The Organic Material Contains Organic Compound Containing Nitrogen, Except If Present Solely As Nh4+ Patents (Class 516/102)
  • Patent number: 11186801
    Abstract: An oil gel capsule includes an oil gel including an oil and a gelator, and at least one surfactant bonded to the oil gel. A contact part for a vehicle includes an overlay layer formed on a surface of the contact part, the overlay layer comprising oil gel capsules, wherein the oil gel capsules including an oil gel including an oil and a gelator, and at least one surfactant bonded to the oil gel.
    Type: Grant
    Filed: September 29, 2020
    Date of Patent: November 30, 2021
    Assignees: Hyundai Motor Company, Kia Motors Corporation, Sahmyook University Industry-Academic Cooperation Foundation
    Inventors: Jeong-Uk An, Hong-Wook Lee, In-Woong Lyo, Kyung-Ku Yeo, Do-Young Wang, Ju-Yeong An, Myoung-Hwan Park, Yu-Ri Park
  • Patent number: 11180713
    Abstract: The present disclosure relates to manufacturing oil gel capsules and adding the same to an overlay layer of a contact part for a vehicle. The present disclosure may provide a method for manufacturing oil gel capsules and a method for manufacturing a contact part for a vehicle, including the oil gel capsules. The oil gels in the oil gel capsules manufactured by the present disclosure may respond to the temperature environment of a contact part for a vehicle, and an aggregation phenomenon of gelators or an aggregation phenomenon of surfactants may not occur even after an oil is released. Therefore, as oil gel capsules are added to an overlay layer, the present disclosure may improve low friction characteristics and seizure resistance characteristics of a contact part for a vehicle without any side effects caused by the above-described aggregation phenomenon.
    Type: Grant
    Filed: September 21, 2020
    Date of Patent: November 23, 2021
    Assignees: HYUNDAI MOTOR COMPANY, KIA MOTORS CORPORATION, SAHMYOOK UNI. INDUSTRY-ACADEMIC COOPERATION FNDN
    Inventors: Jeong-Uk An, Hong-Wook Lee, In-Woong Lyo, Kyung-Ku Yeo, Do-Young Wang, Ju-Yeong An, Myoung-Hwan Park, Yu-Ri Park
  • Patent number: 9833615
    Abstract: Embodiments of the present disclosure include medical apparatus, and related methods thereof. The apparatus may include a longitudinally extending lead, at least one electrode, an anchor component, and a control module. The lead may include a distal end and a proximal end. The at least one electrode may be coupled to the lead, wherein the at least one electrode may be disposed on the distal end of the lead. The anchor component may be disposed in the lead proximate of the at least one electrode. The anchor component may include solder. The control module may be operably coupled to the proximal end of the lead and may be configured to deliver energy to the at least one electrode.
    Type: Grant
    Filed: June 4, 2015
    Date of Patent: December 5, 2017
    Assignee: Boston Scientific Scimed, Inc.
    Inventors: Peter J. Pereira, David Ernest Wechter, John M. Barker, Jonathan Zoll, Mark W. Boden
  • Patent number: 9623345
    Abstract: Disclosed is a process which comprises mixing an alkylated aromatic acid with a mixture comprising a first liquid and a second liquid, thereby causing formation of an organogel comprising the alkylated aromatic acid and the first liquid.
    Type: Grant
    Filed: December 15, 2011
    Date of Patent: April 18, 2017
    Assignees: XEROX CORPORATION, NATIONAL RESEARCH COUNCIL OF CANADA
    Inventors: Darren A. Makeiff, Rina Carlini
  • Patent number: 9056126
    Abstract: A polymeric prodrug composition including a hydrogel, a biologically active moiety and a reversible prodrug linker. The prodrug linker covalently links the hydrogel and the biologically active moiety at a position and the hydrogel has a plurality of pores with openings on its surface. The diameter of the pores is larger than that of the biologically active moiety at least at all points of the pore between at least one of the openings and the position of the biologically active moiety.
    Type: Grant
    Filed: May 19, 2011
    Date of Patent: June 16, 2015
    Assignee: ASCENDIS PHARMA A/S
    Inventors: Ulrich Hersel, Harald Rau, Robert Schnepf, Dirk Vetter, Thomas Wegge
  • Publication number: 20140296354
    Abstract: Described herein are the one-pot synthesis and characterization of a library of low molecular weight peptoid compounds that are able to form gels at room temperature. The compounds are synthesized from biologically-based starting materials, are biocompatible, and are resistant to degradation by proteases and peptidases.
    Type: Application
    Filed: April 1, 2014
    Publication date: October 2, 2014
    Applicant: OLD DOMINION UNIVERSITY RESEARCH FOUNDATION
    Inventors: Guijun WANG, Hari P. R. MANGUNURU
  • Publication number: 20140148518
    Abstract: The invention discloses an environmentally-friendly pasty discharge agent for textile printing and a method for preparing the environmentally-friendly pasty discharge agent. The environmentally-friendly pasty discharge agent for textile printing is formed by the following raw materials according to part by weight: decamethylcyclopentasiloxane: 30-60 parts; thiourea dioxide: 40-70 parts; surfactant: 1-3 parts; and glycerol: 3-6 parts. Decamethylcyclopentasiloxane is put into a ball mill, a surfactant is added into the ball mill to make the decamethylcyclopentasiloxane dispersed or dissolved uniformly and then stirred uniformly, and then thiourea dioxide is added into the ball mill and ground together for 1-3 hours. In the invention, the special liquid compound decamethylcyclopentasiloxane does not chemically react with the thiourea dioxide; in addition, it isolates the thiourea dioxide from outside water and air, thus increasing the stability of the thiourea dioxide.
    Type: Application
    Filed: December 10, 2012
    Publication date: May 29, 2014
    Applicant: ZHEJIANG SCI-TECH UNIVERSITY
    Inventors: Jianzhong Shao, Lan Zhou, Yani Chen, Dongming Qi, Jinqiang Liu
  • Patent number: 8648120
    Abstract: The present invention provides a liquid rheology modifier containing compounds (A) and (B) selected from combination (1) of compound (A) selected from cationic surfactants and compound (B) selected from anionic aromatic compounds and combination (2) of compound (A) from cationic surfactants and compound (B) selected from brominated compounds; and dicarboxylic acid (C).
    Type: Grant
    Filed: September 5, 2007
    Date of Patent: February 11, 2014
    Assignee: Kao Corporation
    Inventors: Koji Koyanagi, Hotaka Yamamuro, Toshiharu Kojima
  • Publication number: 20130189197
    Abstract: [PROBLEMS TO BE SOLVED] It is an object of the present invention to provide a gelator containing a long chain oxyaminopolyol capable of forming a gel with a small amount thereof over a liquid property range from acidic to alkaline, and a gel having high environmental suitability, biocompatibility and biodegradability. [MEANS FOR SOLVING THE PROBLEMS] A gelator, characterized by containing a long chain oxyaminopolyol of Formula (I): (where R1 is a C12-16 saturated aliphatic group or a C12-16 unsaturated aliphatic group having one double bond; R2 is a substituent which an amino acid has; and X is an oxygen atom or NH) and a pharmaceutically acceptable salt thereof; a self-assembly formed by the self-assembly of the gelator; and a gel containing the gelator or the self-assembly, and water, an aqueous solution, a hydrophilic organic solvent or a hydrophilic organic solution, or a hydrophobic organic solvent or a hydrophobic organic solution.
    Type: Application
    Filed: March 12, 2013
    Publication date: July 25, 2013
    Applicant: NISSAN CHEMICAL INDUSTRIES, LTD.
    Inventor: NISSAN CHEMICAL INDUSTRIES, LTD.
  • Publication number: 20130158135
    Abstract: Disclosed is a composition comprising an organogel which comprises: (a) an alkylated aromatic acid compound of the formula or mixtures thereof, wherein R1, R2, R3, R4, and R5 each, independently of the other, are hydrogen, alkyl, aryl, arylalkyl, or alkyl, provided that at least one of R1, R2, R3, R4, and R5 is —X—Rc, wherein —X— is a linking group between Rc and the aromatic group and Rc is alkyl; and (b) an organic liquid.
    Type: Application
    Filed: December 15, 2011
    Publication date: June 20, 2013
    Applicants: NATIONAL RESEARCH COUNCIL OF CANADA, XEROX CORPORATION
    Inventors: Darren A. Makeiff, Rina Carlini
  • Patent number: 8377616
    Abstract: There is provided a colorant compound improved in the dispersibility of an azo pigment into a water-insoluble solvent. The colorant compound is represented by the following general formula (1). R1 denotes an alkyl group having 1 to 6 carbon atoms, or a phenyl group; R2 to R6 each denote a hydrogen atom, or a substituent represented by the following general formula (2); R7 to R11 each denote a hydrogen atom, a COOR12 group, or a CONR13R14 group; and R12 to R14 each denote a hydrogen atom, or an alkyl group having 1 to 3 carbon atoms; and P1 denotes a polymeric component; L1 denotes an alkylene group having 1 to 3 carbon atoms or an arylene group having 6 to 10 carbon atoms; and * denotes a binding site.
    Type: Grant
    Filed: December 21, 2011
    Date of Patent: February 19, 2013
    Assignee: Canon Kabushiki Kaisha
    Inventors: Yutaka Tani, Masashi Hirose, Takayuki Toyoda, Yasuaki Murai, Masatake Tanaka, Masashi Kawamura, Kei Inoue, Yuki Hasegawa
  • Patent number: 8263533
    Abstract: The present invention relates to a method of treating porous and permeable underground formations or cavities of reservoir rock or sand foundation type. The method consists in injecting a liquid composition comprising microgels into the formations in order to reduce the production of water, gas or sands, and/or for zone abandonment.
    Type: Grant
    Filed: August 22, 2005
    Date of Patent: September 11, 2012
    Assignees: IFP, Ste Exploit. de Produits pour Industries Chimiques
    Inventors: René Tabary, Guy Chauveteau, Paul Mallo, Olivier Braun, Eric Vilain, Alain Zaitoun
  • Publication number: 20120136074
    Abstract: Low molecular weight gelators, methods of making such gelators, organogels comprising such gelators and systems and methods of using such gelators for the containment and/or remediation of a release and/or spill of a crude oil, a petroleum product and/or a chemical is described. In exemplary systems and methods, gels and/or emulsions formed from the combination and/or contact of such gelators and at least one of a crude oil, a petroleum product and a chemical from a release and/or spill into the environment can be used to recover these oils or chemicals while allowing the gelators to be recovered and reused to clean up or contain additional crude oil, petroleum products or chemicals.
    Type: Application
    Filed: August 26, 2011
    Publication date: May 31, 2012
    Applicant: GEORGETOWN UNIVERSITY
    Inventors: Richard G. Weiss, Ajaya Mallia Viswanatha Mallya
  • Patent number: 8084123
    Abstract: The invention relates to a process for preparing a stable sol-gel solution. The solution may be used to form coating materials for metallic substrates, such as silver-based substrates for use in mirrors. The process includes the steps of preparing a sol-gel solution by bringing one or more molecular metal and/or metalloid precursors into contact with a medium comprising an organic solvent, adding at least one mercaptoorganosilane compound to the solution, hydrolyzing the solution obtained, and then adding one or more complexing agents to the solution.
    Type: Grant
    Filed: March 1, 2006
    Date of Patent: December 27, 2011
    Assignee: Commissariat a l'Energie Atomique
    Inventors: Laurence Beaurain, Philippe Prene, Yves Montouillout, Philippe Belleville
  • Patent number: 7989505
    Abstract: The compositions of hydrogel colloidal crystals are made from mixing an aqueous suspension of poly-N-isopropylacrylamide (“PNIPAM”)-co-allylamine microgels with dichloromethane, forming a PNIPAM-co-allylamine/dichloromethane mixture. The PNIPAM-co-allylamine/dichloromethane mixture is incubated for a period of time at a given temperature, forming the colloidal crystal material. The colloidal crystals can be stabilized by diffusing a glutaric dialdehyde solution into the colloidal crystal material. The concentration of polymer matrix microgels can determine the orientation of random or columnar crystals.
    Type: Grant
    Filed: September 21, 2006
    Date of Patent: August 2, 2011
    Assignee: University of North Texas
    Inventors: Zhibing Hu, Jun Zhou, Tong Cai, Shijun Tang, Manuel Marquez
  • Patent number: 7939472
    Abstract: Fluids viscosified with viscoelastic surfactants (VESs) may have their viscosities reduced (gels broken) by the direct or indirect action of a composition that contains at least one metal ion source and optionally at least one second source. An optional second source may be a chelating agent where at least one reducing agent source may be additionally optionally used. Another optional component with the metal ion source includes a second, different metal ion source. The breaking composition is believed to directly attack the VES itself, possibly by disaggregating or otherwise attacking the micellar structure of the VES-gelled fluid, and/or possibly by changing the chemical structure of the VES to give two or more products.
    Type: Grant
    Filed: September 21, 2009
    Date of Patent: May 10, 2011
    Assignee: Baker Hughes Incorporated
    Inventor: James B. Crews
  • Patent number: 7906558
    Abstract: The invention provides the use of novel, binary guanosine gels for simple, rapid and nondestructive solubilization of individual single walled carbon nanotubes (SWNTs) at high concentrations. The gels exhibit selectivity between metallic and semiconducting SWNTs and, further, among SWNTs with different chiralities.
    Type: Grant
    Filed: June 11, 2010
    Date of Patent: March 15, 2011
    Assignee: Rensselaer Polytechnic Institute
    Inventors: Linda B. McGown, Omkaram Nalamasu, Yuehua Yu
  • Publication number: 20110021644
    Abstract: The present invention provides for a composition comprising a siloxane having the formula: M1DM2 wherein M1=(R1)(R2)(R3)SiO1/2; M2=(R4)(R5)(R6)SiO1/2 and D=(R7)(Z)SiO2/2 where R1, R2, R3 R4, R5, R6 and R7 are each independently selected from the group consisting of 1 to 4 carbon monovalent hydrocarbon radicals, aryl, and a hydrocarbon group of 4 to 9 carbons containing an aryl group; Z is a pendant hydrophilic ionic group selected from the group consisting of R8-RA, R9 Rc and R10-RZ; RA being an anionic substituent, Rc a cationic substituent or Rz a zwitterionic substituent on the D group wherein the composition is resistant to hydrolysis under either basic or acidic conditions.
    Type: Application
    Filed: December 26, 2008
    Publication date: January 27, 2011
    Inventors: Mark D. Leatherman, George A. Policello, Wenging N. Peng, Liping Zheng, Roland Wagner, Suresh K. Rajarman, Xia Zijun
  • Patent number: 7850955
    Abstract: Gelling agents which contain a specific N-acylamino acid monoamide monoalkyl ester have a melting temperature of about 100° C., are capable of solidifying a wide variety of oily base materials including silicones, and do not cause “sweating” while retaining a practical level of gel strength. When applied to skin, the resulting gels have a good feeling, good spreadability, and good fittability to skin.
    Type: Grant
    Filed: July 3, 2008
    Date of Patent: December 14, 2010
    Assignee: Ajinomoto Co., Inc.
    Inventors: Keitaro Saito, Takanori Sugimoto, Tatsuya Hattori
  • Patent number: 7846876
    Abstract: The present invention relates to a surfactant composition containing a cationic surfactant (hereinafter referred to as a compound (A)), one or more compounds (hereinafter referred to as a compound (B)) selected from anionic aromatic compounds and bromide compounds and a cationic polymer (C), wherein compound (A) and (B) are selected when meeting the following condition: a combination of the compounds (A) and (B) ensures that that the viscosity (20° C.) of a solution prepared by mixing an aqueous solution SA of the compound (A) and an aqueous solution SB of the compound (B) in the same ratio is at least two times the viscosity of any one of the aqueous solutions (20° C.) before being mixed.
    Type: Grant
    Filed: October 6, 2004
    Date of Patent: December 7, 2010
    Assignee: Kao Corporation
    Inventors: Koji Koyanagi, Sadahara Miyamoto, Hotaka Yamamuro
  • Patent number: 7759401
    Abstract: The present invention relates to microemulsions of immiscible fluids stabilized by reactive ionic liquid surfactant wherein the ionic liquid surfactant has a melting point less than 80° C. The invention also relates to composite materials comprising a copolymer of ethylenically reactive species, wherein one of the species is a reactive ionic liquid surfactant having a melting point less than 80° C., and wherein the material also comprises non-reactive Class I fluid. The invention further relates to methods for synthesizing the composite materials comprising preparing a microemulsion of immiscible Class I fluid and Class II fluid stabilized by reactive ionic liquid surfactant wherein the ionic liquid surfactant has a melting point less than 80° C., and polymerizing the microemulsion to form a composite material.
    Type: Grant
    Filed: March 22, 2007
    Date of Patent: July 20, 2010
    Assignee: Eastern Michigan University
    Inventors: Feng Yan, John Texter
  • Patent number: 7678880
    Abstract: A molecular-oriented polymer gel and its cast film obtained by self-assembly of a self-organizable amphiphilic compound and a monomer interacting with the amphiphilic compound, and then polymerizing the monomer, and their production methods.
    Type: Grant
    Filed: August 7, 2003
    Date of Patent: March 16, 2010
    Assignees: Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Nobuo Kimizuka, Kazuhiro Kagawa, Takuya Nakashima
  • Patent number: 7595284
    Abstract: Fluids viscosified with viscoelastic surfactants (VESs) may have their viscosities reduced (gels broken) by the direct or indirect action of a composition that contains at least one metal ion source and optionally at least one second source. An optional second source may be a chelating agent where at least one reducing agent source may be additionally optionally used. Another optional component with the metal ion source includes a second, different metal ion source. The breaking composition is believed to directly attack the VES itself, possibly by disaggregating or otherwise attacking the micellar structure of the VES-gelled fluid, and/or possibly by changing the chemical structure of the VES to give two or more products.
    Type: Grant
    Filed: June 6, 2005
    Date of Patent: September 29, 2009
    Inventor: James B. Crews
  • Patent number: 7595349
    Abstract: Two new surfactant molecules are reported which contain thermally labile Diels-Alder adducts connecting the polar and non-polar sections of each molecule. The two surfactants possess identical non-polar dodecyl tail segments but exhibit different polar headgroups. The surfactants become soluble in water when anionic salts are formed through the deprotonation of the surfactant headgroups by the addition of potassium hydroxide. When either surfactant is exposed to temperature above about 60° C., the retro Diels-Alder reaction occurs, yielding hydrophilic and hydrophobic fragments or the aqueous solutions of the surfactants subsequently exhibit loss of all surface-active behavior.
    Type: Grant
    Filed: January 26, 2006
    Date of Patent: September 29, 2009
    Assignee: Sandia Corporation
    Inventors: James R. McElhanon, Blake A. Simmons, Thomas Zifer, Gregory M. Jamison, Douglas A. Loy, Kamyar Rahimian, Timothy M. Long, David R. Wheeler, Chad L. Staiger
  • Patent number: 7589054
    Abstract: Storage-stable organosilane quaternary compounds are provided in the form of adducts with urea (clathrates). The urea-organosilane quaternary clathrates enable the shipment, storage and preparation of compositions without hazardous solvents for end-use by manufacturers and consumers. Multifunctional cleansing and coating compositions are prepared employing the clathrates without sacrificing the properties and benefits of the organosilane quats.
    Type: Grant
    Filed: January 2, 2007
    Date of Patent: September 15, 2009
    Assignee: Resource Development L.L.C.
    Inventors: Howard G. Ohlhausen, Jerome H. Ludwig
  • Publication number: 20090176095
    Abstract: In accordance with the present invention, there are provided a triphenylmethane derivative represented by the following general formula (1), an organic gelling agent containing the triphenylmethane derivative, an organic gel and an organic fiber. The triphenylmethane derivatives of the present invention can exhibit a capability of gelling various organic solvents even when used in a small amount notwithstanding these derivatives are low-molecular compounds. The resultant organic gel is useful as materials usable under a high-temperature condition such as chemomechanical system materials, impact and vibration absorbing materials, drug base materials, controlled drug-release materials, and silicone oil gels for solidification of electrolytic solutions and for cosmetics. In addition, an organic nanofiber can be produced from the triphenylmethane derivative by a simple process.
    Type: Application
    Filed: January 19, 2005
    Publication date: July 9, 2009
    Inventor: Dai Oguro
  • Publication number: 20090111897
    Abstract: The invention provides the use of novel, binary guanosine gels for simple, rapid and nondestructive solubilization of individual single walled carbon nanotubes (SWNTs) at high concentrations. The gels exhibit selectivity between metallic and semiconducting SWNTs and, further, among SWNTs with different chiralities.
    Type: Application
    Filed: September 19, 2008
    Publication date: April 30, 2009
    Inventors: LINDA MCGOWN, Omkaram Nalamasu, Yuehua Yu
  • Publication number: 20090104141
    Abstract: A gel comprising a deacylated gellan gum, an effective amount of a sequestrant, an effective amount of a syneresis control agent, and a gelation inducer is described. Also methods for making the gel are disclosed including a method for forming heat-resistant gels comprising mixing deacylated gellan gum and xyloglucan; hydrating the blend; resting the hydrated blend until a gel forms. The gels can be used in a variety of applications such as air freshener gels.
    Type: Application
    Filed: October 19, 2007
    Publication date: April 23, 2009
    Applicant: CP KELCO US, INC.
    Inventors: Shinya Ikeda, Ronnie Yuan, Todd Anthony Talashek
  • Publication number: 20090026145
    Abstract: The present invention provides a process for dewatering a mineral slurry concentrate and increasing the production of the resulting filter cake consisting essentially of mixing an aqueous mineral slurry concentrate with an effective amount of a nonionic surfactant and an effective amount of a cationic polymer to form a nonionic surfactant and cationic polymer treated aqueous mineral slurry concentrate, and subjecting the treated aqueous mineral slurry concentrate to a liquid water removal process for dewatering the treated aqueous mineral slurry and for increasing the production of a resulting filter cake of the dewatered mineral slurry. An improved mineral slurry concentrate composition and an improved mineral concentrate filter cake is also disclosed.
    Type: Application
    Filed: July 24, 2007
    Publication date: January 29, 2009
    Inventors: Keith C. Hovland, Todd W. Groff, Monica A. Yorke, Charles R. Sundberg, Michael P. Lesar, Ruta O Rakutis
  • Publication number: 20080193746
    Abstract: The invention relates to a process for preparing a stable sol-gel solution comprising, in succession, the following steps: a) preparing a sol-gel solution by bringing one or more molecular metal and/or metalloid precursors into contact with a medium comprising an organic solvent; b) adding at least one mercaptoorganosilane compound to the solution obtained in a); c) hydrolyzing the solution obtained in b); and d) adding, to the solution obtained in c), one or more complexing agents chosen from carboxylic acids, ?-diketone compounds and hydroxamate compounds.
    Type: Application
    Filed: March 1, 2006
    Publication date: August 14, 2008
    Applicant: Commissariat a L'Energie Atomique
    Inventors: Laurence Beaurain, Philippe Prene, Yves Montouillout, Philippe Belleville
  • Patent number: 7374699
    Abstract: A slurry rheology modifier comprises a first water-soluble low-molecular compound [referred to hereinafter as compound (A)] and a second water-soluble low-molecular compound [referred to hereinafter as compound (B)] being different from the compound (A), wherein the viscosity of an aqueous solution at 20° C. prepared by mixing an aqueous solution SA (with a viscosity at 20° C. of 100 mPa·s or less) of compound (A) with an aqueous solution SB (with a viscosity at 20° C. of 100 mPa·s or less) of compound (B) in the ratio of 50/50 by weight can be at least twice as high as the viscosity of either aqueous solution before mixed.
    Type: Grant
    Filed: June 14, 2002
    Date of Patent: May 20, 2008
    Assignee: Kao Corporation
    Inventors: Hotaka Yamamuro, Koji Koyanagi, Daisuke Shiba
  • Publication number: 20080045612
    Abstract: The present invention relates to biomedical devices, and particularly contact lenses comprising a polymer having entangled therein at least one acyclic polyamide.
    Type: Application
    Filed: February 14, 2005
    Publication date: February 21, 2008
    Inventors: Osman Rathore, Shivkumar Mahadevan, Frank Molock, Azaan Alli, David Turner, Douglas G. Vanderlaan, Kevin P. McCabe
  • Patent number: 7332529
    Abstract: Thermoreversible organogelator compositions comprising compounds of the formula: where X is C6 to C12 alkylene and R is C9 to C12 alkyl, and their methods of use, including forming a gel to immobilize a solvent using the compound. The method can be used to form gels that can be used for the transportation of volatile organic solvents like gasoline, cooking oil, and contaminated organic liquids to be incinerated.
    Type: Grant
    Filed: October 26, 2004
    Date of Patent: February 19, 2008
    Inventor: Andrew J. Carr
  • Patent number: 7285575
    Abstract: Disclosed herein is a sol-gel polymerization process for synthesizing metal-doped organic gels. The process polymerizes metal salts of hydroxylated benzenes or hydroxylated benzene derivatives with alkyl or aryl aldehydes to form metal-doped, wet, organic gels. The gels can then be dried by supercritical solvent extraction to form metal-doped aerogels or by evaporation to form metal-doped xerogels. The aerogels and xerogels can then be pyrolyzed.
    Type: Grant
    Filed: June 9, 2003
    Date of Patent: October 23, 2007
    Assignee: The Regents of the University of California
    Inventors: Joe H. Satcher, Jr., Theodore F. Baumann
  • Patent number: 7060661
    Abstract: The present invention generally relates to aqueous, acidic compositions thickened with an amidoamine oxide gelling agent and/or viscoelastic surfactant of the general formula I: wherein R1 is a saturated or unsaturated, straight or branched chain aliphatic group of from about 7 to about 30 carbon atoms, R2 is a divalent alkylene group of 2–6 carbon atoms which may be linear or branched, substituted or unsubstituted, and R3 and R4 are independently C1–C4 alkyl or hydroxyalkyl groups or together they form a heterocyclic ring of up to six members, and R5 is hydrogen or a C1–C4 alkyl or hydroxyalkyl group. The aforementioned gelling agents advantageously provide gels that do not undergo phase separation over extended periods of time and exhibit high heat stability. The thickened acid gels of the invention have applications in household and industrial cleaners and degreasers, oilfield stimulation applications and the like.
    Type: Grant
    Filed: May 29, 2002
    Date of Patent: June 13, 2006
    Assignee: Akzo Nobel N.V.
    Inventors: Randy Ezell Dobson, Sr., David Kelly Moss, Raman Sarasamma Premachandran
  • Patent number: 7053127
    Abstract: A quaternary surfactant comprising a cyclic diamine group, compositions comprising the quaternized amido cyclic amine surfactant, a gelled aqueous composition comprising the quaternized amido cyclic amine surfactant, use of the gelled aqueous well treatment applications and methods of preparation and intermediates used to prepare the quaternized amido cyclic amine surfactant.
    Type: Grant
    Filed: September 16, 2002
    Date of Patent: May 30, 2006
    Assignee: Nalco Company
    Inventors: Duane S Treybig, Kin-Tai Chang
  • Patent number: 7041842
    Abstract: A ferrocene-containing, organic gelling compound represented by the following general formula (I): wherein R1 and R2 represent the same or different alkyl groups having 2 or more carbon atoms or alkyl groups containing at least one ether bond, X and Y independently represent a hydrogen atom or a substituent, and n represents an integer of 1 or 2, and a gel and a cast film using the compound.
    Type: Grant
    Filed: March 4, 2003
    Date of Patent: May 9, 2006
    Assignee: Honda Giken Kogyo Kabushiki Kaisha
    Inventors: Nobuo Kimizuka, Noriyuki Matsumoto, Kazuhiro Kagawa, Hiroshi Yokobayashi
  • Patent number: 6964940
    Abstract: This invention is a method of preparing a quaternized amidoamine surfactant comprising reacting an amidotertiaryamine of formula with methyl halide and alkylene oxide, an aqueous quaternized amidoamine surfactant composition, a gelled aqueous composition comprising the quaternized amidoamine surfactant composition and one or more salts or alcohols and use of the gelled aqueous composition for fracturing subterranean formations.
    Type: Grant
    Filed: January 8, 2003
    Date of Patent: November 15, 2005
    Assignees: Nalco Energy Services, L.P., Tomah Products, Inc.
    Inventors: Duane S. Treybig, Grahame N. Taylor, James A. Krogh, Michael J. Williams
  • Patent number: 6930203
    Abstract: The present invention relates to a novel class of gelling agents or thickeners, to a process for preparing gelling agents or thickeners and to their use to prepare the gels. The present gelling agents or thickeners have the form of an N,N?-disubstituted aldaramide or N,N?-disubstituted pentaramide.
    Type: Grant
    Filed: September 5, 2003
    Date of Patent: August 16, 2005
    Assignee: Applied NanoSystems B.V.
    Inventors: Johannes Henricus van Esch, André Heeres
  • Patent number: 6896876
    Abstract: A silica gel abrasive having good cleaning and low abrasion is prepared by combining at least two silica gels before adjusting the pH of the abrasive to a pH in the range of 3-6. One of the gels is washed at relatively lower temperature compared to the wash temperature of a second gel. The two gels are then milled and dried to a median particle size in the range of 5 to 12 microns. The volatiles content of the gel combination is in the range of 20-40% by weight. The resulting mixtures have low abrasion as measured by Einlehner, e.g., in the range of 0.5 to 3 when measured using a brass screen. A dentifrice composition comprising 10 to 25% of the abrasive has a PCR of at least 80 and can obtain PCR's greater than 100.
    Type: Grant
    Filed: January 31, 2002
    Date of Patent: May 24, 2005
    Assignee: W.R. Grace & Co.-Conn.
    Inventors: Cristian Libanati, James George Miller, Sandra Joan Kempske
  • Patent number: 6858673
    Abstract: A composition for hydrogels which comprises (A1) a copolymer which comprises 25 to 97 mol % of unit (a) derived from a compound represented by formula (1) and 3 to 75 mol % of unit (b) derived from a monomer represented by formula (2) and is soluble in aqueous media and (B) a polymer which has hydrophilic groups such as hydroxyl or carboxyl groups and is soluble in aqueous media; and a hydrogel comprising the composition. (X represents a divalent organic residue; Y represents alkyleneoxy, etc.; Z, R1, R2, R3, R4, and L2 each represents hydrogen, etc.; and L1 represents —C6H4—, etc.
    Type: Grant
    Filed: May 9, 2000
    Date of Patent: February 22, 2005
    Assignee: NOF Corporation
    Inventors: Nobuyuki Sakamoto, Kenshiro Shuto, Shujiro Sakaki, Ken Suzuki, Shinji Tanaka
  • Patent number: 6800663
    Abstract: The present invention relates to crosslinked polymers, synthesized through ring-opening polymerization of ethylenically unsaturated epoxides, in combination with &agr;-hydroxy acids using a hydrophilic macroinitiator, such as poly(ethylene glycol), to form substituted copolymers having ethylenically unsaturated functionality randomly distributed along the polyester polymer backbone. That copolymer is subsequently crosslinked to form a hydrogel network. More particularly, the present invention relates to the synthesis of biodegradable poly(&agr;-hydroxy acid-co-glycidyl methacrylate)-block-poly(ethylene glycol)-block-poly(&agr;-hydroxy acid-co-glycidyl methacrylate) copolymers, which are subsequently crosslinked to form hydrogel networks. The invention also relates to the use of these hydrogel networks in various applications, in particular, for the controlled release of drugs and proteins.
    Type: Grant
    Filed: October 18, 2002
    Date of Patent: October 5, 2004
    Assignee: Alkermes Controlled Therapeutics Inc. II,
    Inventors: Firouz Asgarzadeh, Henry R. Costantino
  • Patent number: 6776804
    Abstract: A printing paste containing: (a) 5 to 25% by weight of a polyurethane, (b) 1.5 to 20% by weight of a silicone, (c) 0 to 50% by weight of a further component and (d) water as the remainder, the sum of the amounts of components (a)+(b)+(c)+(d) being 100%, is suitable for printing textile materials.
    Type: Grant
    Filed: May 21, 2002
    Date of Patent: August 17, 2004
    Assignee: Ciba Specialty Chemicals Corporation
    Inventors: Alan Crabtree, Martin Lane, Ian George Potts, Leslie Walter Rouse
  • Publication number: 20040097602
    Abstract: The present invention relates to a novel class of gelling agents or thickeners, to a process for preparing gelling agents or thickeners and to their use to prepare the gels. The present gelling agents or thickeners have the form of an N,N′-disubstituted aldaramide or N,N′-disubstituted pentaramide.
    Type: Application
    Filed: September 5, 2003
    Publication date: May 20, 2004
    Inventors: Johannes Henricus van Esch, Andre Heeres
  • Patent number: 6670402
    Abstract: Methods of more rapidly producing aerogel products by means of a rapid solvent exchange of solvent inside wet gels with supercritical CO2 by injecting supercritical, rather than liquid, CO2 into an extractor that has been pre-heated and pre-pressurized to substantially supercritical conditions or above. Preferably, pressure waves are applied to the supercritical CO2 to enhance the solvent exchange. The rapid solvent exchange process is followed by depressurization, optionally with a gas exchange. Preferably, pressure waves are used to speed up the depressurization. The process greatly reduces the time for forming aerogel products.
    Type: Grant
    Filed: October 20, 2000
    Date of Patent: December 30, 2003
    Assignee: Aspen Aerogels, Inc.
    Inventors: Kang P. Lee, Redouane Begag, Zlatko Altiparmakov
  • Patent number: 6653355
    Abstract: An oil treating agent of W/O emulsion, wherein an aqueous dispersed phase is dispersed in an oily continuous phase, and wherein the dispersed phase is an alkaline mixture solution obtained by mixing water, a solution comprising water and an alcohol, or a water-free alcohol solution with an alkali hydroxide e.g. sodium hydroxide or with a metal alkoxide e.g. sodium alkoxide and the continuous phase comprises a liquid incompatible with the dispersed phase.
    Type: Grant
    Filed: September 5, 2000
    Date of Patent: November 25, 2003
    Assignees: Hakugen Co., Ltd., Prest Corporation
    Inventors: Tatsuo Kasahara, Tomohiro Shiiya, Kunimitsu Tamura
  • Patent number: 6579909
    Abstract: The present invention relates to a method for preparing microgels of controlled size. According to the method, a gelling composition comprising a polymer and a crosslinking additive intended for the polymer is injected into a porous and permeable medium, and a monodisperse solution of microgels of substantially constant size is recovered at the outlet. The invention also relates to an application of the method for reducing the permeability of porous and permeable formations of reservoir rock type.
    Type: Grant
    Filed: September 20, 2000
    Date of Patent: June 17, 2003
    Assignee: Institut Francais du Petrole
    Inventors: Guy Chauveteau, René Tabary, Michel Renard, Aziz Omari
  • Patent number: 6576679
    Abstract: A hydrogel formed by adding an anion having a molecular weight of 90 or more to an aqueous dispersion of a cationic amphiphile comprising a linear or branched alkyl group having 10 or less carbon atoms in a hydrophobic moiety. The hydrogel has a network having a bilayer-membrane, nano-fiber structure and undergoes a reversible gel-sol transformation.
    Type: Grant
    Filed: September 18, 2001
    Date of Patent: June 10, 2003
    Assignees: Honda Giken Kogyo Kabushiki Kaisha, Nobuo Kimizuka
    Inventors: Nobuo Kimizuka, Takuya Nakashima, Kazuhiro Kagawa
  • Patent number: 6506710
    Abstract: A method for controlling the rheology of aqueous systems, particularly for those intended for underground use, includes injecting an aqueous viscoelastic fluid containing a surfactant gelling agent into the system. The viscoelastic surfactant composition of the invention comprises, as a gelling agent, at least one fatty aliphatic amidoamine oxide in a glycol solvent. The composition also maintains the levels of free fatty acid and free amine within critical parameters in order to achieve superior performance. The additives may be incorporated in the viscoelastic fluid to tailor its use in stimulation fluids, drilling muds, fracture fluids, and in applications such as permeability modification, gravel packing, cementing, and the like.
    Type: Grant
    Filed: April 20, 2000
    Date of Patent: January 14, 2003
    Assignee: Akzo Nobel N.V.
    Inventors: Michael D. Hoey, Ralph Franklin, Douglas M. Lucas, Maurice Dery, Randy E. Dobson, Michael Engel, James F. Gadberry, Ramanair S. Premachandran, Glenda Del Carmen Vale
  • Patent number: RE41585
    Abstract: A method for controlling the rheology of aqueous systems, particularly for those intended for underground use, includes injecting an aqueous fluid containing a surfactant gelling agent into the system. The surfactant gelling agents are, for example, fatty aliphatic amidoamine oxides, salts of an alkoxylated monoamine with an aromatic dicarboxylic acid, and salts of an alkyldiamine with an aromatic dicarboxylic acid. The surfactant gelling agents can be absorbed onto particulate supports to facilitate delivery of the gelling agent. The additives may be incorporated in the viscoelastic fluid to tailor its use in hydraulic fluids, drilling muds, fracture fluids, and in applications such as permeability modification, gravel packing, cementing, and the like.
    Type: Grant
    Filed: May 30, 2002
    Date of Patent: August 24, 2010
    Inventors: Robert F. Farmer, Andress K. Doyle, Glenda Del Carmen Vale, James F. Gadberry, Michael D. Hoey, Randy E. Dobson