby forming said relief (37). The relief (13) of the mould (3) is replicated on the glass substrate (27). The method described enables a relief of small dimensions (10.times.10 .mu.m) to be seamlessly provided on a large fiat surface (1.times.1 m), without being hindered by large release forces.
    Type: Grant
    Filed: March 15, 1994
    Date of Patent: June 20, 1995
    Assignee: U.S. Philips Corporation
    Inventors: Jan Haisma, Martinus Verheijen, Johannes T. Schrama
  • Patent number: 5424102
    Abstract: An optical recording medium comprises a substrate, a recording layer overlying the substrate in a manner such that it is not present at the inner and outer peripheral portions of the substrate, a metal reflective layer overlying the recording layer in a manner such that the inner periphery of the metal reflective layer is coterminous with that of the recording layer while the outer peripheral portion of the reflective layer extends over the outer periphery of the recording layer, and a protective layer wholly covering the metal reflective layer extending over the recording layer, both at the inner and outer peripheral portions. The optical recording medium exhibits an excellent adhesion strength of the protective layer even when stood under high humidity and high temperature conditions for a long period of time, and the protective layer is not peeled off when subjected to a tape peeling test.
    Type: Grant
    Filed: January 3, 1994
    Date of Patent: June 13, 1995
    Assignee: Mitsui Toatsu Chemicals, Inc.
    Inventors: Tadahiko Mizukuki, Kouichi Yabuuchi, Shinichi Murakami, Tomoyoshi Sasakawa, Kouhei Shizuka, Nobuhisa Kitagawa, Sumio Hirose
  • Patent number: 5413814
    Abstract: Articles, such as plastic parts, having the appearance of a naturally-occurring material such as wood or leather are formed by the techniques of (1) providing a plurality of grooves in a surface of the article, (2) applying a surfactant to the surface of the article, and (3) applying one or more color solutions to the surface of the article. The article may be a solid substrate, a part or a film. A topcoat is preferably applied to the surface of the article. The techniques include controlling movement of an applicator implement for applying the surfactant and color solutions to the surface of the substrate, and controlling movement of a saturator tool for modifying and synthesizing the surfactant and color solutions on the surface of the part and permeating the surfactant and color solutions into the plurality of grooves.
    Type: Grant
    Filed: March 15, 1994
    Date of Patent: May 9, 1995
    Inventors: Robert L. Bowen, Manuel C. Turchan
  • Patent number: 5413810
    Abstract: A seamless belt is fabricated by application of a coating to an endless substrate. The substrate is elastically stretched over a hollow cylindrical elongated support mandrel. The mandrel is formed of a porous material. Fluid is applied under pressure through the mandrel to form a layer of fluid between the outer surface of the mandrel and the inner surface of the substrate. The flow of fluid is manipulated to axially displace and to rotate the substrate on the outer surface of the mandrel. The flow of fluid is manipulated to orient a selected portion of the surface of the substrate to an angle to a direction of application of a coating. The temperature of fluid is manipulated to assist in substrate temperature control at steps of the coating and drying process.
    Type: Grant
    Filed: January 3, 1994
    Date of Patent: May 9, 1995
    Assignee: Xerox Corporation
    Inventor: Henry T. Mastalski
  • Patent number: 5409741
    Abstract: The method for metallizing the surface of dielectric materials according to the invention comprises a first step wherein a metal powder, the size of the grains of which is comprised between 10 and 5000 nm, is deposited and then incorporated into the surface of the dielectric material. In a second step of the method, the dielectric material which is so impregnated with metal, is immersed into an autocatalytic bath to coat the impregnated zones of the material with a layer of the metal contained in the bath in a thickness which is proportional to the immersion time. This method enables to metallize materials such as oxides, polymers and composites containing these oxides and/or these polymers. The characteristics of the metal deposits are controlled, on the one hand, by the type of metal, and the size and the geometry of the metal powder grains and, on the other hand, by the type and the structure of the dielectric materials coated with these deposits.
    Type: Grant
    Filed: February 14, 1992
    Date of Patent: April 25, 1995
    Inventor: Lucien D. Laude
  • Patent number: 5399373
    Abstract: Various processes are disclosed for repairing damage to one or more articles having wood-like appearance and formed from synthetic resins.
    Type: Grant
    Filed: September 2, 1993
    Date of Patent: March 21, 1995
    Inventor: John B. Mrozinski
  • Patent number: 5397607
    Abstract: Missing thin film metallurgy on substrates is replaced during the manufacture of thin film electronic circuits. The process allows the missing thin film metallurgy, such as an input/output (I/O) pad or pads, to be replaced quickly and simply, without damaging the other I/O pads or thin film metallurgy already applied to the substrate. The process essentially uses lift-off technology without building a complete lift-off stencil.
    Type: Grant
    Filed: May 17, 1994
    Date of Patent: March 14, 1995
    Assignee: International Business Machines Corporation
    Inventors: Ronald R. Shields, Kurt A. Smith, Ronald J. McDonald
  • Patent number: 5393580
    Abstract: A method for preparing high resolution negative-working wash-off relief images comprising the sequential steps of: (a) providing a non-photosensitive, aqueous processable layer, preferably on a substrate, said layer comprising a dispersion of solvent-coalesceable particles in a polymer matrix; (b) imagewise applying an ink to the non-photosensitive layer to coalesce the particles and form a water-insoluble polymer blend between the particles and the polymer matrix in the ink applied areas; and (c) washing the layer with an aqueous developer solution to remove the non-ink applied areas of the layer.
    Type: Grant
    Filed: December 20, 1993
    Date of Patent: February 28, 1995
    Assignee: E. I. Du Pont de Nemours and Company
    Inventors: Sheau-Hwa Ma, Andrew E. Matthews
  • Patent number: 5368902
    Abstract: Method for providing a patterned thin film on a flexible web-like substrate having at least one surface. A patterned release coating which carries the desired pattern is deposited on the surface and has openings therein through which the surface of the substrate is exposed. A thin film is deposited over the patterned release coat and onto the portions of the surface exposed through the openings. The patterned release coating is then removed and the thin film portions carried thereby to provide a patterned thin film on the substrate.
    Type: Grant
    Filed: May 5, 1993
    Date of Patent: November 29, 1994
    Assignee: Flex Products, Inc.
    Inventors: David W. Todd, Lindsey Brown, Roger W. Phillips, Elliot E. Overshiner
  • Patent number: 5362513
    Abstract: A pattern forming method comprises at least a lower pattern forming step for printing a setting ink on a substrate, a setting step for setting the setting ink, an upper layer pattern forming step for forming a metalo-organic compound paste layer on the lower layer pattern by a printing method, and a firing step for firing at high temperature to remove the lower layer pattern. In the upper layer pattern forming step, the metalo-organic compound paste is printed so that the metalo-organic compound paste may be divided on the hardened setting ink so as to fill up gaps of the lower layer pattern. Otherwise the metalo-organic compound paste is printed on the hardened setting ink, and the metalo-organic compound paste is mechanically cut off, before the metalo-organic compound paste is dried, on the hardened setting ink, thereby forming an upper layer pattern. The setting ink comprises a thermo-setting resin, a setting agent, and an organic solvent, with an amount of nonvolatile materials of 50 to 70 wt.
    Type: Grant
    Filed: May 10, 1991
    Date of Patent: November 8, 1994
    Assignee: Matsushita Electric Industrial Co., Ltd.
    Inventors: Mikinari Shimada, Hirotoshi Watanabe, Satoru Fujii, Masato Hagino, Masahide Tsukamoto
  • Patent number: 5362516
    Abstract: Method of preparing an adhesive sheet comprising (1) a backing, and (2) an adhesive layer having at least one topologically microstructured surface comprising a plurality of pegs, optionally containing one or more beads, substantially uniformly distributed and protruding outwardly from the adhesive layer, wherein the pegs have essentially flat tops that comprise less than 25% of the total surface contact area of the adhesive layer, and have a height of at least 15 .mu.m.
    Type: Grant
    Filed: December 7, 1993
    Date of Patent: November 8, 1994
    Assignee: Minnesota Mining and Manufacturing Company
    Inventors: Kenneth D. Wilson, Larry A. Meixner, Sharon R. Bemis, Clyde D. Calhoun, Buren R. Ree
  • Patent number: 5358604
    Abstract: The invention provides an apparatus and methods of using the apparatus to transfer conductive patterns onto substrates under conditions of heat and pressure. The apparatus comprises a master mold with a printing surface on which is produced a permanent mirror image of the conductive pattern to be created. This pattern is then coated with a loosely adherent film of conductive metal, such as copper, which is transferred onto a substrate to be printed.
    Type: Grant
    Filed: September 29, 1992
    Date of Patent: October 25, 1994
    Assignee: Microelectronics and Computer Technology Corp.
    Inventors: Charles W. C. Lin, Chung J. Lee, Tom J. Hirsch, Kimcuc T. Tran