Mixing Combined With Non-mixing Operation Or Step, Successively Or Simultaneously (e.g., Heating, Cooling, Ph Change, Ageing, Milling) Patents (Class 516/928)
  • Patent number: 6065903
    Abstract: Methods are disclosed for preparation of chemically-stabilized emulsions of tall oil in water. Temperature and pH are controlled during preparation of the emulsions so as to prevent saponification and neutralization of acids in the tall oil component. The final emulsions have pHs in the range of from about 3.0 to 5.0 and remain phase stable for extended periods of time. Methods are disclosed for using the emulsions for soil treatment to improve soil stabilization and load bearing capacity for roadbed use, for treatment of reclaimed asphalt pavement for reuse as a stabilized base course for roadway construction and for remediation of heavy metal contaminated soil.
    Type: Grant
    Filed: December 22, 1998
    Date of Patent: May 23, 2000
    Assignee: Vinzoyl Technical Services, L.L.C.
    Inventor: Michael P. Doyle
  • Patent number: 6022525
    Abstract: Microcapsules are prepared by a process comprising the steps of (i) spray-drying a solution or dispersion of a wall-forming material in order to obtain intermediate microcapsules and (ii) reducing the water-solubility of at least the outside of the intermediate microcapsules.Suitable wall-forming materials include proteins such as albumin and gelatin.The microcapsules have walls of 40-500 nm thick and are useful in ultrasonic imaging. The control of median size, size distribution and degree of insolubilisation and cross-linking of the wall-forming material allows novel microsphere preparations to be produced.
    Type: Grant
    Filed: August 22, 1995
    Date of Patent: February 8, 2000
    Assignee: Quadrant Healthcare (UK) Limited
    Inventors: Andrew D. Sutton, Richard A. Johnson, Peter J. Senior, David Heath
  • Patent number: 6001886
    Abstract: A petroleum derived oil is subjected to crude oil distillation or propane deasphalting to yield a viscous asphalt residue. The viscous asphalt residue is combined with an aqueous emulsifier comprising an EO-PO-EO block copolymer and passed through a mixer at 60.degree. C. to 70.degree. C. to form an emulsion. Criticality has been found in the amount of propylene oxide in the block copolymer and in the asphalt particle size. These emulsions are stable and can be transported by pumping through a pipeline. They are used as boiler fuel. They are also gasified with insufficient oxygen to produce synthesis gas.
    Type: Grant
    Filed: October 13, 1998
    Date of Patent: December 14, 1999
    Assignee: Texaco Inc.
    Inventor: Shailaja Madhusudhan Shirodkar
  • Patent number: 5976403
    Abstract: A process for producing dispersions of atmospherically stable, coated alkali metal particles and atmospherically stable, coated alkali metal powders by agitating a mixture of molten alkali metal in a hydrocarbon oil at dispersion speeds, optionally in the presence of a dispersing agent, contacting the molten alkali metal-hydrocarbon oil dispersion, above or below the surface of the dispersion, with up to 3 weight percent anhydrous carbon dioxide while agitating the dispersion for at least 1 minute. The dispersion in oil can be used directly in chemical reactions. The bulk of the oil can be removed from the dispersions to produce oil wet particles, the oil wet particles car be washed with a low boiling hydrocarbon to produce hydrocarbon wet particles which can be dried to produce atmospherically stable powders of coated metal particles. The dispersed particles in oil, the oil wet particles, the hydrocarbon wet particles and the atmospherically stable powders can each be used in chemical reactions.
    Type: Grant
    Filed: April 23, 1998
    Date of Patent: November 2, 1999
    Assignee: FMC Corporation
    Inventors: B. Troy Dover, Conrad W. Kamienski, Robert C. Morrison, R. Thomas Currin, Jr., James A. Schwindeman
  • Patent number: 5977190
    Abstract: A process of washing an emulsion such as a silver halide emulsion which contains a hydrophilic colloid comprises deionizing the emulsion and coagulating the emulsion with an anionic polymer and separating the coagulum from the supernatant and resuspending the coagulum with hydrophilic colloid, water and a base.
    Type: Grant
    Filed: January 14, 1998
    Date of Patent: November 2, 1999
    Assignee: Eastman Kodak Company
    Inventors: Lloyd A. Lobo, Kenneth B. Quinn
  • Patent number: 5957828
    Abstract: A silver sol comprises silver particles having a particle size ranging from 1 to 100 nm and a silver solid content ranging from 1 to 80% by weight. The silver sol can be prepared by a method comprising the steps of reacting a solution of a silver compound with a reducing agent at a temperature ranging from 5 to 50.degree. C. and a stirring speed falling within the range of from 1,000 to 10,000 rpm to form silver fine particles; recovering the resulting silver fine particles using a centrifugal separator; and then dispersing the silver fine particles in a medium to give a silver sol having a silver solid content ranging from 1 to 80% by weight. The silver sol or a coating material obtained by diluting the sol to a desired silver solid content and, if desired, adding a binder permits the formation of a transparent conductive film on, for instance, a cathode-ray tube while reducing the production cost.
    Type: Grant
    Filed: May 7, 1998
    Date of Patent: September 28, 1999
    Assignee: Mitsui Mining and Smelting Co., Ltd.
    Inventor: Takao Hayashi
  • Patent number: 5928126
    Abstract: A process for homogeneously dispersing at least one reactant in a fluid matrix, characterized in that capsules of a first type containing the reactant(s) are prepared with a first encapsulation product and capsules of a second type containing the fluid matrix are prepared with a second encapsulation product which is compatible with the first, these two types of capsules bearing electric charges of opposite polarity, the capsules of the two types are combined by electric attraction and the first and second encapsulation products are removed so as to obtain a composite material consisting of the fluid matrix containing the reactant(s) in homogeneous dispersion form, and products obtained according to this process.
    Type: Grant
    Filed: December 6, 1996
    Date of Patent: July 27, 1999
    Assignee: AIMCO SA (Automatic Instant Mesures et Controle Optique)
    Inventor: Philippe Guillot
  • Patent number: 5906962
    Abstract: Stable, concentrated non-aqueous suspensions of water-soluble solids are prepared by using a water soluble active compound comprising water hydratable polysaccharides, biocides, fertilizers and mixtures thereof dispersed in water-miscible organic liquid carriers, preferably lower alkadiols in conjunction with a specific three component surfactant system, i.e., a system comprising a nonionic polymeric viscosity modifier surfactant; an anionic surfactant; and a nonionic surfactant having a bulky hydrophobic substituent group.
    Type: Grant
    Filed: September 10, 1997
    Date of Patent: May 25, 1999
    Assignee: Rhodia Inc.
    Inventors: Norman Robert Pallas, James L. Hazen, Robert Jene Riedemann, Thomas E. Ruch
  • Patent number: 5902226
    Abstract: A propanol sol of silica having a specific surface area of 25 to 550 m.sup.2 /g, the sol having an SiO.sub.2 concentration of 10 to 50% by weight of SiO.sub.2 and a residual content of a medium containing 7.5% by weight or less of water based on the SiO.sub.2 content and 90% by weight or more of propanol, is prepared by an improved process involving replacing the aqueous medium in an acidic aqueous sol of silica containing 5 to 50% by weight of SiO.sub.2 and a medium having a water content of 15% by weight or more with propanol by an atmospheric distillation method in which a concentration of 5 to 50% by weight of SiO.sub.2 in the sol and 1 to 85% by weight of methanol in the medium in the sol is maintained when the medium in the sol during the replacement contains 15 to 0.5% by weight of water.
    Type: Grant
    Filed: March 15, 1996
    Date of Patent: May 11, 1999
    Assignee: Nissan Chemical Industries, Ltd.
    Inventors: Keiko Tasaki, Yasuyoshi Hamada, Takafumi Yokoyama
  • Patent number: 5895347
    Abstract: Methods are disclosed for preparation of chemically-stabilized emulsions of tall oil in water. Temperature and pH are controlled during preparation of the emulsions so as to prevent saponification and neutralization of acids in the tall oil component. The final emulsions have pHs in the range of from about 3.0 to 5.0 and remain phase stable for extended periods of time. Methods are disclosed for using the emulsions for soil treatment to improve soil stabilization and load bearing capacity for roadbed use, for treatment of reclaimed asphalt pavement for reuse as a stabilized base course for roadway construction and for remediation of heavy metal contaminated soil.
    Type: Grant
    Filed: March 17, 1997
    Date of Patent: April 20, 1999
    Assignee: Vinzoyl Technical Services, L.L.C.
    Inventor: Michael P. Doyle