To Hydrate The Glass Patents (Class 65/30.12)
  • Patent number: 11548806
    Abstract: A glass body manufacturing apparatus includes: a first heating furnace including a furnace core tube accommodating the soot and a first heater, to supply a dehydration gas into the furnace core tube and heat the soot at a first treatment temperature lower than a softening point of the porous portion by the first heater; a second heating furnace including a structural body accommodating the soot and a second heater, to heat the soot at a second treatment temperature equal to or higher than the softening point by the second heater; and a conveyance container, connectable to each of the first and second heating furnaces while keeping airtightness with respect to the atmosphere, to accommodate and hold the soot, and convey the soot between the first and second heating furnaces.
    Type: Grant
    Filed: May 27, 2020
    Date of Patent: January 10, 2023
    Assignee: FURUKAWA ELECTRIC CO., LTD.
    Inventors: Koichi Toyosaki, Hiroshi Miyake, Tsuneo Suzuki
  • Patent number: 11505492
    Abstract: Glass-based articles that include a compressive stress layer extending from a surface of the glass-based article to a depth of compression are formed by exposing glass-based substrates to water vapor containing environments. The glass-based substrates have compositions selected to avoid the formation of haze during the treatment process. The methods of forming the glass-based articles may include elevated pressures and/or multiple exposures to water vapor containing environments selected to avoid the formation of haze during the treatment process.
    Type: Grant
    Filed: May 2, 2022
    Date of Patent: November 22, 2022
    Assignee: Corning Incorporated
    Inventors: Timothy Michael Gross, Jingshi Wu
  • Patent number: 11370696
    Abstract: Glass-based articles that include a compressive stress layer extending from a surface of the glass-based article to a depth of compression are formed by exposing glass-based substrates to water vapor containing environments. The glass-based substrates have compositions selected to avoid the formation of haze during the treatment process. The methods of forming the glass-based articles may include elevated pressures and/or multiple exposures to water vapor containing environments selected to avoid the formation of haze during the treatment process.
    Type: Grant
    Filed: May 12, 2020
    Date of Patent: June 28, 2022
    Assignee: Corning Incorporated
    Inventors: Timothy Michael Gross, Jingshi Wu
  • Patent number: 11023630
    Abstract: A method of making a glass article includes melting batch materials to produce molten glass, heating or cooling the molten glass to a temperature, forming a glass article from the molten glass. The batch materials include a plurality of viscosity-affecting components that become at least part of the glass article. Selection of the batch materials or the temperature was made at least in part using computer-implemented modeling where predicted equilibrium viscosity of the glass at the temperature is a function comprising concentrations of viscosity-affecting components and temperature-independent fitting coefficients for the viscosity-affecting components.
    Type: Grant
    Filed: November 5, 2020
    Date of Patent: June 1, 2021
    Assignee: Corning Incorporated
    Inventors: Douglas Clippinger Allan, Adam James Ellison, John Christopher Mauro
  • Patent number: 8887528
    Abstract: An object of the present invention is to provide a surface-treated glass plate having a concave portion on the order of nanometers, in which the depth of the concave portion is sufficiently large for the size thereof and which is free from an abnormal bump portion and excellent in the transparency to visible light. The present invention relates to a surface-treated glass plate having a plurality of the concave portions provided in a glass surface, in which a plane of the glass surface, excluding a region in which the concave portions are formed, is a flat plane, and the concave portions have an average open pore diameter of 10 nm to less than 1 ?m in a cross-sectional view thereof.
    Type: Grant
    Filed: December 19, 2012
    Date of Patent: November 18, 2014
    Assignee: Asahi Glass Company, Limited
    Inventor: Shirou Tanii
  • Publication number: 20140154439
    Abstract: Methods include providing a glass, wherein the glass is capable of being phase separated; phase separating the glass; leaching at least one surface of the glass to form a leached glass surface layer; and replenishing the leached glass surface layer with constituents to form a replenished glass surface layer, wherein the constituents cause swelling of the replenished glass surface layer.
    Type: Application
    Filed: November 27, 2013
    Publication date: June 5, 2014
    Applicant: Corning Incorporated
    Inventors: Steven Edward DeMartino, Thomas Helmut Elmer, Alexander Usenko
  • Publication number: 20130186139
    Abstract: An object of the present invention is to provide a surface-treated glass plate having a concave portion on the order of nanometers, in which the depth of the concave portion is sufficiently large for the size thereof and which is free from an abnormal bump portion and excellent in the transparency to visible light. The present invention relates to a surface-treated glass plate having a plurality of the concave portions provided in a glass surface, in which a plane of the glass surface, excluding a region in which the concave portions are formed, is a flat plane, and the concave portions have an average open pore diameter of 10 nm to less than 1 ?m in a cross-sectional view thereof.
    Type: Application
    Filed: December 19, 2012
    Publication date: July 25, 2013
    Applicant: ASAHI GLASS COMPANY, LIMITED
    Inventor: ASAHI GLASS COMPANY, LIMITED
  • Publication number: 20120277085
    Abstract: A method for strengthening an alkali-containing glass article including: contacting a standardized glass article and aqueous vapor at about 80 to 500° C. for 0.5 to 400 hours at atmospheric pressure. A method for making a damage resistant, low-alkali, glass article including: contacting a standardized glass article and aqueous vapor at about 100 to 600° C. for about 0.5 to about 200 hours at atmospheric pressure. A strengthened and durable glass article prepared by the disclosed methods is disclosed. A display system that can incorporate the glass article, as defined herein, is also disclosed.
    Type: Application
    Filed: February 14, 2012
    Publication date: November 1, 2012
    Inventors: Dana Craig Bookbinder, Richard Michael Fiacco, Timothy Michael Gross
  • Patent number: 7937967
    Abstract: An object of the present invention is to provide a method of manufacturing a glass substrate containing alkali metals. A glass substrate manufactured by the method exhibits excellent performances including durability by virtue of suppressing elution of alkali metals. A method comprises a step of immersing a glass material in an aqueous solution containing a formate to suppress elution of component of the glass material.
    Type: Grant
    Filed: August 29, 2008
    Date of Patent: May 10, 2011
    Assignee: Fuji Electric Device Technology Co., Ltd.
    Inventor: Hiroshi Minazawa
  • Publication number: 20090233107
    Abstract: A new mixed layer silicate useful for industrial materials is provided. The mixed layer silicate is obtained by a specific synthesis method. The mixed layer silicate includes non-swelling 2:1 type layered silicate layers having a layer charge of 0 or non-swelling 2:1 type layered silicate layers having a layer charge of 0.6 to 1 and including potassium ions between layers and swelling 2:1 type layered silicate layers having a layer charge of 0.2 to 0.6 and including exchangeable cations between layers. The mixed layer silicate has a structure in which individual layers are laminated in a regular order in a lamination direction (regularly mixed layer structure).
    Type: Application
    Filed: September 13, 2006
    Publication date: September 17, 2009
    Applicant: NATIONAL INSTITUTE FOR MATERIALS SCIENCE
    Inventors: Hirohisa Yamada, Kenji Tamura, Shingo Yokoyama
  • Patent number: 7531043
    Abstract: The invention can provide a production method for a magnetic disk substrate capable of reducing the number of surface defects of a glass substrate. When a magnetic disk is produced by using the resulting magnetic disk substrate, the yield and, furthermore, the reliability can be improved. When a surface of a magnetic disk substrate is washed after it is polished, the glass substrate is dipped into a washing solution while the surface of the glass substrate polished is held under a wet condition. The wet condition of the surface of the glass substrate includes a condition in which the glass substrate is dipped into water that may contain a surfactant, and a condition in which a liquid film is formed substantially on the entire surface.
    Type: Grant
    Filed: August 26, 2005
    Date of Patent: May 12, 2009
    Inventors: Hiroyuki Machida, Katsuaki Aida
  • Patent number: 7155934
    Abstract: The method of making borosilicate glass with a surface having reactive SiOH groups on it includes preparing a borosilicate glass melt and dissolving at least 30 mMol per liter of water in the borosilicate glass melt. The borosilicate glass contains from 70 to 87 percent by weight, SiO2; from 7 to 15 percent by weight, B2O3; from 0 to 8 percent by weight, Al2O3; from 0 to 8 percent by weight, Na2O and from 0 to 8 percent by weight of K2O. The borosilicate glass with the easily modified reactive surface can be used as a substrate for chemically covalent immobilization of reactive substances. This substrate can be used to make a biochemical chip, such as a DNA or gene chip, or dirt-proof window glass.
    Type: Grant
    Filed: November 18, 2002
    Date of Patent: January 2, 2007
    Assignee: Schott AG
    Inventors: Gerhard Lauten-Schlaeger, Thomas Kloss, Sandra Von Fintel, Klaus Schneider
  • Patent number: 6993934
    Abstract: Dental glass powders, methods for producing the powders and dental compositions including the glass powders. The powders preferably have a well-controlled particle size, narrow size distribution and a spherical morphology. The method includes forming the particles by a spray pyrolysis technique. The invention also includes dental filler and restorative compositions that include the glass powders.
    Type: Grant
    Filed: September 8, 2003
    Date of Patent: February 7, 2006
    Assignee: Cabot Corporation
    Inventors: Toivo T. Kodas, Mark J. Hampden-Smith, Quint H. Powell, James H. Brewster, Daniel J. Skamser, Klaus Kunze, Paolina Atanassova, Paul Napolitano
  • Patent number: 6898365
    Abstract: A method for manufacturing an article capable of constraining a propagating wave is disclosed. The method includes contacting a crystalline substrate with a source of deuterium ions to create a region in the crystalline substrate having a crystal structure that includes deuterium ions. The region is capable of constraining a propagating wave to the region.
    Type: Grant
    Filed: September 30, 2002
    Date of Patent: May 24, 2005
    Assignee: California Institute of Technology
    Inventor: Lee J. Burrows
  • Patent number: 6339033
    Abstract: A silica glass is provided for use in an optical system processing an excimer laser beam. The silica glass has a molecular hydrogen concentration of about 5×1018 molecules/cm3 or less and is substantially free from defects which become precursors susceptible to an one-photon absorption process and a two-photon absorption process upon irradiation of the excimer laser beam to the silica glass.
    Type: Grant
    Filed: December 15, 2000
    Date of Patent: January 15, 2002
    Assignee: Nikon Corporation
    Inventors: Hiroki Jinbo, Norio Komine, Seishi Fujiwara, Akiko Yoshida
  • Publication number: 20010047665
    Abstract: Deuterium oxide, D2O, also called heavy water, is used for the hydrolysis of silanes and metal compounds. The D2O-hydrolyzed silanes polycondense much easier than H2O-hydrolyzed silanes, resulting in a fast Si—O—Si network build up. The most important feature of using D2O is that the final materials are 100% free of O—H and the residual O—D bond does not have an absorption peak in the wavelength range of 1.0 to 1.8 &mgr;m, which is crucial in reducing optical loss at the wavelengths of 1.3 and especially 1.55 &mgr;m. O—H free sol-gel materials with low optical loss have been developed based on this process. D2O may be applied in all kinds of hydrolysis-processes, such as the sol-gel process of silanes and metal compounds, the synthesis of polysiloxane, and may be extended to other silica and metal-oxides deposition processes for example, flame hydrolysis deposition (FHD) whenever water is used or O—H bond involved.
    Type: Application
    Filed: May 7, 2001
    Publication date: December 6, 2001
    Applicant: Zenastra Photonics Inc.
    Inventors: Zhiyi Zhang, Gaozhi Xiao, Guang Pan, Pinqing Zhang, Ming Zhou