With Chemically Reactive Treatment Of Glass Preform Patents (Class 65/30.1)
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Patent number: 11554978Abstract: A method for forming an optical glass preform from a soot preform is provided. The method includes forming a soot preform, placing the soot preform in a furnace, and applying a vacuum through a centerline hole of the soot preform.Type: GrantFiled: November 18, 2014Date of Patent: January 17, 2023Assignee: Corning IncorporatedInventors: Dana Craig Bookbinder, Richard Michael Fiacco, Ming-Jun Li, Jeffery Scott Stone, Pushkar Tandon
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Patent number: 11261127Abstract: The present invention relates to a process for manufacturing glass sheets with diffuse finish and the resulting glass sheet by this process. The glass sheet is subjected to a series of alternate immersions in acidic solutions and alkaline solutions to remove impurities and waste and to generate a diffuse finish on both sides of the glass sheet. The process generates in the glass sheet in at least one side, a diffuse surface with a peak to valley roughness (Rt) of between 5.8343 ?m and 9.3790 ?m; an average roughness (Ra) value between 0.8020 ?m and 0.9538 ?m; an RMS roughness between 0.9653 ?m and 1.1917 ?m; a solar transmission between 84.8% and 46.50%; a solar reflection between 7.4 and 4.4%; a light transmission between 88.5% and 67.70%; a reflection of light between 6.50% and 5.20%; and UV transmission between 35.60% and 70.20%.Type: GrantFiled: June 11, 2019Date of Patent: March 1, 2022Assignee: Vidrio Plano de México, S.A. de C.V.Inventors: Jose Luis Tavares Cortes, Arturo Si Ming Lamshing Tai, Gerardo Soto Puente, Jorge Sanchez-Gonzalez
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Patent number: 11204280Abstract: A method for determining crystal phases of a glass ceramic sample, including the steps of applying energy to the sample using an excitation source, detecting raw Raman spectral energy that is given off by the sample using a detector, wherein the raw Raman spectral energy includes peak values, determining a plurality of predetermined energy peaks based off a composition of the sample, superimposing the plurality of predetermined energy peaks over the raw Raman spectral energy, applying a baseline value between each predetermined energy peak, subtracting the baseline value from the raw Raman spectral energy, calculating corrected peak values based on the raw Raman spectral energy and baseline value, and determining the crystal phases of the glass ceramic sample based on the corrected peak values.Type: GrantFiled: February 28, 2020Date of Patent: December 21, 2021Assignee: CORNING INCORPORATEDInventors: Chong Pyung An, Ryan Claude Andrews, Galan Gregory Moore, Rohit Rai, Erika Lynn Stapleton, Ljerka Ukrainczyk
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Patent number: 11008246Abstract: Laminated articles comprised of glass core and clad layers, more specifically, to compressively stressed laminated articles comprising a glass core sandwiched between first and second clad layers, the clad layers being formed from photosensitive glass.Type: GrantFiled: December 20, 2018Date of Patent: May 18, 2021Assignee: Corning IncorporatedInventors: Heather Debra Boek, Nicholas Francis Borrelli
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Patent number: 10766810Abstract: Components of an electronic device, such as glass articles, are susceptible to breakage, especially in regions where machining a glass article has created flaws. Chemical strengthening can be performed to create deeper compression layers at regions of a glass article that have been machined, include and/or are adjacent to an edge feature, have greater surface roughness, and/or have more or deeper cracks.Type: GrantFiled: February 6, 2018Date of Patent: September 8, 2020Assignee: Apple Inc.Inventors: Victor Luzzato, Tyler A. Marshall, Christopher C. Bartlow, Dale N. Memering
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Patent number: 10759692Abstract: The glasses of the present disclosure are highly transparent and have very good resistance to solarization. The resistance to solarization arises from the production method. The concentrations of reduced polyvalent ion species are reduced by targeted use of bubbling with an oxidizing gas. Methods for producing glasses and to the uses thereof, particularly as core glasses in optical waveguides, are also provided.Type: GrantFiled: December 27, 2018Date of Patent: September 1, 2020Assignee: Schott AGInventors: Simone Ritter, Uwe Kolberg, Stefanie Hansen, Thomas Weingaertner, Caroline de Luca, Thomas Kirsch, Peter-Franz Skiba
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Patent number: 10722280Abstract: The present disclosure provides a bone-implantable device and methods of use. The bone-implantable device comprises a body having an exterior surface, wherein a portion of the exterior surface includes a cured osteostimulative material comprising MgO.Type: GrantFiled: March 29, 2018Date of Patent: July 28, 2020Assignee: Bone Solutions, Inc.Inventors: Frankie L. Morris, Drew Diaz
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Patent number: 10689287Abstract: A method for preparing a doped optical fibre preform includes formulating, a rare earth material or a functional metal material and a co-doping agent into a doping solution, mixing a high-purity quartz powder with the doping solution, drying same at a temperature of 100° C.-150° C. for 12-48 hours, crushing and screening the same to obtain a doped quartz powder; depositing the doped quartz powder onto the surface of a target rod to form a doped core layer; replacing the doped quartz powder with the high-purity quartz powder, and depositing the high-purity quartz powder onto the surface of the doped core layer to form a quartz outer cladding; and removing the target rod, and gradually collapsing the entirety formed from the doped core layer and the quartz outer cladding at a high temperature to obtain the doped optical fibre preform.Type: GrantFiled: October 21, 2016Date of Patent: June 23, 2020Assignee: FIBERHOME TELECOMMUNICATION TECHNOLOGIES CO., LTDInventors: Cheng Du, Wenyong Luo, Lei Yan, Tao Zhang, Chao Chen, Yili Ke, Ming Kong, Jie Zhang, Zhijian Liu, Lifeng Liu
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Patent number: 10676388Abstract: One aspect relates to a light guide comprising a jacket and one or more cores, wherein the jacket surrounds the cores. Each core has a refractive index profile perpendicular to the maximum extension of the core, wherein at least one refractive index nK of each refractive index profile is greater than the refractive index nM1 of the jacket. The jacket is made of silicon dioxide and has an OH content of less than 10 ppm, a chlorine content of less than 60 ppm, and an aluminium content of less than 200 ppb. One aspect also relates to a silicon dioxide granulate I, characterized by a chlorine content of less than 200 ppm and an aluminium content of less than 200 ppb, in each case based on the total weight of the silicon dioxide granulate I.Type: GrantFiled: December 16, 2016Date of Patent: June 9, 2020Assignee: Heraeus Quarzglas GmbH & Co. KGInventors: Michael Hünermann, Achim Hofmann, Heinz Fabian, Matthias Otter, Thomas Kayser
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Patent number: 10607647Abstract: A magnetic disk substrate having a flat main surface, an end face, and a chamfered face formed between the main surface and the end face. The substrate has an offset portion, present on the main surface within a range of 92.0 to 97.0% in a radial direction from a center of the substrate. A distance from the center of the substrate to the end face of the substrate in a radial direction is 100%, the offset portion being raised or lowered with respect to a virtual straight line connecting two points on the main surface, set at positions of 92.0% and 97.0%. A maximum distance from the virtual straight line to the offset portion in a direction perpendicular to the virtual straight line is a “maximum offset value.Type: GrantFiled: June 1, 2017Date of Patent: March 31, 2020Assignees: HOYA CORPORATION, HOYA LAMPHUN LTD.Inventors: Toshio Takizawa, Kraisorn Phandon, Kenichi Nishimori
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Patent number: 10293081Abstract: The present invention relates to a crystallized glass ceramic comprising 30 wt % to 40 wt % of each of CaSiO3, Ca10(PO4)6(OH)2, and Ca2Mg(Si2O7); a crystallized glass ceramic composition comprising CaSiO3, Ca10(PO4)6(OH)2, and Ca2Mg(Si2O7) in a predetermined weight ratio; a bone graft material comprising the glass ceramic; and an intervertebral spacer or medical device for replacement of bone tissue, which is manufactured using the bone graft material.Type: GrantFiled: May 27, 2015Date of Patent: May 21, 2019Assignee: BIOALPHA CORPORATIONInventors: Mi Young Ryu, Sung Nam Park, Jun Hyuk Seo, Hyun Seung Ryu
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Patent number: 10280112Abstract: An article comprising an ion-exchanged glass material that prevents sharp contact flaws from entering a central region of the material that is under central tension and thus causing failure of the material. The glass material may be a glass or glass ceramic having a surface layer under compression. In some embodiments, the depth of the compressive layer is greater than about 75 ?m. The greater depth of layer prevents flaws from penetrating the compressive layer to the region under tension.Type: GrantFiled: August 14, 2012Date of Patent: May 7, 2019Assignee: CORNING INCORPORATEDInventor: Timothy Michael Gross
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Patent number: 9828286Abstract: A method for producing a chemically strengthened glass, including a step of bringing a glass containing sodium into contact with an inorganic salt containing potassium nitrate, thereby performing ion exchange of a Na ion in the glass with a K ion in the inorganic salt, in which the inorganic salt contains at least one salt selected from the group consisting of K2CO3, Na2CO3, KHCO3, NaHCO3, K3PO4, Na3PO4, K2SO4, Na2SO4, KOH and NaOH, and the method includes: a step of washing the glass after the ion exchange; a step of subjecting the glass to an acid treatment after the washing; and a step of subjecting the glass to an alkali treatment after the acid treatment.Type: GrantFiled: January 19, 2016Date of Patent: November 28, 2017Assignee: ASAHI GLASS COMPANY, LIMITEDInventors: Izuru Kashima, Yusuke Fujiwara, Kiyoshi Tamai, Yuichi Suzuki, Daisuke Kobayashi, Yoichi Sera, Taku Yamada
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Patent number: 9533913Abstract: A method of making colored glass in a float glass process includes the steps of: melting glass batch materials in a furnace to form a glass melt; transporting the glass melt into a float glass chamber having a flame spray device, the glass melt forming a float glass ribbon; supplying at least one coating material to the flame spray device to form a spray having coating particles; and directing the spray onto the float glass ribbon to diffuse the particles into the surface of the float glass ribbon to form a glass sheet of a desired color.Type: GrantFiled: December 30, 2009Date of Patent: January 3, 2017Assignee: Vitro, S.A.B. de C.V.Inventors: Mehran Arbab, Songwei Lu
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Patent number: 9409812Abstract: [Problem] The provision of a synthetic quartz glass heat treatment method that can, by a single heat treatment, and without particular limitations on the OH group concentration distribution of the starting material, regulate the birefringence fast axis direction in the synthetic quartz glass after it has been heat-treated. [Means of overcoming the problem] A heat treatment method for synthetic quartz glass whereby columnar synthetic quartz glass having two opposing end faces and a lateral face is heat-treated covered with thermal insulator; wherein said heat treatment is performed using as end face thermal insulator which covers said two end faces, and as lateral face thermal insulator which covers said lateral face, thermal insulators that differ in at least either type or thickness to afford different thermal insulation effects such that the birefringence fast axis direction of said synthetic quartz glass is regulated.Type: GrantFiled: July 18, 2013Date of Patent: August 9, 2016Assignees: Heraeus Quarzglas GmbH & Co. KG, Shin-Etsu Quartz Products Co., Ltd.Inventor: Shigeo Harada
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Patent number: 9321678Abstract: A glass element having a thickness from 25 ?m to 125 ?m, a first primary surface, a second primary surface, and a compressive stress region extending from the first primary surface to a first depth, the region defined by a compressive stress ?I of at least about 100 MPa at the first primary surface. Further, the glass element has a stress profile such that it does not fail when it is subject to 200,000 cycles of bending to a target bend radius of from 1 mm to 20 mm, by the parallel plate method. Still further, the glass element has a puncture resistance of greater than about 1.5 kgf when the first primary surface of the glass element is loaded with a tungsten carbide ball having a diameter of 1.5 mm.Type: GrantFiled: January 22, 2015Date of Patent: April 26, 2016Assignee: Corning IncorporatedInventors: Theresa Chang, Polly Wanda Chu, Adam James Ellison, Timothy Michael Gross, Guangli Hu, Nicholas James Smith
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Patent number: 9321677Abstract: A glass element having a thickness from 25 ?m to 125 ?m, a first primary surface, a second primary surface, and a compressive stress region extending from the first primary surface to a first depth, the region defined by a compressive stress ?I of at least about 100 MPa at the first primary surface. Further, the glass element has a stress profile such that when the glass element is bent to a target bend radius of from 1 mm to 20 mm, with the center of curvature on the side of the second primary surface so as to induce a bending stress ?B at the first primary surface, ?I+?B<0. Still further, the glass element has a puncture resistance of ?1.5 kgf when the first primary surface of the glass element is loaded with a tungsten carbide ball having a diameter of 1.5 mm.Type: GrantFiled: January 21, 2015Date of Patent: April 26, 2016Assignee: Corning IncorporatedInventors: Theresa Chang, Polly Wanda Chu, Michael Patrick Donovan, Adam James Ellison, Timothy Michael Gross, Guangli Hu, Gautam Narendra Kudva, Nicholas James Smith
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Patent number: 9321679Abstract: A glass element having a thickness from 25 ?m to 125 ?m, a first primary surface, a second primary surface, and a compressive stress region extending from the first primary surface to a first depth, the region defined by a compressive stress ?I of at least about 100 MPa at the first primary surface. Further, the glass element has a stress profile such that it does not fail when it is held at a bend radius from about 1 mm to about 20 mm for at least 60 minutes at about 25° C. and about 50% relative humidity. Still further, the glass element has a puncture resistance of greater than about 1.5 kgf when the first primary surface of the glass element is loaded with a tungsten carbide ball having a diameter of 1.5 mm.Type: GrantFiled: January 22, 2015Date of Patent: April 26, 2016Assignee: Corning IncorporatedInventors: Theresa Chang, Polly Wanda Chu, Adam James Ellison, Timothy Michael Gross, Guangli Hu, Nicholas James Smith
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Patent number: 9133412Abstract: The present application is directed to methods and devices for altering material properties of lubricants and other cross-linkable compounds comprising organic or organometallic materials through exposure to energized gaseous species. The energized gaseous species may create reactive sites among lubricant molecules that may alter their material properties by cross-linking at least a portion of the lubricant molecules. The cross-linked lubricant may reduce the ability of the lubricant to migrate away when force is applied between lubricated sliding friction surfaces.Type: GrantFiled: March 15, 2013Date of Patent: September 15, 2015Assignee: TriboFilm Research, Inc.Inventors: Jackson Thornton, Vinay G. Sakhrani, Charles Tomasino, Robert A. Mineo
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Patent number: 9073102Abstract: A method for cleansing a mold of the present invention suppresses generation of damage is a method for cleansing a nanoimprinting mold, in which a mesa type mold is immersed in cleansing fluid and ultrasonic cleansing is performed in a state in which a mold release layer containing a fluorine compound is provided on a patterned region of the mesa type mold.Type: GrantFiled: July 1, 2013Date of Patent: July 7, 2015Assignee: FUJIFILM CorporationInventor: Masafumi Yoshida
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Patent number: 9061933Abstract: Provided is a method of producing a tempered glass sheet, comprising applying tempering treatment to a glass sheet by increasing the content of SiO2 in terms of mass in a surface region of a glass sheet through application of thermal treatment to the glass sheet to 1.03 or more times that in an interior region positioned at a depth of 1 ?m from a surface of the glass sheet.Type: GrantFiled: August 21, 2012Date of Patent: June 23, 2015Assignee: NIPPON ELECTRIC GLASS CO., LTD.Inventors: Hiroshi Komori, Masahiro Tomamoto, Yoshinari Kato
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Publication number: 20150135772Abstract: An apparatus and method are provided for sintering a hollow cylindrical body of porous synthetic silica. The apparatus comprises a hollow mandrel for supporting the body in a horizontal position, and the mandrel is housed within a vacuum furnace having heating elements arranged to surround the body circumferentially along its entire length. The method includes supporting the body on a hollow horizontally-oriented mandrel in a vacuum furnace in which heating elements are disposed surrounding the body, and heating the body by means of the elements to a sintering temperature.Type: ApplicationFiled: November 11, 2014Publication date: May 21, 2015Inventors: Alan Mundy, Ian George Sayce, Richard Benjamin Coapes
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Patent number: 9016090Abstract: A method for manufacturing a plurality of glass microspheres comprises: melting a batch into a first glass melt in a melter system, processing the first glass melt into a second glass, pulverizing the second glass into a plurality of glass fragments, thermally processing the plurality of glass fragments into a plurality of glass microspheres, providing at least one of a plurality of redox reactions and a plurality of events in at least one of the first glass melt and a melt of the second glass, and the plurality of redox reactions and the plurality of events are induced by a plurality of redox active group (RAG) components.Type: GrantFiled: June 12, 2013Date of Patent: April 28, 2015Inventors: Hamid Hojaji, Laura Gabriela Kocs
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Patent number: 9016092Abstract: A glass for a magnetic recording medium substrate permitting the realization of a magnetic recording medium substrate affording good chemical durability and having an extremely flat surface, a magnetic recording medium substrate comprised of this glass, a magnetic recording medium equipped with this substrate, and methods of manufacturing the same. The glass is an oxide glass not including As or F.Type: GrantFiled: March 18, 2009Date of Patent: April 28, 2015Assignee: Hoya CorporationInventors: Yoichi Hachitani, Kinobu Osakabe
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Patent number: 8978414Abstract: Disclosed herein are methods for strengthening glass articles having strength-limiting surface flaws, together with strengthened glass articles produced by such methods, and electronic devices incorporating the strengthened glass articles. The methods generally involve contacting the glass articles with a substantially fluoride-free aqueous acidic treating medium for a time at least sufficient to increase the rupture failure points of the glass articles.Type: GrantFiled: November 9, 2012Date of Patent: March 17, 2015Assignee: Corning IncorporatedInventors: Dana Craig Bookbinder, Richard Michael Fiacco, Timothy Michael Gross
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Patent number: 8950215Abstract: Apparatus, systems and methods for reducing surface roughness on surface of a glass member using a non-contact polishing process are disclosed. According to one aspect, a method for processing a glass member suitable for use in a handheld electronic device includes obtaining the glass member and chemically strengthening the glass member. The glass member has at least one surface, and chemically strengthening the glass member increases roughness associated with the at least one surface. The method also includes applying a first non-contact polishing process to the glass member after chemically strengthening the glass member. Applying the first non-contact polishing process reduces the roughness associated with the at least one surface.Type: GrantFiled: May 14, 2011Date of Patent: February 10, 2015Assignee: Apple Inc.Inventors: Benjamin M. Rappoport, Christopher Prest
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Patent number: 8938990Abstract: For an information storage medium a glass substrate is produced in a method including the steps of: polishing a glass substrate with a polishing agent applied thereon; and subsequently, chemically strengthening a major surface of the glass substrate. The polishing agent contains cerium oxide at a purity equal to or larger than 99% by mass for CeO2/TREO, and has an alkaline earth metal content having a total mass equal to or smaller than 10 ppm by mass. The step of polishing is performed with a soft polishing pad to polish the glass substrate.Type: GrantFiled: September 13, 2011Date of Patent: January 27, 2015Assignee: Hoya CorporationInventors: Hazuki Nakae, Toshiharu Mori
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Publication number: 20150013388Abstract: Vacuum ultraviolet light with a wavelength of 200 nm or less is applied on the joining surfaces of first and second workpieces made from a crystal substrate and a glass substrate, or a glass substrate and a glass substrate from a light irradiation unit. The workpieces are conveyed to a workpiece cleaning and laminating mechanism by a conveyance mechanism, the joining surfaces are subjected to mega-sonic cleaning as needed, and the workpieces are aligned with the joining surfaces thereof facing each other, and laminated such that the joining surfaces are in contact with each other. After being laminated, the laminated workpieces are conveyed to a workpiece heating mechanism and heated to increase the workpiece temperature to a predetermined temperature, and this temperature is maintained until joining is completed. The laminated workpieces are brought into a thermally expanded state upon heating, and are joined in this state.Type: ApplicationFiled: February 15, 2013Publication date: January 15, 2015Applicant: USHIO DENKI KABUSHIKI KAISHAInventors: Akira Kato, Kinichi Morita, Shinji Suzuki
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Publication number: 20140305929Abstract: A volume-colored monolithic glass ceramic cooking plate is provided. The plate includes a first zone in which the coloration of the glass ceramic differs from that of a second, adjacent zone, so that an absorption coefficient of the first zone is lower than the absorption coefficient of the second, adjacent zone and so that integral light transmission in the visible spectral range is greater in the first zone than the integral light transmission of the second, adjacent zone. The light scattering in the glass ceramic of the first zone differs from light scattering in the glass ceramic of the second zone by not more than 20 percentage points, preferably by not more than 5 percentage points.Type: ApplicationFiled: April 15, 2014Publication date: October 16, 2014Applicant: SCHOTT AGInventors: Evelin Weiss, Bernd Hoppe, Martin Spier, Daniela Seiler
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Patent number: 8821747Abstract: A method for manufacturing a glass substrate for a magnetic disk comprises a surface grinding step of processing a mirror-surface plate glass, having a main surface in the form of a mirror surface, to a required flatness and surface roughness using fixed abrasive particles. The method comprises, before the surface grinding step using the fixed abrasive particles, a surface roughening step of roughening the surface of the mirror-surface plate glass by frosting.Type: GrantFiled: October 5, 2009Date of Patent: September 2, 2014Assignee: Hoya CorporationInventors: Takanori Mizuno, Yosuke Suzuki
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Patent number: 8771532Abstract: A glass article having an anti-glare surface. The anti-glare surface has a distinctness-of-reflected image of less than 95, and a haze of less than or equal to 50%. In one embodiment, the glass article further includes a smudge-resistant surface disposed on the anti-glare surface. Methods of making the glass article and anti-glare surface are also described.Type: GrantFiled: March 24, 2010Date of Patent: July 8, 2014Assignee: Corning IncorporatedInventors: Krista L Carlson, Shandon D Hart, Kelvin Nguyen, Robert Sabia, Daniel A Sternquist, Lu Zhang
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Patent number: 8735308Abstract: The present invention relates to an optical member including a TiO2-containing silica glass having: a TiO2 concentration of from 3 to 10% by mass; a Ti3+ concentration of 100 wt ppm or less; a thermal expansion coefficient at from 0 to 100° C., CTE0-100, of 0±150 ppb/° C.; and an internal transmittance in the wavelength range of 400 to 700 nm per a thickness of 1 mm, T400-700, of 80% or more, in which the optical member has a ratio of variation of Ti3+ concentration to an average value of the Ti3+ concentration, ?Ti3+/Ti3+, on an optical use surface, is 0.2 or less.Type: GrantFiled: March 5, 2010Date of Patent: May 27, 2014Assignee: Asahi Glass Company, LimitedInventors: Akio Koike, Chikaya Tamitsuji, Kunio Watanabe, Tomonori Ogawa
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Patent number: 8728638Abstract: Provided are a magnetic disk substrate that can be adapted to a reduction in flying height of a head in an HDD and to an increase in rotational speed therein, and a method of manufacturing such a substrate. In an annular glass substrate for a magnetic recording medium, a main surface (12) of the glass substrate is uniformly inclined from an inner peripheral end (13) to an outer peripheral end (14) and has an isotropic shape with respect to an axis passing through the center of the glass substrate. That is, it is rotationally symmetric with respect to an arbitrary angle rotation about the axis passing through the center of the glass substrate.Type: GrantFiled: June 29, 2009Date of Patent: May 20, 2014Assignee: Hoya CorporationInventors: Hideki Isono, Hiroshi Tsuchiya
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Patent number: 8722138Abstract: In a method of manufacturing a glass substrate for an information recording medium including a step for chemically strengthening the glass substrate by contacting the glass substrate with chemical strengthening processing liquid containing chemical strengthening salt, concentration of Fe and Cr is 500 ppb or less in said chemical strengthening salt, respectively. The concentration may be detected by the use of an ICP (Inductively Coupled Plasma) emission spectrometry analyzing method or a fluorescent X-ray spectroscopy analyzing method.Type: GrantFiled: March 18, 2013Date of Patent: May 13, 2014Assignee: Hoya CorporationInventors: Hiroaki Ikeda, Masaru Suzuki, Kazuna Sasaki, Yumi Mukai, Jun Ozawa
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Publication number: 20140120278Abstract: Latent colorant material compositions, soda-lime-silica glass compositions, and related methods of manufacturing color-strikable glass containers. The latent colorant material compositions may be introduced into a plurality of base glass compositions having redox numbers in the range of ?40 to +20 to produce color-strikable glass compositions and color-strikable glass containers. The latent colorant material compositions introduced into the base glass compositions include a mixture of cuprous oxide (Cu2O), stannous oxide (SnO), bismuth oxide (Bi2O3), and carbon (C). After formation, the color-strikable glass containers may be heat-treated to strike red or black therein.Type: ApplicationFiled: November 1, 2012Publication date: May 1, 2014Applicant: Owens-Brockway Glass Container Inc.Inventor: Owens-Brockway Glass Container Inc.
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Publication number: 20140117240Abstract: A soda-lime-silica glass container and related methods of manufacturing. A black-strikable glass composition having a base glass portion and a latent colorant portion is prepared. The base glass portion includes soda-lime-silica glass materials and one or more blue colorant materials, and the latent colorant portion includes cuprous oxide (Cu2O), stannous oxide (SnO), bismuth oxide (Bi2O3), and carbon (C). Glass containers may be formed from the black-strikable glass composition, and these glass containers may be heated to a temperature greater than 600 degrees Celsius to strike black therein. The glass containers formed from the black-strikable glass composition may be inspected—before or after striking—by infrared inspection equipment.Type: ApplicationFiled: November 1, 2012Publication date: May 1, 2014Applicant: Owens-Brockway Glass Container Inc.Inventor: Owens-Brockway Glass Container Inc.
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Patent number: 8677782Abstract: This invention relates to a method of making glass. In certain example embodiments, a major surface(s) of the glass is treated with aluminum chloride (e.g., AlCl3) at or just prior to the annealing lehr. The aluminum chloride treatment at or just prior to the annealing lehr, in either a float or patterned line glass making process, is advantageous in that it allows the treatment to be performed at a desirable glass temperature and permits exhaust functions in or proximate the annealing lehr to remove byproducts of the treatment in an efficient manner. In certain example embodiments, the glass may be polished for thinning after the treatment, with the polishing being performed on a major surface of the glass opposite to a major surface which has been treated with aluminum chloride.Type: GrantFiled: July 23, 2007Date of Patent: March 25, 2014Assignees: Guardian Industries Corp., Centre Luxembourg de Recherches pour le Verre er la Ceramique S.A. (C.R.V.C.)Inventors: Bernd Disteldorf, Willem den Boer
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Publication number: 20140072811Abstract: Provided in a facile manner are a black synthetic quartz glass with a transparent layer, which meets demands for various shapes, has a black portion satisfying required light shield property and emissivity in an infrared region, keeps a purity equivalent to that of a synthetic quartz glass in terms of metal impurities, has a high-temperature viscosity characteristic comparable to that of a natural quartz glass, can be subjected to high-temperature processing such as welding, does not release carbon from its surface, and is free of bubbles and foreign matter in the transparent layer and the black quartz glass, and at an interface between the transparent layer and the black quartz glass, and a production method therefor.Type: ApplicationFiled: September 13, 2012Publication date: March 13, 2014Inventors: Hiroyuki WATANABE, Takayuki Imaizumi, Tatsuhiro Sato
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Patent number: 8656735Abstract: To provide a novel fluorination treatment method whereby the surface of oxide glass can be treated for fluorination at low cost and with excellent adhesiveness. A method for treating the surface of oxide glass, which comprises contacting the surface of oxide glass with a gas of a fluorinating agent or a mixed gas having a fluorinating agent diluted with an inert gas, wherein the fluorinating agent is an elemental fluorine, or a fluorine compound capable of cleaving a bond between an oxygen atom and a metal atom in the framework of the oxide glass and forming a bond between a fluorine atom and the metal atom; and the concentration of hydrogen fluoride at the surface of oxide glass with which the fluorinating agent is in contact, is controlled to be at most 1 mol %.Type: GrantFiled: December 17, 2009Date of Patent: February 25, 2014Assignee: Asahi Glass Company, LimitedInventors: Chikaya Tamitsuji, Kunio Watanabe
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Publication number: 20140000315Abstract: A process is provided for obtaining a glassy material that is optically transparent to infrared radiation. The process includes: a step of amorphization, by mechanosynthesis, of an assembly of starting elements including at least one metallic element and at least one chalcogenide element, making it possible to form an amorphous powder; a step of hot densification, in a mould of predetermined dimensions, of the amorphous powder, making it possible to obtain a glass; and heat treatment, carried out during or after the hot densification step, in which the glass is heated to a temperature at which a portion of the glass is converted from an amorphous state to a crystalline state, making it possible to obtain, after cooling, a glass-ceramic.Type: ApplicationFiled: December 6, 2011Publication date: January 2, 2014Applicants: UNIVERSITE DE RENNES 1, CNRSInventors: Laurent Calvez, Xiang Hua Zhang, Mathieu Hubert, Gaëlle Delaizir
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Patent number: 8613206Abstract: This invention provides a method for manufacturing a glass substrate for a magnetic disk comprising a chemical strengthening step. The method provides a glass substrate for a magnetic disk that can suppress the occurrence of very small waves in cooling a glass substrate after the chemical strengthening step, and, while preventing troubles such as head crush and thermal asperity, can realize lowered flying height of a magnetic head and high-density information recording, and is particularly suitable for application to small-size magnetic disks for portable information equipment. In the step of cooling after the chemical strengthening step, cooling treatment is carried out in which the glass substrate is brought into contact with a treatment liquid containing a melt of a material having a solidification temperature below that of a chemical strengthening salt.Type: GrantFiled: March 15, 2007Date of Patent: December 24, 2013Assignee: Hoya CorporationInventor: Katsuyuki Iwata
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Publication number: 20130299378Abstract: A glass container and related methods of manufacturing a glass container. A solution having a composition including a silane, a solvent, a catalyst, and water, is applied to an exterior glass surface of the glass container, at a temperature between 40 and 60 degrees Celsius, such that the solution at least partially fills the surface imperfections. The glass container is heated at a temperature greater than 500 degrees Celsius to produce Si—O—Si bonds with the exterior glass surface of the glass container to result in a coating having between 10% and 20% silicate-based material by weight.Type: ApplicationFiled: May 9, 2012Publication date: November 14, 2013Inventors: Pramod K. Sharma, Carol A. Click
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Publication number: 20130280449Abstract: An industrial decoration method in which a colored pattern (11) is made in the bulk of an article (1) made of transparent glass of composition including at least one metallic oxide of silver, of gold, or of copper, said method including the following successive steps: a step of laser irradiating the zone of said glass article that is to be colored; and a final step of annealing the irradiated glass; and being characterized in that a glass composition is used that includes cerium and that has a total content of antimony plus tin that is less than 100 ppm, and in that the step of laser irradiating the zone that is to be colored is performed with laser irradiation having a pulse duration that is less than or equal to 10?11 s, while delivering power to the glass at greater than 1012 W/cm2, and more preferably lying in the range 1012 W/cm2 to 5×1014 W/cm2 for decorating and marking glass articles.Type: ApplicationFiled: April 22, 2013Publication date: October 24, 2013Applicant: SGD S.A.Inventors: Yannick Samuel RIEZMAN, Joel BOURJOT
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Patent number: 8545733Abstract: Disclosed is a process for the manufacture of glass-crystalline particles comprising a glass component and a crystalline component comprising the steps of: a) providing a precursor solution comprising a solvent, a glass component composition, and a crystalline component composition; b) forming an aerosol comprising finely divided droplets of the precursor solution, wherein the droplet concentration which is below the concentration where collisions and subsequent coalescence of the droplets results in a 10% reduction in droplet concentration; c) heating the aerosol wherein, upon heating, glass-crystalline particles are formed, wherein the glass-crystalline particles comprise a glass component and a crystalline component, and wherein the crystalline component comprises one or more metal oxides; and d) isolating the glass-crystalline particles.Type: GrantFiled: September 27, 2010Date of Patent: October 1, 2013Assignee: E I du Pont de Nemours and CompanyInventors: Eric Lee Brantley, John T. Chaplinsky, Howard David Glicksman, James J. Krajewski, Brian J. Laughlin, Kurt Richard Mikeska, Lawrence V. Triboletti
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Publication number: 20130209731Abstract: Methods and apparatuses for producing a multiplicity of holes in thin workpieces made of glass or glass-like materials and semiconductors are provided. The method includes directing multiple laser beams onto predetermined perforation points of the workpiece in a wavelength range between 1600 and 200 nm and with a radiation intensity that causes local non-thermal destruction of the workpiece material along respective filamentary channels. Subsequently, the filamentary channels are widened to the desired diameter of the holes.Type: ApplicationFiled: July 4, 2011Publication date: August 15, 2013Applicant: SCHOTT AGInventors: Kurt Nattermann, Ulrich Peuchert, Wolfgang Moehl, Stephan Behle
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Publication number: 20130209781Abstract: Methods of fabricating dimensional silica-based substrates or structures comprising a porous silicon layers are contemplated. According to one embodiment, oxygen is extracted from the atomic elemental composition of a silica glass substrate by reacting a metallic gas with the substrate in a heated inert atmosphere to form a metal-oxygen complex along a surface of the substrate. The metal-oxygen complex is removed from the surface of the silica glass substrate to yield a crystalline porous silicon surface portion and one or more additional layers are formed over the crystalline porous silicon surface portion of the silica glass substrate to yield a dimensional silica-based substrate or structure comprising the porous silicon layer. Embodiments are also contemplated where the substrate is glass-based, but is not necessarily a silica-based glass substrate. Additional embodiments are disclosed and claimed.Type: ApplicationFiled: March 20, 2013Publication date: August 15, 2013Inventors: Robert Alan Bellman, Nicholas Francis Borrelli, David Alan Deneka, Shawn Michael O'Malley, Vitor Marino Schneider
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Publication number: 20130192304Abstract: An aspect of the invention is directed to a method for manufacturing a glass substrate for an information recording medium including: a polishing step of polishing a surface of a raw glass plate, with use of a polishing solution containing a polishing agent and water; and a chemically reinforcing step of reinforcing the polished surface of the raw glass plate which has undergone the polishing step, with use of a chemically reinforcing treatment solution. The polishing step is a step of using, as the polishing agent, a polishing agent containing CeO2, and of performing polishing in such a manner that the effective amount of CeO2 per unit area of the surface of the raw glass plate to be used in the polishing is in the range of from 0.05 to 0.5 ?g/cm2.Type: ApplicationFiled: August 23, 2011Publication date: August 1, 2013Inventors: Hazuki Nakae, Kazuyuki Nishi, Toshiharu Mori, Takeshi Endo, Hiroaki Sawada
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Publication number: 20130188366Abstract: An electronic device may have a glass housing structures. The glass housing structures may be used to cover a display and other internal electronic device components. The glass housing structure may have multiple glass pieces that are joined using a glass fusing process. A peripheral glass member may be fused along the edge of a planar glass member to enhance the thickness of the edge. A rounded edge feature may be formed by machining the thickened edge. Raised fused glass features may surround openings in the planar glass member. Multiple planar glass members may be fused together to form a five-sided box in which electronic components may be mounted. Raised support structure ribs may be formed by fusing glass structures to a planar glass member. Opaque masking material and colored glass may be used to create portions of the glass housing structures that hide internal device components from view.Type: ApplicationFiled: January 25, 2012Publication date: July 25, 2013Inventors: Peter Russell-Clarke, Michael K. Pilliod, Jonathan P. Ive
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Publication number: 20130186141Abstract: A method of decorating chemically strengthened glass. The coating deposition process entails maintaining a deposition temperature and a curing temperature below a threshold where the chemically strengthened glass is weakened. The coating composition used in the process is a single phase and comprises alkoxysilane functionalized isocyanurate or alkoxysilane functionalized biuret, wherein the alkoxysilane is linked to the isocyanurate or biuret by an urea linking group.Type: ApplicationFiled: January 14, 2013Publication date: July 25, 2013Inventor: David Henry
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Publication number: 20130189546Abstract: For an information storage medium a glass substrate is produced in a method including the steps of: polishing a glass substrate with a polishing agent applied thereon; and subsequently, chemically strengthening a major surface of the glass substrate. The polishing agent contains cerium oxide at a purity equal to or larger than 99% by mass for CeO2/TREO, and has an alkaline earth metal content having a total mass equal to or smaller than 10 ppm by mass. The step of polishing is performed with a soft polishing pad to polish the glass substrate.Type: ApplicationFiled: September 13, 2011Publication date: July 25, 2013Applicant: Konica Minolta Advanced Layers, Inc.Inventors: Hazuki Nakae, Toshiharu Mori