Of Metal-containing Material Patents (Class 428/312.8)
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Patent number: 7291384Abstract: The piston ring of the present invention comprises a thermal spray coating comprising chromium carbide particles having an average particle size of 5 ?m or less, and a matrix metal composed of a Ni—Cr alloy or a Ni—Cr alloy and Ni at least on an outer peripheral surface, said thermal spray coating having an average pore diameter of 10 ?m or less and a porosity of 8% or less by volume. A piston ring having excellent wear resistance, scuffing resistance and peeling resistance with little attackability on a mating member is obtained by forming a homogeneous thermal spray coating having a fine microstructure.Type: GrantFiled: October 15, 2003Date of Patent: November 6, 2007Assignee: Kabushiki Kaisha RikenInventors: Ryou Obara, Katsumi Takiguchi, Yukio Hosotsubo
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Patent number: 7169465Abstract: A low CTE metal-ceramic composite material featuring carbon fibers reinforcing a matrix featuring silicon metal or silicon alloy. The fibers have a low coefficient of thermal expansion (CTE) in the axial direction, and preferably negative. The principles of making Si/SiC composites can be adapted to produce the instant Si matrix composites. The CTE of the composite body depends not only upon the relative CTE's of the fibers and matrix, and their relative amounts (e.g., loadings), but also upon the relative elastic moduli of the fibers and matrix. Thus, Si/SiC matrices produced by a reaction-bonding process inherently possess low CTE, but the instant inventors prefer to make such composites having relatively large fractions of unreacted silicon, thereby driving composite CTE lower still. Here, the carbon fibers are protected from reaction with the silicon infiltrant with one or more materials disposed between the fibers and the infiltrant.Type: GrantFiled: February 11, 2002Date of Patent: January 30, 2007Inventors: Prashant G. Karandikar, Jai R. Singh, Clarence A. Andersson
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Patent number: 7144617Abstract: A security element (2) comprising a reflective, optically variable surface pattern (3) which is embedded in a layer composite of plastic material and which can be visually recognized from predetermined observation directions is formed from a mosaic of optically active surface elements (13). In the mosaic of the surface pattern (3) at least two of the mosaic surfaces (11; 12) of the surface pattern (3) are arranged substantially adjacent and have microscopically fine light-diffractive relief structures (4). The spatial frequencies of the relief structures in the mosaic surfaces (11; 12) are of values from predetermined spatial frequency ranges in such a way that, in the case of illumination beams which are incident obliquely relative to a normal onto the plane of the layer composite, the relief structures of the mosaic surfaces (11; 12) deflect visible monochromatic light parallel to the normal (32).Type: GrantFiled: May 31, 2002Date of Patent: December 5, 2006Assignee: OVD Kinegram AGInventors: Andreas Schilling, Wayne Robert Tompkin
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Patent number: 7083850Abstract: A porous, flexible, resilient heat transfer material which comprises network of metal flakes. Such heat transfer materials are preferably produced by first forming a conductive paste comprising a volatile organic solvent and conductive metal flakes. The conductive paste is heated to a temperature below the melting point of the metal flakes, thereby evaporating the solvent and sintering the flakes only at their edges. The edges of the flakes are fused to the edges of adjacent flakes such that open pores are defined between at least some of the adjacent flakes, thereby forming a network of metal flakes. This network structure allows the heat transfer material to have a low storage modulus of less than about 10 GPa, while having good electrical resistance properties.Type: GrantFiled: October 18, 2001Date of Patent: August 1, 2006Assignee: Honeywell International Inc.Inventor: Ignatius J. Rasiah
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Patent number: 7074480Abstract: A nanostructure is a porous body comprising a plurality of pillar-shaped pores and a region surrounding them, said region being an oxide amorphous region formed so as to contain C, Si, Ge or a material of a combination of them. Such a nanostructure can be used as functional material that can be used for light emitting devices, optical devices and microdevices. It can also be used as filter.Type: GrantFiled: August 14, 2003Date of Patent: July 11, 2006Assignee: Canon Kabushiki KaishaInventors: Kazuhiko Fukutani, Tohru Den
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Patent number: 7070855Abstract: There are provided a porous material and a process for producing the same. The porous material has a plurality of columnar pores and an area surrounding the pores, and the area is an amorphous area containing C, Si, Ge or a combination thereof.Type: GrantFiled: September 4, 2003Date of Patent: July 4, 2006Assignee: Canon Kabushiki KaishaInventors: Kazuhiko Fukutani, Tohru Den
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Patent number: 7067187Abstract: A spherical porous ceramic body and the production method thereof are provided. As to the porous ceramic body, the total volume of the pores having a pore radius of from 1.8 nm to 100 ?m is about 0.25 cm3/g or more, the mode of pore radius of the pores is from about 1 ?m to about 6 ?m and the packing density is from about 0.7 g/cm3 to about 1 g/cm3. The porous ceramic body is suitably used as a carrier for a catalyst and has high mechanical strength.Type: GrantFiled: March 14, 2002Date of Patent: June 27, 2006Assignee: Sumitomo Chemical Company, LimitedInventors: Hidekatsu Kawazu, Osamu Yamanishi
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Patent number: 7060348Abstract: Flame retardant EMI shielding materials with improved retention of shielding properties are disclosed. The shielding materials are provided with a dispersed flame retardant on the surfaces of the internal interstices. Methods of making the flame retardant shielding materials are also disclosed.Type: GrantFiled: March 8, 2002Date of Patent: June 13, 2006Assignee: Laird Technologies, Inc.Inventors: Larry Creasy, Kevin Hug
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Patent number: 7056577Abstract: A body, such as a grain, for providing ingrowth and growth of bone tissue and/or connective tissue. The body consists of a plastic or non-essentially elastic biocompatible material, preferably metal or metal alloy. It is also porous, having the following porosity characteristics: (a) the porosity is continuous and (b) the opening of cavities/indentations/pockets and the ducts connecting them has the width of >about 50 ?m for bone tissue and >about 10 ?m for connective tissue. In a method of making such a body, the body has been produced by blowing gas into a melt of metal. An advantageous use of bodies according to the invention is enclosing thereof in a casing, formed with openings, for making an implant, such as a spinal implant.Type: GrantFiled: April 28, 2000Date of Patent: June 6, 2006Assignee: Tigran Technologies ABInventors: Ingrid Bruce, Lars Bruce
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Patent number: 7001679Abstract: A xenotime phosphate protective overlayer (22) for protecting a ceramic material (24) from a high temperature, moisture-containing environment. Yttrium phosphate may be used as a protective overlayer to protect an underlying mullite layer to temperatures in excess of 1,500° C. The coating may have porosity of greater than 15% for improved thermal shock protection. To prevent the ingress of oxygen to an underlying ceramic non-oxide material, such as silicon carbide or silicon nitride, an oxygen barrier layer (34) is disposed between the xenotime phosphate coating and the non-oxide material. Such a protective overlayer may be used for an article having a ceramic matrix composite substrate.Type: GrantFiled: August 8, 2002Date of Patent: February 21, 2006Assignee: Siemens Westinghouse Power CorporationInventors: Christian X. Campbell, Jay E. Lane
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Patent number: 6974625Abstract: A composition, a medical implant constructed from the composition, and a method of making the composition are described. The composition is a composite material, comprising a porous, reticulated, open cell network having at least part of its surface coated with blue-black or black oxidized zirconium.Type: GrantFiled: December 16, 2003Date of Patent: December 13, 2005Assignee: Smith & Nephew, Inc.Inventors: Gordon Hunter, Vivek Pawar
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Patent number: 6964817Abstract: A porous sintered metal comprising voids at least partially communicating with each other, and pores provided in walls of the voids, the porous sintered metal having a BET surface area of 700 cm2/cm3 or more, and an average diameter of the pores being 1 ?m or more when measured by a mercury press-in method. The porous sintered metal is produced by blending a metal powder, a binder and resin particles to prepare a mixture in which the resin particles are dispersed; molding the mixture to provide a green body; selectively extracting the resin particles from the green body with a solvent; debinding the extracted green body by heating; and sintering the debound green body.Type: GrantFiled: July 14, 2003Date of Patent: November 15, 2005Assignees: Hitachi Metals, Ltd., Hmy, Ltd.Inventors: Kenji Date, Masumi Nakai
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Patent number: 6953539Abstract: A composite material includes an SiC porous ceramic sintered body, which is formed by preliminarily sintering a porous body, having a coefficient of thermal expansion lower than the coefficient of thermal expansion of copper to construct a network therein. A copper alloy impregnating the porous ceramic sintered body includes copper and one or more additive elements which are prepared to impart a coefficient of thermal conductivity of 160 W/mK or higher to the composite material. The additive elements include up to 5% of at least one element selected from Be, Al, Si, Mg, Ti, Ni, Bi, Te, Zn, Pb, Sn, and mish metal, and also contain unavoidable impurities and gas components.Type: GrantFiled: September 18, 2002Date of Patent: October 11, 2005Assignee: NGK Insulators, Ltd.Inventors: Shuhei Ishikawa, Tsutomu Mitsui, Ken Suzuki, Nobuaki Nakayama, Hiroyuki Takeuchi, Seiji Yasui
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Patent number: 6951682Abstract: Articles comprising substantially uniform porous coatings, which may be photopatterned, are provided. The use of such porous coatings increases the surface density of attached compounds within, for example, ligand arrays prepared by methods such as regionally selective solid-phase chemical synthesis. Arrays prepared using the porous coatings may be used within a variety of diagnostic and drug discovery assays.Type: GrantFiled: September 17, 1999Date of Patent: October 4, 2005Assignee: Syntrix Biochip, Inc.Inventor: John A. Zebala
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Patent number: 6924040Abstract: A ceramic material has particular utility as a thermal insulating or thermal barrier coating on metallic substrates. The ceramic material includes gadolinia and hafnia, preferably forming gadolinia-hafnia. This material exhibits chemical stability, thermal stability and thermal insulating properties superior to those of currently used thermal barrier ceramics, and also provides resistance to sintering and erosion comparable to currently used ceramics. A preferred material has between about 3-70 mol. % hafnia, balance hafnia.Type: GrantFiled: December 21, 2001Date of Patent: August 2, 2005Assignee: United Technologies CorporationInventor: Michael J. Maloney
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Patent number: 6916529Abstract: An abradable coating composition for use on shrouds in gas turbine engines or other hot gas path metal components exposed to high temperatures containing an initial porous coating phase created by adding an amount of inorganic microspheres, preferably alumina-ceramic microballoons, to a base metal alloy containing high Al, Cr or Ti such as ?-NiAl or, alternatively, MCrAlY that serves to increase the brittle nature of the metal matrix, thereby increasing the abradability and oxidation resistance of the coating at elevated temperatures. Coatings having a total open and closed porosity of between 20% and 55% by volume due to the presence of ceramic microballoons ranging in size from about 10 microns to about 200 microns have been found to exhibit excellent abradability for applications involving turbine shroud coatings. An abradable coating thickness in the range of between 40 and 60 ml provides improved performance for turbine shrouds exposed to gas temperatures between 1380° F. and 1800° F.Type: GrantFiled: January 9, 2003Date of Patent: July 12, 2005Assignee: General Electric CompanyInventors: Surinder Singh Pabla, Farshad Ghasripoor, Yuk-Chiu Lau, Liang Jiang, Canan Uslu Hardwicke, William Emerson Martinez Zegarra
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Patent number: 6902798Abstract: A flexible seal for use in a solid oxide fuel cell stack is formed from a fiber matrix impregnated with a plurality of solid particles. The fibers and particles are preferably ceramic and may be formed from alumina or zirconia. The seal may be formed by dipping the fiber matrix into a slurry of the particles in an alcohol, drying the seal and precompressing prior to installation in the fuel cell stack.Type: GrantFiled: August 17, 2001Date of Patent: June 7, 2005Assignee: Fuelcell Energy, Ltd.Inventors: Debabrata Ghosh, Scott Thompson
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Patent number: 6902797Abstract: A gypsum-based composite structure is prepared from a slurry comprising a mixture of calcium sulfate hemihydrate, a cellulose ether additive other than CMC and an amount of water that is sufficient to form a slurry. The calcium sulfate hemihydrate is hydrated by the water forming a wallboard core reinforced by the cellulose ether additive. The concentration, viscosity grade and degree of substitution of the cellulose ether are selected to give the composite improved nail pull resistance and greater flexural strength.Type: GrantFiled: May 27, 2003Date of Patent: June 7, 2005Assignee: Innovative Construction and Building MaterialsInventors: Jacob Freas Pollock, Christopher D. Tagge, Lennard Torres, David S. Soane
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Patent number: 6893702Abstract: The present invention relates to a substrate for a magnetic recording medium that ensures a floating height on a magnetic head. This substrate is made of a sintered body provided with pores having a diameter in the range of 0.05 ?m to 2.0 ?m extending across 5% to 50% of the surface area of the substrate.Type: GrantFiled: January 20, 2004Date of Patent: May 17, 2005Assignee: Fujitsu LimitedInventor: Shinichi Takahashi
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Patent number: 6869671Abstract: A thin film based nanoporous alumina template has been developed which allows the in situ removal of an electrically insulating alumina barrier layer at the pore bases. This barrier free nanoporous system has great utility for electrodeposition of a wide variety of nanowire materials. An exemplary multilayer thin film precursor is provided comprising Al (anodization layer), Ti (diffusion barrier) and Pt (active electrode) on a Si substrate. Aluminum anodization in sulfuric acid with a subsequent applied voltage ramping program produces a Pt electrode at the base of the nanopores without the additional steps of alumina removal, barrier layer dissolution, and metal deposition onto the pore bottoms.Type: GrantFiled: June 2, 2003Date of Patent: March 22, 2005Assignee: University of Notre DameInventors: Michael M. Crouse, Albert E. Miller, Juan Jiang, David T. Crouse, Subash C. Basu
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Patent number: 6866925Abstract: The invention concerns a heat-stable ordered mesoporous or mesostructured material comprising a mineral phase wherein are dispersed particles of nanometric dimension at least partly crystaline, the global crystallinity index of said mesostructured or ordered mesoporous material being less than 10% in volume. The invention also concern a method for obtaining such a material.Type: GrantFiled: November 2, 2000Date of Patent: March 15, 2005Assignee: Rhodia ChimieInventor: Jean-Yves Chane-Ching
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Patent number: 6866921Abstract: A coated cemented (binder alloy, e.g., cobalt-chromium alloy) tungsten carbide cutting insert that comprises a substrate and a coating. The substrate contains at least about 70 weight percent tungsten and carbon, between about 3 weight percent and about 12 weight percent cobalt, and at least 0.09 weight percent chromium. The substrate presents a surface zone of binder alloy enrichment that begins near (or at) and extends inwardly from a peripheral surface of the substrate. The coating includes a base layer that contains chromium.Type: GrantFiled: March 7, 2003Date of Patent: March 15, 2005Assignee: Kennametal Inc.Inventors: George P. Grab, Mark S. Greenfield, Anakkavur T. Santhanam
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Patent number: 6855408Abstract: A composite metallic material 1 according to the invention is used for, e.g., electrolytic capacitors, and includes a metallic material substrate 10 and a high polymer thin layer 11 having a fine pattern 12 formed on at least one surface of the substrate 10 by self-organization. This high polymer thin film 11 is formed by, for example, drying hydrophobic organic solvent solution of high polymer compound. By subjecting this composite metallic material 1 to etching processing, etching pits are formed uniformly with high density based on the fine pattern.Type: GrantFiled: January 27, 2003Date of Patent: February 15, 2005Assignee: Showa Denko K.K.Inventors: Masatsugu Shimomura, Masaru Tanaka, Hiroshi Yabu, Masafumi Takebayashi, Ryuji Monden, Tamami Koyama, Yoshikazu Hosoda, Masashi Sakaguchi
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Patent number: 6846558Abstract: A dense or porous coating of material is deposited onto a substrate by forcing a colloidal suspension through an ultrasonic nebulizer and spraying a fine mist of particles in a carrier medium onto a sufficiently heated substrate. The spraying rate is essentially matched to the evaporation rate of the carrier liquid from the substrate to produce a coating that is uniformly distributed over the surface of the substrate. Following deposition to a sufficient coating thickness, a single sintering step may be used to produce a dense ceramic coating. Using this method, coatings ranging in thickness from about one to several hundred microns can be obtained. By using a plurality of compounds in the colloidal suspension, coatings of mixed composition can be obtained. By using a plurality of solutions and separate pumps and a single or multiple ultrasonic nebulizer(s), and varying the individual pumping rates and/or the concentrations of the solutions, a coating of mixed and discontinuously graded (e.g.Type: GrantFiled: January 28, 2002Date of Patent: January 25, 2005Assignee: The Regents of the University of CaliforniaInventors: Ai-Quoc Pham, Robert S. Glass, Tae H. Lee
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Patent number: 6841232Abstract: A reinforced wallboard core is prepared from a slurry comprising a mixture of ?-calcium sulfate hemihydrate, a cellulose ether additive other than CMC and an amount of water that is sufficient to form a slurry and resulting in a wallboard density of less than 0.8 g/cc. The ?-calcium sulfate hemihydrate is hydrated by the water forming a wallboard core reinforced by the cellulose ether additive. The cellulose ether, having a molecular weight of at least about 20,000 and a viscosity grade of at least about 100 cps, is selected to give the reinforced wallboard core improved nail pull resistance and greater flexural strength than unreinforced wallboard of the same density. The reinforced wallboard core may be used for reduced-paper wallboard and/or for lightweight wallboard, for example.Type: GrantFiled: January 23, 2003Date of Patent: January 11, 2005Assignee: Innovative Construction and Building MaterialsInventors: Christopher D. Tagge, Jacob Freas Pollock, Lennard Torres, David S. Soane
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Patent number: 6824866Abstract: Methods are provided for making and using thin films of porous silica substrates to synthesize arrays of polymers. Methods are also provided for assaying such polymers on porous silica substrates. The porous silica substrates offer an increase in array density and signal enhancement over conventional flat glass substrates. Examples of polymers that can be synthesized and assayed include biological polymers such as nucleic acids, polynucleotides, polypeptides, and polysaccharides. Arrays of nucleic acids or polynucleotides can be used for a variety of hybridization-based experiments such as nucleic acid sequence analysis, nucleic acid expression monitoring, nucleic acid mutation detection, speciation, effects of drug therapy on nucleic acid expression, among others.Type: GrantFiled: April 7, 2000Date of Patent: November 30, 2004Assignee: Affymetrix, Inc.Inventors: Marc I. Glazer, Jacqueline A. Fidanza, Glenn McGall, Curtis W. Frank, Richard Vinci
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Patent number: 6777369Abstract: The present invention relates to the effective utilization of a used catalyst containing at least molybdenum, an A element (at least one element selected from the group consisting of phosphorus and arsenic) and an X element (at least one element selected from the group consisting of potassium, rubidium and cesium), and provides a process for producing a catalyst, which comprises dispersing said used catalyst in water, adding thereto an alkali metal compound and/or ammonia solution, adjusting the resulting mixture to pH 6.5 or less to generate a precipitate containing at least molybdenum and the A element, and using the precipitate as a material for catalyst-constituting elements.Type: GrantFiled: November 19, 2001Date of Patent: August 17, 2004Assignee: Mitsubishi Rayon Co., Ltd.Inventors: Toru Kuroda, Seiichi Kawato, Masanori Nitta, Hideyasu Takezawa
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Publication number: 20040146705Abstract: A fluid control device has very fine pores with an average diameter not greater than 10 nm and provides a large flux. The fluid control device comprises an anodized alumina film having fine pores and a silicon based micro-porous film having very fine pores and made from an AlSi mixed film and the fine pores and the very fine pores are at least partly linked with each other. The fluid control device is prepared from a film including at least an aluminum layer and an AlSi mixed film by forming an anodized alumina film having fine pores by way of an anodization process for the aluminum layer part and also forming a silicon based micro-porous film having very fine pores containing silicon as principal ingredient by way of an anodization process or etching process for the AlSi mixed film. The fluid control device can be used as filter or ultrafilter film that allows fluid and gas to pass through it.Type: ApplicationFiled: December 11, 2003Publication date: July 29, 2004Inventors: Tohru Den, Kazuhiko Fukutani
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Publication number: 20040142616Abstract: A flame retardant, electromagnetic interference (EMI) shielding gasket construction. The construction includes a resilient core member formed of a foamed elastomeric material, an electrically-conductive fabric member surrounding the outer surface of the core member, and a flame retardant layer coating at least a portion of the interior surface of the fabric member. The flame retardant layer is effective to afford the gasket construction with a flame class rating of V-0 under Underwriter's Laboratories (UL) Standard No. 94.Type: ApplicationFiled: January 7, 2004Publication date: July 22, 2004Inventors: Michael H. Bunyan, William I. Flanders
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Patent number: 6749931Abstract: A diamond foam article comprises diamond deposited material on a substrate having an open contiguous structure that permits the flow of fluids in at least one direction through the material. Methods for forming a diamond foam article comprise providing a foam substrate; preparing the foam substrate for diamond deposition; and depositing diamond material on the foam substrate by one of several diamond deposition methods.Type: GrantFiled: November 1, 2000Date of Patent: June 15, 2004Assignees: P1 Diamond, Inc., Sun Microsystems, Inc.Inventors: John M. Pinneo, Howard Davidson
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Patent number: 6749930Abstract: A corrosion-resistive member is provided, including a corrosion-resistive face that is exposed to a corrosive gas causing ion bombardmemt. At least a part of the corrosion-resistive member is composed of a sintered silicon nitride body having an open porosity of not more than 5%. The sintered silicon nitride body constitutes the corrosion-resistive face, and if two auxiliary planes are formed by cutting the corrosion-resistive member to intersect vertically with the corrosion-resistive face and to be located vertically with respect to each other, the orientation index between the two auxiliary planes is in a range of 0.8 to 1.2, and the orientation index between the corrosion-resistive face and each of the auxiliary faces is at least 1.5.Type: GrantFiled: October 18, 2001Date of Patent: June 15, 2004Assignee: NGK Insulators, Ltd.Inventor: Tsuneaki Ohashi
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Patent number: 6720066Abstract: The present invention is directed to a process for obtaining a substrate provided with a coating having photocatalytic properties, wherein the coating includes crystallized particles of an oxide of a metal A having photocatalytic properties. The crystallized particles are incorporated into the coating using a mineral binder comprising at least one oxide of a metal B also having photocatalytic properties in the crystallized state. The coating optionally includes at least oxide of a metal M devoid of photocatalytic properties and/or at least one silicon compound of the silicon oxide SiO2 type. The coating is deposited from liquid-phase dispersions containing the crystallized particles of the oxide of metal A and at least one precursor compound for the oxide of metal B of the binder and optionally a precursor compound for the oxide of metal M and for the Si compound, in a relative proportion A/(B+M+Si) by weight of the metals and Si ranging between 60/40 and 40/60.Type: GrantFiled: September 5, 2002Date of Patent: April 13, 2004Assignees: Saint-Gobain Glass France, Rhodia ChimieInventors: Xavier Talpaert, Michel Simonet, Corinne Lehaut, Thierry Chopin, Frédéric Magnin-Feysot
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Publication number: 20040018336Abstract: The present invention is directed to articles of apparel comprising insulating components having insulating structures with low thermal conductivity. Preferred insulating components for use in apparel have an insulating structure comprising a gas impermeable envelope and a porous material contained within the envelope where the insulating structure has a thermal conductivity of less than 25 W/m K.Type: ApplicationFiled: July 29, 2002Publication date: January 29, 2004Inventor: Brian Farnworth
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Patent number: 6670039Abstract: A method of carbonizing cellulose-containing plants is disclosed. Wood is used as a precursor material which is carbonized under controlled temperature and atmosphere conditions to produce a porous carbon product having substantially the same cellular structure as the precursor wood. The porous carbonized wood may be used for various applications such as filters, or may be further processed to form carbon-polymer or carbon-carbon composites. The carbonized wood may also be converted to a ceramic such as silicon carbide. Additional processing may be used to form ceramic-metal or ceramic-ceramic composites.Type: GrantFiled: April 6, 2000Date of Patent: December 30, 2003Inventors: Dennis C. Nagle, Christopher E. Byrne
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Patent number: 6649559Abstract: The invention provides a supported metal membrane which contains a metal membrane on a support surface of a porous membrane support. The supported metal membrane is obtainable by applying the metal membrane to the support surface of the membrane support, wherein the pores in the membrane support are sealed, at least in the region of the support surface, prior to applying the metal membrane and are opened by removing the auxiliary substance only after applying the metal membrane.Type: GrantFiled: July 26, 2001Date of Patent: November 18, 2003Assignee: dmc2 Degussa Metals Catalysts Cerdec AGInventors: Ernst Drost, Werner Kuhn, Meike Roos, Stefan Wieland, Bernd Kempf
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Patent number: 6649255Abstract: An article and method for producing extremely small pore inorganic membranes. The method enables reduction of the pore size of a porous inorganic membrane, such as metal oxides, metal carbides, metal nitrides and cermets. Mean pore diameters of below about 10 Å. Can readily and efficiently be achieved. After the conventional formation of an inorganic membrane, the pore size of the membrane is progressively reduced in a controlled manner to deposit one or more layers of an inorganic compound on the pore walls. This is done by exposing the membrane to the vapor of an inorganic precursor compound. The compound reacts with hydroxyl groups and or absorbed water molecules on the surface of the membrane and is thus bonded to the surface. Water vapor, oxygen, or vapors containing one or more oxygen ligands such as an alcohol are used to hydrolyze the deposited material to the inorganic membrane.Type: GrantFiled: March 4, 1999Date of Patent: November 18, 2003Inventors: Douglas E. Fain, Sr., Bruce B. Marshall, Kenneth D. Adcock, Michael R. Phillips, George E. Roettger
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Publication number: 20030194546Abstract: A composite foam material formed of combined foam that is combined on a mechanical level to obtain hybrid properties.Type: ApplicationFiled: April 11, 2002Publication date: October 16, 2003Inventor: Brock McCabe
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Publication number: 20030175496Abstract: A reaction-bonded &agr;-alumina filter element is provided. The filter element includes a monolith of porous material having multiple passageways extending from one end face to an opposing end face. The monolith is extruded from a mixture containing at least aluminum metal and alumina powders in a proportion such that on sintering the volume change of the monolith is minimized. The filter body can be used as a filter or as a membrane support for crossflow or dead end flow filter elements. A method for making the filter element is also provided.Type: ApplicationFiled: March 13, 2002Publication date: September 18, 2003Inventors: Bruce A. Bishop, Peter J. Hayward, Robert L. Goldsmith, Garry G. Haacke
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Patent number: 6592981Abstract: A lightweight insulating sandwich tile (110) having applications such as spacecraft and reusable launch vehicle thermal protection is disclosed. In one embodiment, the lightweight insulating sandwich tile (110) includes an outer structural facesheet (120) that is bonded or co-cured with an inner insulating core (130). The outer structural facesheet (120) is comprised of carbon-carbon and includes an oxidation resistant layer (140) on an outer surface thereof. The oxidation resistant layer (140) may comprise a coating or surface treatment of, for example, MoSi2, amorphous SiCN, amorphous SiCBN, Ti3SiC2, HfC, HfO2, HfB2, SiC, Ir, and ZrB2. The inner insulating core (130) is comprised of bonded discontinuous carbon fibers, a network of vitreous carbon ligaments, carbon aerogel, or graphite felt or a hybrid combination of these materials.Type: GrantFiled: July 20, 2000Date of Patent: July 15, 2003Assignee: Lockheed Martin CorporationInventors: Suraj P. Rawal, Frank M. Kustas
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Patent number: 6558785Abstract: The present invention discloses an insulated reentry heat shield for minimizing heat transfer to a spacecraft structure or the like during atmospheric reentry. The heat shield (10) comprises an outer heat resistant layer (12) including an ablative first material backed by an inner insulating layer (14) including an insulating second material. The outer and inner layers (12, 14) are bonded to one another by a middle layer (16) disposed therebetween. The middle layer is formed by disposing at least one layer of a phenolic loaded third material between the outer and inner layers and heating all three layers simultaneously to remove phenolic volatiles from the middle layer. In one embodiment, the ablative first material is carbon-carbon, the insulating second material is carbon foam, and the phenolic loaded third material is carbon scrim cloth. The present invention also discloses a method for use in constructing a heat shield.Type: GrantFiled: August 5, 1999Date of Patent: May 6, 2003Assignee: Lockheed Martin CorporationInventors: Suraj Prakash Rawal, Janine M. Thornton, William H. Willcockson
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Tough and durable insulation boards produced in-part with scrap rubber materials and related methods
Publication number: 20030082365Abstract: A composite recovery board (10, 20, 30) comprises a foam core (11) having lower (12) and upper (13) surfaces, wherein the foam core is selected from the group consisting of polyisocyanurate and polyurethane materials and mixtures thereof; and a filler within said foam core selected from the group consisting of rubber-tire vents, EPDM scrap material, plastic chips, polyurethane scrap, polyisocyanurate scrap, scrap rubber from recycled tires, wood chips, fiberglass strands and mixtures thereof. A method of re-roofing a roof comprising applying composite boards (10, 20, 30) of the present invention to a roof deck and applying a weather protective layer over the composite boards. A continuous method of making composite recovery boards (10) of the present invention comprises is also provided.Type: ApplicationFiled: October 30, 2001Publication date: May 1, 2003Inventors: John R. Geary, Bruce F. Douglas, Terence J. O'Connor, Greg A. Brandt, John B. Letts -
Publication number: 20030068485Abstract: An insect resistant extruded or expanded polystyrene foam boards containing from 2 to 25 weight-% acicular particles such as fiberglass, stone wool, metal wool, gypsum, quartz and wollastonite, and insulation panels made from such boards. The fibers are preferably milled or chopped and range in size from 0.0156 inch (0.396 mm) inch to 0.5 inch (12.7 mm) in length and 10 to 20 micrometers in diameter.Type: ApplicationFiled: September 18, 2002Publication date: April 10, 2003Inventor: William J. Ramsey
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Patent number: 6544637Abstract: An inorganic porous material, having uniform pores defined by pore walls of crystalline titanium oxide. The inorganic porous material may be produced by heating an organic inorganic mesostructured material containing titanium and having a hexagonal crystal phase at a temperature and for a period of time sufficient to form a porous material having a multiplicity of pores defined by pore walls containing crystalline titanium oxide.Type: GrantFiled: November 14, 2000Date of Patent: April 8, 2003Assignee: Secretary of Agency of Industrial Science and TechnologyInventor: Katsunori Kosuge
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Publication number: 20030054188Abstract: A composite material has SiC produced by preliminarily sintering a porous body having a coefficient of thermal expansion lower than the coefficient of thermal expansion of copper to construct a network therein, the SiC being impregnated with a copper alloy. The copper alloy comprises copper and one or more additive elements which are prepared to impart a coefficient of thermal conductivity of 160 W/mK or higher to the composite material. The additive elements comprise up to 5% of at least one element selected from Be, Al, Si, Mg, Ti, Ni, Bi, Te, Zn, Pb, Sn, and mish metal, and also contains unavoidable impurities and gas components.Type: ApplicationFiled: September 18, 2002Publication date: March 20, 2003Applicant: NGK Insulators, Ltd.Inventors: Shuhei Ishikawa, Tsutomu Mitsui, Ken Suzuki, Nobuaki Nakayama, Hiroyuki Takeuchi, Seiji Yasui
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Patent number: 6495240Abstract: In conjunction with a so-called patterned medium comprising recording tracks each having an array of unit minute recording portions of a magnetic material separated by non-recording portions of a nonmagnetic material, the invention aims to prevent the recorded information from being disrupted by contact of a magnetic head slider with the medium. The magnetic recording medium of the invention includes recording tracks each having an array of unit minute recording portions (14) of a magnetic material separated by non-recording portions (16) of a nonmagnetic material. The surface height of the unit minute recording portions (14) is set lower than the surface height of the non-recording portions (16).Type: GrantFiled: February 9, 2000Date of Patent: December 17, 2002Assignee: TDK CorporationInventors: Yoshimitsu Wada, Tsutomu Aoyama
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Publication number: 20020187334Abstract: A two-metal TAB tape, double-sided CSP tape, and BGA tape in which the tape has an insulating substrate and wiring layers at least on both sides of the insulating substrate, sprocket holes are made at regular intervals in the longitudinal direction along the edges in the direction of the width, through holes are made in the substrate by punching press, the through holes are filled with conductor by punching press, and the conductor is electrically connected to the wiring layers, characterized in that pilot round holes are made among the sprocket holes made in the longitudinal direction. Methods for producing such two-metal TAB tape, double-sided CSP tape, and BGA tape are disclosed.Type: ApplicationFiled: May 13, 2002Publication date: December 12, 2002Inventors: Akira Ichiryu, Tatsuo Kataoka, Hirokazu Kawamura, Katsuhiko Hayashi, Masahito Ishii
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Publication number: 20020155271Abstract: The present invention provides a method of manufacturing a wiring board, including the steps of preparing a composite sheet having an adherent sheet containing a thermosetting resin adhered to a porous film or impregnated with at least a part thereof, laminating at least the composite sheet on a wiring layer having a wiring pattern formed on an insulating layer, and heating and pressurizing the laminated product thus obtained or heating and pressurizing it after the pressurization to integrate the laminated product. The present invention provides a composite sheet for manufacturing a wiring board which is laminated on a wiring layer having a wiring pattern formed on an insulating layer and is thus used, wherein an adherent sheet containing a thermosetting resin is adhered to a porous film or at least a part thereof is impregnated therein.Type: ApplicationFiled: April 19, 2002Publication date: October 24, 2002Inventors: Toshiyuki Kawashima, Nobuharu Tahara, Kenichi Ikeda
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Patent number: 6465088Abstract: The present invention is directed to a process for obtaining a substrate provided with a coating having photocatalytic properties, wherein the coating includes crystallized particles of an oxide of a metal A having photocatalytic properties. The crystallized particles are incorporated into the coating using a mineral binder comprising at least one oxide of a metal B also having photocatalytic properties in the crystallized state. The coating optionally includes at least oxide of a metal M devoid of photocatalytic properties and/or at least one silicon compound of the silicon oxide SiO2 type. The coating is deposited from liquid-phase dispersions containing the crystallized particles of the oxide of metal A and at least one precursor compound for the oxide of metal B of the binder and optionally a precursor compound for the oxide of metal M and for the Si compound, in a relative proportion A/(B+M+Si) by weight of the metals and Si ranging between 60/40 and 40/60.Type: GrantFiled: September 5, 2000Date of Patent: October 15, 2002Assignee: Saint-Gobain Glass FranceInventors: Xavier Talpaert, Michel Simonet, Corinne Lehaut, Thierry Chopin, Frédéric Magnin-Feysot
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Patent number: 6455145Abstract: This invention intends to provide a friction member which is high in an anti-fading character and low in mate attacking character. For such purpose, in a friction member composed of a fiber containing substrate, a bonding agent and a filling agent, an accumulated blow hole rate of blow holes having hole diameter not less than 3.5 &mgr;m is selected to be not larger than 2 volume %, and an accumulated blow hole rate of blow holes having hole diameter from 0 to 3.5 &mgr;m is selected to be not less than 3 volume %.Type: GrantFiled: March 12, 1999Date of Patent: September 24, 2002Assignees: Aisin Kako Kabushiki Kaisha, Aisin Seiki Kabushiki KaishaInventors: Masahito Mizuno, Osamu Shimase, Katsumi Uemura, Satoshi Narazaki
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Publication number: 20020132105Abstract: An anodized micro-pore aluminum tag bearing indicia thereon wherein the micro-pore anodized aluminum has its micro-pores filled with the cured reside of a composition, which contains silicone resin having pendant groups selected from one or more of methyl groups or phenyl groups. The composition in the micro-pores was cured to a degree effective for marking by blackening thereof with a, e.g., CO2, laser beam, in the form of indicia thereon. The surface of the tag preferably is substantially free of said composition. The method for treating the surface of the anodized micro-pore aluminum tag for forming indicia thereon commences by applying the composition to the surface. Excess of the composition from the surface is removed to leave composition resident in said micro-pores. The composition in the micro-pores then is at least partially cured. A laser then can create the indicia by blackening the composition in the micro-pores.Type: ApplicationFiled: March 19, 2001Publication date: September 19, 2002Inventors: John A. Robertson, Edward S. O'Neal, Ken R. Vaughn, Christopher D. Speakman