Melamine Per Se, Or Salt Thereof Patents (Class 544/200)
  • Patent number: 11731948
    Abstract: Improved processes for producing high purity acesulfame potassium. In one embodiment, the process comprises the steps of contacting a solvent, e.g., dichloromethane, and a cyclizing agent, e.g., sulfur trioxide, to form a cyclizing agent composition and reacting an acetoacetamide salt with the cyclizing agent in the composition to form a cyclic sulfur trioxide adduct. The contact time is less than 60 minutes. The process also comprises forming from the cyclic sulfur trioxide adduct composition a finished acesulfame potassium composition comprising non-chlorinated, e.g., non-chlorinated, acesulfame potassium and less than 35 wppm 5-halo acesulfame potassium, preferably less than 5 wppm.
    Type: Grant
    Filed: March 19, 2021
    Date of Patent: August 22, 2023
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 11724994
    Abstract: A process for producing acesulfame potassium, the process comprising the steps of providing a cyclizing agent composition comprising a cyclizing agent and a solvent and having an initial temperature, cooling the cyclizing agent composition to form a cooled cyclizing agent composition having a cooled temperature less than 35° C., reacting an acetoacetamide salt with the cyclizing agent in the cooled cyclizing agent composition to form a cyclic sulfur trioxide adduct composition comprising cyclic sulfur trioxide adduct; and, forming from the cyclic sulfur trioxide adduct in the cyclic sulfur trioxide adduct composition the finished acesulfame potassium composition comprising non-chlorinated acesulfame potassium and less than 39 wppm 5-chloro-acesulfame potassium. The cooled temperature is at least 2° C. less than the initial temperature.
    Type: Grant
    Filed: March 19, 2021
    Date of Patent: August 15, 2023
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 11724993
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of forming a cyclic sulfur trioxide adduct; hydrolyzing the cyclic sulfur trioxide adduct to form an acesulfame-H composition comprising acesulfame-H; neutralizing the acesulfame-H in the acesulfame-H composition to form a crude acesulfame potassium composition comprising acesulfame potassium and less than 2800 wppm acetoacetamide-N-sulfonic acid, wherein the neutralizing step is conducted or maintained at a pH at or below 11.0; and treating the crude acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 37 wppm acetoacetamide-N-sulfonic acid.
    Type: Grant
    Filed: March 19, 2021
    Date of Patent: August 15, 2023
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 11718594
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of providing a crude acesulfame potassium composition comprising acesulfame potassium and acetoacetamide, concentrating the crude acesulfame potassium composition to form a water stream and an intermediate acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide, and separating the intermediate acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide. The concentrating step is conducted at a temperature below 90° C. and the separating step is conducted at a temperature at or below 35° C.
    Type: Grant
    Filed: March 19, 2021
    Date of Patent: August 8, 2023
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 11472779
    Abstract: A hydrogen-bonded organic framework (HOF) and a method of making the HOF. The HOF has at least one amine substituted organic linker and at least one carboxylic acid-based organic linker. The HOF is prepared by dissolving the linkers separately in water and mixing the aqueous solutions, without using any organic solvents, additional catalysts, or any other reagents.
    Type: Grant
    Filed: May 13, 2022
    Date of Patent: October 18, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Mohd Yusuf Khan, Abuzar Khan, Aasif Helal, Zain H. Yamani
  • Patent number: 10975047
    Abstract: Improved processes for producing high purity acesulfame potassium. In one embodiment, the process comprises the steps of contacting a solvent, e.g., dichloromethane, and a cyclizing agent, e.g., sulfur trioxide, to form a cyclizing agent composition and reacting an acetoacetamide salt with the cyclizing agent in the composition to form a cyclic sulfur trioxide adduct. The contact time is less than 60 minutes. The process also comprises forming from the cyclic sulfur trioxide adduct composition a finished acesulfame potassium composition comprising non-chlorinated, e.g., non-chlorinated, acesulfame potassium and less than 35 wppm 5-halo acesulfame potassium, preferably less than 5 wppm.
    Type: Grant
    Filed: August 4, 2020
    Date of Patent: April 13, 2021
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10961207
    Abstract: A process for producing acesulfame potassium, the process comprising the steps of providing a cyclizing agent composition comprising a cyclizing agent and a solvent and having an initial temperature, cooling the cyclizing agent composition to form a cooled cyclizing agent composition having a cooled temperature less than 35° C., reacting an acetoacetamide salt with the cyclizing agent in the cooled cyclizing agent composition to form a cyclic sulfur trioxide adduct composition comprising cyclic sulfur trioxide adduct; and, forming from the cyclic sulfur trioxide adduct in the cyclic sulfur trioxide adduct composition the finished acesulfame potassium composition comprising non-chlorinated acesulfame potassium and less than 39 wppm 5-chloro-acesulfame potassium. The cooled temperature is at least 2° C. less than the initial temperature.
    Type: Grant
    Filed: August 4, 2020
    Date of Patent: March 30, 2021
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10954204
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of forming a cyclic sulfur trioxide adduct; hydrolyzing the cyclic sulfur trioxide adduct to form an acesulfame-H composition comprising acesulfame-H; neutralizing the acesulfame-H in the acesulfame-H composition to form a crude acesulfame potassium composition comprising acesulfame potassium and less than 2800 wppm acetoacetamide-N-sulfonic acid, wherein the neutralizing step is conducted or maintained at a pH at or below 11.0; and treating the crude acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 37 wppm acetoacetamide-N-sulfonic acid.
    Type: Grant
    Filed: August 4, 2020
    Date of Patent: March 23, 2021
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10954203
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of providing a crude acesulfame potassium composition comprising acesulfame potassium and acetoacetamide, concentrating the crude acesulfame potassium composition to form a water stream and an intermediate acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide, and separating the intermediate acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide. The concentrating step is conducted at a temperature below 90° C. and the separating step is conducted at a temperature at or below 35° C.
    Type: Grant
    Filed: August 4, 2020
    Date of Patent: March 23, 2021
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10781190
    Abstract: A process for producing acesulfame potassium, the process comprising the steps of providing a cyclizing agent composition comprising a cyclizing agent and a solvent and having an initial temperature, cooling the cyclizing agent composition to form a cooled cyclizing agent composition having a cooled temperature less than 35° C., reacting an acetoacetamide salt with the cyclizing agent in the cooled cyclizing agent composition to form a cyclic sulfur trioxide adduct composition comprising cyclic sulfur trioxide adduct; and, forming from the cyclic sulfur trioxide adduct in the cyclic sulfur trioxide adduct composition the finished acesulfame potassium composition comprising non-chlorinated acesulfame potassium and less than 39 wppm 5-chloro-acesulfame potassium. The cooled temperature is at least 2° C. less than the initial temperature.
    Type: Grant
    Filed: November 15, 2019
    Date of Patent: September 22, 2020
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10781191
    Abstract: Improved processes for producing high purity acesulfame potassium. In one embodiment, the process comprises the steps of contacting a solvent, e.g., dichloromethane, and a cyclizing agent, e.g., sulfur trioxide, to form a cyclizing agent composition and reacting an acetoacetamide salt with the cyclizing agent in the composition to form a cyclic sulfur trioxide adduct. The contact time is less than 60 minutes. The process also comprises forming from the cyclic sulfur trioxide adduct composition a finished acesulfame potassium composition comprising non-chlorinated, e.g., non-chlorinated, acesulfame potassium and less than 35 wppm 5-halo acesulfame potassium, preferably less than 5 wppm.
    Type: Grant
    Filed: November 15, 2019
    Date of Patent: September 22, 2020
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10759770
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of providing a crude acesulfame potassium composition comprising acesulfame potassium and acetoacetamide, concentrating the crude acesulfame potassium composition to form a water stream and an intermediate acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide, and separating the intermediate acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide. The concentrating step is conducted at a temperature below 90° C. and the separating step is conducted at a temperature at or below 35° C.
    Type: Grant
    Filed: November 15, 2019
    Date of Patent: September 1, 2020
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10759771
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of forming a cyclic sulfur trioxide adduct; hydrolyzing the cyclic sulfur trioxide adduct to form an acesulfame-H composition comprising acesulfame-H; neutralizing the acesulfame-H in the acesulfame-H composition to form a crude acesulfame potassium composition comprising acesulfame potassium and less than 2800 wppm acetoacetamide-N-sulfonic acid, wherein the neutralizing step is conducted or maintained at a pH at or below 11.0; and treating the crude acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 37 wppm acetoacetamide-N-sulfonic acid.
    Type: Grant
    Filed: November 15, 2019
    Date of Patent: September 1, 2020
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10669475
    Abstract: Surface-modified nanoparticles are produced by associating ligand interactive agents with the surface of a nanoparticle. The ligand interactive agents are bound to surface modifying ligands that are tailored to impart particular solubility and/or compatibility properties. The ligand interactive agents are crosslinked via a linking/crosslinking agent, such as hexamethoxymethylmelamine or a derivative thereof. The linking/crosslinking agent may provide a binding site for binding the surface modifying ligands to the ligand interactive agents.
    Type: Grant
    Filed: June 14, 2019
    Date of Patent: June 2, 2020
    Assignee: Nanco Technologies Ltd.
    Inventor: Imad Naasani
  • Patent number: 10590097
    Abstract: A process for producing acesulfame potassium, the process comprising the steps of providing a cyclizing agent composition comprising a cyclizing agent and a solvent and having an initial temperature, cooling the cyclizing agent composition to form a cooled cyclizing agent composition having a cooled temperature less than 35° C., reacting an acetoacetamide salt with the cyclizing agent in the cooled cyclizing agent composition to form a cyclic sulfur trioxide adduct composition comprising cyclic sulfur trioxide adduct; and, forming from the cyclic sulfur trioxide adduct in the cyclic sulfur trioxide adduct composition the finished acesulfame potassium composition comprising non-chlorinated acesulfame potassium and less than 39 wppm 5-chloro-acesulfame potassium. The cooled temperature is at least 2° C. less than the initial temperature.
    Type: Grant
    Filed: February 12, 2019
    Date of Patent: March 17, 2020
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10590095
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of providing a crude acesulfame potassium composition comprising acesulfame potassium and acetoacetamide, concentrating the crude acesulfame potassium composition to form a water stream and an intermediate acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide, and separating the intermediate acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide. The concentrating step is conducted at a temperature below 90° C. and the separating step is conducted at a temperature at or below 35° C.
    Type: Grant
    Filed: February 12, 2019
    Date of Patent: March 17, 2020
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10590096
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of forming a cyclic sulfur trioxide adduct; hydrolyzing the cyclic sulfur trioxide adduct to form an acesulfame-H composition comprising acesulfame-H; neutralizing the acesulfame-H in the acesulfame-H composition to form a crude acesulfame potassium composition comprising acesulfame potassium and less than 2800 wppm acetoacetamide-N-sulfonic acid, wherein the neutralizing step is conducted or maintained at a pH at or below 11.0; and treating the crude acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 37 wppm acetoacetamide-N-sulfonic acid.
    Type: Grant
    Filed: February 12, 2019
    Date of Patent: March 17, 2020
    Assignee: Celenese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10590098
    Abstract: Improved processes for producing high purity acesulfame potassium. In one embodiment, the process comprises the steps of contacting a solvent, e.g., dichloromethane, and a cyclizing agent, e.g., sulfur trioxide, to form a cyclizing agent composition and reacting an acetoacetamide salt with the cyclizing agent in the composition to form a cyclic sulfur trioxide adduct. The contact time is less than 60 minutes. The process also comprises forming from the cyclic sulfur trioxide adduct composition a finished acesulfame potassium composition comprising non-chlorinated, e.g., non-chlorinated, acesulfame potassium and less than 35 wppm 5-halo acesulfame potassium, preferably less than 5 wppm.
    Type: Grant
    Filed: February 12, 2019
    Date of Patent: March 17, 2020
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10233163
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of providing a crude acesulfame potassium composition comprising acesulfame potassium and acetoacetamide, concentrating the crude acesulfame potassium composition to form a water stream and an intermediate acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide, and separating the intermediate acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide. The concentrating step is conducted at a temperature below 90° C. and the separating step is conducted at a temperature at or below 35° C.
    Type: Grant
    Filed: June 21, 2018
    Date of Patent: March 19, 2019
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10233164
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of forming a cyclic sulfur trioxide adduct; hydrolyzing the cyclic sulfur trioxide adduct to form an acesulfame-H composition comprising acesulfame-H; neutralizing the acesulfame-H in the acesulfame-H composition to form a crude acesulfame potassium composition comprising acesulfame potassium and less than 2800 wppm acetoacetamide-N-sulfonic acid, wherein the neutralizing step is conducted or maintained at a pH at or below 11.0; and treating the crude acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 37 wppm acetoacetamide-N-sulfonic acid.
    Type: Grant
    Filed: June 21, 2018
    Date of Patent: March 19, 2019
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10227316
    Abstract: A process for producing acesulfame potassium, the process comprising the steps of providing a cyclizing agent composition comprising a cyclizing agent and a solvent and having an initial temperature, cooling the cyclizing agent composition to form a cooled cyclizing agent composition having a cooled temperature less than 35° C., reacting an acetoacetamide salt with the cyclizing agent in the cooled cyclizing agent composition to form a cyclic sulfur trioxide adduct composition comprising cyclic sulfur trioxide adduct; and, forming from the cyclic sulfur trioxide adduct in the cyclic sulfur trioxide adduct composition the finished acesulfame potassium composition comprising non-chlorinated acesulfame potassium and less than 39 wppm 5-chloro-acesulfame potassium. The cooled temperature is at least 2° C. less than the initial temperature.
    Type: Grant
    Filed: June 21, 2018
    Date of Patent: March 12, 2019
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10208004
    Abstract: Improved processes for producing high purity acesulfame potassium. In one embodiment, the process comprises the steps of contacting a solvent, e.g., dichloromethane, and a cyclizing agent, e.g., sulfur trioxide, to form a cyclizing agent composition and reacting an acetoacetamide salt with the cyclizing agent in the composition to form a cyclic sulfur trioxide adduct. The contact time is less than 60 minutes. The process also comprises forming from the cyclic sulfur trioxide adduct composition a finished acesulfame potassium composition comprising non-chlorinated, e.g., non-chlorinated, acesulfame potassium and less than 35 wppm 5-halo acesulfame potassium, preferably less than 5 wppm.
    Type: Grant
    Filed: June 21, 2018
    Date of Patent: February 19, 2019
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10029999
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of providing a crude acesulfame potassium composition comprising acesulfame potassium and acetoacetamide, concentrating the crude acesulfame potassium composition to form a water stream and an intermediate acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide, and separating the intermediate acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 33 wppm acetoacetamide. The concentrating step is conducted at a temperature below 90° C. and the separating step is conducted at a temperature at or below 35° C.
    Type: Grant
    Filed: September 14, 2017
    Date of Patent: July 24, 2018
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10029998
    Abstract: Compositions and processes for producing high purity acesulfame potassium are described. One process comprises the steps of forming a cyclic sulfur trioxide adduct; hydrolyzing the cyclic sulfur trioxide adduct to form an acesulfame-H composition comprising acesulfame-H; neutralizing the acesulfame-H in the acesulfame-H composition to form a crude acesulfame potassium composition comprising acesulfame potassium and less than 2800 wppm acetoacetamide-N-sulfonic acid, wherein the neutralizing step is conducted or maintained at a pH at or below 11.0; and treating the crude acesulfame potassium composition to form the finished acesulfame potassium composition comprising acesulfame potassium and less than 37 wppm acetoacetamide-N-sulfonic acid.
    Type: Grant
    Filed: September 14, 2017
    Date of Patent: July 24, 2018
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10030000
    Abstract: A process for producing acesulfame potassium, the process comprising the steps of providing a cyclizing agent composition comprising a cyclizing agent and a solvent and having an initial temperature, cooling the cyclizing agent composition to form a cooled cyclizing agent composition having a cooled temperature less than 35° C., reacting an acetoacetamide salt with the cyclizing agent in the cooled cyclizing agent composition to form a cyclic sulfur trioxide adduct composition comprising cyclic sulfur trioxide adduct; and, forming from the cyclic sulfur trioxide adduct in the cyclic sulfur trioxide adduct composition the finished acesulfame potassium composition comprising non-chlorinated acesulfame potassium and less than 39 wppm 5-chloro-acesulfame potassium. The cooled temperature is at least 2° C. less than the initial temperature.
    Type: Grant
    Filed: September 14, 2017
    Date of Patent: July 24, 2018
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 10023546
    Abstract: Improved processes for producing high purity acesulfame potassium. In one embodiment, the process comprises the steps of contacting a solvent, e.g., dichloromethane, and a cyclizing agent, e.g., sulfur trioxide, to form a cyclizing agent composition and reacting an acetoacetamide salt with the cyclizing agent in the composition to form a cyclic sulfur trioxide adduct. The contact time is less than 60 minutes. The process also comprises forming from the cyclic sulfur trioxide adduct composition a finished acesulfame potassium composition comprising non-chlorinated, e.g., non-chlorinated, acesulfame potassium and less than 35 wppm 5-halo acesulfame potassium, preferably less than 5 wppm.
    Type: Grant
    Filed: September 14, 2017
    Date of Patent: July 17, 2018
    Assignee: Celanese International Corporation
    Inventors: Christoph Mollenkopf, Peter Groer, Arvind Yadav
  • Patent number: 9840664
    Abstract: Surface-modified nanoparticles are produced by associating ligand interactive agents with the surface of a nanoparticle. The ligand interactive agents are bound to surface modifying ligands that are tailored to impart particular solubility and/or compatibility properties. The ligand interactive agents are crosslinked via a linking/crosslinking agent, such as hexamethoxymethylmelamine or a derivative thereof. The linking/crosslinking agent may provide a binding site for binding the surface modifying ligands to the ligand interactive agents.
    Type: Grant
    Filed: August 21, 2015
    Date of Patent: December 12, 2017
    Assignee: Nanoco Technologies Ltd.
    Inventor: Imad Naasani
  • Patent number: 9499547
    Abstract: The present invention relates to amino-substituted imidazopyridazine compounds of general formula (I): in which A, R1, R3 and n are as defined in the claims, to methods of preparing said compounds, to pharmaceutical compositions and combinations comprising said compounds and to the use of said compounds for manufacturing a pharmaceutical composition for the treatment or prophylaxis of a disease, in particular of a hyper-proliferative and/or angiogenesis disorder, as a sole agent or in combination with other active ingredients.
    Type: Grant
    Filed: September 5, 2012
    Date of Patent: November 22, 2016
    Assignee: BAYER INTELLECTUAL PROPERTY GMBH
    Inventors: Knut Eis, Florian Puehler, Ludwig Zorn, Arne Scholz, Philip Lienau, Mark Jean Gnoth, Ulf Bömer, Judith Günther, Marion Hitchcock
  • Patent number: 9493353
    Abstract: A process for producing a pyrophosphate, particularly melamine pyrophosphate useful as a flame retardant, efficiently in high yield is provided. The process includes firing an orthophosphate, preferably melamine orthophosphate, in the presence of a silicone oil, preferably methylphenyl silicone oil preferably at 120° to 350° C. Examples of useful firing equipment include a hot air dryer, a kneader, a Henschel mixture, a fluidized bed dryer, a rotary kiln, a paddle dryer, an extruder, a vibrating dryer, a far-infrared conveyor furnace, and a microwave firing furnace.
    Type: Grant
    Filed: February 14, 2014
    Date of Patent: November 15, 2016
    Assignee: ADEKA CORPORATION
    Inventors: Genta Harada, Yutaka Yonezawa, Michio Nakamura, Yuri Okamoto, Kohei Omori
  • Patent number: 8802848
    Abstract: The present invention relates to Melamine based Mannich compounds of the general formulae (1)-(12) and a process for synthesizing melamine based Mannich-products comprising the steps of a) reacting at least one substituted melamine with at least one aldehyde, in particular formaldehyde, under basic conditions to form at least one OH-containing compound, b) reacting the at least one OH-containing compound in the presence of a catalyst to form at least one mannich-base, c1) reacting the at least one mannich-base with at least one enol-forming carbonyl compound, or c2) reacting the at least one mannich-base with at least one aromatic compound, and d) working up the reaction mixture. The invention relates further to precondensates obtainable from these products.
    Type: Grant
    Filed: November 17, 2010
    Date of Patent: August 12, 2014
    Assignee: Borealis Agrolinz Melamine GmbH
    Inventors: René Dicke, Christoph Hahn, Martin Burger, Andreas Endesfelder, Katarina Rot, Clemens Schwarzinger, Klaus Bretterbauer, Heinrich Trischler, Harald Schmidt
  • Patent number: 8722674
    Abstract: Disclosed herein are a 1,3,5-triazine-2,4,6-triamine compound or a pharmaceutically acceptable salt thereof, a preparation method thereof, and a composition for preventing or treating metabolic syndromes, diabetes, or cancers with deletion of P53 gene, which comprises the same.
    Type: Grant
    Filed: August 28, 2008
    Date of Patent: May 13, 2014
    Assignee: Hanall Biopharma Co., Ltd.
    Inventors: Hyae Gyeong Cheon, Kwang-Rok Kim, Sang Dal Rhee, Won Hoon Jung, Jong-Cheol Lee, Sung Wuk Kim, Sung Soo Jun
  • Publication number: 20130190493
    Abstract: Surface-modified nanoparticles are produced by associating ligand interactive agents with the surface of a nanoparticle. The ligand interactive agents are bound to surface modifying ligands that are tailored to impart particular solubility and/or compatibility properties. The ligand interactive agents are crosslinked via a linking/crosslinking agent, such as hexamethoxymethylmelamine or a derivative thereof. The linking/crosslinking agent may provide a binding site for binding the surface modifying ligands to the ligand interactive agents.
    Type: Application
    Filed: December 21, 2012
    Publication date: July 25, 2013
    Applicant: NANOCO TECHNOLOGIES, LTD.
    Inventor: Nanoco Technologies, Ltd.
  • Patent number: 8471007
    Abstract: Process for preparing higher 1,3,5-triazine carbamates and 1,3,5-triazine ureas from lower 1,3,5-triazine carbamates.
    Type: Grant
    Filed: April 8, 2005
    Date of Patent: June 25, 2013
    Assignee: BASF SE
    Inventors: Yvonne Heischkel, Eva Wagner, Joerg Schneider, Reinhold Schwalm, Guenter Scherr, Karl Haeberle
  • Publication number: 20120271050
    Abstract: The present invention relates to a method for recycling water in a melamine production process comprising—a wet process comprising the steps of aqueous treatment of a melamine melt from a melamine synthesis plant with an aqueous alkali containing solution and crystallization for producing solid melamine and a triazine containing alkaline mother liquor,—a wastewater treatment process comprising the steps of thermal treatment of said triazine containing alkaline motor liquor, and—a recycling process, whereby at least parts of the thermally treated alkaline mother liquor are being recycled to the wet process.
    Type: Application
    Filed: October 8, 2010
    Publication date: October 25, 2012
    Applicant: BOREALIS AGROLINZ MELAMINE GMBH
    Inventors: Arne Schadt, Robert Schlesinger, Gregor Demel, Christoph Neumüller, Franz Hintermüller
  • Publication number: 20120252987
    Abstract: The present invention relates to a method for producing amphiphilic functionalized highly branched melamine-polyamine polymers by condensing melamine and optionally a melamine derivate having at least one different amine having at least two primary amino groups and optionally also with urea and/or at least one urea derivative and/or with at least one at least difunctional diisocyanate or polyisocyanate and/or at least one carbolic acid having at least two carboxyl groups or at least one derivative thereof, optionally quaternizing a portion of the amino groups of the polymer thereby obtained, reacting the polymer thus obtained with at least one compound capable of undergoing a condensation or addition reaction with amino groups, and optionally quaternizing at least part of the amino groups of the polymer obtained in the first step.
    Type: Application
    Filed: December 15, 2010
    Publication date: October 4, 2012
    Applicant: BASF SE
    Inventors: Maxim Peretolchin, Marta Reinoso Garcia, Holger Tuerk, Daniel Schoenfelder, Sophia Ebert
  • Patent number: 8263766
    Abstract: A melamine skeleton-bearing organosilicon compound has a film forming ability, water solubility and compatibility with resins. It is prepared by reacting cyanuric chloride with a primary and/or secondary amine compound and neutralizing with a base.
    Type: Grant
    Filed: June 30, 2010
    Date of Patent: September 11, 2012
    Assignee: Shin-Etsu Chemical Co., Ltd.
    Inventor: Kazuhiro Tsuchida
  • Patent number: 8044197
    Abstract: Radiation-curable 1,3,5-triazine carbamates and 1,3,5-triazine ureas, processes for preparing them and their use.
    Type: Grant
    Filed: April 8, 2005
    Date of Patent: October 25, 2011
    Assignee: BASF SE
    Inventors: Yvonne Heischkel, Joerg Schneider, Reinhold Schwalm, Guenter Scherr
  • Patent number: 8034929
    Abstract: The invention relates to a process for preparing polymethylolated melamine and polymethylolated melamine compounds polyetherified with alkanol, wherein the methylolation reaction is carried out in a kneading reactor.
    Type: Grant
    Filed: January 13, 2005
    Date of Patent: October 11, 2011
    Assignee: BASF SE
    Inventors: Jörg Schneider, Günter Scherr, Rainer Erhardt, Andreas Eichfelder, Martin Reif, Stefan Hirsch, Hans Schupp, Christel Hittinger, Alain Robert
  • Patent number: 8030485
    Abstract: The invention relates to a process for preparing free-flowing, pulverulent alkoxycarbonylaminotriazine from an alkanolic reaction mixture which is obtained in the preparation of alkoxycarbonylaminotriazines and comprises at least one alkoxycarbonylaminotriazine, at least one cyclic and/or acyclic carbonic ester, at least one C1-C13-alkanol which optionally comprises one or two oxygen atoms in the form of ether bonds and is optionally substituted by C1-C4-alkyl and/or hydroxyl, and also at least one alkali metal or alkaline earth metal alkoxide, with or without melamine and with or without catalyst, by atomizing and drying the reaction mixture in a spray drier.
    Type: Grant
    Filed: May 31, 2006
    Date of Patent: October 4, 2011
    Assignee: BASF Aktiengesellschaft
    Inventors: Joerg Schneider, Guenter Scherr, Rainer Erhardt, Andreas Eichfelder, Martin Reif, Stefan Hirsch, Georg Sieder, Thomas Holtmann, Juergen Ciprian, Hermann Ascherl
  • Patent number: 7893380
    Abstract: An arc-interrupting compound, such as melamine, and to a method of extinguishing an arc by disposing the composition along the path of the arc, for contacting the arc. In one embodiment, the binder, or at least a portion of the binder, is a polymer that contains a functional group that binds to a coupling agent that is included in the arc-extinguishing composition. The coupling agent ties the polymeric binder to the arc-extinguishing compound, e.g., melamine, to provide new and unexpected physical strength and stability to the composition. In this embodiment, the molded composition, including the arc-interrupting compound coupled to the binder, maintains excellent arc-interrupting capability, while providing chemical stability and electrical insulating properties as well as unexpected physical strength.
    Type: Grant
    Filed: January 4, 2008
    Date of Patent: February 22, 2011
    Assignee: S&C Electric Company
    Inventor: Jeffrey A. Moore
  • Publication number: 20100063249
    Abstract: Provided is a proton-conducting compound which provides proton conductivity without humidification and is suitable for electrochemical device materials such as solid electrolytes for fuel cells and electrolytes for batteries. Provided also is a proton-conducting polymer. The proton-conducting compound is composed of a melamine compound salt obtained from a melamine compound represented by the following formula (1) and a Bronsted acid and the proton-conducting polymer is obtained by homopolymerizing or copolymerizing the melamine compound salt. In formula (1), R1, R2, R3, R4, and R5 each is independently an alkyl group, an aryl group, an alkenyl group, a heterocyclic group, or a hydrogen atom; at least one of them is a group other than hydrogen; R2 and R3 or R4 and R5 may join together to form a heterocyclic structure; and the alkyl group, the aryl group, the alkenyl group, or the heterocyclic group may have a substituent.
    Type: Application
    Filed: October 30, 2007
    Publication date: March 11, 2010
    Applicant: NIPPON STREEL CHEMICAL CO., LTD
    Inventors: Atsushi Kawada, Aya Tashiro
  • Publication number: 20100028971
    Abstract: The invention discloses a carrier made from an organic foam having open pores for enzymes or cells immobilization and the methods for preparing immobilized enzymes or cells. The invention uses flocculation and crosslinking technology to immobilize enzyme protein or cells on the organic foam material having open pores. The resultant immobilized products have larger specific surface area, higher specific activity and can be made into various shapes.
    Type: Application
    Filed: September 25, 2006
    Publication date: February 4, 2010
    Applicant: GENEHARBOR (HONG KONG) TECHNOLOGIES LTD.
    Inventors: Caike Jin, Jun Wang
  • Patent number: 7645496
    Abstract: A compound of formula (A): wherein L1 and L2 each independently are a single bond or a divalent linking group, R1 and R2 each independently are a hydrogen atom or a substituent, and R is a group having a polymerizable group; and a composition, containing at least one of the compound; an optically anisotropic material, containing the compound or the composition; and a liquid crystal display device, containing the optically anisotropic material.
    Type: Grant
    Filed: June 15, 2007
    Date of Patent: January 12, 2010
    Assignee: Fujifilm Corporation
    Inventors: Shigeki Uehira, Hiroshi Takeuchi
  • Publication number: 20090134007
    Abstract: This invention consists essentially in the employment of the melanines, precursors of the melanines, derivates of the melanines, variants, analogues of the melanines, or their precursors natural or synthetic, pure or mixed with organic or inorganic compounds, metals ions drugs; as water electrolyzing materials, employing as its only or main energy source light, natural or synthetic, coherent or not, in the hydrogen producing systems from water known as photoelectrochemical. These systems integrate a semiconductor material and a water electrolyzing element within a monolytic design to produce hydrogen directly from water, employing light (from 200 to 900 nm wavelengths) as its only or main energy source Although simple in concept, the challenge was to find a material that could bear or sustain the whole process.
    Type: Application
    Filed: October 13, 2005
    Publication date: May 28, 2009
    Inventor: Arturo Solis Herrera
  • Patent number: 7507819
    Abstract: The present invention relates to a method for preparing amino phosphate flame retardants. Melamine and phosphoric acid substances are used as a starting material, AND then the starting material reacts in the absence of solvents at a temperature ranging from 40 to 200° C. to obtain powdery amino phosphate compounds used as flame retardants. Since the reaction free of solvents is carried out under a condition of lower temperature, the powdery amino phosphate compounds can be obtained without drying steps. Therefore, not only the contaminations caused by solvent volatilization can be avoided, but also the process of preparing the product is simplified and the cost of the product is reduced.
    Type: Grant
    Filed: November 7, 2005
    Date of Patent: March 24, 2009
    Assignee: Chang Chun Plastics Co., Ltd.
    Inventors: Kuen-Yuan Hwang, An-Bang Duh, Chih-Fu Chen, Cheng-Jung Chiang
  • Patent number: 7507818
    Abstract: In a process for preparing alkoxycarbonylaminotriazines, di- or triaminotriazines are reacted with cyclic carbonic esters and optionally with minor amounts of acyclic carbonic esters in the presence of an alcohol and of an alkali metal alkoxide or alkaline earth metal alkoxide as a base.
    Type: Grant
    Filed: December 16, 2003
    Date of Patent: March 24, 2009
    Assignee: BASF Aktiengesellschaft
    Inventors: Joerg Schneider, Guenter Scherr, Hans Schupp, Andreas Eichfelder, Alain Robert, Martin Reif
  • Publication number: 20080275234
    Abstract: The invention relates to a method for producing pure melamine by preparing a melamine melt, which is obtained in a high pressure process and from which the reaction gases are removed. Said method is characterized in that the melamine melt is quenched by water with a purity in excess of 95 wt. %, that NH3 and CO2 are subsequently removed from the obtained melamine solution and that alkali is added to said melamine solution and the mixture is then left to rest, whereby pure melamine is obtained by crystallization. Thus a melamine can be obtained with the same quality as that produced in known comparative methods, using smaller quantities of alkali.
    Type: Application
    Filed: April 12, 2005
    Publication date: November 6, 2008
    Inventor: Wolfgang Ruech
  • Publication number: 20080146518
    Abstract: The present invention relates to cationic lipids capable of forming complexes with nucleic acids and the use thereof for the transfection of eukaryotic cells. The cationic lipids according to the invention have general formulas (I) and (Ia): (see formulas (I) and (Ia), wherein E is a heteroaryl; R1 and R2 are selected from H, —R7-NH2, aklyl; R7 is selected from alkyl, alkenyl, aryl, (C1-C20) alkyl-aryl-(C0-C20) alkyl; R3 and R4 are selected from: H, —R8-SH, R8-NH—NH2/—R8-CO—R9 or —R8-NH2; R8 is selected from: alkyl, alkenyl, aryl, (C1-C20) alkyl-aryl-(C0-C20) alkyl; R9 is selected from: H, alkyl; R5 and R6 are selected from: H, alkyl, alkenyl, aryl, (C1-C20) alkyl-aryl.
    Type: Application
    Filed: February 13, 2006
    Publication date: June 19, 2008
    Applicant: POLITECNICO DI MILANO
    Inventors: Matteo Zanda, Luca Bruche, Massimo Fricerio, Fiorenza Viani, Luca Chiamenti, Walter Panzeri, Nadia Zaffaroni, Marco Folini, Maria Angela Greco
  • Patent number: 7371856
    Abstract: A process is described for preparing alkoxycarbonylaminotriazines by reacting di- or triaminotriazines with dimethyl carbonate in the presence of an alcohol and of an alkali metal or alkaline earth metal methoxide base.
    Type: Grant
    Filed: December 12, 2006
    Date of Patent: May 13, 2008
    Assignee: BASF Aktiengesellschaft
    Inventors: Joerg Schneider, Guenter Scherr, Hans Schupp, Andreas Eichfelder, Alain Robert, Martin Reif
  • Publication number: 20080103233
    Abstract: The invention relates to a composition comprising melamine particles, said composition comprising melamine particles that are obtainable in a crystallising step done on an aqueous phase comprising melamine in solution (melamine A particles), whereby the composition also comprises melamine particles obtainable in a crystallising step done on a melamine melt or on melamine vapour (melamine D particles).
    Type: Application
    Filed: October 7, 2005
    Publication date: May 1, 2008
    Inventor: Saskia I. Dijk Van