Abstract: The analyzing apparatus includes a reactor, a detector, a carrier gas supplier, a carrier gas flow rate adjustor, a flow control program memory, and a flow rate controller. The detector communicates with an internal space of the reactor, and detects a target substance generated by reaction of a specific component in the internal space. The carrier gas supplier supplies, to the internal space, carrier gas for transporting the target substance generated in the internal space. The carrier gas flow rate adjustor adjusts a carrier gas flow rate supplied from the carrier gas supplier to the internal space. The flow control program memory stores a flow control program set to increase the carrier gas flow rate during measurement from the process of introduction of a sample into the internal space to the process of detection of the target substance by the detector.

Abstract: Products and processes are provided herewith for analyzing octane content in a fuel sample that include the step or steps of receiving an octane measurement of a fuel sample from a octane analyzer, rounding the octane measurement to a nearest recognized octane rating, comparing the rounded octane measurement with a listed octane rating for the fuel sample, and communicating results of the comparison to a user of the octane analyzer. The octane analyzer may be incorporated into a fuel pump or a vehicle. The results of the comparison may also be used to adjust the vehicle operating parameters to account for the actual octane rating of the fuel dispensed into the vehicle.

Abstract: A sensor device, a method for operating a sensor device and an electronic assembly comprising a sensor device are disclosed. In an embodiment a sensor device includes a first sensor unit and a second sensor unit in a common housing, wherein each of the first and second sensor units comprises a heater element and a temperature sensor element, wherein the housing comprises a cover element having an opening, the cover element covering the first sensor unit, and wherein the opening is arranged over the second sensor unit.

Abstract: The present disclosure relates to a combustion tube for a device for elemental analysis of a sample, comprising an outer tube including an outlet and an inner tube including an inlet, the inner tube detachably insertable into the outer tube, wherein the outer and inner tubes are arranged such that the sample passes through the inlet, through the inner tube into the outer tube, and out of the combustion tube through the outlet, wherein the inner and outer tubes are configured such that, at least in a region in which the inner tube is surrounded by the outer tube, the sample is essentially inside the inner tube. The outer tube is made of a quartz glass, and the inner tube is made of a ceramic. The present invention further relates to a device for elemental analysis of a sample comprising a combustion tube according to the present disclosure.

Abstract: A method of and apparatus (41) for determining the organic carbon content of soil in heated air or gas is forced through a soil sample (36) to burn off or oxidize organic carbon in the sample with the change of weight of the sample (36) indicating the carbon content in the soil sample (36) and thus the soil from which the sample (36) is taken. The apparatus (41) includes a housing (47) in which one or more soil samples (36) may be located, a heater unit (51) for heating the air or gas for passage through the soil samples (36) to burn off organic materials therein including organic carbon. The apparatus (41) also includes a weighing device (76) which enables the change of weight of the soil samples (36) to be determined while the samples (36) remain within the housing (47).

Abstract: A method and an apparatus for determining the calorific value parameter describing the calorific value of a gaseous fuel. The apparatus comprises a test burner with a test combustion chamber. An air ratio sensor is arranged in an exhaust gas duct of the test burner and measures an air ratio signal that corresponds to the air ratio of the exhaust gas. As a function of the received air ratio signal, at least one setting signal is generated for a test supply unit via a test control unit. The setting signal controls the amount and/or the proportion of a gaseous fuel or an oxygen-containing gas that is supplied to the test combustion chamber. A calorific value sensor arrangement is provided in the combustion chamber and has an ionization sensor and, a temperature sensor. The sensor signal of the calorific value sensor is transmitted to a determination unit.

Abstract: A process combustion transmitter is provided. The transmitter includes a process probe extendible into a flow of process combustion exhaust. The process probe has a measurement cell with an operating temperature that is above a flashpoint of process combustion fuel. The process probe includes a heater configured to heat the measurement cell to the operating temperature. Electronic circuitry is coupled to the measurement cell and to the heater. The electronic circuitry is configured to disengage power to the heater once process combustion heat is sufficient to maintain the measurement cell at the operating temperature and thereafter to maintain the heater in a de-energized state.

Abstract: A method for analyzing a gas at a heatable element for a lambda probe includes reading a value of a heating power available to the heatable element for maintaining a predetermined temperature of the heatable element, and determining a gas composition of the gas at the heatable element using the value of the heating power.

Abstract: Methods are provided for conducting chemical analyses by combusting a sample in a combustion tube. A primary combustion chamber receives and combusts a sample to form first combustion products. A secondary combustion chamber receives and combusts the first combustion products to form second combustion products. The secondary chamber is disposed around the primary chamber and comprises a plurality of—preferably, three—combustion compartments. Each successive compartment is disposed around the preceding compartment and defines a respective gas flow channel having an inlet opening and an outlet opening at opposite ends. Each successive gas flow channel shares its inlet opening with the outlet opening of the preceding channel. The plurality of combustion compartments define a substantially continuous gas flow conduit from the inlet opening of the innermost compartment to the outlet opening of the outermost compartment. Static gas mixers may be employed to enhance mixing of the combustion products.

Abstract: The invention relates to a method and to a device for sulfur characterization and quantification in a sample of sedimentary rocks or of petroleum products wherein the following stages are carried out: heating said sample in a pyrolysis oven (1) in a non-oxidizing atmosphere, oxidizing part of the pyrolysis effluents and continuously measuring the amount of SO2 generated by said part after oxidation, then transferring the pyrolysis residue of said sample into an oxidation oven (1?) and continuously measuring the amount of SO2 contained in the effluents resulting from said oxidation heating.

Abstract: A particulate matter generator implemented as a “mini-burner”, and used in conjunction with a larger test system for the specific purpose of enhancing the particulate matter content of exhaust gas. The exhaust stream of the larger system is supplemented with exhaust from the mini-burner to produce exhaust with desired particulate matter characteristics. The exhaust gas may then be used for various test purposes, such as testing emissions control devices.

Abstract: The invention relates to a device for producing CO2, N2 and/or SO2 from a sample for a quantitative analysis of the sample, comprising a reactor structure and metals acting in an oxidizing manner or metal oxides in the reactor. According to the invention, the reactor structure has at least two zones through which the sample can flow, which is to say a first zone with reactor metal and reservoir metal, or only reactor metal, and following the first zone, a second zone with reactor metal and reservoir metal, or only reservoir metal, wherein both metals can form oxides, and wherein the ratio of the reactor metal to the reservoir metal in the first zone is greater than in the second zone.

Abstract: With a device for combustion analysis, comprising an induction furnace with a furnace chamber, in which carrier gas can flow during operation via at least one gas inlet to a gas outlet, and in which a sample to be analyzed can be arranged and burned in a sample container, a hollow protective element is provided and, with normal operation of the device, is arranged in the furnace chamber directly above the sample in such a way that the end of the protective element facing towards the sample, together with the sample container, forms a constriction for the carrier gas flow, wherein the protective element is desgned to convey gases produced during the combustion of the sample through the protective element and to the gas outlet.

Abstract: An analyzer with a combustion furnace includes a flow path of byproducts of combustion coupled to a bidirectional ballast chamber by valves which are sequentially actuated for alternately filling and exhausting byproducts of combustion from opposite sides of the chamber during combustion. Alternately, a plurality of low volume ballast chambers are employed. A method of determining the concentration of elements in a sample includes the steps of combusting a sample; and alternately collecting and exhausting the byproduct gases of combustion in opposite sides of a bidirectional ballast. The bidirectional ballast chamber has an outer wall defining a chamber with sealed enclosures at opposite ends of the wall, a movable piston positioned within the chamber, and gas ports associated with the chamber on opposite sides of the piston.

Abstract: A method is provided for controlling the operating temperature of a catalytic reactor using a closed-loop system that provides for varying the reactor input and other operating parameters in order to maintain the operating temperature of the reactor at or near the initial setpoint temperature for operation of the reactor. In one example, maximum and minimum operating temperatures with a catalytic partial oxidation reactor are controlled, as well as maintaining control over the corresponding minimum required ratio of oxygen atoms to carbon atoms, such that the operating temperature within the reactor is maintained below the material limits but above threshold temperatures for coking.

Abstract: A particulate matter generator implemented as a “mini-burner”, and used in conjunction with a larger test system for the specific purpose of enhancing the particulate matter content of exhaust gas. The exhaust stream of the larger system is supplemented with exhaust from the mini-burner to produce exhaust with desired particulate matter characteristics. The exhaust gas may then be used for various test purposes, such as testing emissions control devices.

Abstract: A method of operating a furnace having process tubes and multiple burners where it is desired to conform the temperatures of the process tubes to selected target temperature criterion. The present method provides a systematic and quantitative approach to determine how to adjust burner flow rates to result in desired tube wall temperatures, for example to minimize the temperature deviation between tube wall temperatures at a predetermined elevation in the furnace.

Abstract: A dust monitor is disclosed that is suitably deployed in dusty environments and capable of providing near real-time indications of exposure to airborne particulates. The monitor includes a filter and filter assembly made of materials that do not interfere with subsequent instrumental (such as spectrometric) analysis for detecting and/or quantitating an analyte. In some disclosed embodiments, the filter is made of nylon or other material that is readily subjected to thermal destruction prior to spectrometric analysis. The dust monitor also includes a humidity correction feature that permits the filter to be made of ashable organic materials even if those materials are not highly hydrophobic. Transport devices are provided for shipment of the filter and/or filter assembly to an analytical laboratory which prevent loss of particulate matter and which facilitate an accurate analysis procedure.

Abstract: An apparatus and method are disclosed for measuring the kinetic parameters of a catalyst powder, which include the reaction rate constants, active site concentration and intraparticle diffusivity. The measurement of the active site concentration selectively measures just the active sites and not the entire exposed atom concentration. The apparatus and method use surface concentrations less than 50% and larger than 1% the total active site concentration and a dynamic pulsed flow to avoid including weak adsorption sites not involved in the catalysis. The measurement is more accurate because (1) it uses a reactant gas and non-steady state adsorption at temperatures near to reaction temperatures, and (2) it uses the chemical kinetics expressions to extract the measured active site concentration to perform the measurement so as to count just those sites actually active for that reactant.

Abstract: The invention relates to a method allowing to determine at least one petroleum characteristic of a geologic sediment sample, wherein the sample is heated in an oxidizing atmosphere, its temperature being successively raised to a first, then to a second value, said first value below 200° C. being reached very quickly, then maintained substantially constant for a certain time, said second value ranging between 600° C. and 850° C. being reached with a temperature gradient ranging between 1 and 30° C./min, from said first value. According to the invention, the amount of SO2 contained by the effluent resulting from said oxidizing heating is measured continuously, every moment of the heating period of said sample.

Abstract: A method for testing the performance of catalysts used for conversion of FCC regenerator gases comprises subjecting the catalyst simultaneously to a mixture of gases including an oxidizing gas and a reducing gas in more than one cycle in which the ratio of the oxidizing gas to the reducing gas varies over the time of the cycle. Test gases comprising O2, CO, CO2, steam, nitrogen-containing gases and sulfur-containing gases in which the ratio of O2 to CO varies over time for each cycle and in which the products of combustion formed during each cycle can be measured periodically over the cycle yields important data on the usefulness of the catalysts for treatment of regenerator flue gas.

Abstract: A method of using a burner-based system to produce diesel exhaust gas that contains particulate matter of a desired composition, to simulate the PM matter in exhaust produced by a production-type diesel internal combustion engine.

Abstract: A liquid analyser has a reactor portion and an associated measurement portion. A sample pump is operable to deliver a liquid sample to a reactor vessel. A base pump supplies a base solution to the reactor vessel. An ozone generator supplies ozone to the reactor vessel. The liquid sample is oxidised in the reactor vessel by means of hydroxyl radicals which are generated using the base solution and ozone to reduce complex components of the liquid sample to their lowest state in solution. The oxidised sample solution is delivered to an optical detector in the measurement portion to determine the concentration of one or more selected materials such as nitrogen, phosphorous or a heavy metal in the oxidised sample solution.

Abstract: A novel Flame Temperature Analyzer (FTA) method and apparatus for measuring combustible gas concentration and oxygen content in a sample gas includes supplying a mixture of oxidant and fuel to a sensing flame and measuring the temperature of the flame as the sample is added to the combustion chamber.

Abstract: Apparatus and method for determining incomplete combustion in a combustion analyzer comprising a combustion chamber (60). A sample is supplied to the combustion chamber and combusted to produce combustion products. A target gas characteristic of incomplete combustion of the sample is detected in the combustion products by a target gas sensor (72). The target gas may be carbon monoxide, methane, methanal and/or methanol, among others. Preferably, the gas sensor is an electronic or catalytic combustible gas sensor. Whether incomplete combustion of the sample has occurred may be determined. A signal indicative of incomplete combustion is output from the target gas sensor to a controller (78). The combustion products can be directed to waste and/or further supply of the sample/oxygen may be stopped/adjusted. Faulty analysis measurements and/or contamination of downstream components, which would otherwise result from incomplete combustion—in particular, from soot formation—can thereby be avoided.

Abstract: A method and device are provided for dynamic flash combustion reaction connected with gas chromatography for the elemental analysis of C H N S O in an automatic elemental analyzer. A combustion reactor is provided with a sampling device and an oxygen feed line. Controlled volumes of oxygen are admitted with the oxygen feed line into the combustion reactor depending on the sample for the complete combustion thereof. A pneumatic circuit is provided, in which the oxygen feed line converges and the pneumatic circuit creates a continuous flow of a carrier gas that is able to carry the oxygen to the reactor and the gases of the combustion through the reactor, then through a gas chromatographic analyzer, and after their separation, into a thermal conductivity detector. An electronic apparatus with a data processor is provided for controlling the process systems. The difference in the pressure of the gas upstream and downstream of a restrictor or restriction is determined.

Abstract: The invention relates to a process for the detection of hydrocarbons other than methane in a gas predominantly or essentially comprising oxygen, as well as methane and the said hydrocarbons other than methane, the said process comprising: a stage of detection of the combined hydrocarbons in the said gas, providing a first value for the combined hydrocarbons, a stage of combustion of the hydrocarbons other than methane, a stage of detection of methane in the said gas, providing a second value, a stage of calculation of the amount of hydrocarbons other than methane by the difference between the first value and the second value. The invention also relates to a device for implementing this process.

Abstract: Carbon monoxide contained in reformate gas is removed by a preferential oxidation reaction in a catalyst, two preferential oxidation reactors (20A, 20B) being disposed in series. Valves (7, 8) supply air containing oxygen as an oxidizing agent individually to these preferential oxidation reactors (20A, 20B). Temperature sensors (9, 10) detect the catalyst temperatures of the preferential oxidation reactors (20A, 20B), and a controller (5), by adjusting the flow rate of the valves (7, 8) based on the detected temperatures, maximizes the carbon monoxide removal performance of the preferential oxidation reactors (20A, 20B), while preventing excessive catalyst temperature rise.

Abstract: The present invention relates to a method for measuring the content of Lanthanides dissolved in uranium oxide, wherein the Lanthanides content in the nuclear fuel pellet is measured using the thermo gravimetric analysis which measures the weight variation caused by the oxidation and heat treatment of the nuclear fuel pellet. This method provides an advantage in that the Lanthanide content can be measured using relatively simple equipments such as an electric furnace and a balance.

Abstract: A more efficient method for combustion or oxidation of samples containing nitrogen, phosphorus and/or sulfur to their corresponding oxides is disclosed, where method uses multi-staged addition of an oxidizing agent to enhance oxidation and liberation of nitrogen, phosphorus and/or sulfur oxides for subsequent detection. The method of the present invention allows for the injection of larger samples or the introduction of a greater amount of sample per unit of time which results in a larger amount of analyte being delivered to the detector per unit of time, thereby improving detection limits and detection efficiency.

Abstract: Disclosed are a closed heat-decomposing appliance comprising a heating section with one side closed and other side having common ground portion, screw portion or O-ring-mounted portion and a closed introducing section that allows to connect to this heating section and common ground portion, screw portion or O-ring via O-ring-mounted portion and has cock or valve as a mechanism for closing and introducing the absorbing liquid to absorb the testing components from outside after heat-decomposition, or has packing or septum to introduce the absorbing liquid with needle pipe as well, and a pretreatment method of sample using this appliance.

Abstract: Methods and apparatus are described for preventing nitrogen interference in the detection of a substance. In particular, it relates to new methods and apparatus for preventing interference due to nitrogen in pyro-electrochemical methods for measuring substances, for example sulfur content, contained within liquids such as petroleum products and beverages. One preferred apparatus and method comprises a catalytic converter or thermal converter to selectively remove the nitrogen-containing interferant, for example NO2, in the pyrolyzed gas stream to NO without affecting the sulfur content. A second preferred apparatus and method comprises a chemical scrubber to selectively remove the nitrogen-containing interferant from the gas stream without affecting the sulfur content.

Abstract: A package with a locking mechanism provided with a package main body to be inserted into and removed from a cage and locked fastenably and releasably with the cage, a locking-dislocking mechanism for locking and dislocking the package main body with the cage, and an operation lever for the locking-dislocking mechanism wherein the locking-dislocking mechanism is attached to the package main body, the operation lever has a plurality of members to be pivoted detachably on the package main body, and any one of the members to be pivoted which is selected arbitrarily therefrom is pivoted on the package main body so as to rotate the operation lever.

Abstract: A method and apparatus for measuring the concentration of at least one gaseous component and/or vaporous component of a gaseous mixture in which a controlled sensor flame is introduced into the gaseous mixture and at least one narrow spectral band in the controlled sensor flame is optically measured. The concentration of the gaseous component using a result obtained from the optical measuring of the at least one narrow spectral band is then calculated. The method of this invention is particularly suitable for substantially real-time control of combustion processes.

Abstract: There are provided a detector agent which is effectively discolored at a lower concentration for various halogen compounds and a method for detecting halogen compounds by use of said detector agent. A detector agent for halogen compounds, which contains curcumin or Bromocresol Green as a discoloring component, and said discoloring component is preferably supported on granular activated alumina.

Abstract: An element analyzer D comprises a combustion section 1 for burning a sample S, a sample injection member 2 for injecting the sample S into the combustion section 1, and a detection section 29 for measuring a gasified sample formed by burning the sample S in the combustion section 1. The element analyzer D further includes a cleaning-agent injection member 2 for injecting a cleaning agent W into the combustion section 1.

Abstract: The invention features methods and systems for detecting the presence of an energetic material in a sample in which the presence of the energetic material is unknown. The method includes the steps of: heating the sample; measuring heat flow between the sample and its surrounding environment, e.g., by using differential scanning calorimetry (DSC); and analyzing the measured heat flow between the sample and its surrounding environment. An exothermal peak in the measured heat flow indicates the presence of the energetic material in the sample. The system includes a thermal measuring apparatus for performing the heating and measuring steps, and an analyzer for detecting the presence of the energetic material based on the measured heat flow. The invention also features methods and systems for identifying contraband materials (e.g., explosives and drugs) by measuring the thermogram (e.g., by DSC) of a sample to be identified and comparing it to reference thermograms for known contraband materials.

Abstract: Elemental analysis of a sample is carried out in an oxygen atmosphere in a combustion reactor and the volume of oxygen required for analysis is determined by means of the algorithm Qo=&Dgr;(Qc)  [1] where Qo is the volume of oxygen required and Qc is the weight of the sample to be analyzed and &Dgr;=Qo1/Qc1 where Qo1 is the volume of oxygen necessary for the combustion of a predetermined quantity Qc1 of the sample to be analyzed, the volume of oxygen Qo is then fed in pulsed mode to the combustion reactor, by means of a flow detector.

Abstract: The present invention discloses a system for analyzing elements contained in a sample in very slight amounts, such as C, S, O, N, H and the like in materials, such as steel and ceramics. An element analyzer can gasify the sample elements in an appropriate gas, such as oxygen gas in a high-frequency heating furnace or an electric resistant furnace. Resulting gas can be introduced into a mass spectrometer to permit a quantitative analysis of the sample elements. A metal sample can be levitated and heated and melted with induction current for producing the resultant gas for introduction to a mass spectrometer.

Abstract: The invention provides an ozone hydroxy radical analysis method for a liquid carrying a suspension of organic matter. The analyser includes a reactor vessel 2 having sample inlets and outlets 3 and 4 respectively for a liquid stream 5. The reactor vessel 2 is connected to a control system 10 and is fed from an acid vessel 15, a base vessel 16 and an ozone generator 20. The reactor vessel 2 contains glass beads and a catalyst is introduced into the reactor vessel. With a manganese catalyst and glass beads, the manganese coats the glass beads which therefore retain catalyst with the reactor vessel.

Abstract: An apparatus (1) for determining the concentration of a critical first component, such as hydrogen, of an atmosphere or environment (E), wherein the first component is capable of forming a combustible mixture with a second component, such as oxygen; the apparatus comprises: (A) a sampling unit (10) including: (A1) a small measuring chamber (12) operatively connected with an ignition means (135) capable of being operated so as to initiate in said chamber a combustion of said critical first component by reaction with said second component, and (A2) at least one sensor (15) operatively connected with said measuring chamber for generating a signal formed by essentially proportionate contributions from all significant components contained in said measuring chamber; (B) at least one flame arrestor (14) intervening between said measuring chamber (12) and aid environment (E) of interest; and (C) a control unit (16) capable of imposing a mode of operation in at least two distinct phases wherein, during a first phase,

Abstract: Disclosed are a closed heat-decomposing appliance comprising a heating section with one side closed and other side having common ground portion, screw portion or O-ring-mounted portion and a closed introducing section that allows to connect to this heating section and common ground portion, screw portion or O-ring via O-ring-mounted portion and has cock or valve as a mechanism for closing and introducing the absorbing liquid to absorb the testing components from outside after heat-decomposition, or has packing or septum to introduce the absorbing liquid with needle pipe as well, and a pretreatment method of sample using this appliance.

Abstract: A new laboratory test for evaluating the tendency of a gasoline, which may contain additives, to produce deposits during running of an engine involves the following steps: a tube is placed in the injector oven of a gas chromatograph; said tube is kept at a constant temperature in a constant flow of air; the gasoline or additive-containing gasoline to be evaluated is injected through said tube; and the quantity of deposits formed is determined by weighing said tube after dismantling.

Abstract: A method and device are provided for dynamic flash combustion reaction connected with gas chromatography for the elemental analysis of C H N S O in an automatic elemental analyzer. A combustion reactor is provided with a sampling device and an oxygen feed line. Controlled volumes of oxygen are admitted with the oxygen feed line into the combustion reactor depending on the sample for the complete combustion thereof. A pneumatic circuit is provided, in which the oxygen feed line converges and the pneumatic circuit creates a continuous flow of a carrier gas that is able to carry the oxygen to the reactor and the gases of the combustion through the reactor, then through a gas chromatographic analyzer, and after their separation, into a thermal conductivity detector. An electronic apparatus with a data processor is provided for controlling the process systems. The difference in the pressure of the gas upstream and downstream of a restrictor or restriction is determined.

Abstract: The present invention provides a method for analyzing particulate matter in a gas for analyzing simply and with high precision the particulate matter in an engine emission and an apparatus therefor by which dry soot, SOF and sulfate in PM contained in an engine emission can be fractionated individually even in a trifle amount. The present invention further provides a carbon differentiating and analyzing apparatus capable of differentiating and analyzing with precision the organic carbon and the elemental carbon contained in a sample and capable of performing a predetermined analysis with precision in a short time by reducing the period of time required for the analysis. The present invention is constituted such that a heating furnace is provided with a filter which has caught PM contained in engine emission. The filter is heated at a predetermined temperature while passing an inert gas into the heating furnace to evaporate the SOF and sulfate contained in PM.

Abstract: A self-adjusting, free-flowing pneumatic nebulizer interface is described for coupling fluid phase separation apparatus such as capillary electrophoresis apparatus or fluid-phase analyte delivery apparatus such as flow-injection analysis apparatus to gas phase, post-separation detection apparatus such as mass spectrometers, chemiluminescence detectors, or other similar gas phase detection apparatus. The interface combines the analytes with only the needed amount of sheath fluid to produce a combined flow whose magnitude automatically matches the self-aspiration rate of the pneumatic nebulizer interface, and which is combined with a gas flow to produce an aerosol. The resulting aerosol can then be either deposited directly on a surface, forwarded directly to a detection system or forwarded first to a conversion apparatus such as an oxidizer and the oxidized sample components are then forwarded to a detector.

Abstract: A method and apparatus for measuring the concentration of at least one gaseous component and/or vaporous component of a gaseous mixture in which a controlled sensor flame is introduced into the gaseous mixture and at least one narrow spectral band in the controlled sensor flame is optically measured. The concentration of the gaseous component using a result obtained from the optical measuring of the at least one narrow spectral band is then calculated. The method of this invention is particularly suitable for substantially real-time control of combustion processes.

Abstract: The present invention provides a method and apparatus for accurately determining weight loss of a sample during heating in a furnace. The method includes the steps of placing a sample in a heated furnace, heating the sample while measurements of sample weight are made, determining rate function from the sample weight measurements, producing a weight loss correction factor using the rate function and using the weight loss correction factor to obtain a corrected weight loss for the sample.

Abstract: A method and apparatus are provided for collecting a sample gaseous mercury, to differentiate between different gaseous mercury components. A quartz denuder module is provided having a coated extended surface for adsorbing reactive gaseous mercury. After collection of a sample, the coating it is heated to desorb the mercury as elemental gaseous mercury, which can then be detected and measured in conventional analyzer. During the sampling phase, as reactive gaseous mercury is removed from the sample flow in the denuder, the sample can then be passed to the analyzer for detection of elemental gaseous mercury. Where particulate mercury may be present, a filter trap can be provided downstream from the denuder. Separate steps can be provided for heating and pyrolysis of particulate mercury, for separate measurement in the analyzer. The pump module can be configured to a past the gas sample through scrubbers, to generate zero air as a flushing gas.

Abstract: Convenient methods for judging mouth odor with the use of an artificial mouth odor prepared by a convenient method which load any burdens neither on the operator nor on the subjects. Saliva collected immediately after wake-up is cultured under anaerobic conditions and head space components of the thus cultured saliva are analyzed, or anaerobic bacteria contained in the collected saliva are counted.