Solidification Patents (Class 62/601)
  • Patent number: 11119177
    Abstract: The invention relates to a method for the hyperpolarization of a material sample (4), which hits a number of first spin moments (10) of a first spin moment type, wherein the number of first spin moments (10) is brought into interaction with a second spin moment (16) of a second spin moment type, wherein the first spin moments (10) are nuclear spin moments and the second spin moment (16) is an election spin moment, wherein the first and second spin moments (10, 16) are exposed to a homogeneous magnetic field (B), wherein the second spin moment (16) is polarized along the magnetic field (B), wherein the second spin moment (16) is coherently manipulated by means of a, preferably repeated, sequence (S) having a number of successive high-frequency pulses (Pki, Pk?i) temporally offset to each by durations (Tki, Tk?i, T), in such a way that a polarization transfer from the second spin moment (16) to the first spin moments (10) occurs, and wherein durations (Tki, Tk?i, T) inversely proportional to a Lamor frequency (
    Type: Grant
    Filed: December 21, 2017
    Date of Patent: September 14, 2021
    Assignee: NVision Imaging Technolgies GmbH
    Inventors: Ilai Schwartz, Martin Plenio, Qiong Chen, Zhenyu Wang
  • Patent number: 9261295
    Abstract: Embodiments of the disclosed invention relate to providing cooling to instruments or other components. More particularly, hydrogen from a store is provided to pre-cool helium contained within a closed loop refrigeration circuit. Helium pre-cooled by the hydrogen, for example after expansion of the hydrogen in an expansion valve, is itself passed through an expansion valve, and applied to a heat load. The helium can be circulated through the refrigeration circuit using a compressor. The hydrogen used for pre-cooling the helium can be from a store of hydrogen that also provides fuel to a hydrogen consumer, for example for propulsion of a vehicle carrying the cooling system or for the production of electrical power. A hydrogen consumer can also be provided with hydrogen that has first been used to pre-cool the helium refrigeration circuit.
    Type: Grant
    Filed: March 26, 2013
    Date of Patent: February 16, 2016
    Assignee: BALL AEROSPACE & TECHNOLOGIES CORP.
    Inventors: Jeffrey A. Schmidt, Eric Marquardt
  • Publication number: 20150027165
    Abstract: The present invention is a novel method for removing tritium oxide contamination from a solution with water. The method captures the tritium oxide in a much smaller volume suitable for economical disposal. In so doing the original water is decontaminated of the tritium oxide and may be discharged.
    Type: Application
    Filed: May 27, 2014
    Publication date: January 29, 2015
    Inventors: Randall N. Avery, Charlie Booth, Keith Moser
  • Patent number: 8857212
    Abstract: The invention provides a process for the separation of a contaminant or mixture of contaminants from a CH4-comprising gaseous feed stream, comprising the subsequent steps of: a) passing a CH4-comprising gaseous feed stream comprising the contaminant or the mixture of contaminants into and through a cold porous body having a temperature below the sublimation temperature of the contaminant or the mixture of contaminants and contacting the CH4-comprising gaseous feed stream at elevated pressure with the surface of the cold porous body to obtain a porous body comprising solid contaminant or mixture of contaminants and a contaminant-depleted product gas; and b) reducing the pressure to obtain fluid contaminant or mixture of contaminants and a cold porous body. c) removing the fluid contaminant or mixture of contaminants, wherein the contaminant is selected from CO2, hydrogen sulphide, mercaptans, siloxanes and carbonyl sulphide, or a mixture thereof.
    Type: Grant
    Filed: October 10, 2011
    Date of Patent: October 14, 2014
    Assignee: Shell Oil Company
    Inventors: Martin Van Sint Annaland, Martin Jan Tuinier
  • Patent number: 8844155
    Abstract: The invention relates to a hopper of an injection molding machine, which comprises a combined hopper, an electric heating air-blasting system and a temperature control system, wherein the combined hopper comprises two or more than two sub-hoppers; each sub-hopper is provided with an independent sub-feed inlet, an independent sub-discharge outlet and a branch air-blasting port capable of being controlled independently; all the sub-discharge outlets of the sub-hoppers are communicated with a thermostatic chamber arranged below the sub-discharge outlets; a main discharge outlet and a main air supply port are arranged at the lower part of the thermostatic chamber; and the thermostatic chamber and each sub-hopper are provided with independent temperature control systems respectively.
    Type: Grant
    Filed: September 30, 2011
    Date of Patent: September 30, 2014
    Inventor: Zhengrong Lou
  • Publication number: 20130240236
    Abstract: In a thermally insulated double pipe, a structure is provided in which an inner pipe may be prevented from being appreciably offset relative to an outer pipe due to thermal contraction. The structure includes an inner pipe 101, within which a superconducting cable is mounted, an outer pipe 103 within which the inner pipe is housed, with the inner and outer pipes constituting a thermally insulated double pipe, and an inner pipe support member 104 supporting the inner pipe. The inner pipe support member 104 is secured to the inner and outer pipes.
    Type: Application
    Filed: September 5, 2011
    Publication date: September 19, 2013
    Applicant: CHUBU UNIVERSITY EDUCATIONAL FOUNDATION
    Inventors: Sataro Yamaguchi, Hirofumi Watanabe
  • Patent number: 8511113
    Abstract: The invention provides a process for the separation of CO2 from a gaseous feed stream, comprising the subsequent steps of: a) cooling a porous body in the form of a fixed bed (101,102,103) to a temperature below the sublimation temperature of CO2 to obtain a cold body; b) contacting a gaseous feed stream (120) comprising CO2 and one or more other gaseous compounds with the surface of the cold body to obtain a body comprising solid CO2 and a CO2-depleted effluent gas (124); and c) removing the solid CO2 by exposing the porous body comprising solid CO2 to a fluid CO2 stream (130) having a temperature above the sublimation temperature of CO2 whereby fluid CO2 (136) and a warm porous body are obtained.
    Type: Grant
    Filed: October 10, 2008
    Date of Patent: August 20, 2013
    Assignee: Shell Oil Company
    Inventors: Gerrit Jan Barend Assink, Gert Jan Kramer, Martin Van Sint Annaland, Martin Jan Tuinier
  • Publication number: 20130206912
    Abstract: A method of reducing the amount of water in a region of air including: forming seed ice crystals; dispensing the seed ice crystals towards the region of air; allowing water in the region of air to freeze or deposit onto the seed ice crystals; and allowing the resulting ice crystals to move from the region of air so as to reduce the amount of water in the region of air. An ice crystal seeding assembly arranged to reduce the amount of water in a region of air, the seeding assembly includes an ice crystal seeder and dispensing means, the dispensing means being arranged to dispense seeded ice crystals towards the region of air so that water in the region of air freezes or deposits onto the seed ice crystals and that the resulting ice crystals move from the region of air.
    Type: Application
    Filed: February 10, 2012
    Publication date: August 15, 2013
    Applicant: ROLLS-ROYCE PLC
    Inventor: Christopher G. BRIGHT
  • Patent number: 8408025
    Abstract: A raw material recovery method for recovering a raw material of an organic metallic compound, which has the property of being stable toward a specific refrigerant without being decomposed thereby, from exhaust gas discharged from a treatment container in which a metallic thin film is formed on the surface of an object to be treated by using source gas obtained by vaporizing the raw material is characterized by being provided with a solidification step for solidifying the unreacted source gas by cooling the exhaust gas by bringing the exhaust gas into contact with the refrigerant and reprecipitating the raw material, and a recovery step for separating and recovering the raw material reprecipitated in the solidification step from the refrigerant. To provide a method for controlling an exhaust gas flow rate so that flow of gas in a processing chamber becomes uniform.
    Type: Grant
    Filed: August 4, 2009
    Date of Patent: April 2, 2013
    Assignee: Tokyo Electron Limited
    Inventors: Atsushi Gomi, Yasushi Mizusawa, Tatsuo Hatano, Masamichi Hara, Kaoru Yamamoto, Chiaki Yasumuro
  • Publication number: 20130074541
    Abstract: Systems and methods are described for re-moving solidifiable gas from a process gas stream by direct contact with a cold liquid. The process gas stream includes at least gas that is frozen by the cold liquid while one or more other gases of the process gas stream remain in a gaseous state. The process gas stream may include water, and will have a different composition than the cold liquid. The contacting of the cold liquid with the process gas stream may be at a pressure that is less than 200 psia, and optionally less than 100 psia, 50 psia, or even 30 psia, and the solidified gas may be removed from the contacting assembly as a slurry with cold liquid.
    Type: Application
    Filed: January 5, 2011
    Publication date: March 28, 2013
    Inventors: Robert D. Kaminsky, Moses Minta
  • Publication number: 20120318017
    Abstract: A method and apparatus for condensing vapor in a gas. A cryogen, such as liquid nitrogen, may be provided into first and second coil sets in a condenser housing to cool the condensable vapor in the housing to condense the vapor into a liquid or solid form. The flow of cryogen in the first and second coil sets may be independently controlled, coils in the first and/or second coil sets may have a substantially equal length, and/or coils in the first and/or second coil sets may have uppermost portions that are located at a substantially equal height.
    Type: Application
    Filed: June 19, 2012
    Publication date: December 20, 2012
    Inventor: Alan T. Cheng
  • Patent number: 8181469
    Abstract: A refrigerating method and a refrigerating system utilizing a large decomposition heat absorbed at the time of decomposition of the gas hydrate and building up, by a pump, the pressure of liquid components generated due to the decomposition of gas hydrate and compressing only gas components by a compressor, the refrigerating method comprising the steps of generating the gas hydrate (H) by a hydrate generating reactor (11), decomposing the gas hydrate (H) into the liquid components (L) and the gas components (G) after depressurization to absorb heat, separating the decomposed liquid components (L) and gas components (G) from each other, building up the pressure of the liquid components (L) by the pump (16) and transferring to the hydrate generating reactor (11), and pressurizing and compressing only the gas components (G) by the compressor (17) and transferring to the hydrate generating reactor (11).
    Type: Grant
    Filed: February 19, 2003
    Date of Patent: May 22, 2012
    Assignee: Mitsui Zosen Plant Engineering Inc.
    Inventors: Toshio Ichijo, Kikuo Nakamura
  • Patent number: 8048208
    Abstract: A method and device for separation of chalcogens from waste gases in process installations are provided so that complete and reliable removal of chalcogens occurs continuously during nonstop operation of the process installation in the most effective manner possible. The process installation is connected via a pipeline to an input connector of the device for separation of chalcogens arranged outside of the process installation. The pipeline and the input connector have a heat connection to the process chamber. The device for separation of chalcogens is provided with an outlet connector as well as a gas outlet is equipped with a cooling device so that the input connector is excluded from cooling.
    Type: Grant
    Filed: September 11, 2008
    Date of Patent: November 1, 2011
    Assignee: Centrotherm Photovoltaics AG
    Inventors: Dieter Schmid, Hans-Peter Voelk, Robert Michael Hartung
  • Publication number: 20110203310
    Abstract: A raw material recovery method for recovering a raw material of an organic metallic compound, which has the property of being stable toward a specific refrigerant without being decomposed thereby, from exhaust gas discharged from a treatment container in which a metallic thin film is formed on the surface of an object to be treated by using source gas obtained by vaporizing the raw material is characterized by being provided with a solidification step for solidifying the unreacted source gas by cooling the exhaust gas by bringing the exhaust gas into contact with the refrigerant and reprecipitating the raw material, and a recovery step for separating and recovering the raw material reprecipitated in the solidification step from the refrigerant. To provide a method for controlling an exhaust gas flow rate so that flow of gas in a processing chamber becomes uniform.
    Type: Application
    Filed: August 4, 2009
    Publication date: August 25, 2011
    Applicant: TOKYO ELECTRON LIMITED
    Inventors: Atsushi Gomi, Yasushi Mizusawa, Tatsuo Hatano, Masamichi Hara, Kaoru Yamamoto, Chiaki Yasumuro
  • Publication number: 20110128002
    Abstract: The present invention relates to a polarized xenon gas manufacturing supply device that is provided with a polarization cell 6 that produces a polarized xenon gas by polarizing a mixture of xenon gas and a diluent gas that consists primarily of a high-boiling-point gas that has a boiling point higher than that of the xenon gas, and a condenser (9) that cools the mixed gas discharged from the polarization cell (6) and condenses and separates the high-boiling-point gas by using the difference in boiling points between the xenon gas and the high-boiling-point gas, wherein the supply device is constructed so as to re-vaporize the condensed liquid of the high-boiling-point gas produced by the condenser (9) and introduce it to the polarization cell (6). This polarized xenon gas manufacturing supply device makes it possible to continuously manufacture and supply highly polarized and highly concentrated xenon gas.
    Type: Application
    Filed: July 29, 2009
    Publication date: June 2, 2011
    Inventors: Hideaki Fujiwara, Hirohiko Imai, Satoshi Iguchi, Hironobu Yoshimura, Atsuomi Kimura
  • Patent number: 7841190
    Abstract: Methods and devices for the management of cryogenic agents within analytical systems using freeze thaw valving having an expansion chamber that limits the flow of the cryogenic agent. The expansion chamber is fitted with an expansion nozzle through which a cryogen flows and a porous frit that allows the cryogen to be exhausted. The porous frit initially allows a rapid flow of cryogen into the expansion chamber. This rapid flow lowers the temperature of the expansion chamber causing fluid contents within a freeze thaw segment to freeze. As the cryogen expands into the expansion chamber and turns into a solid, the porous frit is occluded causing the rapid flow to be restricted. The restriction of the cryogen flow by the occlusion of the porous frit allows the freeze thaw valve to use significantly less cryogen. Sublimation of the cryogen trapped within the porous frit provides sufficient cooling to maintain the valve in its closed position.
    Type: Grant
    Filed: March 16, 2005
    Date of Patent: November 30, 2010
    Assignee: Waters Technologies Corporation
    Inventors: Geoff C. Gerhardt, Theodore Dourdeville
  • Patent number: 7740812
    Abstract: The present invention relates to a method and an apparatus for continuously separating aromatic dialdehyde from a reaction mixture obtained by gas-phase oxidation of dimethylbenzene. The method for continuously separating aromatic dialdehyde includes the steps of congealing aromatic dialdehyde by cooling the gas-phase reaction mixture including the aromatic dialdehyde, which is obtained by gas-phase oxidation of dimethylbenzene, to 5-70° C. and separating the congealed aromatic dialdehyde from the remaining reaction mixture. Using the method and apparatus in accordance with the present invention, aromatic dialdehyde can be effectively and selectively separated from a reaction mixture obtained by gas-phase oxidation of dimethylbenzene in high yield.
    Type: Grant
    Filed: June 2, 2008
    Date of Patent: June 22, 2010
    Assignee: LG Chem, Ltd.
    Inventors: Jong-Hyun Chae, Won-Ho Lee, Dong-Il Lee, Hyun-Kyung Yoon
  • Publication number: 20100147022
    Abstract: A process for removal of sour species from a dehydrated natural gas feed stream is provided. The dehydrated natural gas feed stream is cooled to conditions where a slurry of solid sour species and hydrocarbon liquids is formed together with a gaseous stream containing gaseous sour species. The gaseous stream containing gaseous sour species is then separated from the slurry and treated with a liquid solvent, thereby forming a liquid solution of the sour species and a dehydrated sweetened natural gas product stream. An apparatus for removing sour species from a dehydrated natural gas feed stream is also provided. The apparatus has a vessel with a solids formation zone in fluid communication with a gas solvation zone. The solids formation zone is configured to facilitate formation of a slurry of solid sour species and hydrocarbon liquids and a gaseous stream containing gaseous sour species. The gas solvation zone is configured to facilitate formation of a liquid solution of sour species.
    Type: Application
    Filed: September 15, 2006
    Publication date: June 17, 2010
    Applicant: COOL ENERGY LIMITED
    Inventors: Allan Hart, Robert Amin
  • Patent number: 7591138
    Abstract: An apparatus for producing a slush fluid wherein a liquid and solid particles are mixed together, comprising product tank (1) for storing the slush fluid (50) in its saturated condition; liquid nitrogen supply nozzle (10) provided at an upper part of the product tank (1); and compressor (15) for evacuating the interior of the product tank, which apparatus is adapted to spray a liquid in microparticulate form through the liquid nitrogen supply nozzle (10) into the product tank evacuated by the compressor (15) and to solidify the liquid particles by evaporative latent heat, thereby forming solid nitrogen (51).
    Type: Grant
    Filed: October 24, 2007
    Date of Patent: September 22, 2009
    Assignee: Mayekawa Mfg. Co., Ltd.
    Inventors: Masamitsu Ikeuchi, Akito Machida, Kouichi Matsuo
  • Patent number: 7526925
    Abstract: A method for producing slush nitrogen comprises the steps of: spraying liquid nitrogen from a nozzle into a vessel kept under a reduced pressure with a nozzle diameter and a spraying pressure being so adjusted as for the liquid nitrogen to maintain the form of droplets, to thereby form liquid nitrogen fine particles having a uniform particle diameter and disperse said particles in the vessel; vaporizing nitrogen from the droplet particles during the stay thereof in the space of the vessel, to solidify liquid nitrogen particles by vaporization latent heat and form fine solid nitrogen particles having a uniform particle diameter; and mixing the solid nitrogen particles with liquid nitrogen.
    Type: Grant
    Filed: August 4, 2006
    Date of Patent: May 5, 2009
    Assignee: Mayekawa Mfg. Co., Ltd.
    Inventors: Akito Machida, Kazuhiro Hattori, Kouichi Matsuo
  • Publication number: 20090095016
    Abstract: In a hydrogen consuming system and a method for the operation thereof wherein the system comprises a hydrogen-consuming unit and a hydrogen storage arrangement comprising a compressed gas storage part and a solid material storage part and a cooling circuit with a radiator extending through the solid material storage part and the consuming unit, hydrogen bypass lines are provided for the solid material storage part and for the hydrogen consuming unit together with control valves for selectively by-passing the solid material storage part and the hydrogen consuming unit.
    Type: Application
    Filed: October 27, 2008
    Publication date: April 16, 2009
    Inventors: Eberhard Schmidt-Ihn, David Wenger
  • Patent number: 7503186
    Abstract: In a method of condensing an unprocessed well stream from an offshore gas or gas condensate field the well stream taken from one or more wellheads is cooled and directly expanded, isentropically, or near isentropically, to a state in which the pressure is close to that of a storage tank. Part of the well stream is condensed and condensed fractions thereof is drawn off the expander and fed to the storage tank along with condensation products from the exit of the expander. Hence, without any preprocessing, a condensed well stream product is produced which comprises a mixture of liquids and solids which is collected in the storage tank for transport therefrom to land. A system for carrying out the method is also disclosed. The invention makes the condensation of an unprocessed well stream possible without any preprocessing thereof, such as extraction of solid particles, e.g. sands, removal of water, cleaning or drying.
    Type: Grant
    Filed: December 23, 2003
    Date of Patent: March 17, 2009
    Assignee: Institutt for Energiteknikk
    Inventors: Istvan Bencze, Jan Bosio, Guttorm O. Endrestøl, Terje Sira, Dag Thomassen
  • Publication number: 20080264845
    Abstract: Desalination apparatus based on porous restraint panels fabricated from a number of different layers of metal, thermoplastic, or other substances are used as sophisticated heat exchangers to control the growth of gas hydrate. The gas hydrate is produced after infusion of liquid hydrate-forming material into water to be treated, which liquid hydrate-forming material can also be used to carry out all the refrigeration necessary to cool seawater to near the point of hydrate formation and to cool the porous restraint panels. Hydrate forms on and dissociates through the porous restraints. The composite restraint panels can also be used in gaseous atmospheres where, for instance, it is desired to remove dissolved water.
    Type: Application
    Filed: June 23, 2008
    Publication date: October 30, 2008
    Inventor: Michael David Max
  • Patent number: 7281393
    Abstract: A method and apparatus for the accumulation of hyperpolarized 129Xe is described. A gas mixture comprising 129Xe is flowed through a heat exchanger tube from the first end to the second end. Concurrently, the outer surface of the heat exchanger tube is controllably refrigerated, beginning with the second end, to a temperature low enough to freeze the 129Xe on the inner surface of the heat exchanger tube.
    Type: Grant
    Filed: April 21, 2005
    Date of Patent: October 16, 2007
    Assignee: University of New Hampshire
    Inventor: F. William Hersman
  • Patent number: 7272894
    Abstract: A drum dryer provided with a liquid splash and scatter preventing equipment, which enables continuous operation by preventing a scattering liquid from making dry powder in the case in which the equipment is provided above a neighborhood of a liquid concentration section. A double drum type drum dryer including a liquid splash and scatter preventing equipment is provided in a horizontal above a neighborhood of a liquid concentration section between drums and has a cooling function.
    Type: Grant
    Filed: November 25, 2003
    Date of Patent: September 25, 2007
    Assignee: Ajinomoto Co., Inc.
    Inventors: Shundo Harada, Shigehira Uda, Hideshi Matoba
  • Patent number: 7201018
    Abstract: The invention relates to a process and apparatus for delivering an ultra high purity fluid comprising at least one component to a point of use at a required pressure without mechanical pumping. In one embodiment, a high purity feed comprising at least one component in gaseous or liquid form is charged into a vessel and at least partially converted to a solid phase source. As the feed is converted to a solid phase source, additional feed may be added until the vessel is at least substantially filled with a solid phase source or slush. Once filled, the solid phase source or slush may be isochorically heated whereby the solid phase source is converted to a product at an elevated pressure.
    Type: Grant
    Filed: January 9, 2004
    Date of Patent: April 10, 2007
    Assignee: Air Products and Chemicals, Inc.
    Inventors: Vladimir Yliy Gershtein, Alexander Schwarz, Wayne Thomas McDermott, John Frederick Cirucci, John Christopher Ivankovits
  • Patent number: 7155930
    Abstract: Liquid nitrogen is filled in a low temperature vessel; an ejector that sucks liquid nitrogen by blowing a cooling agent (liquid or gas) such as low temperature helium gas or liquid helium of pressure higher than in the space within the vessel is disposed in the vessel; the liquid nitrogen blown with the cooling agent is cooled by the cooling agent to become fine particles of solid nitrogen which fall down; and gas in a space of the vessel is discharged out of the vessel so as to maintain the pressure of the space higher than the atmospheric pressure. A gaseous phase of liquid nitrogen in an adiabatic vessel is depressurized to vaporize nitrogen in a liquid phase so that a temperature of the nitrogen is reached to the triple point of nitrogen by lowering temperature thereby and solid nitrogen is produced by keeping at the triple point, and that the produced solid nitrogen is transformed into slush by stirring the content of the adiabatic vessel.
    Type: Grant
    Filed: June 23, 2005
    Date of Patent: January 2, 2007
    Assignee: Mayekawa Mfg. Co., Ltd.
    Inventors: Kuniaki Kawamura, Akito Machida, Masamitsu Ikeuchi, Kazuhiro Hattori, Kouichi Matsuo, Hideharu Yanagi
  • Patent number: 7137274
    Abstract: Apparatus for producing liquid or solid xenon comprises a duct 12 having an inlet 14 for receiving gaseous xenon and an outlet 16 for outputting gaseous xenon at a reduced temperature to a nozzle located in a vacuum chamber 60. A housing 18 extends about the duct and contains a halocarbon coolant in thermal contact with the duct, and a second duct 24 in thermal contact with the halocarbon coolant for conveying a flow of liquid nitrogen through the housing 18 to control the temperature of the halocarbon. In view of the difference in the pressure of the xenon gas output from the duct and the pressure in the chamber, the thus-cooled gas is caused to liquefy or solidify in the vicinity of the nozzle.
    Type: Grant
    Filed: September 24, 2003
    Date of Patent: November 21, 2006
    Assignee: The BOC Group plc
    Inventors: Darren Mennie, Ron Clark Lee, Colin Michael Harrison, Makoto Kaneko, Joanne Rachel Greenwood
  • Patent number: 7013673
    Abstract: Processes and apparatus are disclosed for separating and purifying aqueous solutions such as seawater by causing a substantially impermeable mat of gas hydrate to form on a porous restraint. Once the mat of gas hydrate has formed on the porous restraint, the portion of the mat of gas hydrate adjacent to the restraint is caused to dissociate and flow through the restraint, e.g., by lowering the pressure in a collection region on the opposite side of the restraint. The purified or desalinated water may then be recovered from the collection region. The process may be used for marine desalination as well as for drying wet gas and hydrocarbon solutions. If conditions in the solution are not conductive to forming hydrate, a heated or refrigerated porous restraint may be used to create hydrate-forming conditions near the restraint, thereby causing gas hydrates to form directly on the surface of the restraint.
    Type: Grant
    Filed: March 25, 2005
    Date of Patent: March 21, 2006
    Assignee: Marine Desalination Systems, L.L.C.
    Inventor: Michael D. Max
  • Publication number: 20040154333
    Abstract: This invention relates to a process and apparatus for delivering an ultra high purity fluid comprising at least one component to a point of use at a required pressure without pumping. In one embodiment, a high purity feed comprising at least one component in gaseous or liquid form is charged into a vessel and at least partially solidified, i.e., converted to a solid phase source. As the feed is converted to a solid phase source, additional feed may be added until the vessel is at least substantially filled with a solid phase source or slush. Once filled, the solid phase source or slush may be isochorically heated whereby the solid phase source is converted to a product at an elevated pressure. In other embodiments, an apparatus and a method for the production and collection of a high purity solid phase source or slush comprising at least component is disclosed herein.
    Type: Application
    Filed: January 9, 2004
    Publication date: August 12, 2004
    Inventors: Vladimir Yliy Gershtein, Alexander Schwarz, Wayne Thomas McDermott, John Frederick Cirucci, John Christopher Ivankovits
  • Patent number: 6735977
    Abstract: An apparatus and a method for providing a magnetic holding field about a chamber for accumulating frozen 129Xe. The apparatus includes a magnetic field source and a yoke for supporting the magnetic field source about the chamber. The magnetic field source provides a magnetic holding field having a field strength of greater than 2 kiloGauss. The apparatus may further include yoke for coupling the magnetic holding field through a portion of the chamber.
    Type: Grant
    Filed: August 19, 2002
    Date of Patent: May 18, 2004
    Assignee: Medi-Physics, Inc.
    Inventors: Nicholas N. Kuzma, Ian Nelson
  • Patent number: 6651459
    Abstract: The present invention relates to a method of hyperpolarizing a gas sample. The method cryogenically forming a solidified gas structure from the sample gas, the solidified gas structure being surrounded by 3He. A magnetic field is then to the solidified gas structure and the 3He to thereby polarize the solidified gas structure, before the 3He is removed to thereby leave a solidified gas structure of hyperpolarized sample gas.
    Type: Grant
    Filed: November 25, 2002
    Date of Patent: November 25, 2003
    Assignee: Oxford Instruments Superconductivity Limited
    Inventor: Neal Frederick Kalechofsky
  • Publication number: 20030121279
    Abstract: The present invention relates to a method of hyperpolarizing a gas sample. The method cryogenically forming a solidified gas structure from the sample gas, the solidified gas structure being surrounded by 3He. A magnetic field is then to the solidified gas structure and the 3He to thereby polarize the solidified gas structure, before the 3He is removed to thereby leave a solidified gas structure of hyperpolarized sample gas.
    Type: Application
    Filed: November 25, 2002
    Publication date: July 3, 2003
    Inventor: Neal Frederick Kalechofsky
  • Publication number: 20030033830
    Abstract: An apparatus and a method for providing a magnetic holding field about a chamber for accumulating frozen 129Xe. The apparatus includes a magnetic field source and a yoke for supporting the magnetic field source about the chamber. The magnetic field source provides a magnetic holding field having a field strength of greater than 2 kiloGauss. The apparatus may further include yoke for coupling the magnetic holding field through a portion of the chamber.
    Type: Application
    Filed: August 19, 2002
    Publication date: February 20, 2003
    Inventors: Nicholas N. Kuzma, Ian Nelson
  • Patent number: 6363743
    Abstract: Method for formulating particles from solutions, wherein cooling the solution down to the initial freezing point, to mix the solution under pressure with an inert medium, to expand the solution to solid, fluidable frozen particles comprising the insert medium and the solution in a frozen shape.
    Type: Grant
    Filed: February 2, 2001
    Date of Patent: April 2, 2002
    Assignee: Leiv Eiriksson Nyfotek AS
    Inventors: Ola Jonassen, Ingvald Strommen, Per Arne Schieflo, Odilio Alves-Filho
  • Patent number: 6180843
    Abstract: An apparatus for producing gas hydrates includes a reactor vessel having a fluidized or expanded bed reaction zone. The reactor vessel has an upper portion and a lower portion, wherein a cross-sectional area of the upper portion is larger than a cross-sectional area of the lower portion. Water is introduced into the reactor vessel, and hydrate-forming gas is introduced, under an elevated pressure, into the lower portion of the reactor vessel. Preferably, the water and gas flow in a countercurrent manner through the reactor and into the fluidized or expanded bed reaction zone. The apparatus can include a mechanism for withdrawing unreacted hydrate-forming gas from the upper portion of the reactor vessel and recycling it back into the fluidized or expanded reaction bed. A defrosting device can be included with the reactor so that at least a portion of at least one wall of the reactor vessel can be defrosted.
    Type: Grant
    Filed: October 14, 1997
    Date of Patent: January 30, 2001
    Assignee: Mobil Oil Corporation
    Inventors: Robert Frederick Heinemann, David Da-Teh Huang, Jinping Long, Roland Bernard Saeger
  • Patent number: 6079222
    Abstract: The object of the invention is to provide a method for preparing deep-frozen liquid gas for the purpose of recovering process energy for a downstream process, with which the refrigerating capacity of the deep-frozen liquid gas can also be used in the downstream process. According to the invention, this is achieved by the fact that the refrigerating capacity of the deep-frozen liquid gas (1) is fed as a heat sink to at least one of the part-steps of the downstream process via at least one heat-exchange medium (28, 54, 79) and, if said heat-exchange medium (28, 54, 79) is not available, the deep-frozen liquid gas (1) is regasified with an additional heat-exchange medium (32).
    Type: Grant
    Filed: March 18, 1998
    Date of Patent: June 27, 2000
    Assignee: Asea Brown Boveri AG
    Inventors: Mircea Fetescu, Lutz Lowel
  • Patent number: 6079213
    Abstract: Methods of collecting, thawing, and extending the useful polarized life of frozen polarized gases include heating a portion of the flow path and/or directly liquefying the frozen gas during thawing. A polarized noble gas product with an extended polarized life product is also included. Associated apparatus such as an accumulator and heating jacket for collecting, storing, and transporting polarized noble gases include a secondary flow channel which provides heat to a portion of the collection path during accumulation and during thawing.
    Type: Grant
    Filed: December 12, 1997
    Date of Patent: June 27, 2000
    Assignee: Magnetic Imaging Technologies Incorporated
    Inventors: Bastiaan Driehuys, David Zollinger, Daniel Deaton, K. C. Hasson
  • Patent number: 6003332
    Abstract: A process and system for producing pellets of high density carbon dioxide or other gases utilize a chamber containing a plurality of cell-like freezing compartments within which ice is to be formed. A gas desired to be frozen into ice is introduced into the chamber while the internal pressure of the chamber is maintained at a level which is below the equilibrium triple pressure of the gas. The temperature of the freezing compartments is lowered to a temperature which is below the equilibrium vapor pressure temperature of the gas at the chamber pressure so that the gas condenses into ice within the compartments. The temperature of the freezing compartments is thereafter raised so that the ice is thereby released from and falls out of the compartments as pellets for collection.
    Type: Grant
    Filed: May 26, 1998
    Date of Patent: December 21, 1999
    Assignee: Cyrogenic Applications F, Inc.
    Inventor: Christopher A. Foster
  • Patent number: 5724831
    Abstract: For cooling food products in a container, a distributor pipe for supplying liquid carbon dioxide extends into an interior of the container and a plurality of nozzles are arranged on the distributor pipe so that liquid carbon dioxide is discharged from the nozzles in jets extending substantially parallel to a longitudinal axis of the distributor pipe and against one another to collide at the midpoint between two neighboring nozzles.
    Type: Grant
    Filed: November 24, 1995
    Date of Patent: March 10, 1998
    Inventors: Lev Reznikov, Zachary Schulman
  • Patent number: 5644923
    Abstract: A system for filtering contaminants from a gas stream through atomized ultrafreezing including: a housing having an inlet mouth and an outlet mouth; a fluid temperature regulating element disposed within the inlet mouth; a venturi-type valve having a fluid speed regulator disposed downstream of the temperature regulating element; a down pipe disposed downstream of the venturi-type valve; at least one atomized water injector at the inlet of the down pipe which is capable of spraying the contaminated gas stream exiting the venturi-type valve; at least one liquid nitrogen shower element disposed in the down pipe downstream of the water injector which is capable of freezing the water, wherein water containing the contaminant is capable of solidifying into hail and precipitating; and a decanter connected to the outlet of the down pipe having a first separator for removing the hail from the gas stream, a discharge valve at the bottom of the decanter for discharging the hail from the decanter, and a second separator
    Type: Grant
    Filed: December 18, 1995
    Date of Patent: July 8, 1997
    Inventor: Eusebio Moro-Franco