The Solid Phase Contains Organic Material Patents (Class 516/99)
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Patent number: 12157672Abstract: Provided is a method for recycling supercritical waste liquid and a method for producing a silica aerogel blanket capable of reducing the production costs and preventing the deterioration in thermal insulation performance of a silica aerogel blanket, the method including adding sulfuric acid to supercritical waste liquid to remove ammonium ions in the form of ammonium sulfate salt, the ammonium ions which are present in the supercritical waste liquid, and reusing supercritical waste liquid from which the ammonium ions are removed.Type: GrantFiled: November 13, 2018Date of Patent: December 3, 2024Assignee: LG CHEM, LTD.Inventors: Mi Ri Kim, Myung Eun Oh, Kyoung Shil Oh, Je Kyun Lee
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Patent number: 11360381Abstract: Provided are: a support frame for pellicle that has both low dust generation property and high light resistance, and further has an ion elution amount which is reduced to the utmost limit to an extent that haze is not generated even when a short wavelength laser is used for exposure light source, a pellicle using the support frame for pellicle, and a method for efficiently manufacturing the support frame for pellicle, support frame for pellicle which comprises a frame member comprising aluminum or aluminum alloy and an inorganic coating layer formed on the surface of the frame member, wherein the main chain of the inorganic coating layer is constituted by a —Si—O—Si—O— bond. An anodized film is preferably formed between the frame member and the inorganic coating layer.Type: GrantFiled: August 29, 2017Date of Patent: June 14, 2022Assignee: NIPPON LIGHT METAL COMPANY, LTD.Inventor: Takayuki Yamaguchi
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Patent number: 10714758Abstract: Electrodes and methods of creating co-continuous composite electrodes based on a highly porous current collector are provided. In one embodiment, a method for creating an electrode includes depositing a thin layer of material on the polymer template, removing polymer material of the polymer template and depositing a second material. The method may also include controlling internal surface area per unit volume and the active material thickness of at least the second material to tune the electrochemical performance of the electrode. In one embodiment, a composite electrode is provided including interpenetrating phases of a metal current collector, electrolytically active phase, and electrolyte.Type: GrantFiled: June 10, 2016Date of Patent: July 14, 2020Assignee: The Regents of the University of CaliforniaInventors: Jessica Witt, Ali Mohraz, Daniel Mumm
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Patent number: 10273405Abstract: Colloidal perovskite nanoplatelets can provide a material platform, with tunability extending from the deep UV, across the visible, into the near-IR. The high degree of spectral tunability can be achieved through variation of the cation, metal, and halide composition as well as nanoplatelet thickness.Type: GrantFiled: May 3, 2017Date of Patent: April 30, 2019Assignee: MASSACHUSETTS INSTITUTE OF TECHNOLOGYInventors: Mark Clayton Weidman, Michael Seitz, William Alfred Tisdale
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Publication number: 20150141532Abstract: Provided are a solvent-substitution solvent for producing a hydrophobized aerogel and a method for producing a hydrophobized aerogel. The solvent-substitution solvent includes pentanol in an amount of 41 wt % to 100 wt % and n-butanol in an amount of 0 wt % to 59 wt %. The method includes performing a solvent substitution process using the solvent-substitution solvent. If the solvent-substitution solvent is used for solvent substitution and/or hydrophobization in an aerogel production process, water (moisture) contained in a wet gel may be effectively substituted with the solvent-substitution solvent, and the solvent-substitution solvent may easily be collected at a high degree of purity and may be reused if necessary. Therefore, the rate of solvent loss may be minimized.Type: ApplicationFiled: May 9, 2013Publication date: May 21, 2015Inventors: Byoung-Hoon Kim, Jeong-Kun Yoo, Jung-Ho Han, Roshan Wagle
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Patent number: 8946305Abstract: The disclosure provides a method for crosslinking a colloid, including: (a) providing a colloid solution; (b) adding a crosslinking agent and solid particles to the colloid solution, wherein the amount of solid particles added is enough to convert the colloid solution into a solid mixture, and wherein a crosslinking reaction proceeds in the solid mixture; and (c) removing the solid particles from the solid mixture.Type: GrantFiled: September 10, 2012Date of Patent: February 3, 2015Assignee: Industrial Technology Research InstituteInventors: Chun-Jen Liao, Wen-Hsi Wang, Ming-Chia Yang, Wei-Ju Liao
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Patent number: 8916181Abstract: An aerosol glitter composition for achieving the “sugar” glitter effect comprises a solvent, binder, square polyester glitter, optionally a rheology modifier, and propellant.Type: GrantFiled: October 6, 2011Date of Patent: December 23, 2014Assignee: The Sherwin-Williams CompanyInventor: Christina M. Leposa
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Patent number: 8906973Abstract: Disclosed and claimed herein are hybrid silica aerogels containing non-polymeric, functional organic materials covalently bonded at one or both ends to the silica network of the aerogels through a C—Si bond between a carbon atom of the organic material and a silicon atom of the aerogel network. Methods of their preparation are also disclosed.Type: GrantFiled: November 30, 2011Date of Patent: December 9, 2014Assignee: Aspen Aerogels, Inc.Inventors: Wendell E Rhine, Decio Coutinho, Kiranmayi Deshpande
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Patent number: 8753534Abstract: Formulations useful for preparing hydrous aluminum oxide gels contain a metal salt including aluminum, an organic base, and a complexing agent. Methods for preparing gels containing hydrous aluminum oxide include heating a formulation to a temperature sufficient to induce gel formation, where the formulation contains a metal salt including aluminum, an organic base, and a complexing agent.Type: GrantFiled: January 7, 2010Date of Patent: June 17, 2014Inventor: Jack L. Collins
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Patent number: 8697758Abstract: A urea compound of the present invention is represented by general formula (I) shown below: wherein each of X1, X2 and X3 independently represents a hydrogen atom, an alkyl group or an aryl group. The aryl group may have one or more functional groups selected from the group consisting of halogen groups, alkyl groups and alkoxy groups.Type: GrantFiled: September 15, 2009Date of Patent: April 15, 2014Assignees: National University Corporation Shizuoka University, Nissian Chemical Industries, Ltd.Inventor: Masamichi Yamanaka
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Patent number: 8664143Abstract: A metal oxide-carbon composite includes a carbon aerogel with an oxide overcoat. The metal oxide-carbon composite is made by providing a carbon aerogel, immersing the carbon aerogel in a metal oxide sol under a vacuum, raising the carbon aerogel with the metal oxide sol to atmospheric pressure, curing the carbon aerogel with the metal oxide sol at room temperature, and drying the carbon aerogel with the metal oxide sol to produce the metal oxide-carbon composite. The step of providing a carbon aerogel can provide an activated carbon aerogel or provide a carbon aerogel with carbon nanotubes that make the carbon aerogel mechanically robust.Type: GrantFiled: October 25, 2011Date of Patent: March 4, 2014Assignee: Lawrence Livermore National Security, LLC.Inventors: Marcus A. Worsley, Thomas Yong-Jin Han, Joshua D. Kuntz, Octavio Cervantes, Alexander E. Gash, Theodore F. Baumann, Joe H. Satcher, Jr.
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Patent number: 8633255Abstract: Fluids viscosified with viscoelastic surfactants (VESs) may have their viscosities affected (increased or reduced, e.g. gels broken) by the indirect or direct action of a composition that contains at least one fatty acid that has been affected, modified or reacted with an alkali metal base, an alkali earth metal base, ammonium base, and/or organic base compound, optionally with an alkali metal halide salt, an alkali earth metal halide salt, and/or an ammonium halide salt. The composition containing the resulting saponification product is believed to either act as a co-surfactant with the VES itself to increase viscosity and/or possibly by disaggregating or otherwise affecting the micellar structure of the VES-gelled fluid. In a specific, non-limiting instance, a brine fluid gelled with an amine oxide surfactant may have its viscosity broken with a composition containing naturally-occurring fatty acids in canola oil or corn oil affected with CaOH, MgOH, NaOH and the like.Type: GrantFiled: July 19, 2012Date of Patent: January 21, 2014Assignee: Baker Hughes IncorporatedInventor: James B. Crews
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Patent number: 8629076Abstract: A metal oxide-carbon composite includes a carbon aerogel with an oxide overcoat. The metal oxide-carbon composite is made by providing a carbon aerogel, immersing the carbon aerogel in a metal oxide sol under a vacuum, raising the carbon aerogel with the metal oxide sol to atmospheric pressure, curing the carbon aerogel with the metal oxide sol at room temperature, and drying the carbon aerogel with the metal oxide sol to produce the metal oxide-carbon composite. The step of providing a carbon aerogel can provide an activated carbon aerogel or provide a carbon aerogel with carbon nanotubes that make the carbon aerogel mechanically robust. Carbon aerogels can be coated with sol-gel silica and the silica can be converted to silicon carbide, improving the thermal stability of the carbon aerogel.Type: GrantFiled: March 18, 2011Date of Patent: January 14, 2014Assignee: Lawrence Livermore National Security, LLCInventors: Marcus A. Worsley, Joshua D. Kuntz, Theodore F. Baumann, Joe H. Satcher, Jr.
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Patent number: 8592516Abstract: A process for producing a water-absorbing polymer by polymerizing a monomer solution and drying the resulting hydrogel by means of a heated gas stream comprises effecting the drying in two or more temperature zones, and/or the gas stream is flowed against the hydrogel upwardly in the upstream sector of the belt dryer and downwardly in the downstream sector of the belt dryer, the direction of flow being reversed at a water content of 15% to 45% by weight for the hydrogel, and/or the hydrogel layer is flowed against in a belt dryer upwardly to some extent at least, the gas velocity being 5% to 30% of the gas velocity required to lift the hydrogel off the belt, also apparatus for carrying out the process and use of the water-absorbing polymers produced by the process to produce hygiene articles.Type: GrantFiled: March 23, 2006Date of Patent: November 26, 2013Assignee: BASF AktiengesellschaftInventors: Matthias Weismantel, Stefan Bruhns, Dominicus van Esbroeck
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Patent number: 8501825Abstract: Formulations useful for preparing hydrous hafnium oxide gels contain a metal salt including hafnium, an acid, an organic base, and a complexing agent. Methods for preparing gels containing hydrous hafnium oxide include heating a formulation to a temperature sufficient to induce gel formation, where the formulation contains a metal salt including hafnium, an acid, an organic base, and a complexing agent.Type: GrantFiled: January 7, 2010Date of Patent: August 6, 2013Inventors: Jack L. Collins, Rodney D. Hunt, Frederick C. Montgomery
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Patent number: 8436052Abstract: Formulations useful for preparing hydrous cerium oxide gels contain a metal salt including cerium, an organic base, and a complexing agent. Methods for preparing gels containing hydrous cerium oxide include heating a formulation to a temperature sufficient to induce gel formation, where the formulation contains a metal salt including cerium, an organic base, and a complexing agent.Type: GrantFiled: January 7, 2010Date of Patent: May 7, 2013Inventors: Jack L. Collins, Anthony Chi
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Patent number: 8263533Abstract: The present invention relates to a method of treating porous and permeable underground formations or cavities of reservoir rock or sand foundation type. The method consists in injecting a liquid composition comprising microgels into the formations in order to reduce the production of water, gas or sands, and/or for zone abandonment.Type: GrantFiled: August 22, 2005Date of Patent: September 11, 2012Assignees: IFP, Ste Exploit. de Produits pour Industries ChimiquesInventors: René Tabary, Guy Chauveteau, Paul Mallo, Olivier Braun, Eric Vilain, Alain Zaitoun
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Patent number: 8236864Abstract: Fluids viscosified with viscoelastic surfactants (VESs) may have their viscosities affected (increased or reduced, e.g. gels broken) by the indirect or direct action of a composition that contains at least one fatty acid that has been affected, modified or reacted with an alkali metal base, an alkali earth metal base, ammonium base, and/or organic base compound, optionally with an alkali metal halide salt, an alkali earth metal halide salt, and/or an ammonium halide salt. The composition containing the resulting saponification product is believed to either act as a co-surfactant with the VES itself to increase viscosity and/or possibly by disaggregating or otherwise affecting the micellar structure of the VES-gelled fluid. In a specific, non-limiting instance, a brine fluid gelled with an amine oxide surfactant may have its viscosity broken with a composition containing naturally-occurring fatty acids in canola oil or corn oil affected with CaOH, MgOH, NaOH and the like.Type: GrantFiled: May 28, 2010Date of Patent: August 7, 2012Assignee: Baker Hughes IncorporatedInventor: James B. Crews
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Patent number: 8222310Abstract: An extruded polypropylene type resin foam having a high expansion ratio of at least 15 times and a closed cell ratio of at least 70% and excellent in the heat insulation property, and its production process, are provided. An extruded polypropylene type resin foam, which is produced by extrusion-foaming a polypropylene type resin composition containing a linear polypropylene type resin having a melt tension at 230° C. of from 5 to 30 g, by using a blowing agent containing at least a hydrocarbon type gas, and which has an expansion ratio of at least 15 times and a closed cell ratio of at least 70%.Type: GrantFiled: September 12, 2008Date of Patent: July 17, 2012Assignee: Asahi Fiber Glass Company, LimitedInventors: Toru Itadani, Masaaki Ono
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Patent number: 8222308Abstract: A method of preparing a porous polymer structure comprising the steps of: forming a liquid composition comprising at least one polymer dissolved in at least one solvent; subjecting the liquid composition to stress, and if necessary also to a reduction in temperature, to cause the liquid composition to form a bi-continuous phase separated composition, the bi-continuous phase separated composition comprising a polymer rich phase and a polymer poor phase; solidifying the at least one polymer in the polymer rich phase; and removing the polymer poor phase from the polymer rich phase to provide the porous polymer structure having a bi-continuous morphology from the polymer rich phase.Type: GrantFiled: April 5, 2007Date of Patent: July 17, 2012Assignee: The University of QueenslandInventors: Justin John Cooper-White, Yang Cao
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Patent number: 8211953Abstract: The present invention relates to a polyolefin resin foam which includes a polyolefin resin composition includes: (A) a rubber and/or a thermoplastic elastomer; (B) a polyolefin resin; and (C) at least one aliphatic compound selected from an aliphatic acid, an aliphatic acid amide and an aliphatic acid metallic soap, the compound having a polar functional group and having a melting point of 50 to 150° C., in which a content of the aliphatic compound is 1 to 5 parts by weight based on 100 parts by weight of the total amount of the rubber and/or thermoplastic elastomer and the polyolefin resin. The polyolefin resin foam of the invention is excellent in flexibility and cushioning properties, and has good processability, especially excellent cutting processability.Type: GrantFiled: September 27, 2007Date of Patent: July 3, 2012Assignee: Nitto Denko CorporationInventors: Makoto Saitou, Yasuyuki Tokunaga, Takio Itou, Hiroki Fujii
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Patent number: 8163807Abstract: A blending apparatus is provided, the blending apparatus including: an outer tube; and at least one inner tube disposed inside the outer tube, wherein a distal end, in a lengthwise direction, of the inner tube is located at an intermediate position, in a lengthwise direction, of the outer tube, and the inner tube has plural of through holes in a vicinity of the distal end thereof.Type: GrantFiled: April 23, 2009Date of Patent: April 24, 2012Assignee: Fuji Xerox Co., Ltd.Inventors: Hideya Katsuhara, Hiroyuki Moriya, Tomohito Nakajima, Kazuya Hongo
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Patent number: 8142899Abstract: To provide a heat-resistant resin composition which has excellent heat resistance, does not show a reduced mechanical strength such as flexural strength even after being passed rough a reflow furnace and heat-treated under high temperature conditions, and also has an excellent flame retardancy; a production method of the heat-resistant resin composition; a heat-resistant resin-molded article; and a surface mount electronic component. The heat-resistant resin composition includes a polyarylene sulfide resin (A) and an aromatic polyamide (B) having terephthalic acid amide as an essential structural unit at a former/latter ratio of 70/30 to 95/5 by mass. In a molded article composed of the heat-resistant resin composition, the average diameter of holes formed by etching a broken-out section of the molded article with an organic solvent is 0.1 to 1.0 ?m, where the broken-out section is observed on a scanning electron microscope (2,500 times).Type: GrantFiled: December 26, 2006Date of Patent: March 27, 2012Assignee: DIC CorporationInventor: Yasuyuki Yoshino
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Patent number: 8133923Abstract: Single domain wafer-scale colloidal crystals and macroporous polymers are formed by dispersing concentrated solutions of colloids, desirably monodisperse silica colloids, in a viscous monomer, desirably ethoxylated trimethylolpropane triacrylate, and spin-coating them onto a substrate. Subsequent photopolymerization produces three-dimensionally ordered colloidal crystals trapped inside a polymer matrix. Selective removal of the polymer matrix, such as by oxygen plasma treatment, or removal of the silica spheres, such as by wet etching, produces large-area colloidal crystals and macroporous polymers, respectively.Type: GrantFiled: May 19, 2010Date of Patent: March 13, 2012Assignee: Corning IncorporatedInventor: Peng Jiang
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Patent number: 8133535Abstract: An antipenetrating agent is to be added to a solvent ink for preventing penetration of the solvent ink into a medium to be printed. The antipenetrating agent includes inorganic fine particles and a resin soluble in an organic solvent.Type: GrantFiled: March 20, 2008Date of Patent: March 13, 2012Assignee: Mimaki Engineering Co., Ltd.Inventors: Tomotaka Furuhata, Satoshi Takezawa, Isao Tabayashi
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Patent number: 8084123Abstract: The invention relates to a process for preparing a stable sol-gel solution. The solution may be used to form coating materials for metallic substrates, such as silver-based substrates for use in mirrors. The process includes the steps of preparing a sol-gel solution by bringing one or more molecular metal and/or metalloid precursors into contact with a medium comprising an organic solvent, adding at least one mercaptoorganosilane compound to the solution, hydrolyzing the solution obtained, and then adding one or more complexing agents to the solution.Type: GrantFiled: March 1, 2006Date of Patent: December 27, 2011Assignee: Commissariat a l'Energie AtomiqueInventors: Laurence Beaurain, Philippe Prene, Yves Montouillout, Philippe Belleville
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Patent number: 8047703Abstract: A method and apparatus for gelling liquid propane and other liquefied gasses includes a temperature controlled churn mixer, vacuum pump, liquefied gas transfer tank, and means for measuring amount of material entering the mixer. The apparatus and method are particularly useful for the production of high quality rocket fuels and propellants.Type: GrantFiled: September 2, 2010Date of Patent: November 1, 2011Assignee: CFD Research CorporationInventors: Adam Elliott, Roberto DiSalvo, Phillip Shepherd, Ryan Kosier
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Patent number: 8044106Abstract: Fluids viscosified with viscoelastic surfactants (VESs) may have their viscosities affected (increased or reduced) by the indirect or direct action of a composition that contains at least one fatty acid that has been affected, modified or reacted with an alkali metal halide salt, an alkaline earth metal halide salt, and/or an ammonium salt and a water soluble base. The composition containing the resulting saponification product is believed to either act as a co-surfactant with the VES itself to increase viscosity and/or possibly by disaggregating or otherwise affecting the micellar structure of the VES-gelled fluid. In a non-limiting instance, a brine fluid gelled with an amine oxide surfactant has its viscosity broken with a composition containing naturally-occurring fatty acids in canola oil reacted with a water soluble base such as NaOH, KOH, NH4OH, and the like with an alkali halide salt such as CaCl2, MgCl2, NaCl, NH4Cl and the like.Type: GrantFiled: October 31, 2007Date of Patent: October 25, 2011Assignee: Baker Hughes IncorporatedInventor: James B. Crews
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Patent number: 8044108Abstract: A porous polymer blend, and a method of producing a porous polymer blend from at least two immiscible polymers. The at least two immiscible polymer being blended together and exhibiting the absence of complete phase separation. The method of producing a porous polymer blend comprising: forming a liquid composition comprising at least two immiscible polymers dissolved in a common solvent; subjecting the liquid composition to a reduction in temperature to cause at least two immiscible polymers to phase separate into a common polymer rich phase and a common polymer poor phase; solidifying the at least two immiscible polymers in the common polymer rich phase so as to avoid complete phase separation of the at least two immiscible polymers; and removing the common polymer pore phase to provide a blend of the at least two immiscible polymers having a porous morphology.Type: GrantFiled: April 5, 2007Date of Patent: October 25, 2011Assignees: The University of Queensland, The University of MelbourneInventors: Justin John Cooper-White, Yang Cao, Andrew Stewart Rowlands
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Patent number: 7989505Abstract: The compositions of hydrogel colloidal crystals are made from mixing an aqueous suspension of poly-N-isopropylacrylamide (“PNIPAM”)-co-allylamine microgels with dichloromethane, forming a PNIPAM-co-allylamine/dichloromethane mixture. The PNIPAM-co-allylamine/dichloromethane mixture is incubated for a period of time at a given temperature, forming the colloidal crystal material. The colloidal crystals can be stabilized by diffusing a glutaric dialdehyde solution into the colloidal crystal material. The concentration of polymer matrix microgels can determine the orientation of random or columnar crystals.Type: GrantFiled: September 21, 2006Date of Patent: August 2, 2011Assignee: University of North TexasInventors: Zhibing Hu, Jun Zhou, Tong Cai, Shijun Tang, Manuel Marquez
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Patent number: 7951849Abstract: The present invention relates to the field of gels. The invention also relates to an improved method for manufacturing gels. In particular the invention relates to a new class of material, fluid-bicontinuous particle-stabilized gels, and a method of making the same. The fluid-bicontinuous particle-stabilized gels comprise at least a first fluid, a second fluid, and a continuous layer of particles positioned at a continuous interface between the first fluid and the second fluid.Type: GrantFiled: July 1, 2005Date of Patent: May 31, 2011Assignee: The University Court of the University of EdinburghInventors: Michael Elmhirst Cates, Paul Stephen Clegg, Stefan Ulrich Egelhaaf, Wilson Che Poon
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Patent number: 7932208Abstract: A method of preparing stable, transparent photocatalytic titanium dioxide sots is disclosed which involves thermal treatment of a suspension of amorphous titanium dioxide in the presence of certain alpha-hydroxy acids. The sots comprise titanium dioxide particles in the anatase form having a crystallite size less than about 10 nm and exhibit excellent stability and transparency at basic, neutral, and acid pH.Type: GrantFiled: June 29, 2010Date of Patent: April 26, 2011Assignee: Millennium Inorganic Chemicals, Inc.Inventors: Guoyi Fu, Billiejo M. Monk, Robert McIntyre
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Patent number: 7863338Abstract: Absorbent polymer granulate comprising the following process steps: i) polymerization of an aqueous monomer solution to obtain a polymer gel; ii) comminution of the polymer gel to obtain a gel granulate; and iii) drying of the gel granulate, and is characterized in that the gel granulate after step ii) has a spread behavior. The production process of an absorbent polymer distinguishes itself by a particularly efficient drying step iii), which enables a particularly gentle and uniform drying of the gel granulate. The obtained absorbent polymers and products and items produced therefrom have a particularly uniform product quality and constant physical-chemical properties.Type: GrantFiled: April 19, 2010Date of Patent: January 4, 2011Assignee: Evonik Stockhausen GmbHInventors: Volker Becker, Heinz-Peter Grupe, Detlef Jung, Armin Reimann
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Patent number: 7846876Abstract: The present invention relates to a surfactant composition containing a cationic surfactant (hereinafter referred to as a compound (A)), one or more compounds (hereinafter referred to as a compound (B)) selected from anionic aromatic compounds and bromide compounds and a cationic polymer (C), wherein compound (A) and (B) are selected when meeting the following condition: a combination of the compounds (A) and (B) ensures that that the viscosity (20° C.) of a solution prepared by mixing an aqueous solution SA of the compound (A) and an aqueous solution SB of the compound (B) in the same ratio is at least two times the viscosity of any one of the aqueous solutions (20° C.) before being mixed.Type: GrantFiled: October 6, 2004Date of Patent: December 7, 2010Assignee: Kao CorporationInventors: Koji Koyanagi, Sadahara Miyamoto, Hotaka Yamamuro
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Patent number: 7816412Abstract: Electrically conductive adhesive hydrogels formed from a composition which generally includes a monomer, an initiator, an organic solvent, and a cross-linking agent are suitable for use as skin contact adhesives and, particularly, suitable for use as an electrical interface for disposable medical devices. The present hydrogels provide for reduced skin irritation and/or malodor properties, hydrate a subject's skin, readily wet around a subject's skin surface hair, and protect against burning of a subject upon or due to electrical stimulation through the hydrogel.Type: GrantFiled: February 23, 2007Date of Patent: October 19, 2010Assignee: ConMed CorporationInventors: Ali Yahiaoui, Anthony Stephen Spencer, Charles Bolian
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Patent number: 7772163Abstract: Well treating composites are composed of an organic lightweight material and a weight modifying agent. The organic lightweight material preferably forms the continuous phase and the weight modifying agent forms the discontinuous phase. The apparent specific gravity (ASG) of the organic lightweight material is less than the ASG of the well treating composite. The composite of the invention is particularly useful in hydraulic fracturing fluids as lightweight proppants as well as in sand control methods, such as gravel packing and frac packing A subterranean formation may be treated by injecting the well treating composite into the formation in order to increase fracture conductivity, reduce the generation of fines, reduced unwanted water production and/or reduce particulate production.Type: GrantFiled: January 9, 2008Date of Patent: August 10, 2010Assignee: BJ Services Company LLCInventors: Harold Dean Brannon, Allan Ray Rickards, Christopher John Stephenson
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Patent number: 7763565Abstract: A method of preparing stable, transparent photocatalytic titanium dioxide sols is disclosed which involves thermal treatment of a suspension of amorphous titanium dioxide in the presence of certain alpha-hydroxy acids. The sots comprise titanium dioxide particles in the anatase form having a crystallite size less than about 10 nm and exhibit excellent stability and transparency at basic, neutral, and acid pH.Type: GrantFiled: August 31, 2007Date of Patent: July 27, 2010Assignee: Millennium Inorganic Chemicals, Inc.Inventors: Guoyi Fu, BillieJo M. Monk, Robert McIntyre
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Patent number: 7737189Abstract: The invention relates to a process for the preparation of monolithic xerogels and aerogels of silica/latex hybrids under subcritical conditions. In the two-stage synthesis of these alcogels in the presence of an acid-base catalyst, the hydrolysis and polycondensation of a silicon alkoxide are carried out in an organic medium containing excess water. A latex consisting of polybutyl methacrylate and polybutyl acrylate, modified with alkoxysilane groups, is first synthesized and then incorporated in the mixture either in the first stage in order to effect its co-hydrolysis with the silicon alkoxide, or in the second stage to effect its co-condensation with the previously hydrolysed colloidal silica. The resulting alcogels are aged, washed, and dried under subcritical conditions. This process gives hybrid products containing 0.1-50 wt-% of latex and having a density of 300-1300 kg/m3, a porosity of 40-85%, a specific surface area of 400-900 m2/g and a mean pore diameter of 2-12 nm.Type: GrantFiled: April 4, 2006Date of Patent: June 15, 2010Assignee: Instituto Superior TecnicoInventors: José Manuel Gaspar Martinho, Laura Maria Ilharco De Almeida Santos, José Paulo Sequira Farinha, Alexandra Marina Abrantes Fidalgo, Pedro Oliveira Martinho
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Patent number: 7732496Abstract: Structurally stable and mechanically strong ceramic oxide aerogels are provided. The aerogels are cross-linked via organic polymer chains that are attached to and extend from surface-bound functional groups provided or present over the internal surfaces of a mesoporous ceramic oxide particle network via appropriate chemical reactions. The functional groups can be hydroxyl groups, which are native to ceramic oxides, or they can be non-hydroxyl functional groups that can be decorated over the internal surfaces of the ceramic oxide network. Methods of preparing such mechanically strong ceramic oxide aerogels also are provided.Type: GrantFiled: November 3, 2005Date of Patent: June 8, 2010Assignees: Ohio Aerospace Institute, The United States of America as represented by the Administrator of the National Aeronautics and Space AdministrationInventors: Nicholas Leventis, Mary Ann B. Meador, James C. Johnston, Eve F. Fabrizio, Ulvi F. Ilhan
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Patent number: 7728044Abstract: Fluids viscosified with viscoelastic surfactants (VESs) may have their viscosities affected (increased or reduced, e.g. gels broken) by the indirect or direct action of a composition that contains at least one fatty acid that has been affected, modified or reacted with an alkali metal base, an alkali earth metal base, ammonium base, and/or organic base compound, optionally with an alkali metal halide salt, an alkali earth metal halide salt, and/or an ammonium halide salt. The composition containing the resulting saponification product is believed to either act as a co-surfactant with the VES itself to increase viscosity and/or possibly by disaggregating or otherwise affecting the micellar structure of the VES-gelled fluid. In a specific, non-limiting instance, a brine fluid gelled with an amine oxide surfactant may have its viscosity broken with a composition containing naturally-occurring fatty acids in canola oil or corn oil affected with CaOH, MgOH, NaOH and the like.Type: GrantFiled: March 10, 2006Date of Patent: June 1, 2010Assignee: Baker Hughes IncorporatedInventor: James B. Crews
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Patent number: 7728045Abstract: The process according to the invention for production of an absorbent polymer comprising the following process steps: i) polymerization of an aqueous monomer solution to obtain a polymer gel; ii) comminution of the polymer gel to obtain a gel granulate; and iii) drying of the gel granulate, and is characterized in that the gel granulate after step ii) has a spread behavior. The production process of an absorbent polymer distinguishes itself by a particularly efficient drying step iii), which enables a particularly gentle and uniform drying of the gel granulate. The obtained absorbent polymers and products and items produced therefrom have a particularly uniform product quality and constant physical-chemical properties.Type: GrantFiled: April 20, 2005Date of Patent: June 1, 2010Assignee: Evonik Stockhausen GmbHInventors: Volker Becker, Heinz-Peter Grupe, Detlef Jung, Armin Reimann
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Publication number: 20100125106Abstract: A blending apparatus is provided, the blending apparatus including: an outer tube; and at least one inner tube disposed inside the outer tube, wherein a distal end, in a lengthwise direction, of the inner tube is located at an intermediate position, in a lengthwise direction, of the outer tube, and the inner tube has plural of through holes in a vicinity of the distal end thereof.Type: ApplicationFiled: April 23, 2009Publication date: May 20, 2010Applicant: FUJI XEROX CO., LTD.Inventors: Hideya KATSUHARA, Hiroyuki MORIYA, Tomohito NAKAJIMA, Kazuya HONGO
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Publication number: 20100079424Abstract: A display medium and a display are provided. The display medium includes a thermal-sensitive solution and a number of micro particles. The micro particles are dispersed in the thermal-sensitive solution. At a first temperature, the thermal-sensitive solution is in a liquid form, such that the micro particles move freely. At a second temperature, the thermal-sensitive solution is in a colloid form, such that the micro particles are fixed. The first temperature differs from the second temperature.Type: ApplicationFiled: January 21, 2009Publication date: April 1, 2010Applicant: CHUNGHWA PICTURE TUBES, LTD.Inventors: Shih-Kang Fan, Cheng-Pu Chiu, Ching-Hsiang Hsu, Mei-Tsao Chiang, Chi-Neng Mo
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Patent number: 7683098Abstract: Methods for manufacturing nanomaterial dispersions, such as nanomaterial concentrates, and related nanotechnology are provided. The nanomaterial concentrates provided can be more cheaply stored and transported compared to non-concentrate nanomaterial forms.Type: GrantFiled: June 21, 2005Date of Patent: March 23, 2010Assignee: PPG Industries Ohio, Inc.Inventor: Tapesh Yadav
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Patent number: 7582231Abstract: The present invention is directed to a composite having tunable radiation diffracting properties which includes a flexible, water-free polymeric matrix and a crystalline colloidal array of particles having a lattice spacing, the array being embedded in the polymeric matrix and the lattice spacing changing responsive to stress applied to the polymeric matrix, thereby causing the radiation diffracting properties to change, wherein the polymeric matrix, the lattice spacing and the radiation diffracting properties all return to their original state essentially immediately upon removal of the stress. The present inventive composite is preferably made by a process, which involves forming a preliminary hydrogel polymerized crystalline colloidal array (PCCA), dehydrating the PCCA, and then forming a final, encapsulating polymeric matrix.Type: GrantFiled: September 16, 2005Date of Patent: September 1, 2009Inventors: Stephen H. Foulger, Ping Jiang
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Publication number: 20090208746Abstract: Methods of sol-gel processing for preparing of stabilized or doped gels and nanoparticles are described. The invention also relates to stabilized or doped gels and nanoparticles prepared by the described methods.Type: ApplicationFiled: December 1, 2006Publication date: August 20, 2009Inventor: Crina Silvia Suciu
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Patent number: 7528178Abstract: A process for the preparation of beads having a crosslinked inorganic matrix with a size controlled in the millimeter range, which comprises pouring a suspension comprising a precursor of the inorganic matrix and an alginate drop wise into a solution of a polyvalent cation salt with a pH of less than 3, to obtain a reaction medium, in which the alginate gels, and crosslinking the precursor of the inorganic matrix by a sol-gel process.Type: GrantFiled: July 18, 2003Date of Patent: May 5, 2009Assignee: Centre National de la Recherche ScientifiqueInventors: Eric Prouzet, Miriam Tokumoto, Aurore Krivaya
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Patent number: 7524441Abstract: A color filter composition comprises a mixture of a binder and a monomer in a predetermined ratio, a pigment, and a solvent. The predetermined ratio is a ratio of the binder to the monomer and ranges from about 50:50 to about 60:40. The color filter composition further comprises a solid powder having a weight percent in the color filter composition ranging from about 12% to about 18%, wherein the solid powder includes the pigment. The pigment has a weight percent in the solid powder ranging from about 28% to about 38%.Type: GrantFiled: March 12, 2004Date of Patent: April 28, 2009Assignee: Samsung Electronics Co., Ltd.Inventors: Sang-Ki Jeong, Dong-Uk Choi, Sung-Ki Jung
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Publication number: 20090023103Abstract: A process of producing a solid dispersion of an organic compound comprising a step in which after solid dispersing an organic compound, a temperature is elevated stepwise to subject the dispersion to heat treatment.Type: ApplicationFiled: September 8, 2008Publication date: January 22, 2009Applicant: FUJIFILM CORPORATIONInventor: Satoru TODA
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Patent number: 7470726Abstract: A method for transiently and controllably enhancing the adhesion of a hydrogel composition to select substrates for facilitating the handling of the hydrogel composition during processing, includes the steps of placing the hydrogel composition in a liquid state onto a plastic film facestock, which has biaxially-oriented polypropylene, microporous cellulose acetate or a combination thereof, for temporarily adhering the hydrogel composition to the sheets of the roll stock during processing of the hydrogel composition, and then removing the hydrogel composition from the sheets of the roll stock, after processing of the hydrogel composition is complete, without any adverse affect on the textural qualities of the hydrogel composition.Type: GrantFiled: November 29, 2005Date of Patent: December 30, 2008Inventor: Robert D. Kross