Comminuting Or Centrifuging Patents (Class 536/77)
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Patent number: 8993747Abstract: The present invention relates to a process for the production of alkali cellulose for the production of alkali cellulose and, optionally, cellulose ethers from cellulose in the presence of alkali and, if applicable, with alkylating and/or hydroxyalkylating agent(s) comprising the reaction of a cellulose with an alkali metal hydroxide, wherein the alkali metal hydroxide is mixed with cellulose in a mixing apparatus, the mixing apparatus (1) having an upper region (20, 102a, 202a) with a first cross-section and a lower region (21, 102b, 202b) with a second cross-section, the second cross-section being the same as or smaller than the first cross-section and comprising at least one non-horizontally oriented mixing device (23, 27, 121, 221, 224).Type: GrantFiled: January 8, 2010Date of Patent: March 31, 2015Assignee: Dow Global Technologies LLCInventors: Matthias Sprehe, Bettina Hoelzer
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Patent number: 8436165Abstract: The present invention relates to a process for producing a decrystallized cellulose having a reduced cellulose I-type crystallinity from a cellulose-containing raw material in an efficient manner with an excellent productivity. In accordance with the present invention, there is provided a process for producing a decrystallized cellulose from a raw material comprising at least 20% by weight, based on the weight of the raw material excluding water contained therein, of a cellulose having a cellulose I-type crystallinity of more than 33% as calculated from the following formula: Cellulose I-type Crystallinity (%)=[(I22.6?I18.5)/I22.6]×100 wherein I22.6 is a diffraction intensity of a lattice plane (002 plane) as measured at a diffraction angle 2? of 22.6° in X-ray diffraction analysis; and I18.5 is a diffraction intensity of an amorphous moiety as measured at a diffraction angle 2? of 18.Type: GrantFiled: February 15, 2008Date of Patent: May 7, 2013Assignee: Kao CorporationInventors: Naoki Nojiri, Masahiro Umehara, Tomohito Kitsuki, Munehisa Okutsu, Keiichiro Tomioka
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Patent number: 6884883Abstract: Pulp is ground by means of a vertical roller mill. The average particle diameter of the resulting powdered pulp is adjusted to 20-300 ?m. The powdered pulp thus obtained is used as a starting material for the production of cellulose ethers.Type: GrantFiled: June 28, 2000Date of Patent: April 26, 2005Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Yukio Shima, Mitsuo Narita, Atsushi Hatayama
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Patent number: 6258539Abstract: The present invention relate to methods and compositions for simultaneously analyzing multiple different polynucleotides of a polynucleotide composition comprising multiple diverse polynucleotide sequences. The subject methods and compositions may also be applied to analyze or identify single polynucleotides; however, the subject methods and compositions are particularly useful for analyzing large diverse populations of polynucleotides, e.g., cDNA libraries. Most embodiments of the invention involve hybridizing terminus probes (of known base sequence) to adapter-modified restriction fragment generated from polynucleotide for analysis, and subsequently joining the terminus probes and internal fragment probes to each other. The terminus probe hybridizes to bases of restriction endonuclease recognition site present at the terminus of a restriction fragment generated from the polynucleotide for analysis.Type: GrantFiled: April 30, 1999Date of Patent: July 10, 2001Assignee: The Perkin-Elmer CorporationInventors: Michael W. Hunkapiller, John H. Richards
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Patent number: 6232067Abstract: The present invention relate to methods and compositions for simultaneously analyzing multiple different polynucleotides of a polynucleotide composition comprising multiple diverse polynucleotide sequences. The subject methods and compositions may also be applied to analyze or identify single polynucleotides; however, the subject methods and compositions are particularly useful for analyzing large diverse populations of polynucleotides, e.g., cDNA libraries. Most embodiments of the invention involve hybridizing terminus probes (of known base sequence) and internal fragment probes (of known base sequence) at adjacent positions on an adapter-modified restriction fragment generated from polynucleotide for analysis, and subsequently joining the terminus probes and internal fragment probes to each other. The terminus probe hybridizes to bases of restriction endonuclease recognition site present at the terminus of a restriction fragment generated from the polynucleotide for analysis.Type: GrantFiled: August 17, 1998Date of Patent: May 15, 2001Assignee: The Perkin-Elmer CorporationInventors: Michael W. Hunkapiller, John H. Richards
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Patent number: 5330642Abstract: Apparatus for filtering cellulose acetate solutions, including a backflush filter to effect filtration so as to avoid solvent losses and filtering aids that must be dumped, dilution means including solvent supply means for diluting the backflush liquid, separation means for eliminating solid insoluble components, and means for recycling backflush liquid freed from solids to a plant for producing new cellulose acetate spin solution.Type: GrantFiled: March 11, 1992Date of Patent: July 19, 1994Assignee: Lenzing AktiengesellschaftInventor: Walter Klein
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Patent number: 5089480Abstract: The invention provides novel compounds having the formula: ##STR1## wherein R when taken individually is H; R.sup.1 when taken individually is H or OH; R and R.sup.1 when taken together represent a double bond;R.sup.2 is an alpha-branched C.sub.3 -C.sub.8 alkyl, alkenyl, alkynyl, alkoxyalkyl or alkylthioalkyl group; a C.sub.3 -C.sub.8 cycloalkyl, C.sub.5 -C.sub.8 cycloalkenyl or C.sub.5 -C.sub.8 cycloalkylalkyl group, any of which may be substituted by methylene or one or more C.sub.1 -C.sub.4 alkyl groups or halo atoms; or a 3 to 6 membered oxygen or sulphur containing heterocyclic ring which may be substituted by one or more C.sub.1 -C.sub.4 alkyl groups or halo atoms;R.sup.3 is hydrogen or methyl;R.sup.4 is H or 4'-(alpha-L-oleandrosyl)-alpha-L-oleandrosyloxy with the proviso that when R.sup.2 is alkyl it is not isopropyl or sec-butyl; when R.sup.4 is H, each of R and R.sup.1 is H, and R.sup.2 is not methyl or ethyl; and when R.sup.4 is H, R is H, R.sup.1 is OH, and R.sup.Type: GrantFiled: January 11, 1988Date of Patent: February 18, 1992Assignee: Pfizer Inc.Inventors: Stephen P. Gibson, Alexander C. Goudie, Kelvin S. Holdom, John D. Bu'lock
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Patent number: 5071599Abstract: A process for the production of cellulose ester fibrets wherein a solution of the cellulose ester is contacted with a non-solvent for the cellulose ester in a precipitation zone under shearing conditions, and a solvent-nonsolvent mixture is separated from the formed fibrets and recycled to the precipitation zone.Type: GrantFiled: December 14, 1990Date of Patent: December 10, 1991Assignee: Hoechst Celanese CorporationInventors: Samuel S. McNair, Jr., Jimmy W. Evans
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Patent number: 5047180Abstract: Cellulose ester microparticles with unique properties are made by a process having the following steps:(a) dissolving a cellulose ester in a liquid comprising a solvent for the cellulose ester and a non-solvent for the cellulose ester, thereby forming a dope;(b) spheronizing the dope thereby forming fine droplets of the dope;(c) dropping the droplets for a finite amount of time; and(d) precipitating the droplets in a bath containing a precipitant.Type: GrantFiled: April 24, 1989Date of Patent: September 10, 1991Assignee: Hoechst Celanese CorporationInventors: Thomas L. Steiner, Kenneth A. Domeshek, William Stitt, Jesse L. Riley, Lance J. Deutsch
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Patent number: 4888420Abstract: Microparticle of cellulose acetate and derivatives thereof characterized by being water soluble, having a large interior void space and having a plurality of open exterior surface pores. These water soluble microparticles can be loaded with a chemical selected from the group consisting of pharmaceuticals, dyes, flavorings, agriculturals, solid catalysts and fragrances.Type: GrantFiled: December 8, 1987Date of Patent: December 19, 1989Assignee: Celanese Fibers, Inc.Inventors: Thomas L. Steiner, Dana T. Minnick, Kenneth A. Domeshek, Donald H. Lester, Jr.
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Patent number: 4415124Abstract: A method for the production of micropowders from cellulose ethers or cellulose comprising(a) subjecting a cellulose ether or a cellulose having a fine-fiber, cottony or woolly structure to a consolidation or embrittlement sufficient whereby in one mill pass through a jet mill under standard conditions 98% by weight of the consolidated or embrittled material charged is recovered as a powder of less than 100.mu., and(b) subjecting the consolidated or embrittled material to a grinding step producing a size reduction sufficient that a grain size distribution with at least 90% by weight of less than 125.mu. is attained.Type: GrantFiled: October 7, 1981Date of Patent: November 15, 1983Assignee: Henkel Kommanditgesellschaft Auf AktienInventors: Franz-Josef Carduck, Wilfried Rahse, Willi Wust, Hans Pabel
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Patent number: 4329451Abstract: An aqueous dispersion of colloidal size particles of a water-insoluble, polysaccharide derivative such as ethylcellulose is prepared by grinding the water-insoluble, polysaccharide derivative in the presence of water. A suspending agent is optionally employed to increase grinding efficiency and to form a stable suspension of the colloidal size particles.Type: GrantFiled: November 3, 1980Date of Patent: May 11, 1982Assignee: The Dow Chemical CompanyInventor: Maurice L. Zweigle
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Patent number: 4158634Abstract: Finely comminuted particles of a normally solid thermoplastic organic polymer, which is particularly useful as a toner base for electrostatic reproduction utilizing pressure fusing on the toner, is prepared by dissolving a polymer in a normally solid first solvent, cooling the resulting solution to form a friable solid, and removing the first solvent from the solid, preferably by extraction with a normally liquid, relatively volatile, second solvent in which the polymer is substantially insoluble. When using the process to make magnetic mono-component toners, powered magnetic material and/or carbon black or other pigment are added to the solution of polymer and first solvent.Type: GrantFiled: September 23, 1977Date of Patent: June 19, 1979Assignee: Apeco CorporationInventors: Luigi Amariti, John S. Juskey, Shapoor Azari, Thomas J. Kucera