To Hydrate The Glass Patents (Class 65/30.12)
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Patent number: 11548806Abstract: A glass body manufacturing apparatus includes: a first heating furnace including a furnace core tube accommodating the soot and a first heater, to supply a dehydration gas into the furnace core tube and heat the soot at a first treatment temperature lower than a softening point of the porous portion by the first heater; a second heating furnace including a structural body accommodating the soot and a second heater, to heat the soot at a second treatment temperature equal to or higher than the softening point by the second heater; and a conveyance container, connectable to each of the first and second heating furnaces while keeping airtightness with respect to the atmosphere, to accommodate and hold the soot, and convey the soot between the first and second heating furnaces.Type: GrantFiled: May 27, 2020Date of Patent: January 10, 2023Assignee: FURUKAWA ELECTRIC CO., LTD.Inventors: Koichi Toyosaki, Hiroshi Miyake, Tsuneo Suzuki
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Patent number: 11505492Abstract: Glass-based articles that include a compressive stress layer extending from a surface of the glass-based article to a depth of compression are formed by exposing glass-based substrates to water vapor containing environments. The glass-based substrates have compositions selected to avoid the formation of haze during the treatment process. The methods of forming the glass-based articles may include elevated pressures and/or multiple exposures to water vapor containing environments selected to avoid the formation of haze during the treatment process.Type: GrantFiled: May 2, 2022Date of Patent: November 22, 2022Assignee: Corning IncorporatedInventors: Timothy Michael Gross, Jingshi Wu
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Patent number: 11370696Abstract: Glass-based articles that include a compressive stress layer extending from a surface of the glass-based article to a depth of compression are formed by exposing glass-based substrates to water vapor containing environments. The glass-based substrates have compositions selected to avoid the formation of haze during the treatment process. The methods of forming the glass-based articles may include elevated pressures and/or multiple exposures to water vapor containing environments selected to avoid the formation of haze during the treatment process.Type: GrantFiled: May 12, 2020Date of Patent: June 28, 2022Assignee: Corning IncorporatedInventors: Timothy Michael Gross, Jingshi Wu
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Patent number: 11023630Abstract: A method of making a glass article includes melting batch materials to produce molten glass, heating or cooling the molten glass to a temperature, forming a glass article from the molten glass. The batch materials include a plurality of viscosity-affecting components that become at least part of the glass article. Selection of the batch materials or the temperature was made at least in part using computer-implemented modeling where predicted equilibrium viscosity of the glass at the temperature is a function comprising concentrations of viscosity-affecting components and temperature-independent fitting coefficients for the viscosity-affecting components.Type: GrantFiled: November 5, 2020Date of Patent: June 1, 2021Assignee: Corning IncorporatedInventors: Douglas Clippinger Allan, Adam James Ellison, John Christopher Mauro
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Patent number: 8887528Abstract: An object of the present invention is to provide a surface-treated glass plate having a concave portion on the order of nanometers, in which the depth of the concave portion is sufficiently large for the size thereof and which is free from an abnormal bump portion and excellent in the transparency to visible light. The present invention relates to a surface-treated glass plate having a plurality of the concave portions provided in a glass surface, in which a plane of the glass surface, excluding a region in which the concave portions are formed, is a flat plane, and the concave portions have an average open pore diameter of 10 nm to less than 1 ?m in a cross-sectional view thereof.Type: GrantFiled: December 19, 2012Date of Patent: November 18, 2014Assignee: Asahi Glass Company, LimitedInventor: Shirou Tanii
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Publication number: 20140154439Abstract: Methods include providing a glass, wherein the glass is capable of being phase separated; phase separating the glass; leaching at least one surface of the glass to form a leached glass surface layer; and replenishing the leached glass surface layer with constituents to form a replenished glass surface layer, wherein the constituents cause swelling of the replenished glass surface layer.Type: ApplicationFiled: November 27, 2013Publication date: June 5, 2014Applicant: Corning IncorporatedInventors: Steven Edward DeMartino, Thomas Helmut Elmer, Alexander Usenko
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Publication number: 20130186139Abstract: An object of the present invention is to provide a surface-treated glass plate having a concave portion on the order of nanometers, in which the depth of the concave portion is sufficiently large for the size thereof and which is free from an abnormal bump portion and excellent in the transparency to visible light. The present invention relates to a surface-treated glass plate having a plurality of the concave portions provided in a glass surface, in which a plane of the glass surface, excluding a region in which the concave portions are formed, is a flat plane, and the concave portions have an average open pore diameter of 10 nm to less than 1 ?m in a cross-sectional view thereof.Type: ApplicationFiled: December 19, 2012Publication date: July 25, 2013Applicant: ASAHI GLASS COMPANY, LIMITEDInventor: ASAHI GLASS COMPANY, LIMITED
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Publication number: 20120277085Abstract: A method for strengthening an alkali-containing glass article including: contacting a standardized glass article and aqueous vapor at about 80 to 500° C. for 0.5 to 400 hours at atmospheric pressure. A method for making a damage resistant, low-alkali, glass article including: contacting a standardized glass article and aqueous vapor at about 100 to 600° C. for about 0.5 to about 200 hours at atmospheric pressure. A strengthened and durable glass article prepared by the disclosed methods is disclosed. A display system that can incorporate the glass article, as defined herein, is also disclosed.Type: ApplicationFiled: February 14, 2012Publication date: November 1, 2012Inventors: Dana Craig Bookbinder, Richard Michael Fiacco, Timothy Michael Gross
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Patent number: 7937967Abstract: An object of the present invention is to provide a method of manufacturing a glass substrate containing alkali metals. A glass substrate manufactured by the method exhibits excellent performances including durability by virtue of suppressing elution of alkali metals. A method comprises a step of immersing a glass material in an aqueous solution containing a formate to suppress elution of component of the glass material.Type: GrantFiled: August 29, 2008Date of Patent: May 10, 2011Assignee: Fuji Electric Device Technology Co., Ltd.Inventor: Hiroshi Minazawa
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Publication number: 20090233107Abstract: A new mixed layer silicate useful for industrial materials is provided. The mixed layer silicate is obtained by a specific synthesis method. The mixed layer silicate includes non-swelling 2:1 type layered silicate layers having a layer charge of 0 or non-swelling 2:1 type layered silicate layers having a layer charge of 0.6 to 1 and including potassium ions between layers and swelling 2:1 type layered silicate layers having a layer charge of 0.2 to 0.6 and including exchangeable cations between layers. The mixed layer silicate has a structure in which individual layers are laminated in a regular order in a lamination direction (regularly mixed layer structure).Type: ApplicationFiled: September 13, 2006Publication date: September 17, 2009Applicant: NATIONAL INSTITUTE FOR MATERIALS SCIENCEInventors: Hirohisa Yamada, Kenji Tamura, Shingo Yokoyama
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Patent number: 7531043Abstract: The invention can provide a production method for a magnetic disk substrate capable of reducing the number of surface defects of a glass substrate. When a magnetic disk is produced by using the resulting magnetic disk substrate, the yield and, furthermore, the reliability can be improved. When a surface of a magnetic disk substrate is washed after it is polished, the glass substrate is dipped into a washing solution while the surface of the glass substrate polished is held under a wet condition. The wet condition of the surface of the glass substrate includes a condition in which the glass substrate is dipped into water that may contain a surfactant, and a condition in which a liquid film is formed substantially on the entire surface.Type: GrantFiled: August 26, 2005Date of Patent: May 12, 2009Inventors: Hiroyuki Machida, Katsuaki Aida
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Patent number: 7155934Abstract: The method of making borosilicate glass with a surface having reactive SiOH groups on it includes preparing a borosilicate glass melt and dissolving at least 30 mMol per liter of water in the borosilicate glass melt. The borosilicate glass contains from 70 to 87 percent by weight, SiO2; from 7 to 15 percent by weight, B2O3; from 0 to 8 percent by weight, Al2O3; from 0 to 8 percent by weight, Na2O and from 0 to 8 percent by weight of K2O. The borosilicate glass with the easily modified reactive surface can be used as a substrate for chemically covalent immobilization of reactive substances. This substrate can be used to make a biochemical chip, such as a DNA or gene chip, or dirt-proof window glass.Type: GrantFiled: November 18, 2002Date of Patent: January 2, 2007Assignee: Schott AGInventors: Gerhard Lauten-Schlaeger, Thomas Kloss, Sandra Von Fintel, Klaus Schneider
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Patent number: 6993934Abstract: Dental glass powders, methods for producing the powders and dental compositions including the glass powders. The powders preferably have a well-controlled particle size, narrow size distribution and a spherical morphology. The method includes forming the particles by a spray pyrolysis technique. The invention also includes dental filler and restorative compositions that include the glass powders.Type: GrantFiled: September 8, 2003Date of Patent: February 7, 2006Assignee: Cabot CorporationInventors: Toivo T. Kodas, Mark J. Hampden-Smith, Quint H. Powell, James H. Brewster, Daniel J. Skamser, Klaus Kunze, Paolina Atanassova, Paul Napolitano
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Patent number: 6898365Abstract: A method for manufacturing an article capable of constraining a propagating wave is disclosed. The method includes contacting a crystalline substrate with a source of deuterium ions to create a region in the crystalline substrate having a crystal structure that includes deuterium ions. The region is capable of constraining a propagating wave to the region.Type: GrantFiled: September 30, 2002Date of Patent: May 24, 2005Assignee: California Institute of TechnologyInventor: Lee J. Burrows
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Patent number: 6339033Abstract: A silica glass is provided for use in an optical system processing an excimer laser beam. The silica glass has a molecular hydrogen concentration of about 5×1018 molecules/cm3 or less and is substantially free from defects which become precursors susceptible to an one-photon absorption process and a two-photon absorption process upon irradiation of the excimer laser beam to the silica glass.Type: GrantFiled: December 15, 2000Date of Patent: January 15, 2002Assignee: Nikon CorporationInventors: Hiroki Jinbo, Norio Komine, Seishi Fujiwara, Akiko Yoshida
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Publication number: 20010047665Abstract: Deuterium oxide, D2O, also called heavy water, is used for the hydrolysis of silanes and metal compounds. The D2O-hydrolyzed silanes polycondense much easier than H2O-hydrolyzed silanes, resulting in a fast Si—O—Si network build up. The most important feature of using D2O is that the final materials are 100% free of O—H and the residual O—D bond does not have an absorption peak in the wavelength range of 1.0 to 1.8 &mgr;m, which is crucial in reducing optical loss at the wavelengths of 1.3 and especially 1.55 &mgr;m. O—H free sol-gel materials with low optical loss have been developed based on this process. D2O may be applied in all kinds of hydrolysis-processes, such as the sol-gel process of silanes and metal compounds, the synthesis of polysiloxane, and may be extended to other silica and metal-oxides deposition processes for example, flame hydrolysis deposition (FHD) whenever water is used or O—H bond involved.Type: ApplicationFiled: May 7, 2001Publication date: December 6, 2001Applicant: Zenastra Photonics Inc.Inventors: Zhiyi Zhang, Gaozhi Xiao, Guang Pan, Pinqing Zhang, Ming Zhou