Particulate Matter (e.g., Sphere, Flake, Etc.) Patents (Class 428/402)
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Patent number: 10113112Abstract: A method of preparing a core-shell nanorod can include growing a shell of a core-shell nanorod (M1X1)M2X2 in a solution through a slow-injection of M2 precursor solution and X2 precursor solution, wherein the core-shell nanorod includes a M1X1 core.Type: GrantFiled: July 1, 2016Date of Patent: October 30, 2018Assignee: Massachusetts Institute of TechnologyInventors: Igor Coropceanu, Moungi G. Bawendi
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Patent number: 10106419Abstract: A method of dispersing graphene and graphitic nanomaterials uses a multiphase fluid dynamic technique. The method includes a device, incorporating a high intensity fluid dynamics technique, controlling the expansion and compression ratio of the working stream that leads to an effective dispersion of the nanomaterial in the matrix. The condensation of the injected steam creates high intensity and controllable cavitation, leading to effective dispersion of the graphitic nanomaterial. The dispersion is most preferably done in a medium that creates a repulsive potential to balance the attractive inter-graphitic layer potential.Type: GrantFiled: July 15, 2015Date of Patent: October 23, 2018Assignee: GRAPHENE NANOCHEM PLCInventor: Shutesh Krishnan
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Patent number: 10106715Abstract: An abrasive grain is disclosed and may include a body. The body may define a length (l), a height (h), and a width (w). In a particular aspect, the length is greater than or equal to the height and the height is greater than or equal to the width. Further, in a particular aspect, the body may include a primary aspect ratio defined by the ratio of length:height of at least about 2:1. The body may also include an upright orientation probability of at least about 50%.Type: GrantFiled: August 21, 2017Date of Patent: October 23, 2018Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventors: Doruk O. Yener, Jennifer H. Czerepinski, Sujatha Iyengar, Michael D. Kavanaugh, Alan J. Brandes, Christopher Arcona, Ralph Bauer, Yves Boussant-Roux, Tracy H. Panzarella
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Patent number: 10100521Abstract: A roofing granule includes a glass substrate and a plurality of pores in the glass substrate such that the roofing granule has a minimum total solar reflectance of at least 50%.Type: GrantFiled: September 6, 2013Date of Patent: October 16, 2018Assignee: 3M Innovative Properties CompanyInventors: Jean A. Tangeman, Craig W. Lindsay, Kenton D. Budd, Rebecca L. Everman
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Patent number: 10100248Abstract: Semiconductor nanocrystal compositions comprising magnesium containing shells and methods of preparing them are described. The compositions provide strong emission in the blue and green wavelengths as well as chemical and photostability that have not been achieved with conventional shell materials.Type: GrantFiled: September 25, 2015Date of Patent: October 16, 2018Assignee: LIFE TECHNOLOGIES CORPORATIONInventor: Joseph Bartel
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Patent number: 10098833Abstract: The present subject matter includes a product formulation made by the process including the steps of: adding a sufficient amount of water to cover a group of long grain seeds to form a first mixture; adding a sufficient amount of water to cover a group of whole grain seeds to form a second mixture; boiling the first and second mixtures, cooling the first mixture to form a thin colorless liquid; separating any solid seeds from the thin colorless liquid; cooling the second mixture to form an opaque thick liquid; separating any solid seeds from the opaque thick liquid; combining the thin colorless liquid and the opaque thick liquid to form a third mixture; cooling the third mixture to allow the formulation of a film; heating the film to form a porous material; cooling the porous material to form a powder residue; and processing the powder residue to form a formulation. The formulation can be used in various cosmetics, and to treat subject in need of treatment for skin conditions, such as acne.Type: GrantFiled: November 3, 2015Date of Patent: October 16, 2018Inventor: Amelia Vaughn
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Patent number: 10096678Abstract: A coated quantum dot and methods of making coated quantum dots are provided.Type: GrantFiled: May 21, 2014Date of Patent: October 9, 2018Assignee: SAMSUNG ELECTRONICS CO., LTD.Inventors: Craig Breen, Wenhao Liu
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Patent number: 10093842Abstract: A moldable mass contains graphite and a phase change material (PCM). The moldable mass further contains a binder and microcapsules having the PCM. A process produces a molding from the moldable mass, and the molding is used to produce various products such as cooling elements, battery temperature control elements, cooling elements for vehicle cabins, electronic components, and motors.Type: GrantFiled: September 15, 2014Date of Patent: October 9, 2018Assignee: SGL Carbon SEInventors: Dieter Kompalik, Sebastian Goepfert
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Patent number: 10094039Abstract: Low-temperature organometallic nucleation and crystallization-based synthesis methods for the fabrication of semiconductor and metal colloidal nanocrystals with narrow size distributions and tunable, size- and shape-dependent electronic and optical properties. Methods include (1) forming a reaction mixture in a reaction vessel under an inert atmosphere that includes at least one solvent, a cationic precursor, an anionic precursor, and at least a first surface stabilizing ligand while stirring at a temperature in a range from about 50° C. to about 130° C. and (2) growing nanocrystals in the reaction mixture for a period of time while maintaining the temperature, the stirring, and the inert-gas atmosphere.Type: GrantFiled: January 22, 2016Date of Patent: October 9, 2018Assignee: National Science FoundationInventors: Michael Hans Risbud Bartl, JacQueline T. Siy
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Patent number: 10086362Abstract: The present invention relates to a manufacturing method of a super absorbent polymer including: carrying out a thermal polymerization or a photopolymerization of a monomer composition including a water-soluble ethylene-based unsaturated monomer and a polymerization initiator to form a hydrogel polymer; drying the hydrogel polymer; pulverizing the dried polymer; classifying the pulverized polymer into a fine powder having a particle diameter of less than 150 ?m and a polymer having a particle diameter of 150 to 850 ?m according to the particle diameter; performing reassembly to form a fine powder reassembly; and mixing the polymer having a particle diameter of 150 to 850 ?m with the fine powder reassembly, followed by surface cross-linking.Type: GrantFiled: November 1, 2016Date of Patent: October 2, 2018Assignee: LG Chem, Ltd.Inventors: Dong Hyun Kim, Chang Sun Han, Dae Woo Nam
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Patent number: 10084187Abstract: Mixed-metal oxides and lithiated mixed-metal oxides are disclosed that involve compounds according to, respectively, NixMnyCozMe?O? and Lii+?NixMnyCozMe?O?. In these compounds, Me is selected from B, Na, Mg, Al, Si, K, Ca, Sc, Ti, V, Cr, Fe, Cu, Zn, Ga, Ge, Zr, Nb, Mo, Ru, Ag, In, and combinations thereof; 0?x?1; 0?y?1; 0?z<1; x+y+z>0; 0???0.5; and x+y+?>0. For the mixed-metal oxides, 1???5. For the lithiated mixed-metal oxides, ?0.1???1.0 and 1.9???3. The mixed-metal oxides and the lithiated mixed-metal oxides include particles having an average density greater than or equal to 90% of an ideal crystalline density.Type: GrantFiled: November 6, 2017Date of Patent: September 25, 2018Assignee: Apple Inc.Inventors: Hongli Dai, Huiming Wu, Dapeng Wang
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Patent number: 10076870Abstract: A filament guide that guides thermoplastic filament to an object being manufactured. A deposition head comprising the disclosed filament guide provides a filament to the intended deposition point. The filament guide comprises a guide member having a filament groove configured to guide the filament along a path of travel. The groove has an upstream end that is configured to receive the filament from a source and a downstream end that is configured to direct the filament toward the deposition point in the intended direction. A notch at the downstream end of the guide member enables the filament to travel toward the deposition point. The portions of the guide member on either side of the notch act to keep the filament centered laterally. A plate that is transparent to electromagnetic radiation from a heat source covers the groove and permits the electromagnetic radiation to reach the filament while providing added support.Type: GrantFiled: November 30, 2017Date of Patent: September 18, 2018Assignee: Arevo, Inc.Inventors: Zachary Aaron August, Erik Oscar Sunden
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Patent number: 10072202Abstract: The invention relates to compositions for inhibiting the formation of deposits in underground formations such as oil wells, comprising, in a solvent medium, polymers P resulting from the radical copolymerization, preferably controlled and in solution, of a mixture including: monomers having an ethylenically unsaturated structure, selected from monomers that form, by polymerization, a polymer that has an effect of inhibiting the formation of organic and/or inorganic deposits; and polyethylenically unsaturated, cross-linking monomers carrying at least one group that can be cleaved between two ethylene unsaturations, said polymers P being present in the solvent in the form of dispersed nanogels.Type: GrantFiled: July 26, 2013Date of Patent: September 11, 2018Assignee: Rhodia OperationsInventors: Dominique Labarre, James Wilson
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Patent number: 10030144Abstract: Moisture curable elastomer compositions are highly suitable for use as sealants, and initially contain an organopolysiloxane having condensable groups, a tri-acyloxy functional organosilicon compound, and as fillers, anhydrite and silica. The compositions have very low modulus and accommodate high joint movement, while being storage stable.Type: GrantFiled: January 18, 2016Date of Patent: July 24, 2018Assignee: WACKER CHEMIE AGInventors: Torsten Sixt, Franz Neuhauser
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Patent number: 10012630Abstract: A hydrolysis-stable mesoporous silica material has surface bearing functional groups of formula OxSiR4-x, where x is in a range from 1-3 and where each of the radicals R independently of any other contains c carbon atoms, n nitrogen atoms and o oxygen atoms, for which c + n o > 0.35 . At least ? of the nitrogen atoms and of the oxygen atoms carries in each case at least one hydrogen atom or is ionic. At least one radical R of a functional group is crosslinked with another radical R of a different functional group. The material is produced by providing a mesoporous silica material and functionalizing the surface of the mesoporous silica material with at least one silane of formula YxSiR4-x, where x is in a range from 1-3 and where Y is a functional group which reacts with a hydroxyl group on the surface of the mesoporous silica material.Type: GrantFiled: April 14, 2016Date of Patent: July 3, 2018Assignee: Robert Bosch GmbHInventors: Thomas Pilz, Markus Widenmeyer
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Patent number: 10014522Abstract: A cathode material for a lithium-ion secondary battery including cathode active material particles which have central particles made of LixAyMzPO4 (0?x?1.1, 0.8?y?1.1, and 0?z?0.2; here, A represents at least one element selected from the group consisting of Fe, Mn, Co, and Ni, and M represents at least one element selected from the group consisting of Mg, Ca, Co, Sr, Ba, Ti, Zn, B, Al, Ga, In, Si, Ge, and rare earth elements) and a carbonaceous film that coats surfaces of the central particles; and inorganic phosphate salt particles.Type: GrantFiled: September 29, 2016Date of Patent: July 3, 2018Assignee: SUMITOMO OSAKA CEMENT CO., LTD.Inventors: Masataka Oyama, Takao Kitagawa
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Patent number: 9999867Abstract: Disclosed is a composite adsorbent material comprising three components, including a porous media, a hygroscopic material, and graphite flakes. Among the many different possibility considered, it may be advantageous for the porous media to be mesoporous silica or the hygroscopic materials to be calcium chloride, lithium bromide, or lithium chloride. It is considered that the graphite flakes may comprise 50 percent or less of the graphite flake-hygroscopic material composition, and certain embodiments may utilize between 15 and 30 percent graphite in the graphite flake-hygroscopic material composition. It is still further considered that the graphite flakes may advantageously be less than 300 microns in size, or may have an average number of carbon planes that is 100 or less. Additional materials may also be incorporated, including biologics, polymers, and catalysts.Type: GrantFiled: June 29, 2017Date of Patent: June 19, 2018Inventor: Howard Y. Yuh
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Patent number: 10000676Abstract: A method of forming a shaped abrasive particle includes applying a mixture into a shaping assembly within an application zone and directing an ejection material at the mixture in the shaping assembly under a predetermined force, removing the mixture from the shaping assembly and forming a precursor shaped abrasive particle.Type: GrantFiled: May 11, 2017Date of Patent: June 19, 2018Assignee: SAINT-GOBAIN CERAMICS & PLASTICS, INC.Inventors: Ralph Bauer, Martin Barnes, Rene G. Demers, Margaret L. Skowron
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Patent number: 10000690Abstract: The present invention relates to lightweight high strength microsphere containing ceramic particles having controlled microsphere placement and/or size and microsphere morphology, which produces an improved balance of specific gravity and crush strength such that they can be used in applications such as proppants to prop open subterranean formation fractions. Proppant formulations are further disclosed which use one or more microsphere containing ceramic particles of the present invention. Methods to prop open subterranean formation fractions are further disclosed. In addition, other uses for the microsphere containing ceramic particles of the present invention are further disclosed, as well as methods of making the microsphere containing ceramic particles.Type: GrantFiled: May 9, 2016Date of Patent: June 19, 2018Assignee: Halliburton Energy Services, Inc.Inventors: Shanghua Wu, Yuming Xie, Christopher E. Coker, Dilip Chatterjee
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Patent number: 9994445Abstract: This invention describes spherical nanoparticle hydrides and a method for making them. A method of producing spherical nanoparticle hydrides comprises obtaining an electrically conductive or semiconductive wire fabricated from a base material capable of forming a hydride; exposing the wire to a hydrogen-containing processing gas under pressure; vaporizing the wire by electrical discharge, to generate a vapor phase; and reacting with hydrogen and condensing the vapor phase, generating a plurality of spherical nanoparticle hydrides.Type: GrantFiled: July 14, 2016Date of Patent: June 12, 2018Assignee: HRL Laboratories, LLCInventors: John H. Martin, Tobias A. Schaedler, Brennan Yahata
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Patent number: 9994795Abstract: An antifoam granule includes a carrier and an antifoam compound deposited on the carrier. The antifoam granule is formed using a method that includes providing an emulsion and contacting the emulsion with a carrier to deposit the antifoam compound on the carrier and form the antifoam granule. The emulsion includes an oil phase, an aqueous phase, and a silicone polyether. The oil phase includes an antifoam compound. The antifoam compound includes a hydrophobic fluid and a hydrophobic filler dispersed in the hydrophobic fluid. The aqueous phase includes a binder and water. The emulsion is formed using a method that includes combining the oil phase, the aqueous phase, and the silicone polyether to form the emulsion. The antifoam granule is also utilized in a method of facilitating rinsing of a detergent from a substrate that includes applying the detergent, including the antifoam granule, to the substrate and rinsing the substrate.Type: GrantFiled: July 24, 2014Date of Patent: June 12, 2018Assignee: Dow Silicones CorporationInventors: Anick Colson, Laurence Gallez, Christel Manette Simon, Nicolas Ziolkowski
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Patent number: 9988506Abstract: A tetrafluoroethylene (TFE) copolymer film having a first endotherm between about 50° C. and about 300° C., a second endotherm between about 320° C. and about 350° C., and a third endotherm between about 350° C. and about 400° C. is provided. In exemplary embodiments, the third endotherm is approximately 380° C. In some embodiments, the second endotherm is between about 320° C. and about 330° C. or between about 330° C. and about 350° C. TFE copolymer films have a methane permeability less than about 20 ?g*micron/cm2/min. In addition, the dense articles have a void volume of less than about 20%. Methods for dense articles from core shell tetrafluoroethylene copolymers are also provided. The dense articles exhibit improved physical and mechanical properties such as adhesion and barrier properties.Type: GrantFiled: April 4, 2017Date of Patent: June 5, 2018Assignees: W. L. Gore & Associates, Inc., W. L. Gore & Associates GmbHInventors: Lawrence A. Ford, Michael E. Kennedy, Shaofeng Ran, Todd S. Sayler, Gregory J. Shafer
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Patent number: 9988501Abstract: A method of producing polymer particles includes, in a system in which a polymer A and a polymer B are dissolved in and mixed with an organic solvent to undergo phase separation into two phases which are a solution phase containing the polymer A as a major component and a solution phase containing the polymer B as a major component, continuously adding an emulsion including the polymer A, the polymer B and the organic solvent, and a poor solvent for the polymer A to a vessel continuously to allow the polymer A to precipitate; and separating polymer A particles from the vessel continuously.Type: GrantFiled: June 1, 2015Date of Patent: June 5, 2018Assignee: Toray Industries, Inc.Inventors: Yoshinori Kondo, Yuji Echigo, Akira Kitamura, Hiroshi Takezaki
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Patent number: 9982109Abstract: A set of spherical inorganic particles having the particular property of being spontaneously individualized, both in dry state in the form of a powder and when they are dispersed in a matrix. The method for producing the particles, and the materials produced by including the particles in the matrices are also described.Type: GrantFiled: May 7, 2015Date of Patent: May 29, 2018Assignee: PYLOTEInventor: Loic Marchin
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Patent number: 9975804Abstract: The invention provides a method for producing composite nanoparticles, the method using a first compound capable of transitioning from a monoclinic to a tetragonal rutile crystal state upon heating, and having the steps of subjecting the first compound to a hydrothermal synthesis to create anisotropic crystals of the compound; encapsulating the first compound with a second compound to create a core-shell construct; and annealing the construct as needed. Also provided is a device for continuously synthesizing composite nanoparticles, the device having a first precursor supply and a second precursor supply; a mixer to homogeneously combine the first precursor and second precursor to create a liquor; a first microreactor to subject the liquor to hydrothermic conditions to create an\isotropic particles in a continuous operation mode; and a second microreactor for coating the particles with a third precursor to create a core-shell construct.Type: GrantFiled: April 13, 2017Date of Patent: May 22, 2018Assignee: UCHICAGO ARGONNE, LLCInventors: Jie Li, Yugang Sun, Ralph T. Muehleisen, Leah B. Guzowski, Xiaojie Yan, Samuel Dull, Ioannina Castano
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Patent number: 9975779Abstract: A CVD-SiC formed body has low light transmittance and high resistivity, and may suitably be used as a member for an etcher that is used for a semiconductor production process, for example. The SiC formed body is formed using a CVD method, and includes 1 to 30 mass ppm of boron atoms, and more than 100 mass ppm and 1000 mass ppm or less of nitrogen atoms. The SiC formed body preferably has a resistivity of more than 10 ?·cm and 100,000 ?·cm or less, and a light transmittance at a wavelength of 950 nm of 0 to 1%.Type: GrantFiled: September 13, 2012Date of Patent: May 22, 2018Assignee: TOKAI CARBON CO., LTD.Inventors: Takaomi Sugihara, Masaaki Asakura, Takeshi Tokunaga, Tetsuya Sadaki
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Patent number: 9976390Abstract: A method of drilling a wellbore in a subterranean formation comprises circulating a water-based or oil-based drilling fluid in the subterranean formation; the water-based or oil-based drilling fluid comprising a carrier, and a superabsorbent polymer present in an amount effective to reduce fluid leakoff during the drilling operation, the superabsorbent polymer comprising crosslinks formed before the superabsorbent polymer is combined with the carrier.Type: GrantFiled: March 29, 2016Date of Patent: May 22, 2018Assignee: BAKER HUGHES, A GE COMPANY, LLCInventor: Scott Gregory Nelson
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Patent number: 9969943Abstract: A method of treating crude oil comprising depleting the content of aromatic hydrocarbons comprising contacting the crude oil with super-paramagnetic or paramagnetic nanoparticles comprising chemical functional groups. The method increases the API gravity of crude oil and reduces the viscosity of said oil. Oil can be depleted in its content of sulphur-containing aromatics using functionalized nanoparticles.Type: GrantFiled: September 30, 2014Date of Patent: May 15, 2018Assignee: MAERSK OLIE OG GAS A/SInventors: Martin Vad Bennetzen, Kristian Mogensen
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Patent number: 9969874Abstract: The present invention relates to: a polymer particle in which a urethane resin (A1) and an acrylic polymer (B1) are included in a single particle, said polymer particle having a gel fraction of 10% or more as measured using N,N-dimethylformamide (DMF) as a solvent; a polymer particle in which a urethane resin (A2) having a sulfonic acid group and an acrylic polymer (B2) are included in a single particle, said polymer particle having a surface acid value of 0.1 to 19 mgKOH/g as measured by a potentiometric titration method; and a method for producing a polymer dispersion. According to the present invention, it becomes possible to provide: a polymer dispersion which has excellent polymerization stability and can have an excellent coating viscosity property and excellent storage stability when used in a coating material; a method for producing the polymer dispersion; and a polymer particle contained in the polymer dispersion.Type: GrantFiled: February 14, 2014Date of Patent: May 15, 2018Assignees: Mitsubishi Chemical Corporation, Japan Coating Resin CorporationInventors: Naohiro Kosugi, Shinya Yamato, Junichi Nakamura, Motomi Tanaka, Masashi Torisaki
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Patent number: 9971263Abstract: Provided is a toner having a toner particle that contains a binder resin and a magnetic particle, wherein the magnetic particle satisfies the following stipulations (i) to (iii): (i) the magnetic particle has a prescribed shape and has a protruded portion on a plane portion thereof, (ii) the magnetic particle has a core particle that contains magnetite and has a coating layer, and (iii) the coating layer contains an iron-containing oxide and at least one of a silicon-containing oxide and an aluminum-containing oxide. In a molecular weight distribution measured on the tetrahydrofuran-soluble matter of the toner, the ratio (Mw/Mn) of a weight-average molecular weight to a number-average molecular weight is at least 10.0.Type: GrantFiled: December 29, 2016Date of Patent: May 15, 2018Assignee: CANON KABUSHIKI KAISHAInventors: Kosuke Fukudome, Shuhei Moribe, Koji Nishikawa, Daisuke Yoshiba, Shotaro Nomura, Atsuhiko Ohmori, Sho Kimura, Katsuhisa Yamazaki
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Patent number: 9972451Abstract: A new multifunctional polyelectrolyte, particularly suitable for a solid-state supercapacitor, is obtainable or obtained by reacting an effective amount of vinyl hybrid silica nanoparticles (VSNPs) and a compound having a structural unit based on acrylic acid or a structural unit derived therefrom in the presence of a polymerization initiator. The polyelectrolyte allows for an advantageous tunable ionic conductivity, exceptional self-healability and super-stretchability. An energy storage device, in particular a solid-state supercapacitor, includes the polyelectrolyte. A method for manufacturing a solid-state supercapacitor as well as for repairing a solid-state supercapacitor having cracks is also disclosed. Benefiting from the superior properties of the polyelectrolyte, the energy storage devices based thereon exhibit highly advantageous stretchability and self-healability and an exceptional performance compared to conventionally known devices.Type: GrantFiled: November 30, 2015Date of Patent: May 15, 2018Assignee: City University of Hong KongInventors: Chunyi Zhi, Yan Huang
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Patent number: 9963526Abstract: Some embodiments herein disclose a process for producing an ethylene polymer or copolymer which contains less than 5 ppm titanium and has a bulk density, in granular form, of at least 22.5 lbs/ft3, using a spheroidal Ziegler-Natta type olefin polymerization catalyst having a particle size distribution characterized by a Dm*/Dn of less than 3.0 and comprising a titanium compound, an aluminum compound, and a spheroidal magnesium chloride support.Type: GrantFiled: April 25, 2016Date of Patent: May 8, 2018Assignee: NOVA Chemicals (International) S.A.Inventors: Qinyan Wang, Savini Udara Suduweli Kondage, Mark Kelly, Amy Marie Baltimore, Jessamyn Ross Logan, Tyler Craig
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Patent number: 9952153Abstract: A method for the transformation of material (e.g. plastic material) into an optically modulating state via laser radiation is described. The optically modulating state may be a state in which light is emitted at a different wavelength than it is absorbed. The plastic material to may be a thermoplastic or elastomeric material, or an organic polymer selected from the group consisting of polyethylene, polypropylene, polystyrene, polycarbonate and polycycloolefin. The laser radiation may comprise the application of an amount of energy of about 0.1 nJoule/?m2 to about 100 ?Joule/?m2 and/or may comprise a radiation of a wavelength of about 355 nm to about 1064 nm. The optically modulating state of the plastic material may absorb light in a wavelength spectrum of about 380 nm to about 540 nm and/or a wavelength spectrum of about 635 nm to about 655 nm. The optically modulating state of the plastic material may emit light in a wavelength spectrum of about 550 nm to about 800 nm.Type: GrantFiled: December 2, 2011Date of Patent: April 24, 2018Assignee: ALERE TECHNOLOGIES GMBHInventors: Torsten Schulz, Daniel Weicherding
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Patent number: 9944813Abstract: The present invention relates to a metal nanoplate, a method for manufacturing same, and a conductive ink composition and a conductive film comprising metal nanoplate. The metal nanoplate does not require application of a high temperature and high pressure and thus can be easily manufactured at a low temperature and at normal pressure, and a conductive film or a conductive pattern, among others, having excellent conductivity can be formed even when the conductive ink composition comprising the metal nanoplate is printed on a substrate and then heat-treated or dried at a low temperature. As a result, the metal nanoplate and the conductive ink composition comprising same can be very appropriately applied to various semiconductor elements, display devices, or when forming a conductive pattern or a conductive film for a solar cell in an environment requiring low-temperature firing.Type: GrantFiled: June 12, 2014Date of Patent: April 17, 2018Assignee: LG Chem, Ltd.Inventors: Won Jong Kwon, Se-Ho Park, Sung-Ho Yoon, Yeo-Jin Jeon
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Patent number: 9944594Abstract: The invention relates to a catalyst comprising an active component based on molybdenum and on potassium and a support based on hydroxyapatite, and also to a process for preparing said catalyst and a process for producing methyl mercaptan in a catalytic process by reaction of carbon monoxide, sulphur and/or hydrogen sulphide and hydrogen, comprising the use of said catalyst.Type: GrantFiled: March 28, 2014Date of Patent: April 17, 2018Assignee: ARKEMA FRANCEInventors: Georges Fremy, Patrice Barre, Karine Sanchou, Alexia Cordova, Carole Lamonier, Pascal Blanchard
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Patent number: 9937470Abstract: The present invention provides a method for producing particles having a reduced particle size distribution, which method comprises the steps of: a) providing a composition comprising particles; b) subjecting the particles in said composition to a size reduction step or to a size growth step; c) feeding said particles to a first membrane separation system to separate said particles according to size; d) recycling those particles that do not meet the size criteria back to step a); e) optionally, collecting in a collection tank the permeate of the first membrane separation system. Particles obtainable according to the method of the invention and characterized by having a near monodisperse particle size distribution are also provided. The particles are preferably characterized by having a particle size distribution with a span of less than 2.0. The invention also provides pharmaceutical compositions comprising particles according to the invention, and also apparatus for carrying out the method of the invention.Type: GrantFiled: March 28, 2013Date of Patent: April 10, 2018Assignee: Hovione International LtdInventors: Jośe Luis Santos, Filipe Gaspar
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Patent number: 9935310Abstract: Providing a silicon-containing material having a novel structure being distinct from the structure of conventional silicon oxide disproportionated to use. A silicon-containing material according to the present invention includes at least the following: a continuous phase including silicon with Si—Si bond, and possessing a bubble-shaped skeleton being continuous three-dimensionally; and a dispersion phase including silicon with Si—O bond, and involved in an area demarcated by said continuous phase to be in a dispersed state.Type: GrantFiled: June 25, 2013Date of Patent: April 3, 2018Assignee: KABUSHIKI KAISHA TOYOTA JIDOSHOKKIInventors: Yoshihiro Nakagaki, Nobuhiro Goda, Manabu Miyoshi, Yushi Kondo, Kensuke Yotsumoto
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Patent number: 9931735Abstract: A method of fabricating a diamond compact includes functionalizing surfaces of diamond nanoparticles with fluorine; combining the functionalized diamond nanoparticles with a non-group-VIII metal to form a particle mixture; and subjecting the particle mixture to high pressure and high temperature (HPHT) conditions to form inter-granular bonds between the diamond nanoparticles. A cutting element for an earth-boring tool includes a plurality of grains of diamond material; a plurality of diamond nanoparticles bonded to the plurality of grains of diamond material; and a non-group-VIII metal fluoride disposed within interstitial spaces between the grains of diamond material and the plurality of diamond nanoparticles. The cutting element is substantially free of a metal-solvent catalyst.Type: GrantFiled: January 25, 2016Date of Patent: April 3, 2018Assignee: Baker Hughes, a GE company, LLCInventors: Valery N. Khabashesku, Vladimir P. Filonenko
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Patent number: 9926649Abstract: Disclosed is a method of: providing a mixture of a polymer or a resin and a transition metal compound, producing a fiber from the mixture, and heating the fiber under conditions effective to form a carbon nanotube-containing carbonaceous fiber. The polymer or resin is an aromatic polymer or a precursor thereof and the mixture is a neat mixture or is combined with a solvent. Also disclosed are a carbonaceous fiber or carbonaceous nanofiber sheet having at least 15 wt. % carbon nanotubes, a fiber or nanofiber sheet having the a polymer or a resin and the transition metal compound, and a fiber or nanofiber sheet having an aromatic polymer and metal nanoparticles.Type: GrantFiled: January 19, 2016Date of Patent: March 27, 2018Assignee: The United States of America, as represent by the Secretary of the NavyInventors: Teddy M. Keller, Matthew Laskoski
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Patent number: 9914827Abstract: The present invention relates to a concentrated polymeric composition which comprises: a) vinyl aromatic polymers and/or copolymers in an amount ranging from 10% to 90% by weight, calculated with respect to the overall composition, with respect to the overall composition, b) at least one compound containing epoxy functional groups in an amount ranging from 0.01% to 5% by weight, calculated with respect to the overall composition, with respect to the overall composition, c) at least one infrared absorbing agent, in an amount ranging from 10% to 90% by weight, calculated with respect to the overall composition, with respect to the overall composition.Type: GrantFiled: October 17, 2013Date of Patent: March 13, 2018Assignee: Versalis S.p.A.Inventors: Antonio Ponticiello, Attilio Arienti, Francesco Pasquali
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Patent number: 9914666Abstract: A nanoheterostructure includes a first inorganic component and a second inorganic component one of which is a matrix, and the other of which is three-dimensionally and periodically arranged in the matrix, and has a three-dimensional periodic structure whose average value of one unit length of a repeated structure is 1 nm to 100 nm.Type: GrantFiled: September 9, 2015Date of Patent: March 13, 2018Assignee: KABUSHIKI KAISHA TOYOTA CHUO KENKYUSHOInventors: Hiroaki Wakayama, Hirotaka Yonekura, Hiromitsu Tanaka
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Patent number: 9916917Abstract: Methods for mixing nylon compounds and compositions useful in mixing nylon compounds are provided. The methods and compositions disclosed are useful in producing nylon for wire and cable jacketing. The disclosed methods provide nylon having a reduced heat history compared to traditional methods. The disclosed methods and composition provide additional mixing capacity by reducing the amount of nylon that must be incorporated with additives per unit of final nylon composition. The disclosed methods and compositions provide the ability to select from a plurality of additive concentration levels in the final product by varying the ratio of a masterbatch compound containing a high concentration of the additive to a resin containing a low concentration or no additive.Type: GrantFiled: March 1, 2016Date of Patent: March 13, 2018Assignee: ADVANSIX RESINS & CHEMICALS LLCInventors: John V. Facinelli, Clark V. Brown, David J. Loy, Robert A. Houck, Jr., Dana A. Germain
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Patent number: 9909053Abstract: Embodiments of a polymer composition are disclosed for use in enhancing the production of oil from a formation. In one embodiment, the composition includes a powder polymer having an average molecular weight of 0.5 to 30 Million Daltons suspended in a water soluble solvent having an HLB of greater than or equal to 8 and selected from the group of surfactants, glycol ethers, alcohols, co-solvents, and mixtures thereof, at a weight ratio of powder polymer to water soluble solvent ranging from 20:80 to 80:20. The polymer composition is substantially anhydrous. The polymer composition is hydrated in an aqueous fluid for an injection solution in less than or equal to 4 hours containing a polymer concentration ranging from 100 ppm to 50,000 ppm and having a filter ratio of less than or equal to 1.5 at 15 psi using a 1.2 ?m filter.Type: GrantFiled: October 29, 2015Date of Patent: March 6, 2018Assignee: CHEVRON U.S.A. INC.Inventors: Varadarajan Dwarakanath, Robert M. Dean, Do Hoon Kim, Dennis Arun Alexis, Sophany Thach, Taimur Malik, Anette Poulsen, Sumitra Subrahmanyan
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Patent number: 9902446Abstract: An amorphous robot includes a compartmented bladder containing fluid, a valve assembly, and an outer layer encapsulating the bladder and valve assembly. The valve assembly draws fluid from a compartment(s) and discharges the drawn fluid into a designated compartment to displace the designated compartment with respect to the surface. Another embodiment includes elements each having a variable property, an outer layer that encapsulates the elements, and a control unit. The control unit energizes a designated element to change its variable property, thereby moving the designated element. The elements may be electromagnetic spheres with a variable polarity or shape memory polymers with changing shape and/or size. Yet another embodiment includes an elongated flexible tube filled with ferrofluid, a moveable electromagnet, an actuator, and a control unit. The control unit energizes the electromagnet and moves the electromagnet via the actuator to magnetize the ferrofluid and lengthen the flexible tube.Type: GrantFiled: January 4, 2016Date of Patent: February 27, 2018Assignee: THE UNITED STATES OF AMERICA AS REPRESENTED BY THE ADMINISTRATOR OF NASAInventor: Arthur T. Bradley
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Patent number: 9902894Abstract: A method for making a polymer suspension for use in enhancing the production of oil from a formation is disclosed. In one embodiment, the method comprises mixing a powder polymer having an average molecular weight of 0.5 to 30 Million Daltons into a water soluble solvent having an HLB of greater than or equal to 8 for less than or equal to 24 hours. The water soluble solvent is selected from a group, at a weight ratio from 20:80 to 80:20. The polymer suspension is stable, pumpable, and substantially anhydrous; and it is hydrated for an injection solution in less than or equal to 4 hours, containing a polymer concentration ranging from 100 ppm to 50,000 ppm and having a filter ratio of less than or equal to 1.5 at 15 psi using a 1.2 ?m filter, by mixing a sufficient amount of the polymer suspension in an aqueous fluid.Type: GrantFiled: October 29, 2015Date of Patent: February 27, 2018Assignee: CHEVRON U.S.A. INC.Inventors: Varadarajan Dwarakanath, Robert M. Dean, Do Hoon Kim, Dennis Arun Alexis, Sophany Thach, Taimur Malik, Anette Poulsen, Sumitra Subrahmanyan
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Patent number: 9902895Abstract: An injection solution for injecting into a subterranean reservoir to enhance production and recovery of oil from the reservoir is disclosed. In one embodiment, the injection solution is prepared by mixing a sufficient amount of a pumpable, stable and substantially anhydrous polymer suspension in an aqueous fluid for the polymer to be hydrated in less than or equal to 4 hours, resulting in the injection solution containing a polymer concentration ranging from 100 ppm to 50,000 ppm. The injection solution has a filter ratio of less than or equal to 1.5 at 15 psi using a 1.2 ?m filter. The polymer suspension comprises a powder polymer having an average molecular weight of 0.5 to 30 Million Daltons suspended in a water soluble solvent having an HLB of greater than or equal to 8 and selected from a group, at a weight ratio from 20:80 to 80:20.Type: GrantFiled: October 29, 2015Date of Patent: February 27, 2018Assignee: CHEVRON U.S.A. INC.Inventors: Varadarajan Dwarakanath, Robert M. Dean, Do Hoon Kim, Dennis Arun Alexis, Sophany Thach, Taimur Malik, Anette Poulsen, Sumitra Subrahmanyan
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Patent number: 9896342Abstract: A method of synthesizing nanostructures from agro-waste can include providing powdered Phoenix dactylifera agro-waste; mixing the powdered Phoenix dactylifera agro-waste with a liquid to provide a Phoenix dactylifera agro-waste solution; heating the Phoenix dactylifera agro-waste solution in a hydrothermal autoclave to provide a heated solution; and centrifuging the heated solution to provide a liquid fraction and a solid fraction. The liquid fraction can include a first plurality of nanostructures. The first plurality of nanostructures can include C-dots. The solid fraction can be further processed to provide a second plurality of nanostructures and a third plurality of nanostructures. The second plurality of nanostructures can include lignin nanoparticles. The third plurality of nanostructures can include cellulose nanocrystals. The nanostructures can be used in various applications, such as three dimensional cell culture, UV-protecting textiles, and bio-imaging.Type: GrantFiled: September 27, 2017Date of Patent: February 20, 2018Assignee: KING SAUD UNIVERSITYInventors: Ali Abdullah Alshatwi, Jegan Athinarayanan, Periasamy Vaiyapuri Subbarayan
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Patent number: 9895842Abstract: A three-dimensional object is manufactured by selective sintering by means of electromagnetic radiation, wherein the powder comprises a polymer or copolymer having at least one of the following structural characteristics: (i) at least one branching group in the backbone chain of the polymer or copolymer, provided that in case of the use of polyaryletherketones (PAEK) the branching group is an aromatic structural unit in the backbone chain of the polymer or copolymer; (ii) modification of at least one end group of the backbone chain of the polymer or copolymer; (iii) at least one bulky group within the backbone chain of the polymer of copolymer, provided that in case of the use of polyaryletherketones (PAEK) the bulky group is not selected from the group consisting of phenylene, biphenylene, naphthalene and CH2— or isopropylidene-linked aromatics; (iv) at least one aromatic group non-linearly linking the backbone chain.Type: GrantFiled: May 18, 2009Date of Patent: February 20, 2018Assignee: EOS GmbH Electro Optical SystemsInventors: Andreas Pfister, Frank Mueller, Martin Leuterer
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Patent number: 9896617Abstract: A method of enhancing oil recovery in a subterranean reservoir is disclosed. In one embodiment, the method comprises providing a wellbore and a polymer suspension. The polymer suspension comprises a powder polymer having an average molecular weight of 0.5 to 30 Million Daltons suspended in a water soluble solvent having an HLB of greater than or equal to 8 and selected from a group, at a weight ratio of 20:80 to 80:20. The method comprises providing an aqueous fluid, mixing a sufficient amount of the polymer suspension in the aqueous fluid for the polymer to be hydrated resulting an injection solution in less than or equal to 4 hours, and injecting the injection solution into the wellbore. The injection solution contains a polymer concentration ranging from 100 ppm to 50,000 ppm and has a filter ratio of less than 1.5 at 15 psi using a 1.2 ?m filter.Type: GrantFiled: October 29, 2015Date of Patent: February 20, 2018Assignee: CHEVRON U.S.A. INC.Inventors: Varadarajan Dwarakanath, Robert M. Dean, Do Hoon Kim, Dennis Arun Alexis, Sophany Thach, Taimur Malik, Anette Poulsen, Sumitra Subrahmanyan
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Patent number: 9879127Abstract: Disclosed is a semiaromatic polyamide resin composition including a semiaromatic polyamide (A), a phosphorus-based flame retardant (B) and an inorganic aluminum compound (C), wherein the mass ratio (A/B) between (A) and (B) is 50/50 to 95/5; the amount of the inorganic aluminum compound (C) is 0.1 to 20 parts by mass in relation to 100 parts by mass of the total amount of (A) and (B); (A) is constituted with an aromatic dicarboxylic acid component, an aliphatic diamine component and a monocarboxylic acid component; and the content of the monocarboxylic acid component is 0.3 to 4.0 mol % in relation to the whole monomer components constituting (A).Type: GrantFiled: March 19, 2014Date of Patent: January 30, 2018Assignee: UNITIKA LTD.Inventors: Junichi Mii, Yutaka Taketani, Taiyo Amari, Hiroo Kamikawa, Yohei Kabashima