Comminuting Or Centrifuging Patents (Class 536/77)
  • Patent number: 8993747
    Abstract: The present invention relates to a process for the production of alkali cellulose for the production of alkali cellulose and, optionally, cellulose ethers from cellulose in the presence of alkali and, if applicable, with alkylating and/or hydroxyalkylating agent(s) comprising the reaction of a cellulose with an alkali metal hydroxide, wherein the alkali metal hydroxide is mixed with cellulose in a mixing apparatus, the mixing apparatus (1) having an upper region (20, 102a, 202a) with a first cross-section and a lower region (21, 102b, 202b) with a second cross-section, the second cross-section being the same as or smaller than the first cross-section and comprising at least one non-horizontally oriented mixing device (23, 27, 121, 221, 224).
    Type: Grant
    Filed: January 8, 2010
    Date of Patent: March 31, 2015
    Assignee: Dow Global Technologies LLC
    Inventors: Matthias Sprehe, Bettina Hoelzer
  • Patent number: 8436165
    Abstract: The present invention relates to a process for producing a decrystallized cellulose having a reduced cellulose I-type crystallinity from a cellulose-containing raw material in an efficient manner with an excellent productivity. In accordance with the present invention, there is provided a process for producing a decrystallized cellulose from a raw material comprising at least 20% by weight, based on the weight of the raw material excluding water contained therein, of a cellulose having a cellulose I-type crystallinity of more than 33% as calculated from the following formula: Cellulose I-type Crystallinity (%)=[(I22.6?I18.5)/I22.6]×100 wherein I22.6 is a diffraction intensity of a lattice plane (002 plane) as measured at a diffraction angle 2? of 22.6° in X-ray diffraction analysis; and I18.5 is a diffraction intensity of an amorphous moiety as measured at a diffraction angle 2? of 18.
    Type: Grant
    Filed: February 15, 2008
    Date of Patent: May 7, 2013
    Assignee: Kao Corporation
    Inventors: Naoki Nojiri, Masahiro Umehara, Tomohito Kitsuki, Munehisa Okutsu, Keiichiro Tomioka
  • Patent number: 6884883
    Abstract: Pulp is ground by means of a vertical roller mill. The average particle diameter of the resulting powdered pulp is adjusted to 20-300 ?m. The powdered pulp thus obtained is used as a starting material for the production of cellulose ethers.
    Type: Grant
    Filed: June 28, 2000
    Date of Patent: April 26, 2005
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventors: Yukio Shima, Mitsuo Narita, Atsushi Hatayama
  • Patent number: 6258539
    Abstract: The present invention relate to methods and compositions for simultaneously analyzing multiple different polynucleotides of a polynucleotide composition comprising multiple diverse polynucleotide sequences. The subject methods and compositions may also be applied to analyze or identify single polynucleotides; however, the subject methods and compositions are particularly useful for analyzing large diverse populations of polynucleotides, e.g., cDNA libraries. Most embodiments of the invention involve hybridizing terminus probes (of known base sequence) to adapter-modified restriction fragment generated from polynucleotide for analysis, and subsequently joining the terminus probes and internal fragment probes to each other. The terminus probe hybridizes to bases of restriction endonuclease recognition site present at the terminus of a restriction fragment generated from the polynucleotide for analysis.
    Type: Grant
    Filed: April 30, 1999
    Date of Patent: July 10, 2001
    Assignee: The Perkin-Elmer Corporation
    Inventors: Michael W. Hunkapiller, John H. Richards
  • Patent number: 6232067
    Abstract: The present invention relate to methods and compositions for simultaneously analyzing multiple different polynucleotides of a polynucleotide composition comprising multiple diverse polynucleotide sequences. The subject methods and compositions may also be applied to analyze or identify single polynucleotides; however, the subject methods and compositions are particularly useful for analyzing large diverse populations of polynucleotides, e.g., cDNA libraries. Most embodiments of the invention involve hybridizing terminus probes (of known base sequence) and internal fragment probes (of known base sequence) at adjacent positions on an adapter-modified restriction fragment generated from polynucleotide for analysis, and subsequently joining the terminus probes and internal fragment probes to each other. The terminus probe hybridizes to bases of restriction endonuclease recognition site present at the terminus of a restriction fragment generated from the polynucleotide for analysis.
    Type: Grant
    Filed: August 17, 1998
    Date of Patent: May 15, 2001
    Assignee: The Perkin-Elmer Corporation
    Inventors: Michael W. Hunkapiller, John H. Richards
  • Patent number: 5330642
    Abstract: Apparatus for filtering cellulose acetate solutions, including a backflush filter to effect filtration so as to avoid solvent losses and filtering aids that must be dumped, dilution means including solvent supply means for diluting the backflush liquid, separation means for eliminating solid insoluble components, and means for recycling backflush liquid freed from solids to a plant for producing new cellulose acetate spin solution.
    Type: Grant
    Filed: March 11, 1992
    Date of Patent: July 19, 1994
    Assignee: Lenzing Aktiengesellschaft
    Inventor: Walter Klein
  • Patent number: 5089480
    Abstract: The invention provides novel compounds having the formula: ##STR1## wherein R when taken individually is H; R.sup.1 when taken individually is H or OH; R and R.sup.1 when taken together represent a double bond;R.sup.2 is an alpha-branched C.sub.3 -C.sub.8 alkyl, alkenyl, alkynyl, alkoxyalkyl or alkylthioalkyl group; a C.sub.3 -C.sub.8 cycloalkyl, C.sub.5 -C.sub.8 cycloalkenyl or C.sub.5 -C.sub.8 cycloalkylalkyl group, any of which may be substituted by methylene or one or more C.sub.1 -C.sub.4 alkyl groups or halo atoms; or a 3 to 6 membered oxygen or sulphur containing heterocyclic ring which may be substituted by one or more C.sub.1 -C.sub.4 alkyl groups or halo atoms;R.sup.3 is hydrogen or methyl;R.sup.4 is H or 4'-(alpha-L-oleandrosyl)-alpha-L-oleandrosyloxy with the proviso that when R.sup.2 is alkyl it is not isopropyl or sec-butyl; when R.sup.4 is H, each of R and R.sup.1 is H, and R.sup.2 is not methyl or ethyl; and when R.sup.4 is H, R is H, R.sup.1 is OH, and R.sup.
    Type: Grant
    Filed: January 11, 1988
    Date of Patent: February 18, 1992
    Assignee: Pfizer Inc.
    Inventors: Stephen P. Gibson, Alexander C. Goudie, Kelvin S. Holdom, John D. Bu'lock
  • Patent number: 5071599
    Abstract: A process for the production of cellulose ester fibrets wherein a solution of the cellulose ester is contacted with a non-solvent for the cellulose ester in a precipitation zone under shearing conditions, and a solvent-nonsolvent mixture is separated from the formed fibrets and recycled to the precipitation zone.
    Type: Grant
    Filed: December 14, 1990
    Date of Patent: December 10, 1991
    Assignee: Hoechst Celanese Corporation
    Inventors: Samuel S. McNair, Jr., Jimmy W. Evans
  • Patent number: 5047180
    Abstract: Cellulose ester microparticles with unique properties are made by a process having the following steps:(a) dissolving a cellulose ester in a liquid comprising a solvent for the cellulose ester and a non-solvent for the cellulose ester, thereby forming a dope;(b) spheronizing the dope thereby forming fine droplets of the dope;(c) dropping the droplets for a finite amount of time; and(d) precipitating the droplets in a bath containing a precipitant.
    Type: Grant
    Filed: April 24, 1989
    Date of Patent: September 10, 1991
    Assignee: Hoechst Celanese Corporation
    Inventors: Thomas L. Steiner, Kenneth A. Domeshek, William Stitt, Jesse L. Riley, Lance J. Deutsch
  • Patent number: 4888420
    Abstract: Microparticle of cellulose acetate and derivatives thereof characterized by being water soluble, having a large interior void space and having a plurality of open exterior surface pores. These water soluble microparticles can be loaded with a chemical selected from the group consisting of pharmaceuticals, dyes, flavorings, agriculturals, solid catalysts and fragrances.
    Type: Grant
    Filed: December 8, 1987
    Date of Patent: December 19, 1989
    Assignee: Celanese Fibers, Inc.
    Inventors: Thomas L. Steiner, Dana T. Minnick, Kenneth A. Domeshek, Donald H. Lester, Jr.
  • Patent number: 4415124
    Abstract: A method for the production of micropowders from cellulose ethers or cellulose comprising(a) subjecting a cellulose ether or a cellulose having a fine-fiber, cottony or woolly structure to a consolidation or embrittlement sufficient whereby in one mill pass through a jet mill under standard conditions 98% by weight of the consolidated or embrittled material charged is recovered as a powder of less than 100.mu., and(b) subjecting the consolidated or embrittled material to a grinding step producing a size reduction sufficient that a grain size distribution with at least 90% by weight of less than 125.mu. is attained.
    Type: Grant
    Filed: October 7, 1981
    Date of Patent: November 15, 1983
    Assignee: Henkel Kommanditgesellschaft Auf Aktien
    Inventors: Franz-Josef Carduck, Wilfried Rahse, Willi Wust, Hans Pabel
  • Patent number: 4329451
    Abstract: An aqueous dispersion of colloidal size particles of a water-insoluble, polysaccharide derivative such as ethylcellulose is prepared by grinding the water-insoluble, polysaccharide derivative in the presence of water. A suspending agent is optionally employed to increase grinding efficiency and to form a stable suspension of the colloidal size particles.
    Type: Grant
    Filed: November 3, 1980
    Date of Patent: May 11, 1982
    Assignee: The Dow Chemical Company
    Inventor: Maurice L. Zweigle
  • Patent number: 4158634
    Abstract: Finely comminuted particles of a normally solid thermoplastic organic polymer, which is particularly useful as a toner base for electrostatic reproduction utilizing pressure fusing on the toner, is prepared by dissolving a polymer in a normally solid first solvent, cooling the resulting solution to form a friable solid, and removing the first solvent from the solid, preferably by extraction with a normally liquid, relatively volatile, second solvent in which the polymer is substantially insoluble. When using the process to make magnetic mono-component toners, powered magnetic material and/or carbon black or other pigment are added to the solution of polymer and first solvent.
    Type: Grant
    Filed: September 23, 1977
    Date of Patent: June 19, 1979
    Assignee: Apeco Corporation
    Inventors: Luigi Amariti, John S. Juskey, Shapoor Azari, Thomas J. Kucera