Abstract: A process is disclosed for forming a protective metal coating on a metal surface using a flux consisting of an alkali metal fluoride, an alkaline earth metal fluoride, an alkali metal fluoaluminate, an alkali metal fluosilicate, and mixtures thereof. The flux, in particulate form, is mixed with particles of a metal coating material which may comprise aluminum, chromium, mixtures thereof, and alloys containing at least 50 wt. % aluminum and the particulate mixture is applied to the metal surface in a single step, followed by heating the coated metal surface to a temperature sufficient to cause the metal coating material to react with the metal surface to form a protective reaction product in the form of a metal coating bonded to the metal surface. The metal surface which reacts with the metal coating material to form the protective coating may comprise Fe, Co, Ni, Ti, V, Cr, Mn, Zr, Nb, Mo, Tc, Hf, Ta, W, Re and alloys thereof.

Abstract: The adhesion of metal to a polyimide substrate is enhanced by depositing onto at least one surface of the polyimide a thin film of metal such as copper and heating in air to cause the deposited metal to texturize that surface by producing asperities that are at least 0.05 .mu.m in average height and average breadth. In doing so, metal oxide clusters are formed at the textured surface. When the textured surface is metallized, the resulting composite resists delamination even at soldering temperatures.

Abstract: A method of manufacturing heat-exchanger excellent in the pitting corrosion resistance is disclosed, wherein, in the manufacture of aluminum heat-exchanger to be brazed under heat in the furnace of inert gas atmosphere using fluoride flux, Zn is disposed at a position of 430.degree. to 620.degree. C. in the furnace to melt and vaporize it and the vapor of Zn is allowed to contact with the fin material and the tube material coated with said flux simultaneously with the brazing under heat of these aluminum components, or the fin material coated with said flux and dried and the tube material without flux are assembled and retained for not less than 1 minute in the vapor of Zn of a temperature lower than the melting point of said flux and higher than the temperature, at which these components are heated, in the inert gas and thereafter brazing is performed at a temperature higher than the melting point of said flux.

Abstract: A method of applying a material of particulate form to the surface of an object by using a liquid, wherein the liquid is applied to the surface of the object to provide a film of the liquid thereon, and then the material of particulate form is applied to the film of the liquid on the surface of the object. Excess liquid may be removed from the surface of the object by using a jet of air current before the material of particulate form is applied to the film of the liquid on the surface of the object.

Abstract: There is disclosed a method of depositing a protective coating on a ferrous substrate comprising the steps of immersing the substrate in an electrolytic solution containing zinc chloride, a fluoride and at least one of NiCl.sub.2 and CoCl.sub.2, electrodepositing on said substrate a thin pre-coating comprising zinc, said electrolytic bath also functioning as a flux such that the thin electrodeposited coating comprising zinc will have thereon a flux coating as the substrate is removed from the electrolytic bath; removing the pre-coated substrate from the electrolytic bath, thereafter immersing the pre-coated substrate in a molten metal bath containing zinc so as to deposit a zinc-containing protective coating on said substrate, and removing said substrate from said molten bath.

Abstract: A method and device of performing plating of an item having a row of fine parts, e.g. a flatpack IC are disclosed. The method comprises immersing said item in a bath of molten solder, removing said item from said bath while maintaining said item in an attitude such that said row of fine parts is sloped with respect to the surface of said molten solder, and causing flux to exert a fluxing action on said molten solder which adheres to said fine parts, thereby decreasing the surface tension of the solder adhering to said fine parts and preventing bridges of solder from forming between said fine parts.

Abstract: Solder flux is applied to the face of a printed circuit board (24) or the like by flowing a foam (30) of liquid flux bubbles upwardly through the top of a chimney flue (10) and into contact with the board face which is top passed over the top of the flue. The size of bubbles adjacent the face of the board is controlled by placing a grid screen (26) within and immediately beneath the top of the flue. The openings (26a) in the grid screen allow passage therethrough of smaller bubbles (34) but prevent passage of larger bubbles (32). The force of the board face on the foam urges the larger bubbles downwardly into contact with the grid screen where the grid wires of the screen pierce and thereby break the larger bubbles into smaller bubbles which then rise to the face of the board.

Abstract: A fluorescent solder paste mixture comprising a fluorescent pigment dispersed in a solder paste is disclosed. The solder paste comprises solder fragments dispersed in a solder flux. A method for making the solder paste mixture and a method for using the solder paste mixture to make a fluorescent solder joint between an electrical component and a circuit board are also disclosed. Use of the fluorescent solder paste mixture facilitates automatic and manual inspection of circuit boards during and after assembly.

Abstract: The present invention concerns processes for making composite materials.The process is characterized essentially by the fact that it consists in making a fibrous preform 1, in pre-treating this fibrous preform by a fluorine containing flux 3 and in wetting the said pre-treated preform by a light alloy.Utilization for the making of composite pieces with a fibrous armature such as carbon wet by a light aluminum-based alloy.

Abstract: A flux bath and its use in treating ferrous articles prior to their being dipped in a molten aluminum-zinc alloy is disclosed. The flux may be molten bath or used as an aqueous solution which contains from 200 to 750 g/l dissolved solids. The dissolved solids are 91 to 98.5 wt. % zinc chloride, 1.5 to 9 wt. % ammonium chloride and, based on zinc chloride and ammonium chloride, from 0.6 to 3 wt. % fluoride ions.

Abstract: A method is disclosed for lining a bearing shell with a babbitt metal which does not require tinning of the bearing shell and does not require premelting of the babbitt metal. An inner cylindrical surface of a bearing shell is covered with a flux and lined with a solid babbitt metal. The shell and babbitt metal are rotated about a horizontal axis coaxial with the cylindrical axis of the shell at a rotational velocity sufficient to generate an acceleration at the radially inner surface of said shell of about 20 g's. The babbitt metal and flux are heated to a temperature sufficient to melt the babbitt and the flux and metallic oxides and other impurities at the interface of the babbitt metal and bearing shell are urged toward the axis of rotation permitting a strong metallurgical bond between the babbitt and bearing shell. The shell is cooled and the impurities are machined from the radially inner surface of the babbitt metal.

Abstract: In a case where filament-like articles (e.g. wires) are dip-coated by upwardly passing the article into a bath of molten metal through the bottom and top vertical openings of a spout containing the molten metal, the article to be coated is wrapped, before it enters the bottom inlet opening in the spout, with a blanket of protective gas at a pressure sufficient to cause the gas to penetrate into the spout simultaneously with the article, to progressively and regularly circulate around the molten metal and to steadily emerge from the upper opening of the spout still effectively shielding the freshly coated article.

Abstract: This invention relates to a process of selective galvanizing of materials adapted to be galvanized by immersion in hot conditions characterized by the application on said materials, prior to immersing them into a bath of melted zinc, on those spots on which no galvanizing is desired, calcium carbonate alone, or a mixture thereof with an alkali metal chlorinated-s-triazine trione, or with an alkali metal salt of an oxygen-containing chlorine compound.

Abstract: A method of making an enamel bead and resulting bead which includes the provision of a short length of copper tubing forming a bead core member wherein the copper tubing is heated to a red hot state and rolled in copper enamel flux one or more times to coat the tubing following which the flux coated tubing is again heated to a red hot state and rolled in particulate enamel material to coat the tubing externally with enamel material, then heating the enamel material coating until it melts and is distributed throughout the tubing outer surface in the desired bead configuration and finally cooling the enamel coating to form a highly durable bead having a copper tubing core with an outer layer of enamel of a selected color.

Abstract: A method is described for metalizing, particularly zinc-coating of steel surfaces in such manner that the production of sewage and/or harmful waste products is substantially eliminated. The various steps employed include degreasing, etching, activation, and metallization of the metal substrate by successive immersion of the substrate in baths containing, respectively, the necessary components to perform the function of each bath and also the components of the preceding bath, recycling the wash products from each bath to a preceding bath containing the same components as said waste products, and rinsing the product with water only after completion of the successive method steps.

Abstract: Electrical and electronic components loosely mounted in a circuit board with their leads extending through holes in the board are temporarily stabilized in position in the board by treating the board and component leads at least in part with a selected material in liquid state, and hardening the material to form a solid, solder-compatible, non-metallic cement having a melting point below that of solder, coupling the board and leads to one another. The component leads may then be trimmed to finish length, and the components soldered in place. Alternatively the board may be placed in storage for future soldering. The cement is melted and displaced simultaneously with soldering. Preferred as cement are naturally occurring and synthetic waxes having a melting point in the range of about 120.degree.195.degree. F.

Abstract: Seafood pots made of wire mesh netting are prepared for galvanizing by first passing them through an incineration chamber to burn, melt and loosen foreign material thereon, and then passing them through a high pressure liquid spray to remove residual burned matter and loosened foreign material. The pots are then ready to be passed through the steps of the galvanizing process, which includes dipping the pots into heated preflux before they are dipped into molten zinc. An inverted drying chamber bridges the distance between the preflux tank and the zinc kettle, through which the seafood pots are moved by conveyor means to dry the preflux, with drying heat within the chamber being drawn from the tank and the kettle. The seafood pots are vibrated as they are withdrawn from the molten zinc to effect an even coating of zinc on the wire mesh netting thereof.

Abstract: An alloy suitable for the galvanization of steels by an immersion galvanization process, including gavanization of steels containing silicon, which alloy comprises zinc of commercial purity and has a lead content of the order of 1000 to 20000 p.p.m. by weight, an aluminium content of from 100 to 5000 p.p.m. by weight, a magnesium content of from 10 to 1000 p.p.m. by weight and a tin content of from 300 to 20000 p.p.m. by weight.A galvanization process using the said alloy is also described.

Abstract: Articles of almost any imaginable configuration are given a uniform, complete coating over all surfaces by placing them in a spinnable perforate container or basket that is suspended from a reversible spinning assembly which is adapted to spin the perforate container and its articles in both directions during steps of the process of pre-coating, coating, quenching or air drying.A new control system is also employed to provide rapid response in reversing directions of rotation of the perforated container or bringing it to a complete stop.

Abstract: Processes and compositions are disclosed for surface coating of metals and alloys of low nobility with gold alloys to provide improved corrosion resistance and surface hardness to the underlying metals.

Abstract: The work-pieces are mechanically cleaned, degreased and washed, and then etched in an aqueous solution containing 0.5-1.0% by weight of citric acid, and 16-24% by weight of hydrochloric acid, having a temperature of 15.degree.-30.degree. C., preferably of 20.degree.-25.degree. C., for the time of 1-20 minutes, preferably 2-5 minutes, whereafter the work-pieces are neutralized in an aqueous ammonia solution having a concentration not exceeding 1% by weight, at a temperature of 15.degree.-25.degree. C., in a time not shorter than 1 minute. After being washed in water at a temperature not exceeding 35.degree. C. in a time not shorter than 1 minute, they are dipped in an agitated aqueous solution of the flux, containing 1.8-2.5% by weight of potassium fluoride, 0.8-1.5% by weight of sodium fluoride, and 1.5-3.0% by weight of potassium fluorozirconate, having a temperature of 40.degree.-80.degree. C.

Abstract: Method and means for continuously contact-coating one side only of a ferrous base metal strip with a molten coating metal. One or more roll means are provided to conduct the strip surface to be coated above the surface of a bath of the molten coating metal. The strip surface to be coated is caused to travel sufficiently close to the molten coating metal bath surface that the surface tension and wetting characteristics of the coating metal will permit the formation of a meniscus which will continuously contact and coat the strip surface. The coating is subjected to jet finishing. The strip is maintained in a protective non-oxidizing atmosphere at least until the one side thereof is coated. Alternatively, at least that side of the strip to be coated with the molten coating metal is coated with a flux which remains on the strip until contacted by the coating metal meniscus.

Abstract: A process for simultaneously preheating and preparing a ferrous surface, prior to the depositing thereon of galvanized zinc coatings, replaces conventional fluxing techniques with the step of immersing a ferrous object in a bath of a molten salt or salts. The salts are chosen so that they are liquid at a temperature below that of the zinc coating step. The liquid acts as a non-fuming flux and preheat for the surface. Particular salts include metallic hydroxides and halides.

Abstract: A metal wick to be used for the absorption of molten solder is deoxidized and flux coated by a process that does not involve the application of heat to the wick or the flux. In one embodiment the wick is cleaned by heating in a reducing atmosphere and is then immersed in a coating bath containing a solution of a rosin flux in an organic solvent. On leaving the bath the welted wick enters a low-pressure chamber in which the solvent rapidly evaporates at room temperature. In another embodiment the deoxidized wick is coated with comminuted solid resin by electro-static means.

Abstract: A method of cladding metal plate with a protective layer of copper or copper base alloy is disclosed. The metal plate is contacted with a standing waveform of molten copper or copper base alloy in order to provide the cladding layer. This clad composite material is used to provide corrosion resistance for the metal plate substrate and an inexpensive alternative to solid thick sheets of copper or copper base alloy to deter corrosion.

Abstract: A partially alloyed galvanized ferrous strand and a method for its production. The method is characterized by the steps of immersing a clean and oxide-free ferrous strand in a molten zinc galvanizing bath to produce on the strand a coating weight of between 0.2 and 0.5 oz. per square foot. After immersion, the zinc-coated ferrous strand is heat treated and cooled to produce a galvanized coating on said ferrous strand, which coating has a duplex structure characterized by an iron-zinc intermetallic layer consisting essentially of the zeta phase, an overlay of free zinc, and an average iron content between about 2 and less than 4% by weight.

Abstract: A protected easy-open metal end for containers is disclosed that contains a scoreline which defines on the central portion of the end a removable panel portion and a residual lip portion. A layer of synthetic resin hot melt material is deposited on one of the central panel surfaces opposite the scoreline, whereupon after the hot melt is solidified, the end is post heated to effect softening of the hot melt so that the metal end surface is wetted thereby. The resultant bond between the hot melt and the metal end is so great that severing of the removable panel from the end effects corresponding severing of the hot melt layer to provide protective hot melt layers on the edges of each of the panel and the residual lip portions. The hot melt layer may be applied to the same or the opposite central panel surface that contains the scoreline, or on both surfaces to provide two-side protection.

Abstract: The gas supplied to a foam fluxer utilized for wave soldering is presaturated with a flux thinner compatable with the flux solvent utilized in the foam fluxer to eliminate evaporation of solvent in the foam fluxer and maintain the temperature and specific gravity of the flux solution constant.

Abstract: A hot-rolled coil having excellent adaptability for pickling can be produced by applying to the sides of the hot-rolled coil, a compound of an alkaline metal or alkaline earth metal, or an oxygen compound of boron, germanium, tin, antimony, lead, bismuth or vanadium. One or more of the aforesaid compositions when applied to a hot-rolled coil serves to suppress the formation of oxide film on the surface of the coil and/or promotes the solubility of the oxide film in the pickling tanks to the extent such oxide film does form.

Abstract: Galvanising fluxes consisting of zinc chloride, one or more of sodium, potassium, calcium and magnesium chlorides, and an acid or acid salt (preferably aluminium chloride). In solution in water, the pH of the solution is less than 5.

Abstract: In wet process hot dip galvanising use is made of a flux which melts at below 500.degree.C and consists of 30 - 70% by weight magnesium chloride and 20 - 70% by weight sodium chloride and/or potassium chloride.