Abstract: A method for producing a lead ferroelectric film having high relative dielectric constant and low dielectric loss by a hydrothermal process is disclosed. The method includes the step of hydrothermally forming a ferroelectric layer on a substrate, followed by the step of hydrothermally treating the resulting film in an aqueous solution having a pH of about 5 to 7.

Abstract: A method and apparatus for treating the atmosphere comprising moving a vehicle through the atmosphere, the vehicle having at least one atmosphere contacting surface and a pollutant treating composition located on said surface. A specific embodiment comprises coating a motor vehicle radiator with pollutant treating catalyst.

Abstract: The invention includes a thin film optical coating having a layer comprising sol-gel derived niobium oxide which is capable of providing an index of refraction of at least about 1.90. The invention also includes a thin film optical coating having a layer comprising a sol-gel derived oxide system including niobium oxide and a second oxide component such as aluminum oxide and/or silicon oxide which is capable of providing an index of refraction of from about 1.60 to about 1.90. Also included in the present invention are processes for producing such thin film coatings. In the processes, a substrate is immersed in a mixture comprising niobium chloride and an alcohol, withdrawn from the mixture, and heat-treated. The mixture may also include aluminum precursors and/or silicon precursors. The heat-treatment may occur at various temperatures, including those under 200° C.

Abstract: A ceramic electronic device is protected at the surface from retention of water, thus having improved operation reliability, and a method of manufacturing the device is provided. A protective layer is formed on the ceramic element and external electrodes by dehydrating condensation of organic silicon compound.

Abstract: The present invention provides a method for preparing mesoporous TiO2 thin films with high antibacterial and photocatalytic activities. The method involves coating onto a substrate a TiO2 sol-gel prepared from hydrolysis and condensation of titanium alkoxide in the presence of a stabilizer and thermally treating the substrate at a temperature ranging from 400° C. to 900° C. The TiO2 thin films fabricated according to the method of the present invention show two times higher antibacterial and photocatalytic activities than the conventional TiO2 thin films.

Abstract: This invention relates to novel process of preparing chemically bonded composite hydroxide ceramics by exposing a thermally treated hydroxide ceramic to phosphate reagent and subsequent heat treating the resulting system to initiate a rapid chemical bonding reaction. Such combined hydroxide/chemical bonding process can be used to fabricate ceramics or ceramic coatings for a variety of high and low temperature applications, including corrosion protection, wear resistance, dielectric properties, metal reinforced ceramics, ceramic membranes, non-sticky surfaces, bio-active ceramics, thermal barrier ceramics, non-wetted surfaces, and others.

Abstract: A method for texturing substrate surfaces and a substrate product, such as for computer disk drives. Microbump textured substrates are produced having a Rp value of about 20-200 Å and a ratio of Rmax:Rp of about 1.4 or less. In an exemplary embodiment, a microbump textured substrate is produced having colloidal particles on a surface thereof at a density of at least about 25 particles per 25 &mgr;m2, wherein the surface topography includes a Rp value of about 20-200 Å, a micro-roughness Rq of about 10 Å or less, and a ratio of Rmax:Rp of about 1.4 or less. An exemplary method includes first providing a substrate surface having a surface micro-roughness Rq of about 10 Å or less and depositing colloidal particles on the surface to provide a Rp value of about 20-200 Å and a ratio of Rmax:Rp of about 1.4 or less. In a further exemplary embodiment, the method increases the micro-roughness Rq, but to a value that is still less than about 10 Å with Rmax:Rp still of about 1.

Abstract: A device (10) is made, having a ceramic thermal barrier coating layer (16) characterized by a microstructure having gaps (18) with a sintering inhibiting material (22) disposed on the columns (20) within the gaps (18). The sintering resistant material (22) is stable over the range of operating temperatures of the device (10), is not soluble with the underlying ceramic layer (16) and is applied by a process that is not an electron beam physical vapor deposition process.

Abstract: Compositions and methods for wrinkle reduction in fabrics, including washable clothes, dry cleanable clothes, linens, bed clothes, draperies, window curtains, shower curtains, table linens, and the like requiring little, if any, pressing, ironing, and/or steaming are disclosed.

Abstract: The invention provides a process for coating a cylindrical carrier structure with a predetermined amount (target take-up) of a coating suspension, wherein the carrier structure has a cylinder axis, two end faces, an encasing face and an axial length L and a large number of channels running from the first end face to the second end face. The process comprises: a) vertically aligning the cylinder axis of the carrier structure and filling the empty volume of the channels up to a predetermined height H1 starting from the lower end face, b) removing the excess coating suspension through the lower end face of the carrier structure down to the target take-up, c) turning the carrier structure 180°, so that the upper and lower end faces are exchanged one for the other, and d) repeating steps a) and b), wherein the height H2, up to which the channels are filled in this case is given by H2=L−x·H1 where x is between 0.8 and 1.0.

Abstract: Manufacturing process of an electrically insulating and mechanically structuring sheath on an electric conductor which applies notably to the manufacture of superconducting magnets, wherein a ceramic precursor (4) in gel form is formed, then a coating of the conductor (2) with this precursor, and this coating is then heat treated to form the ceramic.

Abstract: A method is provided for making a hydrophilic carbon fiber construction comprising the steps of: a) immersing a carbon fiber construction in an aqueous dispersion of one or more metal oxides, comprising: i) 1-15% by weight metal oxide; ii) 0.01%-5% by weight dispersant; and b) subsequently heating the carbon fiber construction sufficiently to remove substantially all of the dispersant. Typically the entire method can be completed in less than 20 minutes. In addition, a hydrophilic carbon fiber construction made according to the method of the present invention is provided, typically having a loading of metal oxide equivalent to 20-50 mg metal per gram of carbon.

Abstract: A composite structure is formed by depositing a one or more coatings on an open-cell foam skeleton to form a higher-density composite foam. In accordance with one aspect of the invention, the composite foam can be at carbon carbon composite formed by a rapid densification process. The form composite structure is suitable for use, for example, as a friction material employed in clutch and brake devices.

Abstract: A honeycomb structure in which the structure has a reinforced part having been loaded with a cordierite powder at least on one end surface of the frontal openings of the substrate of a honeycomb structure made of cordierite. This honeycomb structure does not decrease merits of a small pressure loss and the like as a thin-walled honeycomb structure, and is also excellent in abrasive resistance of the end surfaces of the frontal openings.

Abstract: An impregnated fired, porous ceramic core for use in an investment casting shell mold in the casting of molten metals and alloys is strengthened by impregnating the core with an aqueous emulsion of water-insoluble polymer followed by drying to remove the water.

Abstract: A method to make a mouthpiece body having a predetermined set of desired characteristics for a given application comprises providing a porous ceramic material, infiltrating it with an acrylic resin, and curing the article, wherein the properties of the ceramic material, the acrylic resin, and the infiltration ratio are selected in order to control the modulus of elasticity and internal friction of the mouthpiece.

Abstract: Gas wiping apparatus and method can reliably prevent edge overcoat and splash, and has face gas wiping nozzles extending widthwise of a strip material, a pair of baffle plates spaced from an edge of the strip material, an edge wiping nozzle disposed between baffle plates at its inner edge and adjacent the strip material edge, all with critical spacings relative to each other.

Abstract: A method of sealing the cells of a ceramic honeycomb body (5) and a cell sealing material (1) are disclosed which can suppress the deformation and dissolution of the portions of the ceramic honeycomb body dipped in the cell sealing material. An end surface (50) of the ceramic honeycomb body (5), with the portions of the end surface (50) not to be sealed covered with a masking material, is dipped in the cell sealing material (1) thereby to seal the cells in a predetermined part of the end surface. The cell sealing material (1) is composed of ceramic particles and an assistant for fluidizing the ceramic particles. The assistant has the property of not substantially redissolving a binder contained in the ceramic honeycomb body.

Abstract: The invention relates to the coloring of ceramics by means of ionic or complex-containing solutions. Solutions preferred for this contain defined concentrations of at least one of the salts or complexes of the rare earth elements or the elements of the subgroups. The invention also relates to a kit, which comprises at least one stock bottle with such a coloring solution, a receptacle for the coloring as well as optionally a screen.

Abstract: A process for chemical removal of organically-modified silicate (Ormosil) coatings from aluminum alloy substrates without degradation of the underlying metal. An Ormosil film is treated with a zincate solution. The zincate solution dissolves the Ormosil film and deposits a thin, easily-removed layer of zinc onto the aluminum alloy surface, which prevents base-activated dissolution of the underlying metal. The zinc layer may be removed using dilute phosphoric acid, leaving the surface of the aluminum alloy intact. Consequently, the sol-gel coating may be removed while the integrity of the aluminum alloy substrate is maintained.

Abstract: The invention is directed to a method for producing a corrosion-resistant and oxidization-resistant layer that is applied onto a component part, whereby the method can be simply and cost-beneficially implemented in fabrication-oriented terms and comprises the steps: a) producing a slip by mixing powder containing at least one of the elements Cr, Ni or Ce with a binding agent; b) applying the slip onto the component part; c) drying the slip at temperatures from room temperature through 300° C.; and d) alitizing the slip layer.

Abstract: A turbomachine component includes a silicon nitride substrate and a protective coating on the substrate. The protective coating includes a porous silicon nitride matrix and a noble metal infiltrated in the porous silicon nitride matrix.

Abstract: A method is provided of adaptively controlling a paint system for painting vehicle bodies. The method includes the steps of obtaining an estimated Jacobian that identifies characteristics of the paint system and using the estimated Jacobian to determine initial conditions to be implemented for the next vehicle body to be painted in the paint system. The method also includes the steps of storing a database of appropriate initial conditions that resulted in satisfactory transient response in a rule-base and using the rule-base at start-up of the paint system or if the paint system fails to be satisfactorily controlled.

Abstract: An apparatus for and method of rinsing one side of a two-sided substrate and removing unwanted material from the substrate's edge and/or backside. One embodiment of the method is directed toward rinsing and cleaning a substrate having a front side upon which integrated circuits are to be formed and a backside. This embodiment includes dropping the substrate front side down onto a pool of rinsing liquid in a manner such that the front side of the substrate is in contact with the solution while the substrate is held in suspension by the surface tension of the solution liquid thereby preventing the backside of the substrate from sinking under an upper surface of the pool. Next, while the substrate is in suspension in said rinsing liquid, the substrate is secured by its edge with a first set of fingers and in some embodiments the substrate is subsequently spun. In another embodiment, a method of forming a copper layer on a front side of a substrate is disclosed.

Abstract: A method of prevention maintenance preventing parts of an etcher from being eroded is disclosed. First, a layer of hydrogen-free chemical compound is formed on surface of the parts of the etcher according to one embodiment of the present invention. Otherwise, the parts of the etcher are immersed into a tank containing hydrogen-free chemical compound according to another embodiment of the present invention. After that, a standard process of prevention maintenance is performed by a cleaning agent.

Abstract: The invention includes a bilayer antireflection coating, multilayer antireflection coatings, and a method for making a multilayer antireflective coated substrate. The bilayer and multilayer coatings include layers having metallic oxides, at least one layer in each of such coatings having as a material with an index of refraction at least about 1.90, a layer comprising oxides of zirconium such that when subjected to heat treatments, such as tempering, the coatings substantially retain their optical properties. The coatings further include layers having materials of low index of refraction which include oxides of aluminum which provide coating stability and increased precursor storage life. In the method, the layers are applied by successive dip coating techniques using solvent-based solutions and the resulting coatings can be used to coat large sized substrates which can be later cut, trimmed and/or otherwise shaped and later heat treated with substantial retention of optical properties.

Abstract: A thin-walled honeycomb structure includes: a circumferential wall, numerous partition walls disposed inside the circumferential wall, and numerous cell passages defined by the partition walls. A circumferential portion of the honeycomb structure is reinforced wholly or in a part within a certain distance from an extremity surface of the honeycomb structure by a reinforcing material that dissipates or evaporates at a high temperature, and a method for producing the same.

Abstract: During the deposition of a catalytic component on a carrier, the position of the liquid level of a slurry containing the catalytic component is controlled with high accuracy and the adhesion of the slurry to the lateral face of the carrier is prevented. In the deposition of the liquid substance on the carrier by the introduction of the liquid substance into the carrier from the bottom face thereof, the liquid level near the top face of the carrier is detected by an image-processing sensor.

Abstract: A method for nitriding a metallic base material at low temperatures in a salt bath containing electrolyzed titanium metal. A nitride coating of exceptional depth and hardness is obtained in a very short operating time due to the rapid nitriding process. The method is applicable to steel, titanium, aluminum and alloys thereof.

Abstract: A process for glazing a chinaware article by forming a chinaware article having a bottom including a glazed foot and a dry foot. The glazed foot extends downwardly from the bottom to a point below the dry foot. A glaze is applied to the formed article so that the glaze is applied to the glazed foot and the dry foot is substantially free of the glaze. The article is supported on a supporting device so that the dry foot engages the device and the glazed foot is exposed. The article is heated to mature the article including the glaze. A glazed chinaware article is produced in the process.

Abstract: A method of adjusting the pH of a strengthening melt for use in strengthening glass substrates, e.g., glass disk substrates for use in data storage devices. A non-particle-forming acid is added to the strengthening melt to lower the pH of the strengthening melt to ≦8. The acid is added while the strengthening melt is in a molten state and selected to avoid particle formation. Nitric acid, for example, is non-particle-forming with respect to nitrate based strengthening melts such as potassium nitrate and/or sodium nitrate. A base, e.g., sodium hydroxide, may be added if the pH of the strengthening melt falls below 5. Strengthening melts are subject to pH shift that can cause glass substrates strengthened therein to etch, creating pits on the substrate surface. Glass disk substrates treated in the pH adjusted strengthening melt are essentially free from such pits, as well as contamination caused by particle formation.

Abstract: After a thin liquid agent film is formed by supplying a liquid agent onto a plate-like developer holder, this liquid agent film and the surface of a substrate are opposed. The liquid agent film and the substrate are brought into contact with each other at a point by declining the substrate and moving it close to the liquid agent film, or by curving the substrate toward the liquid agent film. Then, the substrate is made parallel to the liquid agent film, and the liquid agent is supplied such that the contact area of the liquid agent film spreads over the entire surface by the interfacial tension between the liquid agent film and the substrate. Since a thin liquid agent film can be uniformly formed below the substrate, processing can be performed with a small consumption amount. Additionally, the liquid agent can be supplied to the substrate without holding air.

Abstract: The present invention relates to a method of impregnating paper with a suspension of a molecular sieve in waterglass, such as soda waterglass or potassium waterglass, wherein the impregnated paper can be used as a dehumidifying element, and wherein the method comprises the steps of a) providing a piece of paper, such as facing paper and/or fluted paper; b) immersing the paper into a highly concentrated waterglass solution in which a molecular sieve has been suspended, at a temperature in the range of 45-95° C., wherein said suspension of highly concentrated waterglass/molecular sieve has a viscosity of at least 350 mPa.s at a temperature of 45° C.; and c) cooling the immersed paper with air at a temperature of at most 35° C. and preferably at most 25° C.

Abstract: A process for coating the flow channels in a monolithic, cylindrically shaped catalyst carrier with a coating dispersion, wherein the carrier has two end faces which are connected to each other by flow channels arranged parallel to the axis of the cylinder, by vertically aligning the axis of the cylindrical carrier, placing a predetermined amount of coating dispersion from a storage container on the upper end face of the carrier and drawing the dispersion through the flow channels under suction, removing excess coating dispersion from the flow channels by emptying the flow channels under suction, returning the excess dispersion to the storage container and fixing the dispersion coating by calcination. The coating dispersion is drawn through the flow channels under suction at a rate of flow of 0.

Abstract: Disclosed is a method for making low metallic impurity SiO-based dielectric thin films on semiconductor substrates using a room temperature wet chemical growth (RTWCG) process for electronic and photonic (optoelectronic) device applications. The process comprises soaking the semiconductor substrate into the growth solution. The process utilizes a mixture of aqueous inorganic or organic based silicon source solution, an inorganic reduction oxidation (redox) aqueous solution, non-invasive inorganic or organic based liquid additives for adjusting the growth rate and reducing the metallic impurity concentration within the SiO-based film, with or without an electron exchange pyridine based component, and an inorganic homogeneous catalyst for enhancing the growth of the SiO-based film.

Abstract: The present invention relates to a method for manufacturing a dense and crack-free ceramic membrane which selectively transports oxygen when it is subjected to an oxygen partial pressure gradient, by the following steps: a) preparation of a porous ceramic substrate, with an open network of pores, which allows the transport of gas; b) deposition of a film or coating of an oxygen ion conducting material onto the porous ceramic substrate, by contacting the porous substrate with a colloidal dispersion or slip; c) thermally treating the substrate and film or coating to produce a dense, crack-free membrane on the surface of the porous substrate.

Abstract: A process for glazing a chinaware article by forming a chinaware article having a bottom including a glazed foot and a dry foot. The glazed foot extends downwardly from the bottom to a point below the dry foot. A glaze is applied to the formed article so that the glaze is applied to the glazed foot and the dry foot is substantially free of the glaze. The article is supported on a supporting device so that the dry foot engages the device and the glazed foot is exposed. The article is heated to mature the article including the glaze. A glazed chinaware article is produced in the process.

Abstract: A method for treating a metal enclosure to prevent the enclosure from being contaminated, comprises the steps of: (a) sand-blasting the enclosure; (b) preheating the enclosure to a predetermined temperature, and putting the enclosure into the space in a vacuum chamber between two electrodes; (c) introducing reactive gases into the vacuum chamber, the reactive gases including 1,1,3,3-tetramethyldisiloxane and oxygen; (d) applying high electrical power to the electrodes to cause the reactive gases to become an ionized plasma, the plasma reacting with a surface of the enclosure to form a layer of silicon oxide thereon. The layer of silicon oxide resists formation of a fingerprint when it is touched by a user.

Abstract: A composition providing thermal, corrosion, and oxidation protection at high temperatures is based on a synthetic aluminum phosphate, in which the molar content of aluminum is greater than phosphorous. The composition is annealed and is metastable at temperatures up to 1400° C.

Abstract: The present invention provides a method of removing a Cu-contamination from a wafer surface having a Cu-based metal region, comprising the step of: carrying out a cleaning process by use of a cleaning solution free of HF and capable of oxidation to the wafer surface for not only removing the Cu-contamination from the wafer surface but also oxidizing the wafer surface to cause the wafer surface to have a hydrophilicity.

Abstract: Disclosed is a room temperature wet chemical growth (RTWCG) process of SiO-based insulator coatings on silicon substrates for electronic and photonic (optoelectronic) device applications. The process utilizes a mixture of a silicon source, a pyridinium compound, an aqueous redox solution, and a homogeneous aqueous solution.

Abstract: A method for manufacturing thin film and a thin film. The method comprises dipping a substrate in a solution that dries up forming a layer on the surface of the substrate and controlling layer thickness by changing the rate of dipping the substrate in the solution. Before the next dipping after the first dipping, the position of the substrate is changed such that the next dipping will be carried out in a direction which is at an angle to the direction of the previous dipping.

Abstract: A bioactive bone mineral carbonated nano-crystalline apatite is chemically bonded to a variety of substrates, including implantable prostheses. This coating is applied uniformly to substrate surfaces of varying geometry and surface textures. It is firmly secured to the substrate and encourages rapid and effective bone ingrowth. The coating is applied by immersing the substrate in an aqueous solution containing calcium, phosphate and carbonate ions. Other ions, such as sodium, potassium, magnesium, chloride, sulfate, and silicate, may optionally be present in the solution. The solution is exposed in a controlled environment when it reacts with the substrate to form the coating.

Abstract: A method for producing coated strands of metal includes guiding a metal strand through the bottom of a vessel filled with a molten mass of the same or different composition as the metal strip, wherein the residence time of the metal strand is selected as a function of at least one of the molten bath level, the casting speed, the metal strand thickness, and the preheating temperature of the metal strand such that the deposited molten mass on the metal strand has a desired thickness of several times the initial thickness of the metal strand. After exiting from the molten bath, the metal strand with a layer crystallized thereon is subjected to a smoothing path carried out when the surface temperature of the strand crystallized thereon is smaller than the solidus temperature of the molten bath, so that at least the surface of the layer crystallized thereon is solidified. The crystallized layer is applied with a thickness which exceeds the desired final thickness of the coated strand.

Abstract: There is disclosed a method of mixing/dispersing solid phases of a carbon powder 4 and silicon powder 5, impregnating a woven fiber 2 with the powders, and subsequently exposing the woven fiber to a high temperature sufficient for reaction calcining to react/calcine the woven fiber, so that only small amounts of C and Si particles remain, a matrix forming speed is high, and CMC having high airtightness can be manufactured in a short time.

Abstract: The present invention is useful in growing complex films with high quality (low lattice strain, large grain size, high degree of perfection) at high rates and large area, and high efficiency use of material. A solid-state film is grown from a liquid, where atoms are supplied continuously by vapor deposition onto the liquid surface. The desired film material grows from or is precipitated from the liquid flux, which is in thermodynamic equilibrium with the desired film. The desired film growth starts at a substrate interface. If this is a biaxial textured surface suitable in chemical reactivity and lattice constant, the growth will be epitaxial with the substrate. The atomic mixture that forms the deposited film is supplied by the arrival of the atoms from a vapor onto the surface of the liquid flux. An important additional factor in the case of an oxide such as the HTSC YBCO is that activated oxygen needs to be present, along with molecular oxygen.

Abstract: Process for producing a multi-layer lacquer finish, in which a surfacer coating compound is applied to a substrate optionally pre-coated with a priming layer and/or further coating layers, and a top coating comprising a color-imparting and/or special-effect-imparting base lacquer layer and a transparent clear lacquer layer, or a top coating comprising a pigmented one-layer top lacquer, is then applied, in which the surfacer coating compound which is used is one which either contains binders which are curable exclusively by free radical and/or cationic polymerization, wherein the said binders are cured by means of high-energy radiation, or is one which contains binders which are curable by free radical and/or cationic polymerization, wherein the said binders are cured by means of high-energy radiation, and additionally contains chemically cross-linking binders.

Abstract: Defective, e.g. worn or substandard, carbon-carbon fibre composite materials such as frictional materials in brakes or clutches may be restored and/or upgraded by impregnation with a molten reactive metal source comprising a carbide-forming metal or a derivative thereof such as an oxide.

Abstract: Magnetic composites exhibit distinct flux properties due to gradient interfaces. The composites can be used to improve fuel cells and effect transport and separation of different species of materials. A variety of devices can be made utilizing the composites including a separator, a cell, an electrode for channeling flux of magnetic species, an electrode for effecting electrolysis of magnetic species, a system for channeling electrolyte species, a system for separating particles with different magnetic susceptibilities. Some composites can be used to make a dual sensor for distinguishing between two species of materials and a flux switch to regulate the flow of a redox species and a flux switch to regulate the flow of a chemical species. Some composites can control chemical species transport and distribution.

Abstract: A method for manufacturing a filter utilizing a porous ceramic membrane as a separation film is provided, comprising the steps of substituting the air inside fine-pores of the porous substrate with a liquid, isolating the porous substrate face to be provided with a separation film, the other face of the porous substrate face not provided with the separation film, continuously feeding a film deposition slurry containing ceramic framework particles to allow the slurry to contact the face of the porous substrate to be provided with the separation film, applying a differential filtration pressure between the faces of the porous substrate, and depositing the slurry on the surface of the porous substrate. An organic polymer for endowing the deposition film with filtration resistance is added to the slurry.