Carboxylic Acid Or Ester Compound Adjuvant Patents (Class 430/108.4)
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Publication number: 20130171552Abstract: The present invention provides a toner showing an excellent fixing property even in high-speed image formation and inhibiting contamination of the inside of an apparatus and thereby being capable of stably forming high-quality images not having unevenness of gloss over a long period of time. In the toner including toner particles containing a binder resin, an ester wax, and a coloring agent, the ester wax is prescribed by, in GC/MS analysis of components volatilized by heating the wax at 200° C. for 10 minutes, a relationship in the components having carbon atoms in specific ranges.Type: ApplicationFiled: September 6, 2011Publication date: July 4, 2013Applicant: CANON KABUSHIKI KAISHAInventors: Kazumi Yoshizaki, Yasushi Katsuta, Kenichi Nakayama, Takeshi Kaburagi, Hideki Kaneko
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Publication number: 20130164669Abstract: A toner including a binder resin containing an ester bond, and a releasing agent, wherein the releasing agent includes first C30-C50 alkyl monoester compound and second C30-C50 alkyl monoester compound, wherein the number of carbon atoms of the first C30-C50 alkyl monoester compound is different from that of the second C30-C50 alkyl monoester compound, wherein the amount of the first C30-C50 alkyl monoester compound is largest and the amount of the second C30-C50 alkyl monoester compound is second largest or same as the amount of the first C3OC50 alkyl monoester compound, wherein the amount of the first C30-C50 alkyl monoester compound is 30% by mass or more but less than 50% by mass to the releasing agent, and wherein the amount of the second C30-C50 alkyl monoester compound is 10% by mass or more but less than 50% by mass to the releasing agent.Type: ApplicationFiled: August 18, 2011Publication date: June 27, 2013Inventors: Hiroshi Yamashita, Yuichi Shirasu, Tomoki Murayama, Masaki Watanabe
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Publication number: 20130157185Abstract: A toner includes a binder resin, a coloring agent, and a releasing agent containing two or more kinds of alkyl monoester compounds having a different number of carbon atoms in a range of from 30 to 50 carbon atoms. The toner has a crystallinity of 10% or more as measured by x-ray diffraction and/or the binder resin is a crystalline resin in an amount of 50% by weight or more of the binder resin. The two or more kinds of alkyl monoester compounds include a component A accounting for the largest amount ranging from 30% by weight to less than 50% by weight of the releasing agent and a component B accounting for the second largest amount ranging from 10% by weight to less than 50% by weight of the releasing agent.Type: ApplicationFiled: December 5, 2012Publication date: June 20, 2013Inventors: Shingo SAKASHITA, Hiroshi Yamashita, Masahide Yamada, Shinya Nakayama, Atsushi Yamamoto, Yukiko Nakajima
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Publication number: 20130157187Abstract: The disclosure describes a pigment treated with a rosin and a toner particle containing that rosin-treated pigment particle. The toner has a lower level of dielectric loss.Type: ApplicationFiled: December 14, 2011Publication date: June 20, 2013Applicant: Xerox CorporationInventors: Ke Zhou, Rina Carlini, Daryl W. Vanbesien, Cuong Vong, Karen A. Moffat, Richard P.N. Veregin
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Patent number: 8460845Abstract: Provided is a cyan toner which, while being a capsule-type toner having excellent low-temperature fixability, has excellent offset resistance and charging performance and can obtain high-quality images. A cyan toner having at least a resin (a) having a polyester as a main component, a colorant, and a wax, in which glass transition temperatures (° C.) Tg(0.5) and Tg(4.0) obtained at a rate of temperature increase of 0.5° C./min or 4.0° C./min satisfy 40.0?Tg(0.5)?60.0 and 2.0?Tg(4.0)?Tg(0.5)?10.0, and wherein, when the concentration of the cyan toner in an ethyl acetate dispersion is Cc1 (mg/ml), and the light absorbance at a wavelength of 712 nm of the dispersion is A(ethyl acetate)712, A(ethyl acetate)712/Cc1<0.15 is satisfied, and wherein, when the concentration of the cyan toner in a chloroform solution is Cc2 (mg/ml), and the light absorbance at a wavelength of 712 nm of the solution is A(chloroform)712, 2.00<A(chloroform)712/Cc2<8.15 is satisfied.Type: GrantFiled: November 12, 2009Date of Patent: June 11, 2013Assignee: Canon Kabushiki KaishaInventors: Takaaki Kaya, Ayako Sekikawa, Ryoichi Fujita, Shigeto Tamura, Makoto Kambayashi
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Patent number: 8426097Abstract: An electrophotographic toner including a latex, a coloring agent, and a release agent, wherein a difference between an average circularity of toner having a particle size of D16p or less (S16) and an average circularity of toner having a particle size of D50p or less (S50) is about 0.01 or less, wherein the circularity is measured using a flow particle image analyzer (FPIA), and the ratio of an area of wax to a total cross-sectional area of the toner having a particle size of D16p or less is about 8/100 or greater, and wherein the area is measured using a transmission electron microscope (TEM).Type: GrantFiled: December 3, 2009Date of Patent: April 23, 2013Assignee: Samsung Electronics Co., Ltd.Inventors: Yo-da Shin, Jun-young Lee, Jae-hwan Kim, Tae-hoe Koo
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Publication number: 20130071783Abstract: According to an embodiment, provided is a developer, which is used for a full-color image forming apparatus, wherein the developer includes a monochrome toner and a color toner, each including a coloring material, an amorphous polyester resin, a crystalline polyester resin, and an ester wax which includes ester compounds having an alkyl group and also having a carbon number of from 32 to 48, the amorphous polyester resin to be blended in the monochrome toner has a melting point (Tm2) of from 140 to 155° C. and the amorphous polyester resin to be blended in the color toner has a melting point (Tm1) of from 115 to 130° C., and the Tm1 and the Tm2 satisfy the following formula (1): 10(° C.)?Tm2?Tm1?40(° C.).Type: ApplicationFiled: September 6, 2012Publication date: March 21, 2013Applicants: TOSHIBA TEC KABUSHIKI KAISHA, KABUSHIKI KAISHA TOSHIBAInventor: Koichi Kuroyama
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Publication number: 20130065174Abstract: An object of the present invention is to provide a toner in which a charging amount and rise of the charging amount are hardly influenced by change in a temperature and humidity environment, and pigment dispersibility is high in order to provide an image output having high transparency, color mixing properties, and color nuance stability.Type: ApplicationFiled: September 5, 2012Publication date: March 14, 2013Applicant: CANON KABUSHIKI KAISHAInventors: Hitoshi Itabashi, Takashi Kenmoku, Akane Masumoto
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Publication number: 20130059245Abstract: The present invention relates to a polymerized toner and a method for preparing the same, wherein the toner can realize an excellent offset feature, high transfer efficiency, and a uniform image and thus can exhibit excellent performances in the applications of high speed copying, development of transferred photos, etc.Type: ApplicationFiled: February 22, 2011Publication date: March 7, 2013Applicant: LG CHEM, LTD.Inventors: Wook Jang, Hak-Soo Kim, Chang-Soon Lee
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Publication number: 20130052578Abstract: A toner for electrostatic latent image development includes at least a binder resin, a colorant, a charge control agent, and a release agent. The release agent contains a synthetic ester wax and a natural ester wax. When a toner sample is measured by a differential scanning calorimeter in a way that the toner sample is heated from 30° C. to 170° C. at a rate of 10° C./min followed by cooling to 30° C. at a rate of 10° C./min and is then re-heated from 30° C. to 170° C. at a rate of 10° C./min, a fusion-starting temperature TB, a lower endothermic peak temperature T1 derived from one ester wax, an intermediate endothermic peak temperature T2, and a higher endothermic peak temperature T3 derived from another ester wax are respectively a certain temperature, and are observed during the re-heating.Type: ApplicationFiled: August 28, 2012Publication date: February 28, 2013Applicant: KYOCERA DOCUMENT SOLUTIONS INC.Inventor: Masanori Sugahara
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Patent number: 8383307Abstract: The toner includes a binder resin; a release agent; a colorant; and a dispersing resin configured to disperse the release agent. The dispersing resin includes a polyhydroxycarboxylic acid unit obtained from an optically active monomer. The polyhydroxycarboxylic acid unit has an optical purity of not greater than 80%, wherein the optical purity is defined as the absolute value of difference between the mole percentage of a L-monomer in the optically active monomer and the mole percentage of a D-monomer in the optically active monomer.Type: GrantFiled: October 8, 2009Date of Patent: February 26, 2013Assignee: Ricoh Company, LimitedInventors: Ryota Inoue, Akihiro Kotsugai, Toyoshi Sawada, Akiyoshi Sabu
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Patent number: 8383311Abstract: A toner composition that includes at least one low molecular weight amorphous polyester resin, at least one high molecular weight amorphous polyester resin, at least one crystalline polyester resin, at least one wax, at least one biocide and at least one colorant, and wherein the toner composition has a minimum fusing temperature of from about 100° C. to about 125° C.Type: GrantFiled: October 8, 2009Date of Patent: February 26, 2013Assignee: Xerox CorporationInventors: Chieh-Min Cheng, Zhen Lai, Zhaoyang Ou, Dennis A. Mattison, Jr., Phil Dale, Christopher D. Blair, Steven M. Malachowski, Ryan Accetta
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Patent number: 8367289Abstract: A toner is provided which is excellent in development stability in both a low-temperature, low-humidity environment and a high-temperature, high-humidity environment over a long time period. The toner includes toner particles containing at least a binder resin and a colorant, and a fatty acid metal salt. The fatty acid metal salt has a volume-based median diameter (D50s) of 0.15 ?m or more and 0.65 ?m or less, and the liberation ratio of the fatty acid metal salt in the toner is 1.0% or more and 25.0% or less.Type: GrantFiled: February 24, 2009Date of Patent: February 5, 2013Assignee: Canon Kabushiki KaishaInventors: Naoya Isono, Satoshi Handa, Katsuyuki Nonaka, Koji Abe, Yasuhiro Hashimoto, Akira Sugiyama, Yuhei Terui
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Publication number: 20130029261Abstract: The present invention relates to a polymerized toner prepared by suspension polymerization. In particular, the polymerized toner comprises a plurality of toner particles that each comprising a binder resin, a pigment, a pigment stabilizer, a charge control agent, and a wax. The polymerized toner maintains a ratio of toner particles containing at least two wax domains per particle within a defined range. Thereby, the polymerized toner achieves high glossiness and good transfer efficiency.Type: ApplicationFiled: July 26, 2012Publication date: January 31, 2013Applicant: LG CHEM, LTD.Inventors: Wook JANG, Chang-Soon LEE, Woo-Cheul JUNG, Joo-Yong PARK
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Publication number: 20130029259Abstract: A developer for electrostatic latent image development including a positively chargeable toner and a fatty acid metal salt is used, in which the fatty acid metal salt is a metal salt selected from the group consisting of zinc, calcium, and magnesium salts of fatty acids of 12 to 20 carbon atoms and has a certain volume average particle diameter and particle size distribution.Type: ApplicationFiled: July 20, 2012Publication date: January 31, 2013Applicant: KYOCERA DOCUMENT SOLUTIONS INC.Inventors: Masami Tujihiro, Yukinori Nakayama
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Patent number: 8361688Abstract: Disclosed is a toner including: a resin; coloring agent and release agent including compound or compounds represented by the following general formula (1): R1—(COO—R2)n, wherein R1 is a linking group having carbon number of 2 to 8 which may be a cyclic structure and may have a hydroxy group or fatty acid ester group; and each R2 is an alkyl group having carbon number of N, (N-2) or (N-4) independently, N is a natural number from 10 to 30, and n is a natural number from 3 to 4, R2 with carbon number of N is 80 to 97 percent by mass, R2 with carbon number of (N-2) is 0.0 to 7.8 percent by mass, R2 with carbon number of (N-4) is 3.0 to 13.0 percent by mass, R2 with carbon number of (N-4) is included 1.5 percent by mass or more than R2 with carbon number of (N-2).Type: GrantFiled: January 6, 2010Date of Patent: January 29, 2013Assignee: Konica Minolta Business Technologies, Inc.Inventors: Mikio Kouyama, Kenji Hayashi, Hiroaki Obata, Noriyuki Kinpara, Hiroshi Nagasawa, Yasuhiko Muramatsu
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Patent number: 8357479Abstract: A toner comprising: a component consisting of a thermoplastic resin containing an amorphous plant-derived resin having a carboxyl group; a component consisting of a crystalline epoxy resin having a glycidyl group; a component consisting of a cross-linked resin generated through a reaction between the carboxyl group of the plant-derived resin and the glycidyl group of the crystalline epoxy resin; and a colorant.Type: GrantFiled: August 27, 2010Date of Patent: January 22, 2013Assignee: Sharp Kabushiki KaishaInventors: Satoru Ariyoshi, Yasuhiro Shibai
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Publication number: 20120315575Abstract: The present invention is to provide a toner for developing electrostatic images having excellent fixability, peelability, shelf stability (blocking resistance), printing durability, printing durability after being left at high temperature and thin line reproducibility. A toner for developing electrostatic images, comprising colored resin particles comprising a binder resin, a colorant and a wax, wherein the wax contains a natural sunflower wax, and wherein the natural sunflower wax has an acid value of 10 mg KOH/g or less, and a content of the natural sunflower wax is in the range from 1 to 10 parts by weight with respect to 100 parts by weight of the binder resin.Type: ApplicationFiled: March 10, 2011Publication date: December 13, 2012Applicant: ZEON CORPORATIONInventor: Takuya Kaneda
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Publication number: 20120315574Abstract: A toner is provided that exhibits a high long-term image stability even during high-speed printing and that also exhibits an excellent environmental stability. The toner comprises a binder resin, a colorant, and a nonionic surfactant, wherein the nonionic surfactant has an oxyethylene group (EO) and an oxypropylene group (PO) and has a ratio of the number of moles of the oxypropylene group to the number of moles of the oxyethylene group (PO/EO) of at least 0.01 and not more than 5.00; and when A (?g/g) is defined as a nonionic surfactant content on the surface of the toner that can be extracted by methanol from 1 g of the toner and B (m2/g) is defined as a theoretical specific surface area determined from a toner particle diameter distribution obtained by a precision particle diameter distribution analyzer that operates based on an aperture electrical resistance method, a ratio A/B is at least 100 ?g/m2 and not more than 9000 ?g/m2.Type: ApplicationFiled: May 12, 2011Publication date: December 13, 2012Applicant: CANON KABUSHIKI KAISHAInventors: Katsuyuki Nonaka, Yasuhiro Hashimoto, Naoya Isono, Akira Sugiyama, Yuhei Terui
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Publication number: 20120315573Abstract: The present invention provides a modified charge control agent composition exhibiting a high charge-imparting effect, and an electrostatic image developing toner containing such a charge control agent composition and having a high electrostatic charge amount and an environmental stability. A composition comprising a metal compound (A) of aromatic hydroxycarboxylic acid having an aromatic hydroxycarboxylic acid bonded with a metal atom selected from a zirconium atom, a calcium atom, an aluminum atom, a chromium atom, a boron atom and a zinc atom via at least any of ionic bond, covalent bond and coordinate bond; and at least one inorganic pigment (B), wherein the pigment (B) is contained in an amount of from 1 to 20 parts by mass in 100 parts by mass of the composition.Type: ApplicationFiled: August 21, 2012Publication date: December 13, 2012Applicant: HODOGAYA CHEMICAL CO., LTD.Inventors: Hideyuki OTSUKA, Masaki OKUBO, Osamu MUKUDAI
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Publication number: 20120295191Abstract: A toner is provided which has toner particles containing a charging component and containing an aromatic compound represented by the following formula (1): wherein R1 to R3 each independently represent a hydrogen atom, a hydroxyl group, a carboxyl group, an alkyl group having 1 to 18 carbon atom(s) or an alkoxyl group having 1 to 18 carbon atom(s); R4 to R7 each independently represent a hydrogen atom, a hydroxyl group, an alkyl group having 1 to 18 carbon atom(s) or an alkoxyl group having 1 to 18 carbon atom(s); R8 represents a hydrogen atom or a methyl group; and m represents an integer of 1 to 3.Type: ApplicationFiled: April 27, 2012Publication date: November 22, 2012Applicant: CANON KABUSHIKI KAISHAInventors: Hitoshi Itabashi, Akane Masumoto, Takashi Kenmoku
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Publication number: 20120295190Abstract: A toner is provided which has toner particles containing an aromatic compound represented by the following formula (1), and a colorant: wherein R1 to R3 each independently represent a hydrogen atom, a hydroxyl group, a carboxyl group, an alkyl group having 1 to 18 carbon atom(s) or an alkoxyl group having 1 to 18 carbon atom(s); R4 to R8 each independently represent a hydrogen atom, a hydroxyl group, an alkyl group having 1 to 18 carbon atom(s) or an alkoxyl group having 1 to 18 carbon atom(s); and m represents an integer of 1 to 3.Type: ApplicationFiled: April 27, 2012Publication date: November 22, 2012Applicant: CANON KABUSHIKI KAISHAInventors: Hitoshi Itabashi, Takashi Kenmoku, Akane Masumoto
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Publication number: 20120288792Abstract: There is provided a developer that has excellent positive charging characteristics and charging stability, and which is compatible with high-speed developing. The developer of the invention contains toner particles and an insulating liquid, wherein a fatty acid ester is contained as the insulating liquid, a substance A expressed by the following formula (1) and/or a substance B expressed by the following formula (2) is further contained, and the total percentage in which substance A and substance B are contained is at least 0.1 wt % and no more than 3.0 wt %.Type: ApplicationFiled: April 26, 2012Publication date: November 15, 2012Applicant: SEIKO EPSON CORPORATIONInventors: Takashi TESHIMA, Junichi ISHIKAWA
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Publication number: 20120288791Abstract: In accordance with some embodiments, a toner including a first binder resin, a release agent, a release agent dispersing resin, and a colorant is provided. The first binder resin includes an amorphous polyester resin (a) having a polyhydroxycarboxylic acid skeleton in its main chain. The polyhydroxycarboxylic acid skeleton comprises optically-active monomers having an optical purity X of 80% by mole or less. The optical purity X is represented by the following formula: X (% by mole)=|X(L-form)?X(D-form)| wherein X(L-form) and X(D-form) represent ratios (% by mole) of L-form and D-form optically-active monomers, respectively. The release agent includes an ester of a fatty acid having an average carbon number of 18 to 24 with glycerin or a polyglycerin having an average polymerization degree of 2 to 10. The ester has a melting point of 55 to 80° C.Type: ApplicationFiled: April 26, 2012Publication date: November 15, 2012Inventors: Shingo Sakashita, Kazumi Suzuki, Tatsuya Morita
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Patent number: 8293444Abstract: A toner that includes at least one polyester resin wherein the amount of free polyvalent acid monomer in the polyester resin is less than 4 mg/gram, and wherein the percentage of the at least one polyester resin with a MW less than 1500 is less than about 10%.Type: GrantFiled: June 24, 2009Date of Patent: October 23, 2012Assignee: Xerox CorporationInventors: John L. Pawlak, Timothy L. Lincoln, William H. Hollenbaugh, Jr., Yuhua Tong, Brendan H. Williamson
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Publication number: 20120251938Abstract: A method for producing colored resin particles including: dissolving or dispersing at least binder resin and colorant in organic solvent to prepare oil phase; dissolving resin A and basic compound in aqueous medium to prepare aqueous phase, the resin A having solubility <2.0 g/100 g water having temperature 25° C. and pH 3.0 and solubility ?2.0 g/100 g water having temperature 25° C. and pH 10.0; dispersing the oil phase in the aqueous phase to prepare core particle dispersion liquid; dispersing resin particles in aqueous medium to prepare resin particle dispersion liquid, and adding the resin particle dispersion liquid to the core particle dispersion liquid so that the resin particles are attached onto the core particles, to prepare dispersion liquid containing particles each having the core particle and the resin particles attached thereonto; removing the organic solvent from the dispersion liquid; washing the particles; and drying the particles.Type: ApplicationFiled: February 1, 2012Publication date: October 4, 2012Inventors: Atsushi Yamamoto, Takuya Kadota, Yoshihiro Mikuriya, Tsuyoshi Nozaki, Yoshimichi Ishikawa, Kazuoki Fuwa, Tomohiro Fukao, Tomoharu Miki
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Publication number: 20120244466Abstract: A washing process using one or more ionic liquids (ILs) as a washing aid agent for toners, including toners produced using such ILs, such as, low melt toners, is provided. ILs are environmentally sound, green solvents that act to swell toner particle surfaces so that surface absorbed and adsorbed pollutants, such as, surfactants and other manufacturing reactants, can be effectively removed. The resulting toners have good charging, charge maintenance and RH sensitivity.Type: ApplicationFiled: March 22, 2011Publication date: September 27, 2012Applicant: XEROX CORPORATIONInventors: Zhen Lai, Chieh-Min Cheng, Zhaoyang Ou
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Publication number: 20120231387Abstract: A toner including a mother particle and an external additive is provided. The mother particle includes a core including a crystalline polyester, an amorphous polyester, a colorant, and a release agent; and a shell including resin particles. A deformation amount H1 of the toner compressed by a pressure of 0.5 mN under a temperature of 25° C. is between 0.2 and 1.5 ?m. A difference D between the deformation amount H1 and a deformation amount H2 of the toner compressed by a pressure of 0.5 mN under a temperature of 50° C. is between 0.0 and 1.0 ?m. A surface roughness Ra of the toner melted at 90° C. is between 0.02 and 0.40 ?m.Type: ApplicationFiled: February 17, 2012Publication date: September 13, 2012Inventor: Hideki SUGIURA
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Publication number: 20120231386Abstract: A toner composition including a colorant-polyester polymer having at least one colorant and at least one polyester resin, an optional non-colorant polyester polymer, an optional additional colorant, an optional wax, and an optional additive, where the colorant is covalently linked to some or all of the polyester resin and the polyester resin is obtained by polymerizing a lactone using an enzyme catalyst. Methods for preparing a toner composition including an emulsion aggregation process.Type: ApplicationFiled: March 9, 2011Publication date: September 13, 2012Applicant: XEROX CORPORATIONInventors: Santiago FAUCHER, Kimberly D. NOSELLA, Shigang S. QIU
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Patent number: 8252493Abstract: Single component toners are provided with at least one surface additive including a large polymeric spacer, and processes for producing the same. In embodiments, the toner is a non-magnetic single component toner produced by emulsion aggregation methods. The large polymeric spacer additives provide excellent flow characteristics to the resulting toners, and reduce the incidence of clogging failure and print defects such as ghosting, white bands, and low toner density compared with conventionally produced toners.Type: GrantFiled: October 15, 2008Date of Patent: August 28, 2012Assignee: Xerox CorporationInventors: Samir Kumar, Grazyna L. Kmiecik-Lawrynowicz, Maura A. Sweeney, Michael L. Grande, Julie C. Pickering, Timothy L. Lincoln
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Patent number: 8252494Abstract: A fluorescent particle includes a fluorescent pigment, such as a trans-dicarboxylic-indenofluorenone, and at least one stabilizing wax chemically attached to the fluorescent pigment. The stabilizing wax includes an amine group at its terminal end and the fluorescent pigment includes at least one carboxylic acid group, where the amine group reacts with the carboxylic acid group to form an amide bond. A method for making fluorescent particles for use in toners by chemically attaching at least one stabilizing wax to a fluorescent pigment where the at least one stabilizing wax includes an amine group at its terminal end and the fluorescent pigment includes at least one carboxylic acid group. A toner may include a resin and the fluorescent particle.Type: GrantFiled: May 3, 2010Date of Patent: August 28, 2012Assignee: Xerox CorporationInventors: Daryl W. Vanbesien, Maria M. Birau, C. Geoffrey Allen, Carol A. Jennings, Peter G. Odell
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Publication number: 20120214096Abstract: A toner to develop an electrostatic charge image, a method of preparing the toner, a toner supply device employing the toner, an apparatus to form an image employing the toner, and a method of forming an image using the toner are provided. The toner includes a binder resin including a first type of binder resin having a first weight-average molecular weight and a second type of binder resin having a second weight-average molecular weight different than the first weight-average molecular weight, a colorant, and a releasing agent.Type: ApplicationFiled: February 17, 2012Publication date: August 23, 2012Applicant: Samsung Electronics Co., LtdInventors: Kyeong PANG, Tae-hoe Koo, Su-bum Park, Ju-yeon Lee, Jun-young Lee
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Patent number: 8247146Abstract: Use of a wax in a toner, such as carnauba wax, to give an increase in charge control agent in a toner, such as a magenta toner, to give an increased glass transition temperature is disclosed. The toner may contain a resin comprising amorphous and crystalline polyesters to provide good low melt characteristics.Type: GrantFiled: October 5, 2010Date of Patent: August 21, 2012Assignee: Xerox CorporationInventors: Mark E. Mang, Eugene F. Young
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Publication number: 20120208118Abstract: Environmentally friendly resin particles are provided which include a monomer having a color, which is able to impart color to the resulting resin. The resulting resin may be used to form various articles, including toner. A toner of the present disclosure may thus include the bio-based polyester resin, optionally in combination with another amorphous resin and/or a crystalline resin. Methods for providing these resins are also provided.Type: ApplicationFiled: February 14, 2011Publication date: August 16, 2012Applicant: XEROX CORPORATIONInventor: Valerie M. Farrugia
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Publication number: 20120196218Abstract: A toner for developing an electrostatic charge image includes a core layer including a first binder resin, a colorant and a releasing agent; and a shell layer coating the core layer and including a second binder resin. The first binder resin of the core layer includes a low molecular weight amorphous polyester resin having a weight-average molecular weight of about 6000 g/mol to about 20000 g/mol, a high molecular weight amorphous polyester resin having a weight-average molecular weight of about 25000 g/mol to about 100000 g/mol, and a crystalline polyester resin having a weight-average molecular weight of about 8000 g/mol to about 30000 g/mol. The second binder resin of the shell layer includes the low and high molecular weight amorphous polyester resins.Type: ApplicationFiled: January 10, 2012Publication date: August 2, 2012Applicant: Samsung Electronics Co., Ltd.Inventors: Jin-mo HONG, Takeshi Yoshida, Sung-jin Park
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Patent number: 8227164Abstract: A toner, including a colorant; a binder resin; a release agent; and a fixing supplemental component, wherein the toner has a storage elastic modulus G? (Pa) satisfying the following conditions: 5.0×104<G?<5.0×105 at 80° C. 1.0×104<G?<1.0×105 at 90° C. 5.0×103<G?<5.0×104 at 100° C. 1.0×103<G?<1.0×104 at 120° C. 1.0×103<G?<1.0×104 at 150° C.Type: GrantFiled: May 11, 2010Date of Patent: July 24, 2012Assignee: Ricoh Company, LimitedInventors: Tsuyoshi Sugimoto, Naohito Shimota, Hiroshi Yamashita, Satoshi Ogawa, Masana Shiba, Junichi Awamura, Tsuneyasu Nagatomo, Masaki Watanabe
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Publication number: 20120183896Abstract: Disclosed is a polyester resin comprising the polycondensation product of (a) at least one diacid, acid ester, or diester; and (b) at least one diol; wherein either (i) at least one diacid, acid ester, or diester comprises a rosin diacid, rosin acid ester, or rosin diester; or (ii) at least one diol comprises a rosin diol. Also disclosed is a toner composition comprising particles which comprise the disclosed polyester resin and an optional colorant.Type: ApplicationFiled: January 17, 2011Publication date: July 19, 2012Applicant: XEROX CORPORATIONInventors: Guerino G. Sacripante, Ke Zhou, Edward G. Zwartz, Paul J. Gerroir, Michael S. Hawkins
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Patent number: 8216755Abstract: A toner manufactured by a method including the steps of dissolving or dispersing toner components comprising a binder resin, a colorant, and an encapsulated plasticizer to prepare an oily toner components liquid, and emulsifying or dispersing the oily toner components liquid in an aqueous medium to prepare the toner.Type: GrantFiled: June 1, 2009Date of Patent: July 10, 2012Assignee: Ricoh Company, LimitedInventors: Yoshimichi Ishikawa, Chiyoshi Nozaki, Tsuyoshi Nozaki, Takuya Kadota, Katsunori Kurose, Mitsuyo Matsumoto, Atsushi Yamamoto
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Publication number: 20120171604Abstract: The invention relates to a coloured polymer dispersion containing, as main ingredients: (a) a coloured polymer produced by polymerisation of monomer A with monomer B, monomer A being a pigment B which is coated with a polymerisable wax D wherein the polymerisable function is an ethylenically unsaturated group, monomer B being a ethylenically unsaturated compound; (b) at least one non-ionic surface-active additive E based on polyethers and/or polyglycerines; (c) at least one anionic surface-active additive F based on sulfonates, sulfates, phosphonates, phosphates or carboxylates; and (d) water.Type: ApplicationFiled: March 16, 2012Publication date: July 5, 2012Applicant: CLARIANT FINANCE (BVI) LIMITEDInventors: Franz-Leo HEINRICHS, Anais BIALY, Klaus SAITMACHER, Josef RITTER
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Patent number: 8211607Abstract: Toner particles are provided which may, in embodiments, include a gel. In embodiments, the toner particles may have a core-shell configuration, with the gel in the core, the shell, or both. The gel may prevent a crystalline resin in the core of the toner particles from migrating to the toner surface.Type: GrantFiled: August 27, 2008Date of Patent: July 3, 2012Assignee: Xerox CorporationInventors: Ke Zhou, Karen Ann Moffat, Edward G. Zwartz, Richard P. N. Veregin, Maria N. V. McDougall
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Patent number: 8211608Abstract: The present invention relates to a resin emulsion which has a good emulsification performance even when produced by using a crosslinked polyester resin as a binder resin, and also is capable of producing a toner having an excellent storage property therefrom; and a process for producing the resin emulsion. The process for producing a resin emulsion according to the present invention, includes the steps of: (a) mixing a resin containing a polyester having at least one constitutional unit selected from the group consisting of a constitutional unit derived from a trivalent or higher-valent alcohol component and a constitutional unit derived from a trivalent or higher-valent carboxylic acid component, an anionic surfactant, a nonionic surfactant and an aqueous medium with each other at a temperature not lower than a softening temperature (Ts) of the resin as measured by a flow tester method, the nonionic surfactant and the aqueous medium being used in amounts of from 0.1 to 1.Type: GrantFiled: April 17, 2008Date of Patent: July 3, 2012Assignee: Kao CorporationInventors: Hiroshi Mizuhata, Nobumichi Kamiyoshi, Shinichi Sata
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Publication number: 20120156607Abstract: Environmentally friendly toner particles are provided which may include a bio-based amorphous polyester resin, optionally in combination with another amorphous resin and/or a crystalline resin. Methods for providing these toners are also provided. In embodiments, the bio-based amorphous polyester resin is modified with a multi-functional bio-based acid, thereby providing acid-functionalized polyesters, which can be readily emulsified in emulsion aggregation processes for toner fabrication.Type: ApplicationFiled: December 21, 2010Publication date: June 21, 2012Applicant: XEROX CORPORATIONInventors: Valerie M. Farrugia, Guerino G. Sacripante, Sonja Hadzidedic
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Publication number: 20120135344Abstract: The present invention is to provide a toner for developing electrostatic images having a low minimum fixing temperature, and high hot offset resistance and high heat-resistant shelf stability, and a method for producing the toner. Also, the present invention is to provide a toner for developing electrostatic images, comprising a binder resin, a colorant, a release agent and a retention aid, wherein the retention aid is a copolymer of 70 to 98% by weight styrene and 2 to 30% by weight (meth)alkyl acrylate, and the copolymer has a glass transition temperature of 5 to 60° C.Type: ApplicationFiled: November 23, 2011Publication date: May 31, 2012Applicant: ZEON CORPORATIONInventor: Azusa Wada
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Patent number: 8187780Abstract: Environmentally friendly toner particles are provided which may, in embodiments, include a biodegradable semi-crystalline polyester resin and a biodegradable amorphous polyester resin.Type: GrantFiled: October 21, 2008Date of Patent: May 29, 2012Assignee: Xerox CorporationInventors: Gwynne McAneney-Lannen, Guerino G. Sacripante, Edward G. Zwartz, Maria N. V. McDougall
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Patent number: 8182973Abstract: An electrostatic-image-developing toner is obtained by aggregating: resin particles, each of which has a core-shell structure, in which a difference in glass transition temperature between a resin constituting the core and a resin constituting the shell is about 20° C. or more; and releasing agent particles, each of which includes a polyester block copolymer having a weight-average molecular weight of about 3,000 or less and containing a non-crystalline polyester block containing a cyclic structure in the main chain and a crystalline polyester block containing no cyclic structure in the main chain.Type: GrantFiled: March 13, 2009Date of Patent: May 22, 2012Assignee: Fuji Xerox Co., Ltd.Inventors: Yasuo Matsumura, Hirotaka Matsuoka, Hideo Maehata, Takashi Imai
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Publication number: 20120122027Abstract: To provide a toner, containing: a binder resin; a crystalline polyester resin; a colorant; and wax, wherein the toner has a fluidized powder characteristic value of 35% to 45%, and a BET specific surface area of 2.8 m2/g to 4 m2/g, and wherein the toner has an intensity ratio P2850/P828 of 0.10 to 0.20, where P2850 is an intensity of a peak at 2850 cm?1 which is attributed from the wax and the crystalline polyester resin, and P828 is an intensity of a peak at 828 cm?1 which is attributed from the binder resin, as measured by total reflectance infrared spectroscopy.Type: ApplicationFiled: November 2, 2011Publication date: May 17, 2012Inventors: Naohiro WATANABE, Tsuyoshi Sugimoto, Shlnya Hanatanl, Mamru Hozumi, Osamu Uchinokura
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Patent number: 8178269Abstract: Emulsion aggregation toner particles including a resin, polysaccharide particles, an optional wax, and an optional colorant. The toner particles contain about 1 to about 50 wt % polysaccharide particles based on the total weight of the toner particles.Type: GrantFiled: March 5, 2010Date of Patent: May 15, 2012Assignee: Xerox CorporationInventors: Ke Zhou, Guerino G. Sacripante, Paul Joseph Gerroir, Edward Graham Zwartz, Michael S. Hawkins
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Publication number: 20120107737Abstract: Toner particles are provided which may, in embodiments, include a core and a shell formed in situ. The resins utilized to form the core, the shell, or both, may be contacted with a water soluble initiator. The resin, in embodiments present in the shell, cross-links at a temperature near the temperature for coalescence, and may prevent a crystalline resin in the core from migrating to the toner surface.Type: ApplicationFiled: January 6, 2012Publication date: May 3, 2012Applicant: XEROX CORPORATIONInventors: Ke Zhou, Edward G. Zwartz, Karen Ann Moffat
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Patent number: 8168361Abstract: An emulsion aggregation toner composition includes toner particles including: an amorphous polyester resin; an optional crystalline resin; an optional colorant; an optional wax; an optional coagulant; and a polymeric or oligomeric hydroxy ketone photo initiator capable of initiating crosslinking of said polyester resin, wherein at least one of the amorphous polyester resin and the optional crystalline resin when present is unsaturated.Type: GrantFiled: October 15, 2009Date of Patent: May 1, 2012Assignee: Xerox CorporationInventors: Ke Zhou, Daryl W. Vanbesien, Edward G. Zwartz, Guerino G. Sacripante, Karen A. Moffat
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Publication number: 20120100476Abstract: The present invention relates to a pressure fixing toner which can be fixed at a lower temperature to enable energy-efficient high-speed printing, and a preparation method thereof. The pressure fixing toner comprises: a core which comprises a wax mixture including a wax and a pigment; and a shell which comprises a polymer or copolymer of at least one kind of polymerizable monomer selected from the group consisting of an aromatic vinyl-based monomer, an acrylate-based monomer, a methacrylate-based monomer and a diene-based monomer, and surrounds the core. The content of the wax of the core is 44-93 parts by weight based on 100 parts by weight of the total toner.Type: ApplicationFiled: June 16, 2010Publication date: April 26, 2012Applicant: LG CHEM, LTD.Inventors: Wook Jang, Chang-Soon Lee