Detoxification By Using Acid Or Alkaline Reagents (epo/jpo) Patents (Class 588/318)
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Patent number: 11851728Abstract: A method for processing accumulators, batteries and the like, which contain lithium, lithium ions, sodium, potassium and/or nickel as active components. According to the invention, the following steps are carried out; —introducing an accumulator, a battery, cell or the like, that contains lithium, lithium ions, sodium, potassium and/or nickel, into a chamber/reactor (13,23); —introducing water (H2O) (B, B2) in to the reactor (13,23); bringing the content of the reactor (13) to a temperature between 120° C. and 370° C. at a pressure between 2 and 250 bar.Type: GrantFiled: July 15, 2020Date of Patent: December 26, 2023Assignee: ECO-RESEARCHInventors: Werner Tirler, Giulio Voto, Marco Palmitano, Fritz Mödinger
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Patent number: 11828023Abstract: A pulp transportation system is adapted for transporting a pulp among a pulp-supply machine and a plurality of forming machines, and includes a pump unit, a first pipe unit, a second pipe unit and a valve unit. The pump unit is adapted for urging the pulp to flow. The valve unit is operable to control flow of the pulp through the first pipe unit and the second pipe unit, such that the flow of the pulp is convertible between a pulp-supply state, in which the pulp flows out from the pulp supply machine into at least one of the forming machines, and a pulp-return state, in which the pulp flows out from at least one of the forming machines into the pulp supply machine.Type: GrantFiled: August 23, 2022Date of Patent: November 28, 2023Inventor: Fu-Lin Hsiao
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Patent number: 11697043Abstract: A reagent set includes an oxidant, acid, and adsorbent, which is used in a method for reducing the leachability and release of PFAS, mercury, and other contaminants from soils, sediments, and other solid materials or waste when treated materials are exposed to acid rain, snow melt, runoff, landfill leachate, etc. The reagents are mixed with a quantity of contaminated material and water is added as needed in order to reduce the leachability of the contaminants from the treated host material, where the admixture end-product suitably removes contaminants from fluids that contact and/or otherwise permeate and/or pass through and/or around the treated admixture. The reagent set and method of use offer environmental professionals long-term, economically viable waste management solutions for removing contaminants from contamination source areas, spill and manufacturing release sites, impacted media, and landfills, as well as from the fluids that contact reagent-treated material.Type: GrantFiled: April 29, 2020Date of Patent: July 11, 2023Assignee: HMR Solutions, Inc.Inventors: Karl William Yost, Jody Bickford
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Patent number: 11428406Abstract: A tissue digester system includes a container for housing a digestion chamber having an exterior vessel for holding digestor fluid and an interior vessel, the container extending from a first end to a second end, the interior vessel having perforations and having baffles extending from an interior surface of the interior vessel; a lid secured to the exterior vessel and to provide access to the digestion chamber; one or more heating elements positioned to apply heat to the digestion chamber; a motor engaged with the interior vessel and to create rotational movement of the interior vessel; a control system, having a temperature controller; and a movement controller; the control system is to rotate the interior vessel and heat the digestion chamber based on user commands; and the digestion chamber is to break down remains through application of the digestor fluid to the tissue remains.Type: GrantFiled: January 22, 2021Date of Patent: August 30, 2022Inventor: Philip Mason
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Patent number: 11087898Abstract: Methods for disposing of munition components may include separating propellants from heavy metal penetrators and disposing of those separated components into different types of geological formations. The initially solid form propellants may be converted into a stable liquified propellant form, by a particular disclosed process, that may be injected within salt water (injection) disposal wells, where distal portions of such salt water disposal wells may be located in a geological formation of substantially at least one salt. The separated heavy metal penetrators (with or without their associated projectile jackets) may be disposed of within human-made caverns, where such human-made caverns may be located within a deep geological formation that is often 2,000 feet or more below the Earth's surface. The heavy metal penetrators may include uranium (depleted uranium). Portions of a given munition, to be disposed of, may be radioactive.Type: GrantFiled: May 29, 2020Date of Patent: August 10, 2021Inventor: Henry Crichlow
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Patent number: 10751771Abstract: A process for curbing of emissions of toxic metals and chelating agent from remediated soils, sediments and other substrates contaminated with toxic metals, said process comprising: (a) remediation of contaminated soil, sediment and other substrate with washing solution, said washing solution comprising EDTA or other chelating agent from the group of aminopolycarboxylic acids and their salts and mixtures thereof; (b) addition of 0.05-5% (w/w, dry weight) of zero-valent Fe or Fe compounds from the group of Fe-oxides and Fe-oxide-hydroxides into the slurry phase of soil, sediment and other substrate; (c) mixing of Fe-amended slurry; (d) separation of solid phase of remediated and Fe-amended soil, sediment and other substrate; (e) ageing of remediated and Fe-amended soil, sediment and other substrate for 0.5-45 days.Type: GrantFiled: December 4, 2018Date of Patent: August 25, 2020Assignee: ENVIT, ENVIRONMENTAL TECHNOLOGIES AND ENGINEERING LTD.Inventor: Domen Le{hacek over (s)}tan
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Patent number: 9912022Abstract: The invention is directed to systems and methods for the recycling of lithium ion batteries or the like. The system methods include comminution and destruction of used batteries, controlling the explosive reaction of the battery components during processing, and processing the materials into a suitable form for sampling and recycling.Type: GrantFiled: April 5, 2017Date of Patent: March 6, 2018Assignee: RECYCLING COORDINATORS, INC.Inventors: Dennis J. Dunagan, Teague C. Ostrander
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Patent number: 9620828Abstract: The invention is directed to systems and methods for the recycling of lithium ion batteries or the like. The system methods include comminution and destruction of used batteries, controlling the explosive reaction of the battery components during processing, and processing the materials into a suitable form for sampling and recycling.Type: GrantFiled: September 20, 2016Date of Patent: April 11, 2017Assignee: RECYCLING COORDINATORS, INC.Inventors: Dennis J. Dunagan, Teague C. Ostrander
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Patent number: 9492697Abstract: Tissue digestion methods and apparatuses that provide easy, safe and inexpensive disposal of biological tissue, for example animal carcasses and human cadavers, are disclosed. Embodiments include tissue digesters with elongated cylindrical vessels for holding digestive fluid and baskets for holding tissue within said vessel. Embodiments include baskets with perforations to allow circulation of digestive fluid around and about the tissue. In one form the basket holding the tissue is horizontally loaded into a horizontally disposed vessel. The vessel is then tilted to a more vertical orientation. Gravity helps to collect the tissue fragments in a sloped collection region of the basket, which is located near a mixer to allow continual agitation of the tissue fragments as they are digested. The tissue digester can operate efficiently at lower temperature and pressures, is mechanically less complicated, consumes less power and is less expensive to manufacture than conventional tissue digesting systems.Type: GrantFiled: April 29, 2011Date of Patent: November 15, 2016Assignee: Bio-Response Solutions, Inc.Inventors: Joseph H. Wilson, Lucas J. Wilson
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Patent number: 9364876Abstract: Apparatus and a method for decomposing a body of a deceased person, as an alternative to traditional cremation. The apparatus includes a primary vessel where the body is treated with a highly basic solvent to render the body into skeletal remains and liquid remains. A clamp is applied to the skull during processing for solvent access to the skull. A secondary vessel is used to receive the liquid remains from the primary vessel and further treat them. During this further treatment, the skeletal remains left in the primary vessel after the liquefied portion has been transferred to the secondary vessel, can be treated to be decolorized and deodorized, and then returned to the decedent's next of kin as ash-like material.Type: GrantFiled: April 7, 2015Date of Patent: June 14, 2016Assignee: BioSafe Engineering, LLCInventor: Brandon Ross
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Patent number: 9283417Abstract: Disclosed is a method of detoxifying asbestos by using a room-temperature recrystallization scheme. The method includes heat-treating a rock or slate containing asbestos; and putting the heat-treated rock or slate in an aqueous solution, to which organic acid is added, to allow the heat-treated rock or slate to react with the aqueous solution having the organic acid.Type: GrantFiled: November 26, 2014Date of Patent: March 15, 2016Assignee: KOREA INSTITUTE OF GEOSCIENCE AND MINERAL RESOURCESInventors: Young-Nam Jang, Soo-Chun Chae, Myung-Kyu Lee
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Patent number: 9205294Abstract: An exemplary system for treatment and disposal of pharmaceutical waste comprises a sealable pail, a stirring device, a sealable bag, a container, an acidic substance, and a denaturant. The sealable pail receives the pharmaceutical waste and the acidic substance. The acidic substance dissolves the pharmaceutical waste, and the stirring device stirs the acidic substance to ensure that the pharmaceutical waste is completely dissolved. The denaturant is added to the dissolved pharmaceutical waste and renders the dissolved pharmaceutical waste safe for transport. The treated pharmaceutical waste is sealed within the sealable pail, and the sealable bag receives the sealed pail and is sealed. The sealed bag is then placed in the container for transport to a disposal facility.Type: GrantFiled: February 10, 2015Date of Patent: December 8, 2015Inventor: Donald R. Stalons
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Publication number: 20150148583Abstract: Disclosed is a method of detoxifying asbestos by using a room-temperature recrystallization scheme. The method includes heat-treating a rock or slate containing asbestos; and putting the heat-treated rock or slate in an aqueous solution, to which organic acid is added, to allow the heat-treated rock or slate to react with the aqueous solution having the organic acid.Type: ApplicationFiled: November 26, 2014Publication date: May 28, 2015Inventors: Young-Nam JANG, Soo-Chun CHAE, Myung-Kyu LEE
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Publication number: 20150080630Abstract: The invention is directed to systems and methods for the recycling of lithium ion batteries or the like. The system methods include comminution and destruction of used batteries, controlling the explosive reaction of the battery components during processing, and processing the materials into a suitable form for sampling and recycling.Type: ApplicationFiled: September 12, 2014Publication date: March 19, 2015Inventors: Dennis J. Dunagan, Teague C. Ostrander
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Patent number: 8981175Abstract: An exemplary system for treatment and disposal of pharmaceutical waste comprises a sealable pail, a stirring device, a sealable bag, a container, an acidic substance, and a denaturant. The sealable pail receives the pharmaceutical waste and the acidic substance. The acidic substance dissolves the pharmaceutical waste, and the stirring device stirs the acidic substance to ensure that the pharmaceutical waste is completely dissolved. The denaturant is added to the dissolved pharmaceutical waste and renders the dissolved pharmaceutical waste safe for transport. The treated pharmaceutical waste is sealed within the sealable pail, and the sealable bag receives the sealed pail and is sealed. The sealed bag is then placed in the container for transport to a disposal facility.Type: GrantFiled: June 18, 2012Date of Patent: March 17, 2015Inventor: Donald R. Stalons
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Patent number: 8940958Abstract: Method for the stabilization of contaminants within a material selected from soils, mining tailings and by-products, sludge wastes and industrial wastes, by mixing the material with an alum sludge composition. The composition includes one or more aluminum compound(s) and/or complex(es) together with a reactive carbon material.Type: GrantFiled: September 30, 2010Date of Patent: January 27, 2015Assignees: Commonwealth Scientific and Industrial Research Organisation, Ziltek Pty LtdInventor: Michael John McLaughlin
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Publication number: 20140378735Abstract: Disclosed is a method of detoxifying asbestos of waste slate. The method includes concentrating the asbestos by introducing hydrochloric acid aqueous solution into waste slate powder to dissolve and remove a limestone component contained in the waste slate; and mixing the concentrated asbestos with oxalic acid and performing a low-temperature heat treatment. The waste slate is crushed and pulverized and powder of the crushed and pulverized waste slate is formed in a size in a range of 100 meshes to 300 meshes. The detoxified asbestos includes re-crystallized magnesium oxalate having a rhombohedral or amorphous shape.Type: ApplicationFiled: June 19, 2014Publication date: December 25, 2014Inventors: Young-Nam JANG, Kyungsun SONG, Myung Gyu LEE, Soo-Chun CHAE, Hwanju JO, Jun-Hwan BANG, Kyoung Won RYU
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Patent number: 8884093Abstract: The present invention relates to the use of catalysts of general formula (I): (L1)M1-X-M2(L2)??(I) wherein: M1 and M2, either identical or different, represent metal atoms; X represents a nitrogen atom; L1 and L2, either identical or different are coordinated with M1 and M2, respectively, and represent ligands of the tetradentate type, for catalytic oxidation of halogenated compounds.Type: GrantFiled: April 6, 2011Date of Patent: November 11, 2014Assignees: Centre National de la Recherche Scientifique (C.N.R.S.), Universite Claude Bernard Lyon 1Inventors: Alexander Sorokin, Evgeny V. Kudrik
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Patent number: 8865961Abstract: Nitrocellulose propellants and plasticized military munitions, equipment, or contaminated soil are placed in a suitable container. A first option consists of adding a strong base to plasticized munitions in a container or militarization/demilitarization equipment or soil containing plasticized munitions or nitrocellulose propellant; adding an organic solvent; and then adding water to mixture. Alternatively, a second option consists of adding organic co-solvent to plasticized munitions in a container or soil containing plasticized munitions or solid nitrocellulose propellant. A strong base is added to mixture and allowed to react. When the reaction stops or is completed, a sulfur based bulk reductant is added to degrade all nitro and amino compounds. The organic solvent is evaporated and recovered for reuse and water is added to the container to make up for the evaporated organic solvent. If pH is higher than 8.5, a suitable acid is added to drop the pH to near neutral.Type: GrantFiled: July 12, 2012Date of Patent: October 21, 2014Inventor: Valentine Asongu Nzengung
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Publication number: 20140249346Abstract: The process for stabilizing wastes generally comprises blending spent or virgin fullers earth with a hazardous or non-hazardous sludge, soil or sediment to form a matrix. Next, the matrix is blended with a reagent capable of growing a calcium silicate hydrate or Ettringite mineral. In this manner a more stable, less leachable product is formed.Type: ApplicationFiled: October 30, 2013Publication date: September 4, 2014Applicant: Remedial Construction Svc., L.P.Inventor: Steven R. BIRDWELL
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Patent number: 8822750Abstract: A method is described for the treatment of ferrous nuclear waste, produced in operations of pickling of contaminated metallic surfaces, which makes it possible to minimize the volumes of liquid phases to be treated and to recycle the by-products thereof to the process.Type: GrantFiled: November 11, 2011Date of Patent: September 2, 2014Assignee: ECIR—Eco Iniziativa e Realizzazioni—S.r.l.Inventors: Pier Paolo Costa, Lorenzo Costa
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Publication number: 20140243575Abstract: Disclosed is a method of removing asbestos from an asbestos-containing material by 99% through low temperature heat treatment. The method includes mixing an asbestos-containing material with an oxalic acid at a weight ratio in a range of 1:0.002 to 1:1 and performing heat treatment with respect to a mixture at a temperature of 90° C. to 110° C. to remove asbestos from the asbestos-containing material by 99% or more.Type: ApplicationFiled: February 25, 2014Publication date: August 28, 2014Applicant: KOREA INSTITUTE OF GEOSCIENCE AND MINERAL RESOURCESInventors: Young-Nam Jang, Soo-Chun Chae, Myung-Kyu Lee, Hye-In Won, Kyoung-Won Ryu
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Patent number: 8802915Abstract: Presented herein are compositions including a linear tenso-active surfactant which, upon contact and mechanical stirring of a hydrocarbon body, induces emulsification, resulting in oxidation of fatty acid aliphatic bodies. The compositions solve the problem of hydrocarbon pollution. The hydrocarbon decomposer and its by-products dissolve hydrocarbons present in polluted bodies such as clays, soils, water and sand. Methods of the invention create a residue that is a fertilizer, at room temperature and with no need for high pressure.Type: GrantFiled: March 11, 2013Date of Patent: August 12, 2014Inventor: Pedro Murillo Gutierrez
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Publication number: 20140217323Abstract: Disclosed is a method of treating a strong basic aluminum production waste. The method includes preparing an aluminum production waste; and mixing the aluminum production waste with gypsum.Type: ApplicationFiled: January 31, 2014Publication date: August 7, 2014Applicant: KOREA INSTITUTE OF GEOSCIENCE AND MINERAL RESOURCESInventors: Pyeong-Koo Lee, Sang-Woo Ji
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Publication number: 20140206922Abstract: Nitrocellulose propellants and plasticized military munitions, equipment, or contaminated soil are placed in a suitable container. A first option consists of adding a strong base to plasticized munitions in a container or militarization/demilitarization equipment or soil containing plasticized munitions or nitrocellulose propellant; adding an organic solvent; and then adding water to mixture. Alternatively, a second option consists of adding organic co-solvent to plasticized munitions in a container or soil containing plasticized munitions or solid nitrocellulose propellant. A strong base is added to mixture and allowed to react. When the reaction stops or is completed, a sulfur based bulk reductant is added to degrade all nitro and amino compounds. The organic solvent is evaporated and recovered for reuse and water is added to the container to make up for the evaporated organic solvent. If pH is higher than 8.5, a suitable acid is added to drop the pH to near neutral.Type: ApplicationFiled: July 12, 2012Publication date: July 24, 2014Inventor: Valentine Asongu Nzengung
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Patent number: 8785712Abstract: A pharmaceutical drug disposal kit includes a container for receiving pharmaceutical drugs. Water is added to the container to create an aqueous solution with the pharmaceutical drugs, and a constituent in the container makes the solution a basic aqueous solution. A visual and/or taste deterrent is disposed in the container, and an adsorbent or absorbent is also disposed in the container to provide at least partial solidification of the solution. A binding agent is also disposed in the container to bind the ingredients of the pharmaceutical drug, the deterrent, and the adsorbent/absorbent, thereby changing the physical state of the pharmaceutical drugs into a substance that is undesirable to consume, and which enables safe disposal of the pharmaceutical drugs.Type: GrantFiled: June 10, 2010Date of Patent: July 22, 2014Assignee: RX Disposal Solutions, LLCInventors: Brian Deryck, John Heaton
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Patent number: 8766030Abstract: Accelerated dechlorination of soil and water contaminated with chlorinated solvents in situ is achieved by delivering ferric ammonium citrate into the soils and/or water. The induction of ferric ammonium citrate into sulfate-rich reducing conditions initiates a combined abiotic and biotic mechanism for the dechlorination of subsurface contaminants. Initial and rapid removal of chlorinated solvents is achieved by way of reductive transformation, a mechanism utilizing the creation of an iron-bound soil mineral (pyrite) followed by stimulating conditions for enhanced biological natural attenuation.Type: GrantFiled: July 25, 2012Date of Patent: July 1, 2014Assignee: Innovative Environmental Technologies, Inc.Inventor: Michael Scalzi
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Patent number: 8703078Abstract: The invention relates to a system and method for the substantially permanent biogeochemical stabilization of solids impacted with hexavalent chromium/Cr(VI), including chromite ore processing residue (“COPR”). The invention comprises a novel treatment method of adding amendment(s) to COPR or other chromate impacted solids for the purpose of (1) weathering COPR minerals (when present) to convert the minerals that control alkalinity of the COPR to non-alkaline forms and liberate incorporated hexavalent chromium (Cr(VI)) in the process; (2) providing a chemical reductant (ferrous iron) to rapidly and permanently reduce the available Cr(VI) to trivalent form (Cr(III)); and/or (3) supporting longer-term biogeochemical Cr(VI) reduction enhanced by recycling of the chemical reductant, ultimately rendering the material non-hazardous as measured by acceptable methods.Type: GrantFiled: January 13, 2011Date of Patent: April 22, 2014Assignee: ARCADIS Corporate Services, Inc.Inventors: Jeff B. Gillow, John F. Horst, Suthan S. Suthersan
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Publication number: 20130338420Abstract: Cleaning compositions, methods for cleaning exterior surfaces of a vehicle, and cleaning compositions for cleaning exterior surfaces of a vehicle are disclosed. The cleaning compositions include a C8-22 alkyl dimethylamine oxide surfactant, a C6-12 alkyl dimethylamine oxide surfactant, a C8-18 alkyl polyethylene glycol sorbitan fatty ester surfactant, and a C12-14 secondary alcohol ethoxylate surfactant are disclosed. The methods include providing a cleaning composition, applying the cleaning composition to exterior surfaces of a vehicle, and rinsing the exterior surfaces of the vehicle.Type: ApplicationFiled: June 6, 2013Publication date: December 19, 2013Inventors: Alan David Willey, Valerie Jean Bradford, Claire Rebecca Yates, Jacob Robert Adams, Ronak V. Rughani
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Publication number: 20130317274Abstract: A method for removing elements, including heavy metals, from fly ash and from fly ash resulting from removal of SOx/NOx from flue gas using Na2CO3/NaHCO3/trona, is described. An aqueous suspension of the fly ash and/or a solution of the leachate from the fly ash is treated with dissolved ferrous compounds, such as FeSO4.7H2O and/or FeCl2.4H2O, at a chosen initial acidic pH, and the precipitation of the ferrous ions as the solution basifies sequesters the trace elements.Type: ApplicationFiled: May 23, 2013Publication date: November 28, 2013Inventors: Maohong Fan, Morris D. Argyle, Mustafa O.M. Sharrad
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Patent number: 8586817Abstract: A composition to control acid rock drainage is provided. The composition includes a slurry made from water and solids, the solids containing powders of limestone, clay and magnesium oxide or magnesium hydroxide. In some instances, the slurry is thixotropic and contains between 10 to 75 weight percent of solid powders. The solid powders can include between 40 to 75 weight percent limestone, 10 to 35 weight percent clay and 10 to 30 weight percent magnesium oxide or a proportional concentration of magnesium hydroxide.Type: GrantFiled: January 15, 2013Date of Patent: November 19, 2013Assignee: The Penn State Research FoundationInventor: Hubert L. Barnes
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Publication number: 20130281538Abstract: The present invention is directed to a formulation and associated method for neutralizing one or more toxic chemical and/or materials including toxic industrial chemicals and toxic industrial materials, such as irritants, heavy metals, radioactive metals, acids and acid irritants, pesticides, and various agricultural chemicals, (collectively referred to as toxic chemical, materials, or simply toxins) as well as decontaminating surfaces that have come into contact with these agents. As a result, the formulation of the present invention can be used for neutralizing a broad spectrum of toxic chemicals and materials. In one embodiment, the active ingredient comprises 2, 3, butanedione monoxime (also known as diacetyl monoxime (DAM)), and alkali salts thereof such as potassium 2,3-butanedione monoxime (KBDO). The formulation also typically includes a carrier in which the active ingredient is dispersed.Type: ApplicationFiled: June 18, 2013Publication date: October 24, 2013Inventors: Timothy G. Henry, Barbara B. Price
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Publication number: 20130211175Abstract: We provide a process and apparatus for preparing a used catalyst for disposal, comprising: a. hydrolyzing a used ionic liquid catalyst comprising an anhydrous metal halide to produce a hydrolyzed product; and b. separating the hydrolyzed product into a liquid phase and a solid phase; wherein the liquid phase comprises a non-water-reactive aqueous phase and a hydrocarbon phase; and wherein the solid phase comprises a solid portion of the hydrolyzed product, that is not water reactive. A vessel is used for the hydrolyzing and a separator is used for the separating.Type: ApplicationFiled: February 14, 2012Publication date: August 15, 2013Applicant: Chevron U.S.A. Inc.Inventors: Hye-Kyung Timken, Shawn Stephen Healy, Shawn Shlomo Winter
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Patent number: 8497405Abstract: The disclosed invention relates to a decontaminant dispenser which may be used as a projectile. The invention also relates to a decontamination process using the decontaminant dispenser. The decontaminant dispenser may be thrown by hand, launched as an artillery shell or the payload for a missile, or dropped by an airplane into the area to be decontaminated. The dispenser may be placed in the area to be decontaminated. The decontaminant dispenser may be ruggedized for use in hostile environments such as those that may be anticipated for military applications.Type: GrantFiled: February 28, 2013Date of Patent: July 30, 2013Assignee: STERIS Inc.Inventors: Timothy W. Meilander, Paul A. Wiget, Iain F. McVey, Michael A. Centanni
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Publication number: 20130178687Abstract: Tissue digestion methods and apparatuses that provide easy, safe and inexpensive disposal of biological tissue, for example animal carcasses and human cadavers, are disclosed. Embodiments include tissue digesters with elongated cylindrical vessels for holding digestive fluid and baskets for holding tissue within said vessel. Embodiments include baskets with perforations to allow circulation of digestive fluid around and about the tissue. In one form the basket holding the tissue is horizontally loaded into a horizontally disposed vessel. The vessel is then tilted to a more vertical orientation. Gravity helps to collect the tissue fragments in a sloped collection region of the basket, which is located near a mixer to allow continual agitation of the tissue fragments as they are digested. The tissue digester can operate efficiently at lower temperature and pressures, is mechanically less complicated, consumes less power and is less expensive to manufacture than conventional tissue digesting systems.Type: ApplicationFiled: April 29, 2011Publication date: July 11, 2013Applicant: BIO-RESPONSE SOLUTIONS, INC.Inventors: Joseph H. Wilson, Lucas J. Wilson
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Patent number: 8470182Abstract: Apparatus and method for hydrolyzing biological material for safe disposal thereof without the necessity of incineration or use of disinfectants are described. An alkaline solution having a concentration and an amount effective for hydrolyzing the biological material is brought into contact therewith by means of rotating paddles which both pound the biological material into small pieces and thoroughly mix the alkaline solution with the material under pressure and at elevated temperature. Following the hydrolysis of the biological material, a chosen portion of the water is removed from the alkaline solution and from the liquefied biological material, such that the resulting product solidifies when cooled. The present safe disposal of the biological material does not require incineration thereof, the addition of disinfectants thereto, or the discharge of liquid effluent containing processed biological material into the sewage system.Type: GrantFiled: November 29, 2011Date of Patent: June 25, 2013Assignee: Gyver L. Electric, Inc.Inventor: Mark R. Muth
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Publication number: 20130123563Abstract: A self-decontaminating metal organic framework including an acid linked to a metal producing a metal organic framework configured for the sorption of chemical warfare agents and/or toxic industrial chemicals, the metal organic framework including reactive sites for the degradation of the agents and chemicals.Type: ApplicationFiled: January 2, 2013Publication date: May 16, 2013Inventors: Yongwoo Lee, Thomasz Modzelewski, John P. Puglia, Steven E. Weiss, Banglin Chen
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Patent number: 8430803Abstract: The present invention discloses a method for solidifying and stabilizing waste acid including steps of condensing waste acid containing phosphoric acid to reduce the volume; mixing the condensed waste acid with waste acid containing fluoroboric acid to solidify and stabilize the mixed waste acid. The pH of the mixed acid is adjusted by adding barium hydroxide as a neutralizer. The efficiency of solidifying waste acid can be improved by partially granulating and by adding solidifying agent indirectly. The method of the present invention can prevent intensely exothermic reaction caused by adding solidifying agents. Furthermore, the method of the present invention is controlled in a temperature of 30 to 45° C. to improve the polymerization of the mixed waste acid so that the efficiency of solidification thereof can be also improved.Type: GrantFiled: October 24, 2007Date of Patent: April 30, 2013Assignee: Atomic Energy Council—Institute of Nuclear Energy ResearchInventors: Ching-Tsuen Huang, Ching-Tu Chang
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Patent number: 8420881Abstract: The subject invention provides a potentially economically viable process for the destruction of small to large quantities of sulfur and nitrogen mustards and lewisite, their homologous/analogues, and similar chemical warfare agents at ambient conditions without producing any toxic by-products. The process uses the superoxide ion that is either electrochemically generated by the reduction of oxygen in deep eutectic solvents or chemically by dissolving Group 1 (alkali metals) or Group 2 (alkaline earth metals) superoxides, e.g. potassium superoxide, in deep eutectic solvents.Type: GrantFiled: March 26, 2008Date of Patent: April 16, 2013Assignee: King Saud UniversityInventors: Inas Muen Al Nashef, Saeed M. Al Zahrani
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Patent number: 8410330Abstract: A composition to control acid rock drainage is provided. The composition includes a slurry made from water and solids, the solids containing powders of limestone, clay and magnesium oxide or magnesium hydroxide. In some instances, the slurry is thixotropic and contains between 10 to 75 weight percent of solid powders. The solid powders can include between 40 to 75 weight percent limestone, 10 to 35 weight percent clay and 10 to 30 weight percent magnesium oxide or a proportional concentration of magnesium hydroxide.Type: GrantFiled: February 25, 2008Date of Patent: April 2, 2013Assignee: The Penn State Research FoundationInventor: Hubert L. Barnes
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Publication number: 20130053615Abstract: Embodiments of this disclosure relate to tissue digestion and, more particularly, to methods and apparatuses for varying the number, size, and/or location of one or more tissue compartments within a digestive fluid vessel. Some examples include partitions that may be selectively positioned within a vessel (and may be selectively removable from the vessel) to create one or more tissue compartments. The partitions may be positioned, repositioned and rearranged within the vessel to form one or more tissue compartments. The partitions may be solid or include apertures, and may be oriented in horizontally and/or vertically. Alternate embodiments include one or more selectively closeable apertures that permit digestive fluid to circulate along alternate pathways, which can permit tissue digestion with reduced digestive fluid levels. Still further embodiments include baskets that are selectively positionable within the tissue digester.Type: ApplicationFiled: August 24, 2012Publication date: February 28, 2013Inventors: Joseph H. Wilson, Lucas J. Wilson, Samantha J. Sieber, Mark A. Halsey
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Patent number: 8354567Abstract: Described are method of treating a radioactive organic waste stream comprising: (a) mixing a radioactive organic waste stream comprising organic compounds and radionuclides with phosphoric acid to form a reaction mixture; (b) heating the reaction mixture to a desired temperature in the presence of an oxidant to oxidize organic compounds present in the waste stream, and removing oxidized organic compounds from the reaction mixture; (c) optionally, adding a reducing agent to the reaction mixture to form insoluble radioactive metal phosphate compounds comprising one or more of the radionuclides, and separating the insoluble radioactive metal phosphate compounds from the reaction mixture; (d) optionally, adding a fluorine compound to the reaction mixture to react with uranium that may be present in the reaction mixture to form uranium hexafluoride, and removing uranium hexafluoride from the reaction mixture; (e) adding ammonia to the reaction mixture to neutralize phosphoric acid and to form ammonium phosphateType: GrantFiled: January 29, 2009Date of Patent: January 15, 2013Inventors: David Donald Leavitt, Robert Dale Delano
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Publication number: 20120323061Abstract: An exemplary system for treatment and disposal of pharmaceutical waste comprises a sealable pail, a stirring device, a sealable bag, a container, an acidic substance, and a denaturant. The sealable pail receives the pharmaceutical waste and the acidic substance. The acidic substance dissolves the pharmaceutical waste, and the stirring device stirs the acidic substance to ensure that the pharmaceutical waste is completely dissolved. The denaturant is added to the dissolved pharmaceutical waste and renders the dissolved pharmaceutical waste safe for transport. The treated pharmaceutical waste is sealed within the sealable pail, and the sealable bag receives the sealed pail and is sealed. The sealed bag is then placed in the container for transport to a disposal facility.Type: ApplicationFiled: June 18, 2012Publication date: December 20, 2012Inventor: Donald R. Stalons
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Publication number: 20120296147Abstract: Various methods and apparatus are disclosed that relate to one or more aspects of a treatment system that circum-neutralizes the pH of an aqueous stream, removes one or more heavy metals from the aqueous stream, circum-neutralizes the pH of a CCR supply, and/or removes one or more heavy metals from the CCR supply.Type: ApplicationFiled: May 15, 2012Publication date: November 22, 2012Inventors: Jason Swearingen, Lindsay Swearingen
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Publication number: 20120289756Abstract: To provide a treatment agent for asbestos, which has a less influence on human body, the construction and the surrounding environment and can render the asbestos harmless evenly up to the inside of the bulky covering materials, which cover the wall, or the slate materials, and a treatment method of the asbestos using the same. A treatment agent for asbestos, which contains phosphoric acid of 0.5 through 3.0% by weight, hydrogen peroxide of 1 through 20% by weight, alcohol of 0.5 through 20% by weight and pure water and a treatment method of the asbestos using the same are described.Type: ApplicationFiled: November 19, 2010Publication date: November 15, 2012Applicant: SANTEC CORPORATIONInventors: Yoshihiro Taguchi, Teruhiko Kusano, Hiroaki Harano
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Patent number: 8278496Abstract: The invention relates to a method in connection with steel production for handling of hydroxide sludge formed in the neutralization of spent metal-contaminated pickling agents from a pickling step for steel, preferably stainless steel and for using calcium fluoride in the hydroxide sludge to replace the natural fluorspar as a fluxing agent in connection with steel production. Accordingly, the addition of the reactive neutralization medium is monitored by the pH electrodes operated in continuous fashion, and the pH value is adjusted at the range between 9.0 and 9.5.Type: GrantFiled: May 7, 2007Date of Patent: October 2, 2012Assignee: Outokumpu OyjInventor: Sven-Eric Lunner
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Patent number: 8227655Abstract: The present invention discloses a method for solidifying and stabilizing waste acid including steps of condensing waste acid containing phosphoric acid to reduce the volume; mixing the condensed waste acid with waste acid containing fluoroboric acid to solidify and stabilize the mixed waste acid. The pH of the mixed acid is adjusted by adding barium hydroxide as a neutralizer. The efficiency of solidifying waste acid can be improved by partially granulating and by adding solidifying agent indirectly. The method of the present invention can prevent intensely exothermic reaction caused by adding solidifying agents. Furthermore, the method of the present invention is controlled in a temperature of 30 to 45° C. to improve the polymerization of the mixed waste acid so that the efficiency of solidification thereof can be also improved.Type: GrantFiled: October 20, 2011Date of Patent: July 24, 2012Assignee: Atomic Energy Council-Institute of Nuclear Energy ResearchInventors: Ching-Tsuen Huang, Ching-Tu Chang
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Publication number: 20120164199Abstract: This disclosure provides novel compositions comprising an inorganic and organic compound, which provides a means for the indirect attachment of a reactive species, such as an organic reactive molecule, within a binder polymer matrix. Such compositions provide a hydrophilic nanoscale domain that is uniformly dispersed within the polymer matrix. The nanoscale domain comprises inorganic particles having a nanoscale dimension. Such compositions can enhance the performance potential of the re-active species within the polymer material. The polymer composite that results from the introduction of such reactive species into a polymer matrix provides a self-decontaminating feature. The reactive species include those that are capable of associating with a halogen to form a complex that is active in decontamination of chemical or biological agents.Type: ApplicationFiled: July 28, 2008Publication date: June 28, 2012Applicant: Isotron CorporationInventors: Henry LOMASNEY, Christina Lomasney, John Grawe
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Patent number: 8178743Abstract: A method for remediating hazardous materials susceptible to nucleophillic attack is disclosed wherein sodium hydroxide is applied to a treatment zone in situ for raising the pH of the treatment zone to at least about 12.5 so that alkaline hydrolysis effectively breaks down the hazardous substance by replacing a leaving group with a nucleophile. The method is well suited for in situ use in the vadose zone to treat contaminated soil and groundwater.Type: GrantFiled: June 30, 2009Date of Patent: May 15, 2012Assignee: Tetra Tech, Inc.Inventors: Ronald Britto, Madhukant Patel, Mikael L. Spangberg, Richard W. Arnseth, Franklin R. Bogle
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Publication number: 20120107200Abstract: The instant invention relates to a process and plant for the transformation of dangerous wastes containing chromium six as contaminant into non dangerous wastes that can be stored without special care and will be degraded in the environment without time limit. The process basically consists of milling, extracting chromium six in liquid phase and under controlled conditions of stirring, time and temperature, proceeding then, through reduction, to transform the chromium six in chromium three and then precipitating as chromium trioxide, through gasification. The solid resulting from the transformation process can be used as raw material for the manufacturing of firebricks or eventually for the manufacturing of bricks used in the building industry through a process not included in the instant description.Type: ApplicationFiled: December 21, 2011Publication date: May 3, 2012Applicant: CROMOTECNICA MEXICOInventor: Francisco Garcia FERNANDEZ