Hydrocarbon Patents (Class 436/139)
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Patent number: 8476016Abstract: The present invention relates to methods for performing surveys of the genetic diversity of a population. The invention also relates to methods for performing genetic analyses of a population. The invention further relates to methods for the creation of databases comprising the survey information and the databases created by these methods. The invention also relates to methods for analyzing the information to correlate the presence of nucleic acid markers with desired parameters in a sample. These methods have application in the fields of geochemical exploration, agriculture, bioremediation, environmental analysis, clinical microbiology, forensic science and medicine.Type: GrantFiled: February 1, 2011Date of Patent: July 2, 2013Assignee: Taxon Biosciences, Inc.Inventor: Matthew Ashby
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Patent number: 8476075Abstract: A method of estimating the amount of unreacted starting materials (glycerides, methyl esters, etc.) and the composition of a biodiesel using TLC in conjunction with a lipophilic dye, Nile Red is described herein. The dye based TLC method of the present invention is convenient and provides significant advantages over existing methods for estimating the purity of a biodiesel composition.Type: GrantFiled: April 6, 2010Date of Patent: July 2, 2013Assignee: Board of Regents, The University of Texas SystemInventors: Eva Deemer, Wen Yee Lee, Xiomara Carolina Chianelli
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Patent number: 8455261Abstract: A method of measuring the concentration of a halogen in a gas stream using measurement means unsuitable for the direct measurement of halogens in a gas stream includes the step of passing a gaseous conversion compound to the halogen containing gas stream to convert the halogen to a detectable gaseous compound.Type: GrantFiled: March 24, 2009Date of Patent: June 4, 2013Assignee: Edwards LimitedInventors: Derek Martin Baker, Sam Olof, Andrew James Seeley
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Patent number: 8426215Abstract: A gas chromatograph for analyzing natural gas, with a first separation column (6). A first detector (7) is provided following the first separation column, the first separation column and the first detector operable to separate or detect propane and higher hydrocarbons. A second separation column (8) and a second detector (9) following it are provided to separate or detect carbon dioxide and ethane. A third separation column (10) and a third detector (11) following it are provided to separate or detect nitrogen and methane. A controllable changeover device (12) is provided between the second separation column (8) and the third separation column (10) to discharge eluates following methane. The first, second and third separation columns (6, 8, 10) and the first, second and third detectors (7, 9, 11) are connected in series. At least the first and the second detectors (7, 9) are operable to detect a mixture of substances flowing through them in a non-destructive manner.Type: GrantFiled: September 28, 2004Date of Patent: April 23, 2013Assignee: Siemens AktiengesellschaftInventors: Friedhelm Mueller, Udo Gellert
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Patent number: 8420403Abstract: A method for evaluating the caking property of sodium hydrogencarbonate crystal particles, characterized in that sodium hydrogencarbonate crystal particles are hermetically sealed in a packaging material having a water vapor transmission rate of at least 3 g/(m2·24 h) (at 40° C. with a relative humidity difference of 90%) as stipulated in JIS K7129 and left at rest at a temperature of from 17 to 35° C. at a carbon dioxide gas concentration of from 0.03 to 0.05 vol % at a relative humidity of from 40 to 95% for from 2 weeks to 3 months, and the proportion of agglomerated sodium hydrogencarbonate crystal particles is determined to evaluate the caking tendency. A novel test method for evaluating the caking property of sodium hydrogencarbonate crystal particles, capable of providing results of the caking property test with high reproducibility, quantitatively with high versatility, can be provided.Type: GrantFiled: January 3, 2007Date of Patent: April 16, 2013Assignee: Asahi Glass Company, LimitedInventors: Shintaro Kikuchi, Fumiaki Nakashima, Hisakazu Arima, Shigeru Sakurai, Takako Hirano
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Patent number: 8398921Abstract: A chemical sensor using metal nano-particles and a method for manufacturing a chemical sensor using metal nano-particles are provided. The chemical sensor includes: metal nano-particles; single-ligand organic molecules (or a single molecule) that binds to the metal nano-particles by using a metal bonding functional group; a substrate bonding functional group formed at the metal nano-particles and the single-ligand organic molecules as bound to each other; a substrate; electrodes formed on the substrate and having an interdigitate (IDT) structure; and a substrate functional group formed on the substrate and positioned between the electrodes, wherein the substrate bonding functional group and the substrate functional group are covalently bonded.Type: GrantFiled: November 15, 2010Date of Patent: March 19, 2013Assignee: Electronics and Telecommunications Research InstituteInventors: Myung Lae Lee, Young Jun Kim, Sung Hae Jung, Ho Jun Ryu, Jong Moo Lee
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Patent number: 8394643Abstract: The present application relates to copolymers having at least one optionally substituted fluoranthene as a first monomer unit and at least one optionally substituted pyrrole as a second monomer unit. The copolymer may, for example, emit green light when exposed to a blue or ultraviolet radiation. Methods of making the copolymer are also disclosed, as well as methods and apparatuses for producing light and detecting nitroaromatics using the copolymer.Type: GrantFiled: March 3, 2011Date of Patent: March 12, 2013Assignee: Tongji UniversityInventors: Xingui Li, Dunyin Gu, Meirong Huang
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Patent number: 8383050Abstract: A method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces is provided. A device for the parallel study of chemical reactions includes at least the following components: (a) at least two spatially separated reaction spaces; (b) on the reaction space input side, at least one common educt feed for the reaction spaces according to (a); (d) on the reaction space output side, at least one connection per reaction space to at least one holding gas feed common to all the reaction spaces, or subsets of them; (e) on the reaction space output side, and downstream of the connection to the holding gas feed according to (d) in the product flow direction, at least one restrictor per reaction space.Type: GrantFiled: September 28, 2010Date of Patent: February 26, 2013Assignee: HTE AGInventors: Alfred Haas, Wolfgang Strehlau, Armin Brenner, Oliver Koechel, Markus Friess, Torsten Zech
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Patent number: 8367414Abstract: Methods and systems are provided that utilize measured isotopic abundance data to correlate a product to the synthesis process by which it was made. By utilizing the principles described herein, isotopic process profiles for synthetic products can be constructed, products of unknown origin can be inferentially identified to the processes by which they were made, and synthesis processes can be monitored for consistency of process parameters.Type: GrantFiled: May 30, 2007Date of Patent: February 5, 2013Inventor: John P. Jasper
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Publication number: 20130004986Abstract: The present invention relates to the use of luminescent Ir(III) and Ru(II) complexes and their application in electro-chemiluminescence and bio-labelling. The use refers to the labelling and detection of biomolecules.Type: ApplicationFiled: December 3, 2010Publication date: January 3, 2013Inventors: Luisa De Cola, Jesus Miguel Fernandez Hernandez, Francesco Paolucci
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Patent number: 8334142Abstract: Closed-loop control of a hydrocarbon process is provided by an analyzer including an instrument configured for measuring a property of the liquid mixture, and having responsivities to concentrations of one of the components, independent of concentrations of others of the components. A temperature detector generates temperature data for the liquid mixture, and a processor captures data generated by the temperature detector and the instrument, and uses the data in combination with a model of responsivities to various concentrations of the components at various temperatures, to determine a temperature compensated concentration of the components while the liquid mixture flows continuously through the analyzer. A process control module including a process model of the hydrocarbon process, is coupled to the analyzer and is couplable to the hydrocarbon process, to receive the temperature compensated concentration and to generate at least one output configured to affect operation of the hydrocarbon process.Type: GrantFiled: October 15, 2010Date of Patent: December 18, 2012Assignee: Invensys Systems, Inc.Inventors: W. Marcus Trygstad, Russell Jackson, Bruce A. Keen
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Publication number: 20120308992Abstract: A method of preparing a dry stick test device for determining an analyte in a milk sample by chemical assay. At least one reagent pad is provided by impregnating a first porous material with an aqueous solution including a reagent capable of reacting with the analyte, a derivative of the analyte or an indicator compound for the analyte to provide a detectable signal when in a moistened state. The reagent pad is dried. A development pad is provided by impregnating a second porous material with an aqueous solution including at least one controlling compound which, when in a moistened state, is capable of providing a condition required for the reagent to react with the analyte to provide the detectable signal. The impregnated second porous material is dried. The first porous material is immobilized with the second porous material, on a solid support, to obtain the dry stick test device.Type: ApplicationFiled: June 11, 2012Publication date: December 6, 2012Inventor: Lars NYGAARD
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Publication number: 20120288944Abstract: A method for detecting a taggant molecular structure in a fluid includes providing a molecularly imprinted polymer sensor device, contacting a molecularly imprinted crosslinked star polymer with the fluid, and correlating a color change in the fluid with the amount of the taggant molecular structure in the fluid. The device has polymer arms attached to a core, and the core has molecular sized cavities adapted to selectively receive and bind displacement molecules having the taggant molecular structure and a colorimetric indicator. The displacement molecule is selectively removed from the molecularly imprinted crosslinked polymer upon exposure to the taggant molecular structure in the fluid thereby indicating the presence of the taggant molecular structure in the fluid based on a loss of color along a length of a housing.Type: ApplicationFiled: July 20, 2012Publication date: November 15, 2012Applicant: THE JOHNS HOPKINS UNIVERSITYInventors: George M. Murray, Andrew F. Mason, Edward W. Ott, JR.
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Patent number: 8309363Abstract: An apparatus (10) for evaluating a liquid hydrocarbon to determine the propensity for coke formation comprising an injector (12), a supply of air (14) arranged to supply air to the injector (12) and a supply of liquid hydrocarbon (16) arranged to supply liquid hydrocarbon to the injector (12). The injector (12) is arranged to atomise the liquid hydrocarbon and to supply the air and atomised liquid hydrocarbon into a chamber (18) and the chamber (18) is arranged to supply atomised liquid hydrocarbon and air to a test pipe (20) and a heater (22) is arranged to heat the test pipe (20). The test pipe (20) is pivotably mounted on a frame (28) such that the orientation of the test pipe (20) relative to the frame (28) is variable. The apparatus (10) is able to simulate conditions within a vent pipe of a lubricant system of an aero gas turbine engine.Type: GrantFiled: May 11, 2009Date of Patent: November 13, 2012Assignee: Rolls-Royce PLCInventors: John S Askins, Timothy A Shepherd
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Patent number: 8293084Abstract: The present invention relates to methods for the identification of compounds in carbohydrate mixture compositions as well as the determination of carbohydrate mixture composition patterns, based on e.g. orthogonal cross determining migration time (indices) using capillary gel electrophoresis-laser induced fluorescence and identifying said carbohydrate components based on comparing said migration time (indices) with standard migration time (indices) from a database which data are preferably also orthogonal cross determined. In a further aspect, the present invention relates to a method for carbohydrate mixture composition pattern profiling, like glycosylation pattern profiling using capillary gel electrophoresis-laser induced fluorescence (CGE-LIF). In another aspect, the present invention refers to a system for an automated determination and/or identification of carbohydrates and/or carbohydrate mixture composition patterns (e.g.: glycosylation patterns).Type: GrantFiled: April 22, 2009Date of Patent: October 23, 2012Assignee: Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V.Inventors: Erdmann Rapp, Jana Schwarzer, Udo Reichl, Christian Bohne
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Patent number: 8268629Abstract: A system and method for characterizing a liquid hydrocarbon fuel having unknown or variable composition is described and shown herein.Type: GrantFiled: June 21, 2005Date of Patent: September 18, 2012Assignee: dTEC Systems L.L.C.Inventors: Thomas Coleman, Frederick Wolf, James E Bruya
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Publication number: 20120225488Abstract: Disclosed is a vehicle emissions monitoring system capable of providing an accurate, real-time estimate of an amount of particulate matter (PM) within a vehicle's exhaust. The system is capable of accurately differentiating the composition of that PM by identifying amounts attributable to soot, SOF, and sulfate.Type: ApplicationFiled: August 6, 2010Publication date: September 6, 2012Applicant: AVL North America Inc.Inventors: William Martin Silvis, Roland Wanker
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Publication number: 20120225489Abstract: The present application provides a method for measuring coking propensity of a fossil fuel, comprising mixing an iron powder with a fossil fuel, wherein the iron powder has an average particle size of less than or equal to 100 ?m; reacting the iron powder with the fossil fuel at a temperature and a pressure sufficient to allow coking for a period of time; separating a supernatant and a solid product after said coking; and analyzing the solid product for carbon content, wherein the carbon content is proportional to the coking propensity. There is also provided is a method for measuring effectiveness of a coking inhibitor.Type: ApplicationFiled: February 29, 2012Publication date: September 6, 2012Applicant: ConocoPhillips CompanyInventors: Omar Jesus Yepez, Ricky Eugene Snelling
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Publication number: 20120220040Abstract: A method of quantitatively determining 8-isoprostane is provided that includes fluorescently labeling 8-isoprostane with a quinoxalinone derivative in an excess amount relative to 8-isoprostane, separating a fluorescently labeled 8-isoprostane from a unreacted quinoxalinone derivative by contacting a reaction mixture containing the fluorescently labeled 8-isoprostane and the unreacted quinoxalinone derivative with a cation exchange support having a sulfonic acid or a sulfonate immobilized thereon, and quantitatively determining the fluorescently labeled 8-isoprostane that has been separated from the unreacted quinoxalinone derivative.Type: ApplicationFiled: February 2, 2012Publication date: August 30, 2012Applicants: National Institute of Advanced Industrial Science and Technology, Tanita CorporationInventors: Satoshi KOIDE, Kenji YOKOYAMA, Yoshio SUZUKI
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Publication number: 20120220050Abstract: A method of purifying 8-isoprostane is provided that includes a step of contacting a liquid sample containing 8-isoprostane with an ion exchange support having a quaternary ammonium salt immobilized thereon such that 8-isoprostane in the liquid sample is retained on the ion exchange support and a step of eluting 8-isoprostane from the ion exchange support using a first eluent containing a water-soluble organic solvent and water as main components.Type: ApplicationFiled: February 2, 2012Publication date: August 30, 2012Applicants: National Institute of Advanced Industrial Science and Technology, Tanita CorporationInventors: Satoshi Koide, Kenji Yokoyama, Yoshio Suzuki
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Patent number: 8252594Abstract: A composition containing a petroleum hydrocarbon, a biodiesel fuel or an ethanol fuel, and an organic marker compound.Type: GrantFiled: November 15, 2010Date of Patent: August 28, 2012Assignee: Rohm and Haas CompanyInventors: Rajiv Manohar Banavali, Randall Wayne Stephens
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Patent number: 8249816Abstract: Methods for determining deposit formation tendencies for a plurality of fluid samples of different compositions is provided. Each sample includes fuel additive compositions containing one or more fuel additives or fuel compositions containing one or more fuels and one or more fuel additives. The methods can advantageously be optimized using combinatorial chemistry, in which a database of combinations of fuel compositions are generated. As market conditions vary and/or product requirements or customer specifications change, conditions suitable for forming desired products can be identified with little or no downtime.Type: GrantFiled: February 13, 2004Date of Patent: August 21, 2012Assignee: Chevron Oronite Company, LLCInventor: Robert H. Wollenberg
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Patent number: 8206985Abstract: A method of determining the effect of a spill on a marine environment, in which physical and chemical sensors are arranged with living organisms (4, 6) fitted with instruments, at an appropriate distance and position from the object (1) which is to be monitored, wherein the response of the living organism (4, 6), measured online in real time, is compared with known patterns of response, and where upstream and downstream measurements are compared to determine whether a change in response may be caused by a spill from the object, the significance of the real time measurements being validated through sampling of the organisms on a regular basis or as required, in order to analyze the effects on the health of the organisms, biomarkers, for the purpose of assessing the significance of the environmental effect.Type: GrantFiled: January 23, 2007Date of Patent: June 26, 2012Assignee: Biota Guard ASInventors: Odd Kjetil Andersen, Steinar Sanni
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Publication number: 20120156794Abstract: The invention relates to a method for analysis of fat-soluble components, in particular fat-soluble dyes, from biological materials, in particular foods and feeds, having facilitated extraction of the fat-soluble components from the biological materials with use of suitable dilution solutions and of the extractability using pertinent organic solvents or organic solvent mixtures and also an enrichment and separation method, with subsequent digital evaluation and documentation. It is proposed to treat the biological materials first with a dilution medium which makes the fat-soluble components more readily extractable from the complex biological matrix and subsequently with at least one organic solvent which extracts the components; the substances extracted into the organic supernatant are subsequently chromatographically enriched and separated and then visually assessed and/or measured.Type: ApplicationFiled: May 6, 2011Publication date: June 21, 2012Inventor: Florian SCHWEIGERT
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Patent number: 8193000Abstract: A colorimetric test for determining the presence or absence of biodiesel in a diesel fuel sample. The colorimetric test involves adding concentrated sulfuric acid to a sample of diesel fuel and observing any color change of the sample. A darkening of the diesel fuel sample indicates the presence of biodiesel. The degree to which the color changes after the addition of the sulfuric acid is proportional to the amount of biodiesel in the sample and therefore can be used to determine the amount of biodiesel in the sample. The reagent(s), sample containers and any necessary color scale can be provided in a kit for field testing.Type: GrantFiled: December 17, 2008Date of Patent: June 5, 2012Assignee: Heritage Environmental Services, LLCInventor: Linda Osborn
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Patent number: 8155791Abstract: Methods and systems for creating dynamic performance measures (DPMs) for an IBA manufacturing process. Included is a method for monitoring an Isobutyl Alcohol (IBA) recovery system that includes computing at least one of an amount of IBA recovered from the IBA recovery system and an amount of waste material produced from the IBA recovery system, and displaying at least one of the recovered IBA and the waste material produced based on time. The method also includes computing a cost saved based on a cost of virgin IBA and the amount of IBA recovered. Computing an amount of waste material includes measuring waste material flow, and computing a cost of waste material management based on the measured waste material flow and a cost per unit volume to dispose of waste material. The IBA recovery system can include an evaporation IBA recovery system and/or a distillation IBA recovery system.Type: GrantFiled: June 7, 2011Date of Patent: April 10, 2012Assignee: Invensys Systems, Inc.Inventor: Russell Barr
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Patent number: 8129190Abstract: Tagged products (including tagged petroleum products) and methods of detecting the same are disclosed. The tagged petroleum products are tagged with a violanthrone, e.g., a substituted violanthrone and/or an isoviolanthrone, e.g., a substituted isoviolanthrone.Type: GrantFiled: November 17, 2006Date of Patent: March 6, 2012Assignee: Applied Nanotech Holdings, Inc.Inventors: Philip Forshee, Peter Kottenstette
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Patent number: 8114678Abstract: The present invention provides quantitation of seven classes of compounds (saturates, 1-4+ ring aromatics, sulfides, and polars) present in petroleum streams boiling from 550-1050° F. Operating the present invention in the preparative mode will allow us to load and collect multi-milligram amounts of material. In the present invention, all seven fractions are produced in a single run, whereas the most commonly used preparative liquid chromatographic separations requires two or more large scale separations to generate similar fractions. The present invention uses 100 times less solvent. The present invention protocol provides a quicker and cheaper alternative to most commonly used preparative liquid chromatographic separations and is flexible enough to target many refining and chemicals problems.Type: GrantFiled: February 5, 2010Date of Patent: February 14, 2012Assignee: ExxonMobil Research & Engineering CompanyInventors: Birbal Chawla, Larry A. Green
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Patent number: 8093056Abstract: A method and apparatus to determine the fractional amount of at least one constituent of a hydrocarbon mixture, comprising dissolving the hydrocarbon mixture in a substantially hydrogen free solvent to produce a diluted solution, the diluted solution having sufficient solvent to render a NMR property of the diluted solution to be predictably related to the constituent concentrations of the hydrocarbon mixture; making NMR measurements on the diluted solution; and determining the fractional amount of at least one constituent of the hydrocarbon mixture from the NMR measurements.Type: GrantFiled: June 29, 2007Date of Patent: January 10, 2012Assignee: Schlumberger Technology CorporationInventor: Krishnamurthy Ganesan
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Patent number: 8084264Abstract: A method for quantifying the presence of naphthenic acids in a hydrocarbon-comprising liquid that includes: contacting a hydrocarbon-comprising liquid with gaseous ammonia; isolating a reaction product produced by the contacting step; and analyzing the reaction product for the presence of naphthenates using a mass spectrometry technique. The naphthenic acids known to form commercial naphthenate deposits can be (i) ions of tetraprotic carboxylic acids having molecular weights ranging from 1225 to 1270 Daltons, (ii) n-alkyl or branched carboxylic acids having molecular weights ranging from 250 to 650 Daltons, or (iii) both.Type: GrantFiled: January 27, 2010Date of Patent: December 27, 2011Assignee: Florida State University Research Foundation, Inc.Inventors: Alan G. Marshall, Priyanka Juyal, Mmilili M. Mapolelo, Ryan P. Rodgers
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Patent number: 8076155Abstract: A use composition monitor determines the concentration of peracid and/or peroxide in a use composition using a kinetic assay procedure. A sample mixture containing a sample of the use composition, a diluent and at least one reagent is prepared and analyzed using, for example, an optical detector. Response data obtained by the detector is indicative of the optical absorbance of the sample mixture as a function of time. A processor analyzes the response data to determine a corresponding best fit linear relationship. Depending upon an expected concentration range, the initial absorbance and/or the slope of the best fit equation are used to calculate the concentrations of the peracid and peroxide in the use composition.Type: GrantFiled: February 12, 2009Date of Patent: December 13, 2011Assignee: Ecolab USA Inc.Inventors: Eugene Tokhtuev, Christopher Owen, Paul R. Kraus, Joseph Erickson, Paul Schilling, Daniel Kamben, William Christensen, Viktor Slobodyan
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Patent number: 8034624Abstract: A sampling device for analysis of a substance which is chosen from the group consisting of isocyanates, aminoisocyanates, amines, and isothiocyanates, and which is present in an air flow intended to pass through the sampling device is disclosed, as well as a method for the production of said sampling device, and a method for the analysis of said substance in the air flow.Type: GrantFiled: May 8, 2007Date of Patent: October 11, 2011Assignee: Provtagaren ABInventors: Gunnar Skarping, Marianne Dalene
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Patent number: 8013082Abstract: The invention provides a process of polymerizing ethylene and at least one ?-olefin, said process comprises polymerizing the ethylene and the at least one ?-olefin in the presence of 5-ethylidene-2-norbornene, which comprises low levels of impurities, as determined by the absorbances at the following wavelengths: 320 nm and 343 nm. The invention also provides a method of increasing the catalysts efficiency, and a method of determining the expected catalyst efficiency, each in a polymerization of ethylene and at least one ?-olefin in the presence of the 5-ethylidene-2-norbornene, which comprises low levels of impurities, as determined by the absorbances at the above wavelengths. The invention further provides a method of purifying 5-ethylidene-2-norbornene to form a purified 5-ethylidene-2-norbornene, which comprises low levels of impurities, as determined by the absorbances of the above wavelengths.Type: GrantFiled: July 13, 2007Date of Patent: September 6, 2011Assignee: Dow Global Technologies LLCInventors: David L. Ramage, Sarah L. Martin
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Patent number: 7985592Abstract: Methods for determining the compatibility of a plurality of fluid samples of different lubricating oil compositions with elastomers is provided. Each sample includes one or more base oils of lubricating viscosity and one or more lubricating oil additives. The methods can advantageously be optimized using combinatorial chemistry, in which a database of combinations of lubricating oil compositions are generated. As market conditions vary and/or product requirements or customer specifications change, conditions suitable for forming desired products can be identified with little or no downtime.Type: GrantFiled: February 13, 2004Date of Patent: July 26, 2011Assignee: Chevron Oronite Company LLCInventor: Robert H. Wollenberg
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Publication number: 20110151573Abstract: Porous sol-gel material essentially consisting of units of one or more first polyalkoxysilanes chosen from the following compounds: (chloromethyl)triethoxysilane; 1,3-dimethyltetramethoxydisiloxane; ethyl trimethoxysilane; triethoxy(ethyl)silane; triethoxymethylsilane; triethoxy(vinyl)silane; trimethoxymethylsilane; trimethoxy(vinyl)silane; tetraethoxysilane or tetramethoxysilane (TMOS) and of units of one or more second polyalkoxysilanes chosen from the following compounds: (N-(3-(trimethoxysilyl)propyl)ethylenediamine; 3-aminopropyltriethoxysilane (APTES) and 3-aminopropyltrimethoxysilane, in a first polyalkoxysilane/second polyalkoxysilane molar ratio of 1/0.01 to 1/1, optionally comprising a probe molecule, method of preparation and applications in the trapping of monocyclic aromatic hydrocarbons and other pollutants or in their detection.Type: ApplicationFiled: July 10, 2009Publication date: June 23, 2011Inventors: Sabine Crunaire, Thu-Hoa Tran-Thi
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Patent number: 7966096Abstract: Methods and systems for creating dynamic performance measures (DPMs) for an IBA manufacturing process. Included is a method for monitoring an Isobutyl Alcohol (IBA) recovery system that includes computing at least one of an amount of IBA recovered from the IBA recovery system and an amount of waste material produced from the IBA recovery system, and displaying at least one of the recovered IBA and the waste material produced based on time. The method also includes computing a cost saved based on a cost of virgin IBA and the amount of IBA recovered. Computing an amount of waste material includes measuring waste material flow, and computing a cost of waste material management based on the measured waste material flow and a cost per unit volume to dispose of waste material. The IBA recovery system can include an evaporation IBA recovery system and/or a distillation IBA recovery system.Type: GrantFiled: July 19, 2002Date of Patent: June 21, 2011Assignee: Invensys Systems, Inc.Inventor: Russell Barr
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Publication number: 20110124113Abstract: Embodiments provide a method for detecting an unsaturated compound, the method comprising monitoring change in electrical properties of substances such as halides of copper that reacts or interacts with unsaturated compounds such as acetylene. Other embodiments provide a sensor for detecting acetylene gas comprising a substrate having a surface, electrodes in electrical communication with said surface, and a sensor layer formed of metal halide.Type: ApplicationFiled: November 25, 2009Publication date: May 26, 2011Inventors: Abdul-Majeed Azad, Desikan Sundararajan
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Patent number: 7939335Abstract: A method and apparatus for determining the presence of heavy hydrocarbons (including those from unprocessed crude oil) in distillate streams and/or reformer feed includes taking at least one sample, spectrally analyzing the at least one sample for at least one heavy hydrocarbon component, determining the concentration of the analyzed hydrocarbon component using the spectrally determined concentration in an appropriate mathematical model, and determining the total heavy hydrocarbon concentration from the determined values for each sample.Type: GrantFiled: November 6, 2008Date of Patent: May 10, 2011Assignee: Marathon Ashland Petroleum LLCInventors: Nicole R. Triche, Axel J. Lubeck
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Patent number: 7923261Abstract: This invention is directed to a method for determining a source of carbon feed used in manufacturing product produced from the carbon feed. The invention further provides a method for tracking products, particularly MTO products, derived from a particular carbon feed. In general, the method involves a variety of steps that include one or more of determining, comparing, inventorying, and tracking the 13C:12C ratio (or HD:H2 ratio) of the product that is being tracked to the measured or predetermined 13C:12C ratio (or HD:H2 ratio) of the feed used to make the product.Type: GrantFiled: June 6, 2008Date of Patent: April 12, 2011Assignee: ExxonMobil Chemical Patents Inc.Inventor: Thomas H. Colle
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Patent number: 7875244Abstract: A gas sensor has shock resistance and temperature resistance attributes. The gas sensor includes at least one catalytic measuring element (3), which is arranged in a sensor housing (1) forming a combustion chamber (2). The sensor housing (1) has at least one gas-permeable housing opening (4) for the gas exchange between the environment and the combustion chamber (2). The catalytic measuring element (3) is arranged between at least two disk-shaped support elements (5) made of a heat-insulating and temperature-resistant material.Type: GrantFiled: June 3, 2008Date of Patent: January 25, 2011Assignee: Dräger Safety AG & Co. KGaAInventors: Mladen Schlichte, Erik Stender
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Patent number: 7875458Abstract: Rapid determination of low temperature residual wax contamination in basestock oil provides a basis for real time correlation of basestock quality with the low temperature viscometric properties of fully formulated oils made using said basestock oil.Type: GrantFiled: November 5, 2004Date of Patent: January 25, 2011Assignee: ExxonMobil Research and Engineering CompanyInventors: James Douglas Eagan, James William Gleeson, Lisa I-Ching Yeh, Charles Lambert Baker, Jr., Christine A. Zielinski
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Publication number: 20110014718Abstract: The present invention relates to a method and a device for the parallel study of chemical reactions in at least two spatially separated reaction spaces. In particular, the invention is suitable for reactions which are not constant volume reactions and/or for reactions in which fluid flows through at least two spatially separated reaction spaces are intended to be controlled together for all the reaction spaces, or for related subsets of them, in the most straightforward way possible.Type: ApplicationFiled: September 28, 2010Publication date: January 20, 2011Applicant: hte Aktiengesellschaft the high throughput experimentation companyInventors: Alfred Haas, Wolfgang Strehlau, Armin Brenner, Oliver Koechel, Markus Friess, Torsten Zech
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Patent number: 7871572Abstract: Provided are mixed ligand metal nanoparticle chemical sensors in which metal nanoparticles are encapsulated by at least two kinds of different molecule ligands having a relatively low conductivity and various composition ratios, and a chemical sensor array in which a film of the metal nanoparticle sensor is formed on the substrate. The metal nanoparticle sensor using the mixed ligand improves sensitivity and reaction speed with respect to an analyte, and selectivity with respect to various analytes, and a kind and a composition of a ligand of the mixed ligand constituting the metal nanoparticle sensor are adjusted to allow the high sensitivity nanoparticle sensor to be applied to the sensor array technology, thereby enabling a design of sensor properties as well as systematic access to a configuration of the sensor array the most efficient for the analytes.Type: GrantFiled: September 21, 2004Date of Patent: January 18, 2011Assignee: Electronics and Telecommunications Research InstututeInventors: Young Jun Kim, Yong Shin Kim, Yoon Seok Yang, Seung Chul Ha, Hae Sik Yang, Yun Tae Kim, Dae Sik Lee, Young Sik Hong
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Patent number: 7871826Abstract: A method for determining a carbon content value of a hydrocarbon-containing mixture. At least one composition-dependent bulk property of the hydrocarbon-containing mixture is measured and optionally at least one non-hydrocarbon component concentration is measured with the resulting measurements used in a carbon content correlation for calculating the carbon content of the hydrocarbon-containing mixture. The carbon content may be used in a hydrogen and/or synthesis gas production process for calculating a target flow rate of steam to be combined with the hydrocarbon-containing mixture to form a mixed feed having a target steam-to-carbon ratio.Type: GrantFiled: September 26, 2007Date of Patent: January 18, 2011Assignee: Air Products and Chemicals, Inc.Inventors: Xiang-Dong Peng, Blaine Edward Herb, Matthew H. MacConnell, Winfried Stephen Hoglen
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Patent number: 7871822Abstract: A method for selecting at least one catalyst from a catalyst library on the basis of the reactivity thereof in a chemical conversion process includes: (a) testing the catalytic activity of a first catalyst from said catalyst library with respect to a reaction medium containing, as the compounds to be converted, at least one reactivity probe having a labeling system and including at least one reaction unit capable of reacting in said chemical conversion; (b) analyzing the reaction medium after said catalytic test for the purpose of qualitatively and/or qualitatively characterizing the resulting compounds; (c) repeating steps (a) and (b) for at least one other catalyst in said library; and (d) comparing the analysis results for each catalyst in order to characterize at least one catalyst having the required reactivity in said chemical conversion.Type: GrantFiled: January 28, 2005Date of Patent: January 18, 2011Assignee: Novalyst DiscoveryInventors: Alain Wagner, Cédric Catala
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Patent number: 7867766Abstract: An apparatus and method are disclosed for measuring the kinetic parameters of a catalyst powder, which include the reaction rate constants, active site concentration and intraparticle diffusivity. The measurement of the active site concentration selectively measures just the active sites and not the entire exposed atom concentration. The apparatus and method use surface concentrations less than 50% and larger than 1% the total active site concentration and a dynamic pulsed flow to avoid including weak adsorption sites not involved in the catalysis. The measurement is more accurate because (1) it uses a reactant gas and non-steady state adsorption at temperatures near to reaction temperatures, and (2) it uses the chemical kinetics expressions to extract the measured active site concentration to perform the measurement so as to count just those sites actually active for that reactant.Type: GrantFiled: February 11, 2007Date of Patent: January 11, 2011Inventor: Dezheng Wang
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Patent number: 7851221Abstract: The invention provides a system for designing, operating, monitoring and/or diagnosing a chemical reaction, particularly a hydrotreating process, using a fixed bed catalytic reactor.Type: GrantFiled: July 31, 2008Date of Patent: December 14, 2010Assignee: Exxonmobilchemical Patents Inc.Inventors: Ronald D. Garton, David G. Woods, Hans G. Korsten, Pierre J. Osterrieth, Brian C. McClaine
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Patent number: 7829343Abstract: The invention relates to a method for determining the smoke point of a hydrocarbon, comprising, among the different steps defined in the ASTM D 1322 standard or equivalents thereof, the identification, among different aspects of the flame according to the position of the burner in the lamp, of a particular aspect of the flame and the reading of the height of this flame on a graduated scale in mm. The invention is characterized by the fact that a series of digital images of the flame is taken and recorded with the aid of a digital camera or the like at intervals sufficiently close for permitting, by analyzing these digital images, the detection of a sudden change in the shape of the flame, and that the height of this flame is measured at the moment of this sudden change in its shape, said height being considered as the smoke point of the tested hydrocarbon.Type: GrantFiled: December 28, 2005Date of Patent: November 9, 2010Assignee: Total Raffinage MarketingInventors: Myriam Reminiac, Pierre Pestiaux
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Publication number: 20100261281Abstract: A method of estimating the amount of unreacted starting materials (glycerides, methyl esters, etc.) and the composition of a biodiesel using TLC in conjunction with a lipophilic dye, Nile Red is described herein. The dye based TLC method of the present invention is convenient and provides significant advantages over existing methods for estimating the purity of a biodiesel composition.Type: ApplicationFiled: April 6, 2010Publication date: October 14, 2010Applicant: BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEMInventors: Eva Deemer, Wen Yee Lee, Carolina Kretschmer
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Publication number: 20100255587Abstract: This invention relates to methods and apparatus for determination of ion concentrations, particularly in downhole water from hydrocarbon wells, aquifers etc. It is useful in a wide range of applications, including predicting the formation of scale and fingerprinting waters from different sources. More particularly, the invention relates to the use of ligands whose electronic configuration is altered by the binding of the scaling ions within a water sample. These alterations are detected electrochemically by applying varying potential to electrodes and measuring current flow as potential is varied, from which is derived the concentration of scaling ions in the fluid.Type: ApplicationFiled: June 22, 2010Publication date: October 7, 2010Applicant: Schlumberger Technology CorporationInventors: Li Jiang, Timothy Gareth John Jones, Andrew Meredith, Markus Pagels, Amilra Prasanna De Silva