Abstract: Ice slurry is manufactured in direct contact heat transfer in a tank comprising a layer of heavy solvent, of water dissolving a freezing point depressant, of ice slurry, and of light solvent. The heavy solvent is heavier in density than water, and the light solvent lighter than ice. The heavy solvent, water, and light solvent are immiscible with each other. The freezing point depressant is insoluble in the heavy and light solvents. The light solvent is chilled in a chiller, and injected into the heavy solvent layer, where bubbles of light solvent are generated without ice clogging. The cold liquid bubbles ascending through the water layer produce ice. Ice slurry is continuously withdrawn below the light solvent layer. The light solvent side of the chiller is coated with a hydrophobic coating material to prevent formation of sessile ice particles of the undissolving water molecules from the light solvent.

Abstract: The present invention relates to a method for separating off a substance from a solution, in which electromagnetic radiation is radiated into the solution, an intensity of the electromagnetic radiation which has been scattered by crystals located in the solution is detected, the detected intensity is compared with a desired intensity (IS) and the temperature of the solution is regulated depending on the difference between the detected intensity and the desired intensity (IS) in such a way that the amount of this difference is reduced. If the amount of the difference between the detected intensity and the desired intensity (IS) is less than a limiting value, a crystallization method is started in which crystals of the substance are obtained which are then separated off.

Abstract: A pressure and prevacuum testing system for an AC system in a vehicle includes an air pressure source for pressurizing a cooling circuit of the AC system to a predetermined high pressure threshold and a vacuum source for prevacuuming the cooling circuit either to a predetermined prevacuum low pressure level or for a predetermined time period. The system also includes a pressure gauge for operatively measuring a pressure level in the cooling circuit. A controller is operatively connected to the air pressure source, the vacuum source and the pressure gauge. The controller compares the pressure level as measured by the pressure gauge to the predetermined high pressure threshold during a pressurized test of the cooling circuit and to the predetermined prevacuum low pressure level during a prevacuum test of the cooling circuit to determine if leaks are present in the cooling circuit.

Abstract: A system for the drying of exhaust gases from a fuel cell system comprises two heat exchangers alternately exposed to exhaust gas, which ice and accumulate water vapour from the exhaust gas by means of a coolant. A valve arrangement with a number of valves is adapted in such a manner that it operates one of the heat exchangers in an icing phase and the other heat exchanger in a regeneration phase, in which the accumulated ice melts and is extracted. This system is especially suitable in aircraft for drying an oxygen-depleted exhaust gas from a fuel cell system for inerting a tank.

Abstract: Systems, methods and apparatus are provided for utilizing a substantially condensed phase cryogenic fluid for the purpose of remediation and retrieval of, e.g., spilled crude oil and other “oil spill”-related products from marine/aquatic and terrestrial environments. In some implementations, systems and apparatus are provided for applying a substantially condensed phase cryogenic fluid to a volume of spilled oil, and further having structure for collecting the spilled oil. Some implementations are environmentally-neutral. Substances other than oil may be remediated as well.

Abstract: Disclosed herein are a method of recycling LiCl salt wastes comprising radionuclides and an apparatus using the same. The method includes a) solidifying a LiCl salt contained in the LiCl salt wastes and contacting the outer wall of a housing, by charging a crystallizer comprising the housing having an internal accommodating space and an air cooler in the internal accommodating space into a crystallizing furnace accommodating the LiCl salt wastes comprising the radionuclides, and by cooling the housing to a temperature of two-phase region where the liquid state and the solid state of the LiCl salt waste coexist, b) separating the crystallizer where the LiCl salt is solidified from the crystallizing furnace, c) recycling the LiCl salt by heating the separated crystallizer to melt the solidified LiCl salt.

Abstract: Systems, methods and apparatus are provided for utilizing a substantially condensed phase cryogenic fluid for the purpose of remediation and retrieval of, e.g., spilled crude oil and other “oil spill”-related products from marine/aquatic and terrestrial environments. In some implementations, systems and apparatus are provided for applying a substantially condensed phase cryogenic fluid to a volume of spilled oil, and further having structure for collecting the spilled oil. Some implementations are environmentally-neutral. Substances other than oil may be remediated as well.

Abstract: A process for purifying removal of crystals from their suspension in mother liquor by means of a washing column having forced transport in which the process chamber is encased by a metal wall which, on its side facing away from the process chamber, is heated at least along the length of the pure melt zone.

Abstract: Volatile vapors are removed from a storage vessel by establishing a flow of a stream of volatile vapors from the storage vessel and directing the stream through a first low temperature condenser for condensing a portion of the stream flowing through the first low temperature condenser. Since a portion of the condensed condensate freezes and causes a pressure drop in the first low temperature condenser, further steps may include directing the stream from the first low temperature condenser through a second low temperature condenser after the pressure drop exceeds a setpoint, stopping the flow of the refrigerant through the first low temperature condenser and using the heat of the volatile vapor stream to melt the frozen condensate in the first low temperature condenser. The stream is switched between the condensers as necessary to prevent excessive plugging due to frozen condensate formation. The system includes the means for implementing the method.

Abstract: A method and apparatus for producing particles, the apparatus includes a solution source that supplies a solution, and a fluid source that supplies a fluid. The solution includes a solvent and a solute. A mixer receives the solution and the fluid from the sources, and mixes the solution and the fluid together to form a mixture. The mixture is supplied from the mixer to an expansion assembly at first pressure. The expansion assembly sprays and expands the mixture substantially simultaneously to form frozen droplets, and preferably to form a low-density powder of frozen droplets. A freeze-dry apparatus sublimes the solvent from the particles. A high mass-transfer rate and a uniform open-structure of the powder bed enhances the freeze-drying process. Solid particles having a controlled size distribution are obtained. The particles preferably have a hollow or porous morphology suitable for differing drug delivery applications to include aerosol formulations.

Abstract: In a method of controlling progressive freeze-concentration by circulating a cooling medium through a cooling-medium flow route while circulating a target liquid for freeze-concentration through a target-liquid flow route so as to gradually form ice crystals on wall surfaces of the target-liquid flow route, a volume expansion detecting device is used to detect volume expansion of the target liquid and thickness of the ice crystals in the target-liquid flow route is obtained from the volume expansion detected by this volume expansion detecting device.

Abstract: A method and apparatus for producing particles, the apparatus includes a solution source that supplies a solution, and a fluid source that supplies a fluid. The solution includes a solvent and a solute. A mixer receives the solution and the fluid from the sources, and mixes the solution and the fluid together to form a mixture. The mixture is supplied from the mixer to an expansion assembly at first pressure. The expansion assembly sprays and expands the mixture substantially simultaneously to form frozen droplets, and preferably to form a low-density powder of frozen droplets. A freeze-dry apparatus sublimes the solvent from the particles. A high mass-transfer rate and a uniform open-structure of the powder bed enhances the freeze-drying process. Solid particles having a controlled size distribution are obtained. The particles preferably have a hollow or porous morphology suitable for differing drug delivery applications to include aerosol formulations.

Abstract: A phase change particulate saline slurry and methods and apparatus are provided for producing phase change particulate saline slurries. One method for producing phase change particulate saline slurries includes the steps of providing a liquid with a set percentage freezing point depressant, such as, a set percentage saline solution; subcooling the saline solution to a freezing point to produce ice particles; and increasing an ice particle concentration under controlled temperature for a period of time to provide a set ice particle concentration for the phase change particulate saline slurry. In another method for producing phase change particulate saline slurries, water and a first set amount of sodium chloride are provided to produce a saline solution. The saline solution is cooled to a set temperature. A selected percentage of chunk ice is added to the saline solution and the chunk ice is broken into ice particles. The ice particles have a small size.

Abstract: An apparatus for treating water to produce potable water includes a filter connected to an inlet of a heating unit in turn connected at an outlet to an input of a container with cooling components for separating out heavy water. The heavy water separator is coupled at an outlet to a tank having cooling and heating components and an ultraviolet radiation source for irradiating the water sample from the heavy water separator with ultraviolet radiation during a freezing and subsequent warming of the water sample. A storage vessel and a silver ionizer are disposed on a downstream side of the ultraviolet treatment tank. Various operations, including timing and water transfer, heating cooling and irradiating, are controlled by a programmed computer. Temperature sensors are disposed in the heating unit, the heavy water separator and the irradiation tank for monitoring temperatures of the water in the heating unit, the container and/or the tank.

Abstract: Apparatus comprising a vessel capable of receiving a variable supply of an aqueous ice slurry in which an upper packed ice bed can float on an aqueous volume; a hollow conduit having a first end located in the lower internal space of the vessel and a second end located exterior of the vessel; a float positioned in the vessel lower internal space; and a movable line in the hollow conduit joined at one end to the float, and the line second end extending out of the conduit second end thus permitting it to be displaced to indicate the position of the float, and thus the bottom of the packed ice bed, when it contacts a packed ice bed bottom.

Abstract: A vessel is provided with a flexible plastic tube containing an electrical contact switch. Impure water is added to the vessel between the tube and the wall of the vessel. The vessel is then placed in a home freezer. Upon partial freezing of the impure water, the ice expands to flex or compress the tube to close the switch so as to actuate a detector or alarm. The user then removes the unfrozen water, and allows a fraction of the ice to melt. The just formed water is checked for purity by a conductivity measurement. If impure, the water is removed, and the ice is allowed to further melt until the desired purity level is reached at which time the remaining ice is melted to obtain purified water. The device and method are particularly suitable for home use to economically obtain purified water.

Abstract: A plant for treatment of sediment of natural and waste waters comprises a crystallizer (1), a melter (2), a condensing heat exchanger (4), a compression refrigerating unit (3) communicating with the crystallizer (1) and the melter (2) which is in communication with the sediment dehydration apparatus (5). The evaporator (8) of a crystallizer (1) has two cylinders (9). The plant comprises a refrigerant feed unit (13) and a refrigerant discharge unit (15), a planetary gear drive, a sediment application unit (17) and a sediment removal unit (19). The crystallizer (1) has a recirculation station (6). The sediment application unit (17) is made in the form of pour-on nozzles (18). Installed between the cylinders (9), at an angle to their walls with a clearance (.delta..sub.1, .delta..sub.2) are screens (12). The sediment removal unit (19) has at least two cutting tools (20) with flexible pick-ups.

Abstract: A crystallization/separation apparatus is disclosed for material mixtures having vertical crystallization column, cooling and heating devices, feeding-in and withdrawal connections, pumps, valves, connecting conduit tubings and drive motor, a cylindrical tube contains perpendicular aisles, rotatable at a central axis. The tube is distributed into segment-shaped chambers by said aisles, each substantially the same size. Also disclosed is a method for the separation of material mixtures.

Abstract: An improved crystallization process is disclosed for separating a crystallizable material and an excluded material which is at least partially excluded from the solid phase of the crystallizable material obtained upon freezing a liquid phase of the materials. The solid phase is more dense than the liquid phase, and it is separated therefrom by relative movement with the formation of a packed bed of solid phase. The packed bed is continuously formed adjacent its lower end and passed from the liquid phase into a countercurrent flow of backwash liquid. The packed bed extends through the level of the backwash liquid to provide a drained bed of solid phase adjacent its upper end which is melted by a condensing vapor.

Abstract: A method for treating in counter current of suspended particles with a liquid, whereby the particles and the liquid are transferred in opposite directions through a contact zone which, at some places, spaced in axial direction, is stirred in planes perpendicular to the center line of the contact zone, in which the contact zone is one continuous space and that the volume fraction of the solid matter in the contact zone is maintained at a value between 0.20 and 0.55.

Abstract: Apparatus for separating ice from concentrated liquid and washing the ice, including a vessel having a bottom and vertical wall joined to the bottom; a plurality of vertical tubular members in the vessel extending upwardly from the bottom; perforations in the upper portion of the tubular members through which concentrated liquid in the vessel can drain into the tubes; a first conduit for feeding a slurry of ice and concentrated liquid to the vessel; a second conduit communicating with the tubes for withdrawing concentrated liquid from the tubes; a concentrated liquid withdrawal third conduit communicating with the vessel lower interior portion for withdrawing concentrated liquid from the vessel; and control means to maintain a predetermined concentrated liquid level, and a predetermined pressure distribution, in the vessel.

Abstract: A system for extracting heat from low temperature water includes a source of water at a temperature between approximately 0.degree. C. and 10.degree. C. and a heat pump removing heat from the water and transporting it for transfer to an external heating circuit. The heat pump has a closed circuit containing a heat transport fluid, a condenser, and an evaporator. The water, acting as a heat source, is fed into a vacuum vessel and subjected to triple-point conditions thereby concomitantly forming water vapor and a water/ice crystal suspension. The evaporator is disposed in the vacuum vessel out of direct contact with the water/ice crystal suspension for absorbing heat from the evaporated water vapor.

Abstract: A telemetry system for reporting the status of a number of physical parameters occurring during operation of industrial equipment, such as the monitoring of refrigeration/air conditioning safety controls and anticipatory refrigeration controls. Activation of the safety or anticipatory controls generate electrical signals to activate a four input alarm transmitter, which automatically dials a pre-programmed telephone number and reports the status of the various inputs to a special monitor receiver at a remote location. An interface board is coupled to the safety and anticipatory controls, and multiplexes the signals therefrom into four transmitter inputs. An indicator panel connected to the interface board provides a maintained visual indication of which input(s) have caused a transmission. The anticipatory controls are set to trip before the safety controls, which latter controls effect shut-down of the system, and provide anticipatory signals warning of impending system problems.

Abstract: Apparatus for separating paraffin from oil in refineries wherein such separation is accomplished by a cooling process, in a heat exchanger, the apparatus controlling the cooling process by sensing either the pressure upstream of the heat exchanger and directly controlling the flow through a heat exchanger bypass, or sensing the temperature downstream of the heat exchanger and inversely controlling the flow through a heat exchanger bypass, the flow control in each case regulating the flow of cooling liquid through the heat exchanger.

Abstract: Method and apparatus for separation of mixtures wherein a mixture is cooled very slowly in a quiescent, nondisturbed condition to produce large dendritic crystals of solidified solvent, then heated very slowly while liquid of high solute concentration is drained from the large interstices between the crystals, the cooling and reheating being effected by slowly conveying containers of mixture through a long heat transfer conduit or tunnel having a central refrigeration zone; parallel trains of containers preferably travel through the conduit in opposite directions. The residence time of the mixture in traveling through the conduit or tunnel will be of the order of many hours or a few days, depending upon many factors, and in a large industrial installation the length of a pass through it will be several hundred feet; such factors are interrelated to the quantity and compositions of mixtures being processed.