Base Metal One Or More Of Beryllium(be), Magnesium(mg), Or Aluminum(al) Patents (Class 75/249)
  • Patent number: 5635654
    Abstract: A particulate reinforced NiAl-AlN composite alloy has a NiAl matrix and greater than about 13 volume percent fine particles of AlN within the matrix. The particles preferably have a diameter from about 15 nanometers to about 50 nanometers. The particulate reinforced NiAl-AlN composite alloy may be prepared by cryomilling prealloyed NiAl in liquid nitrogen using grinding media having a diameter of from about 2 mm to about 6 mm at an impeller speed of from about 450 RPM to about 800 RPM. The cryomilling may be done for a duration of from about 4 hours to about 20 hours to obtain a cryomilled powder. The cryomilled powder may be consolidated to form the particulate reinforced NiAl-AlN composite alloy. The particulate reinforced alloy can further include a toughening alloy. The toughening alloy may include NiCrAlY, FeCrAY and FeAl.
    Type: Grant
    Filed: May 5, 1994
    Date of Patent: June 3, 1997
    Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space Administration
    Inventors: Mohan G. Hebsur, John D. Whittenberger, Carl E. Lowell
  • Patent number: 5614036
    Abstract: A high heat resisting and high abrasion resisting aluminum alloy and aluminum alloy powder have superior toughness, abrasion resistance, high temperature strength, and creep resistance and are useful to form engine parts for automobiles, airplanes, etc. The high heat resisting and high abrasion resisting aluminum alloy comprises 2 to 15 wt % of Ni, 0.2 to 15 wt % of Si, 0.6 to 8.0 wt % of Fe, one or two of 0.6 to 5.0 wt % of Cu and 0.5 to 3 wt % of Mg, the total amount of Cu and Mg being equal to or less than 6 wt %, one or two of 0.3 to 3 wt % of Zr and 0.3 to 3 wt % of Mo, the total amount of Zr and Mo being equal to or less than 4 wt %, 0.05 to 10 wt % of B, and the balance of Al and unavoidable impurities, and is produced by powder metallurgy.
    Type: Grant
    Filed: January 30, 1996
    Date of Patent: March 25, 1997
    Assignees: Toyota Jidosha Kabushiki Kaisha, Toyo Aluminium Kabushiki Kaisha
    Inventors: Kunihiko Imahashi, Hirohisa Miura, Yasuhiro Yamada, Hirofumi Michioka, Jun Kusui, Akiei Tanaka
  • Patent number: 5614684
    Abstract: A method for the production of a superplastic Mg-based composite material comprises preparing a composite material consisting of ceramic particles formed of at least one compound selected from among TiC, AlN, Si.sub.3 N.sub.4, and TiB.sub.2 and a matrix formed of a magnesium alloy, dispersing the ceramic particles in the matrix, hot extruding the composite material, and then hot rolling the resultant extrudate; and a superplastic Mg-based composite material produced by the method.
    Type: Grant
    Filed: October 3, 1995
    Date of Patent: March 25, 1997
    Assignee: Agency of Industrial Science and Technology, Ministry of International Trade & Industry
    Inventors: Suk-Won Lim, Tsunemichi Imai, Yoshinori Nishida, Takao Choh
  • Patent number: 5613184
    Abstract: An aluminium alloy made by a powder metallurgy route and a method for its production are described. The method comprises the steps of producing a first powder of a near-eutectic aluminium-silicon based alloy; producing a second powder of a hypereutectic aluminium-silicon based alloy; mixing desired proportions of the two powders together; compacting the powder mixture and sintering the compacted powder.
    Type: Grant
    Filed: November 30, 1995
    Date of Patent: March 18, 1997
    Assignees: The Aluminium Powder Company Limited, Brico Engineering Limited
    Inventors: Charles G. Purnell, Paul Smith, Mohammad S. Mahmoud
  • Patent number: 5605558
    Abstract: A nitrogenous Al--Si powder metallurgical alloy contains at least 4 wt % and at most 15 wt % of nitrogen, with the remaining part consisting essentially of Al, Si and an unavoidable component. Consequently, a highly safe material which is lightweight and has a density of at most 3.0 g/cm.sup.3, a thermal expansion coefficient in the range of 5 to 10.times.10.sup.-6 /.degree.C., and a thermal conductivity coefficient of at least 0.2 cal/cm.multidot.sec.multidot..degree.C. has been obtained.
    Type: Grant
    Filed: November 4, 1994
    Date of Patent: February 25, 1997
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Shin-ichi Yamagata, Yoshishige Takano, Tetsuya Hayashi, Yugaku Abe
  • Patent number: 5597967
    Abstract: Two-phase Al--Si alloy foils are made directly from Al--Si alloy powders by hot pressing. These Al--Si alloy foils are characterized by having a thickness of 0.017 in. or less, and by the fact that they are fine-grained and substantially free of oxygen, nitrogen and deformation-induced defects. The as-pressed Al--Si foils where the primary phase is the Al solid-solution phase are also generally ductile and adapted for subsequent forming operations, including cold rolling. The reduction in thickness imparted in a single pass to an Al-11.6Si alloy foil through cold-rolling was at least about 10%, with up to about 90% reduction in thickness accomplished by a plurality of such passes. These reductions in thickness were accomplished without stress relief annealing, but such annealing may be employed if desirable for microstructural modification.
    Type: Grant
    Filed: June 27, 1994
    Date of Patent: January 28, 1997
    Assignee: General Electric Company
    Inventors: Ann M. Ritter, Melvin R. Jackson, John R. Hughes
  • Patent number: 5589652
    Abstract: In the metallic member of the invention, ceramic super fine particles, and solid lubricant particles or short size fibers are dispersed, and the grain size of the ceramic particles is smaller than the solid lubricant particle size or fiber diameter.
    Type: Grant
    Filed: February 23, 1994
    Date of Patent: December 31, 1996
    Assignee: Hitachi, Ltd.
    Inventors: Toshiaki Arato, Yasuhisa Aono, Shigeo Tsuruoka, Katsuhiro Komuro
  • Patent number: 5561829
    Abstract: A method of preparing a metal alloy product from a powder blend. The method comprising: (a) cold pressing a blend to form a compact, the metal blend comprising a metal powder phase and at least one reinforcement phase having a hardness greater than the metal phase; (b) heating the compact to form a preheated compact; and (c) hot working the heated compact. In a preferred method, the powder metal blend comprises 50 to 90 vol. % of an aluminum alloy powder and 10 to 50 vol. % of silicon carbide; the heating of the compact perforated in a nitrogen atmosphere to form a preheated compact; and the extruded hot compact is hot worked. Hot working may take the form of forging, rolling, upset forging, exuding, compacting or other processes known in the art.
    Type: Grant
    Filed: April 27, 1995
    Date of Patent: October 1, 1996
    Assignee: Aluminum Company of America
    Inventors: Ralph R. Sawtell, Warren H. Hunt, Jr., Thomas J. Rodjom, Erik J. Hilinski, John H. Milsom
  • Patent number: 5551997
    Abstract: Disclosed is a practical aluminum based alloy containing 1 to 99 weight percent beryllium, and improved methods of semi-solid processing of aluminum alloys containing beryllium. The present methods avoid molten beryllium, agitation of molten aluminum-beryllium alloys and the need for introducing shear forces by utilizing atomized or ground particles of beryllium mixed with solid, particulate or liquidus aluminum.
    Type: Grant
    Filed: March 31, 1994
    Date of Patent: September 3, 1996
    Assignee: Brush Wellman, Inc.
    Inventors: James M. Marder, Warren J. Haws
  • Patent number: 5508116
    Abstract: A metal matrix composite reinforced with shape memory alloy is disclosed ch is formed by blending metal particles and shape memory alloy particles to form a homogeneous powder blend, and consolidating the powder blend to form a unitary mass. The unitary mass is then plastically deformed such as by extrusion in the presence of heat so as to cause an elongation thereof, whereby the metal particles form a matrix and the shape memory alloy partices align in the direction of elongation of the unitary mass. The composite can be used in structural applications and will exhibit shape memory characteristics.
    Type: Grant
    Filed: April 28, 1995
    Date of Patent: April 16, 1996
    Assignee: The United States of America as represented by the Secretary of the Navy
    Inventor: David J. Barrett
  • Patent number: 5478418
    Abstract: An aluminum alloy powder for sliding members includes Fe in an amount of from 0.5 to 5.0% by weight, Cu in an amount of from 0.6 to 5.0% by weight, B in an amount of from 0.1 to 2.0% by weight and the balance of Al. An aluminum alloy includes a matrix made from the aluminum alloy powder and at least one member dispersed, with respect to whole of the matrix taken 100% by weight, in the matrix, and selected from the group consisting of B in an amount of from 0.1 to 5.0% by weight, boride in an amount of from 1.0 to 15% by weight and iron compound in an amount of from 1.0 to 15% by weight, and thereby it exhibits the tensile strength of 400 MPa or more. The aluminum alloy powder and the aluminum alloy are suitable for making sliding members like valve lifters for automobiles.
    Type: Grant
    Filed: April 28, 1994
    Date of Patent: December 26, 1995
    Assignees: Toyota Jidosha Kabushiki Kaisha, Toyo Aluminum Kabushiki Kaisha
    Inventors: Hirohisa Miura, Yasuhiro Yamada, Hirohumi Michioka, Jun Kusui, Akiei Tanaka
  • Patent number: 5464463
    Abstract: Disclosed are heat resistant aluminum alloy powder and alloy including Ni in an amount of from 5.7 to 20% by weight, Si in an amount of from 6.0 to 25% by weight, at least one of Fe in an amount of from 0.6 to 8.0% by weight and Cu in an amount of from 0.6 to 5.0% by weight, and at least one of B in a form of the simple substance in an amount of from 0.05 to 2.0% by weight (or from 0.05 to 10% by weight for the alloy) and graphite particles (especially for the alloy) in an amount of from 0.1 to 10% by weight. The alloy powder and alloy are not only superb in the tensile strength at room temperature and high temperatures but also superior in the sliding characteristic, they can be further upgraded in the wear resistance and the fretting fatigue resistance by dispersing at least one of nitride particles, boride particles, oxide particles and carbide particles in an amount of from 0.
    Type: Grant
    Filed: April 14, 1993
    Date of Patent: November 7, 1995
    Assignees: Toyota Jidosha Kabushiki Kaisha, Toyo Aluminum Kabushiki Kaisha
    Inventors: Hirohisa Miura, Kunihiko Imahashi, Hirohumi Michioka, Yasuhiro Yamada, Jun Kusui, Akiei Tanaka
  • Patent number: 5460640
    Abstract: A fully dense ceramic-metal body including 40-88 v/o of an oxide hard phase of, in v/o of the body, 4-88 v/o M-aluminum binary oxides, where the binary oxide has a C-type rare earth, garnet, .beta.-MAl.sub.11 O.sub.18, or perovskite crystal structure, and M is a lanthanide or indium, and 0-79 v/o .alpha.-alumina; about 10-50 v/o of a hard refractory carbide, nitride, or boride as a reinforcing phase; and about 2-10 v/o of a dispersed metal phase combining Ni and Al mostly segregated at triple points of the microstructure. The preferred metal phase contains a substantial amount of the Ni.sub.3 Al ordered crystal structure. In the preferred body, the reinforcing phase is silicon carbide partially incorporated into the oxide grains, and bridges the grain boundaries. The body including a segregated metal phase is produced by densifying a mixture of the hard phase components and the metal component, with the metal component being present in the starting formulation as Ni powder and Al powder.
    Type: Grant
    Filed: August 17, 1992
    Date of Patent: October 24, 1995
    Assignee: Valenite Inc.
    Inventor: Sergej-Tomislav Buljan
  • Patent number: 5455738
    Abstract: A circuit card assembly thermal core includes a composite material that includes particles of diamond and a conductive metal such as aluminum, copper, nickel and beryllium and which may be made by pressure infiltration casting. The diamond particles are 110 to 160 microns in size and 10 to 80 percent by volume, and preferably 140 to 160 microns in size and 40 to 60 percent by volume. The composite material has both a high thermal conductivity and low density which may be matched with the coefficient of thermal expansion of other materials with which used.
    Type: Grant
    Filed: July 28, 1993
    Date of Patent: October 3, 1995
    Assignee: E-Systems, Inc.
    Inventors: Mark J. Montesano, John T. Wigand, Joseph C. Roesch
  • Patent number: 5454855
    Abstract: A compacted and consolidated material of an aluminum-based alloy obtained by compacting and consolidating a rapidly solidified material having a composition represented by the general formula: Al.sub.a Ni.sub.b X.sub.c M.sub.d, Al.sub.a Ni.sub.b X.sub.c Q.sub.e or Al.sub.a 'Ni.sub.b X.sub.c M.sub.d Q.sub.e, wherein X represents at least one element selected from the group consisting of La, Ce, Mm (misch metal), Ti and Zr; M represents at least one element selected from the group consisting of V, Cr, Mn, Fe, Co, Y, Nb, Mo, Hf, Ta and W; Q represents at least one element selected from the group consisting of Mg, Si, Cu and Zn; and a, a', b, c, d and e are, in atomic percentages, 85.ltoreq.a.ltoreq.94.4, 83.ltoreq.a.ltoreq.94.3, 5.ltoreq.b.ltoreq.10, 0.5.ltoreq.c.ltoreq.3, 0.1.ltoreq.d.ltoreq.2 and 0.1.ltoreq.e.ltoreq.2.
    Type: Grant
    Filed: October 27, 1992
    Date of Patent: October 3, 1995
    Assignee: YKK Corporation
    Inventors: Kazuhiko Kita, Hidenobu Nagahama, Takeshi Terabayashi, Makoto Kawanishi
  • Patent number: 5447549
    Abstract: A hard alloy suitable for use in cutting tools, which exhibits excellent wear and fracture resistance, is disclosed. The hard alloy includes a hard dispersed phase and a binder metal phase, and the binder metal phase is constructed so that compressive stress, preferably of no less than 98 MPa (10 kgf/mm.sup.2), is retained therein. The hard alloy may be a cermet which includes a hard dispersed phase of at least one compound of titanium carbonitride and composite carbonitrides of titanium with at least one element of tantalum, tungsten, molybdenum, niobium, vanadium, chromium, zirconium or hafnium, and a binder metal phase of one or more of cobalt, nickel, iron and aluminum.
    Type: Grant
    Filed: February 17, 1993
    Date of Patent: September 5, 1995
    Assignee: Mitsubishi Materials Corporation
    Inventor: Hironori Yoshimura
  • Patent number: 5443616
    Abstract: A dimensionally stable hydride composition and a method for making such a composition. The composition is made by forming particles of a metal hydride into porous granules, mixing the granules with a matrix material, forming the mixture into pellets, and sintering the pellets in the absence of oxygen. The ratio of matrix material to hydride is preferably between approximately 2:1 and 4:1 by volume. The porous structure of the granules accommodates the expansion that occurs when the metal hydride particles absorb hydrogen. The porous matrix allows the flow of hydrogen therethrough to contact the hydride particles, yet supports the granules and contains the hydride fines that result from repeated absorption/desorption cycles.
    Type: Grant
    Filed: July 14, 1993
    Date of Patent: August 22, 1995
    Assignee: The United States of America as represented by the United States Department of Energy
    Inventor: James W. Congdon
  • Patent number: 5443917
    Abstract: A densified ceramic or cermet armor material comprises greater than fifty percent by weight titanium nitride or greater than eight percent by weight of a mixture of titanium nitride and aluminum nitride to impart low compressive strength to said armor material and may additionally comprise components suitable for densification with said titanium nitride or titanium nitride-aluminum nitride mixture where the resulting armor material has high density and low porosity with a Young's modulus greater than 200 GPa and a compressive strength of less than 5.5 GPa.
    Type: Grant
    Filed: May 24, 1991
    Date of Patent: August 22, 1995
    Assignee: GTE Products Corporation
    Inventor: Christopher A. Tarry
  • Patent number: 5435825
    Abstract: Disclosed herein is an aluminum matrix composite powder comprising 1 to 40% by weight of ceramic particles dispersed in a matrix of aluminum-silicon alloy. The matrix of the composite may further comprise at least one of Cu, Mg and transition metals.The aluminum matrix composite is prepared by a rapid solidification.In the aluminum matrix composite, the ceramic particles are very uniformly dispersed in the matrix, thereby the improvement of mechanical properties of product prepared therefrom can be obtained.
    Type: Grant
    Filed: August 7, 1992
    Date of Patent: July 25, 1995
    Assignee: Toyo Aluminum Kabushiki Kaisha
    Inventors: Jun Kusui, Fumiaki Nagase, Akiei Tanaka, Kohei Kubo, Takamasa Yokote
  • Patent number: 5422069
    Abstract: Master alloys and methods of producing same are disclosed, wherein an intermetallic compound, for example Al.sub.3 Cb is first prepared via thermite processing, then size reduced, then mixed with other components in amounts yielding a mixture in the desired proportion for the master alloy. The mixture is compacted, then heated to produce the master alloy by fusion.
    Type: Grant
    Filed: December 29, 1993
    Date of Patent: June 6, 1995
    Assignee: Reading Alloys, Inc.
    Inventor: Frederick H. Perfect, deceased
  • Patent number: 5395700
    Abstract: In this invention, a cutting tool comprises two layers of hard sintered compact of cBN. The first sintered compact layer comprises about 75-98% by volume of cBN and a first binder material. The first binder material comprises from about 1 to out 40% by weight of Al. The second sintered compact layer comprises from about 40 to about 65% by volume of cBN and a second binder material. The second binder material comprises about 2 to about 30% by weight of Al. The first sintered compact layer is bonded to the second sintered compact layer. This composite material is bonded directly or indirectly to a tool holder to form a cutting tool. The first sintered compact layer constitutes a rake face of the cutting tool.
    Type: Grant
    Filed: June 25, 1992
    Date of Patent: March 7, 1995
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Tetsuo Nakai, Mitsuhiro Goto
  • Patent number: 5387272
    Abstract: The present invention provides an Al-Si based sintered alloy of high strength and high ductility, a method for production thereof and use thereof. The alloy comprises 1-45% of Si, 0.1-20% of an element of Group IIIa, 0.01-5% of at least one element of Groups IVa and Va, the balance of substantially Al. This alloy can further contain at least one of 0.01-5% of Cu, 0.01-5% of Mg, 2.0% or less of Fe, 1.5% or less of Mn and 1.5% or less of Co and the oxygen content is reduced to 0.15% or less by sintering under vacuum. The present invention is applied to automobile parts such as a piston and scroll compressors. The alloy has a tensile strength of about 40 kg/mm.sup.2 or higher and an elongation of 1.5% or more at 150.degree. C.
    Type: Grant
    Filed: April 8, 1992
    Date of Patent: February 7, 1995
    Assignees: Hitachi, Ltd., Hitachi Powdered Metals Company, Limited
    Inventors: Yasuo Kamitsuma, Yusaku Nakagawa, Mitsuo Chigasaki, Tadashi Iizuka, Kooichi Inaba, Keiichi Nakamura, Masaki Minabe, Tsuyoshi Kagaya
  • Patent number: 5384087
    Abstract: The present invention relates to a process for making an aluminum silicon carbide composite material in strip form. The process comprises blending a powdered aluminum matrix material and a powdered silicon carbide material, roll compacting the blended powdered materials in an inert atmosphere to form a green strip having a first thickness, and directly hot working the blended and roll compacted materials to bond the aluminum matrix material particles and the silicon carbide particles and to form a thin strip material having a desired thickness.
    Type: Grant
    Filed: April 6, 1992
    Date of Patent: January 24, 1995
    Assignee: Ametek, Specialty Metal Products Division
    Inventor: Clive Scorey
  • Patent number: 5374295
    Abstract: Disclosed are heat resistant aluminum alloy powders and alloys including Ni, Si, either at least one of Fe and Zr or at least one of Zr and Ti. For instance, the alloy powders or alloys consist essentially of Ni in an amount of from 5.7 to 20% by weight, Si in an amount of from 0.2 to 25% by weight, at least one of Fe in an amount of from 0.6 to 8.0% by weight and Cu in an amount of from 0.6 to 5.0% by weight, and the balance of Al. The alloy powders or alloys are optimum for a matrix of heat and wear resistant aluminum alloy-based composite materials including at least one of nitride particles and boride particles in an amount of 0. 5 to 10% by weight with respect to the whole composite material taken as 100% by weight. The alloy powders, alloys and composite materials are satisfactory applicable to the component parts of the recent automobile engines which should produce a high output.
    Type: Grant
    Filed: March 3, 1993
    Date of Patent: December 20, 1994
    Assignees: Toyota Jidosha Kabushiki Kaisha, Toyo Aluminum Kabushiki Kaisha
    Inventors: Hirohisa Miura, Kunihiko Imahashi, Yasuhiro Yamada, Hirohumi Michioka, Jun Kusui, Akiei Tanaka
  • Patent number: 5372663
    Abstract: Ti powders and Al powders are combined to prepare a mixture of 40.about.55 at % of Al and the balance of Ti. After CIP and degassing, plastic working by hot extrusion is applied to form a shaped mixture of Ti and Al. The shaped mixture is then processed by HIP to synthesize titanium aluminide while diffusing Al into the Ti structure to form an Al.sub.2 O.sub.3 phase occurring from both the reaction between Al and oxygen contained in the Ti structure and the oxides on the Al surface, and to disperse the Al.sub.2 O.sub.3 to form the Al.sub.2 O.sub.3 protective film. With the reaction between Al and oxygen contained in the Ti structure and with the "Pegging" effect, both the Al.sub.2 O.sub.3 a phase formed at the grain boundaries of crystals or in the crystal grains of titanium aluminide and the Al.sub.2 O.sub.3 phase existing on the surface of raw material Al powder peg the surface Al.sub.2 O.sub.3 film to the surface of the titanium aluminide body.
    Type: Grant
    Filed: January 3, 1992
    Date of Patent: December 13, 1994
    Assignee: Sumitomo Light Metal Industries, Ltd.
    Inventors: Kazuhisa Shibue, Mok-Soon Kim, Masaki Kumagai
  • Patent number: 5368629
    Abstract: The rapidly solidified aluminum alloy powder is preformed in a cold or warm environment to form a powder compact having a relative density of 75-93%. Then, the preformed compact is heated and degassed in the atmosphere of an inert gas at temperature of 300.degree. C. to 560.degree. C. for 0.25-3 hours. Immediately thereafter, the compact is subjected to hot coining at 300.degree.-560.degree. C. to obtain a solidified compact having pores at a rate of 2-5%. The solidified compact is then subjected to sizing. Since the inorganic gas prevents reaction between the evaporated water and aluminum while preheating the compact, the hot coining can be carried out in a state where solid state diffusion easily occurs. Thus, the powder particles can be bonded together strongly with a single forging. Also, at the end of hot coining, pores remain in the solidified compact at the rate of 2-5%. Utilizing these pores, the compact can be subjected to sizing to improve its dimensional accuracy.
    Type: Grant
    Filed: December 3, 1992
    Date of Patent: November 29, 1994
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventors: Katsuyoshi Kondo, Yoshinobu Takeda
  • Patent number: 5342571
    Abstract: Dual phase sputter targets consisting essentially of TiN and Al, methods of manufacture thereof, and cathodic sputtering methods using such targets are disclosed. The targets are prepared by blending TiN and Al powders followed by compaction to full density. The thus compacted materials are optionally sintered and are then formed into the desired target shape. The targets are used in cathodic sputtering processes to form opaque, dark colored decorative and wear resistant coatings.
    Type: Grant
    Filed: February 19, 1992
    Date of Patent: August 30, 1994
    Assignee: Tosoh SMD, Inc.
    Inventors: Mark B. Dittmar, Paul E. Scheiderer
  • Patent number: 5332415
    Abstract: The present invention provides a compacted and consolidated aluminum-based alloy material which has been obtained by compacting and consolidating a rapidly solidified material having a composition represented by the general formula: Al.sub.a Ni.sub.b X.sub.c wherein X is one or two elements selected from Zr and Ti and a, b and c are, in atomic percentages, 87.5.ltoreq.a.ltoreq.92.5, 5 .ltoreq.b.ltoreq.10, and 0.5.ltoreq.c.ltoreq.5; and a production process comprising melting a material of the above composition; quenching and solidifying the resultant molten material into powder or flakes; compacting, compressing, forming and consolidating the powder or flakes by conventional plastic working. The consolidated material of the present invention has. elongation (toughness) sufficient to withstand secondary working, even when secondary working is applied. Moreover, the material allows the secondary working to be performed easily while retaining the excellent properties of its raw material.
    Type: Grant
    Filed: August 14, 1992
    Date of Patent: July 26, 1994
    Assignee: Yoshida Kogyo K.K.
    Inventor: Kazuhiko Kita
  • Patent number: 5322666
    Abstract: The invention provides a method of mechanical alloying a titanium-base metal powder. Titanium-base metal powder is provided in a mechanical alloying apparatus. The mechanical alloying apparatus has a controlled atmosphere to prevent excessive oxidation of the titanium-base metal powder. An effective amount of tin process control agent is added to the mechanical alloying apparatus. The mechanical alloying apparatus is operated to weld and fracture the titanium-base metal powder in a manner controlled by the tin process control agent. The controlled welding and fracturing ultimately forms a titanium-base mechanically alloyed powder.
    Type: Grant
    Filed: March 24, 1992
    Date of Patent: June 21, 1994
    Assignee: Inco Alloys International, Inc.
    Inventor: Arunkumar S. Watwe
  • Patent number: 5304426
    Abstract: A beryllium metal matrix phase includes up to 70% by volume of beryllium oxide single crystals dispersed therein. The composites are useful for electronics applications because of their light weight, high strength and effective thermal properties.
    Type: Grant
    Filed: August 17, 1992
    Date of Patent: April 19, 1994
    Assignee: Brush Wellman Inc.
    Inventor: Fritz C. Grensing
  • Patent number: 5292358
    Abstract: A sintered aluminum-alloy consisting essentially in weight of 0.1-2.0% Mg, 0.1-2.0% Si, 0.2-6.0% Cu and Al and unavoidable impurities in balance is produced by sintering a mixture of a first aluminum-alloy starting powder and at least one second aluminum-alloy starting powder. The first aluminum-alloy powder consists of 0.1-3.0% Cu and Al and unavoidable impurities in balance and the second aluminum-alloy is selected from (1) an aluminum alloy starting powder consisting of 4-20% Mg, 12-30% Si and Al and unavoidable impurities in balance and (2) an aluminum-alloy starting powder consisting of from 0.1-20.0% Mg, 1-20% Si, 30-50% Cu and Al and unavoidable impurities in balance.
    Type: Grant
    Filed: October 19, 1992
    Date of Patent: March 8, 1994
    Assignee: Showa Denko K.K.
    Inventors: Shin Miura, Youichi Hirose, Yoshio Machida, Mitsuaki Sato
  • Patent number: 5288670
    Abstract: This invention relates generally to a novel method of preparing self-supporting bodies, and to novel products made thereby. In its more specific aspects, this invention relates to a method of producing self-supporting bodies comprising one or more boron-containing compounds, e.g., a boride or a boride and a carbide, by reactive infiltration of a molten parent metal actinide into (1) a bed or mass containing boron carbide and, optionally, (2) at least one of a boron donor material (i.e., a boron-containing material) and a carbon donor material (i.e., a carbon-containing material), (3) a bed or mass comprising a mixture of a boron donor material and a carbon donor material and, optionally, (4) one or more inert fillers in any of the above masses, to form the body.
    Type: Grant
    Filed: November 23, 1992
    Date of Patent: February 22, 1994
    Assignee: Lanxide Technology Company, LP
    Inventor: Paul V. Kelsey
  • Patent number: 5279786
    Abstract: Multi-layer, porous material and process of manufacturing same produced from aluminum scrap powder by means of a centrifugal atomizer for use in noise absorbing devices and filter elements. The multi-layers are arranged according to increasing particle size so that a first layer contains the largest particle size and a last layer contains the smallest particle size. Arranging the layer sin this manner produces a multilayer porous material having a shell configuration of a conch which effectively absorbs noise.
    Type: Grant
    Filed: October 13, 1992
    Date of Patent: January 18, 1994
    Assignee: Jae Chang Byun
    Inventor: Seong S. Cho
  • Patent number: 5277989
    Abstract: A net shaped ceramic-reinforced aluminum matrix composite is formed by forming a permeable mass of ceramic material with a defined surface boundary having a barrier, and contacting a molten aluminum-magnesium alloy with the permeable mass of ceramic material in the presence of a gas comprising from about 10 to 100% nitrogen, by volume, balance nonoxidizing gas, e.g. hydrogen or argon. Under these conditions, the molten alloy spontaneously infiltrates the ceramic mass under normal atmospheric pressures until it reaches the barrier. A solid body of the alloy can be placed adjacent to a permeable bedding of ceramic material having a barrier, and brought to the molten state, preferably to at least about 700.degree. C., in order to form the net shape aluminum matrix composite by infiltration. In addition to magnesium, auxiliary alloying elements may be employed with aluminum. The resulting composite products may contain a discontinuous aluminum nitride phase in the aluminum matrix.
    Type: Grant
    Filed: August 24, 1992
    Date of Patent: January 11, 1994
    Assignee: Lanxide Technology Company, LP
    Inventors: Michael K. Aghajanian, Terry D. Claar
  • Patent number: 5271758
    Abstract: A dense cermet article including about 44-93% of a granular first hard phase, about 4-44% of a granular second hard phase, and about 2-20% of a metal phase, all expressed in % by volume. The first hard phase consists essentially of alumina and from 0% to less than 5% of one or more oxides selected from magnesia, zirconia, yttria, hafnia, and silica. The second hard phase consists essentially of a hard refractory carbide, nitride, or boride, or mixture or solid solution thereof. Preferred materials for inclusion in the second hard phase are titanium carbide, hafnium carbide, tantalum carbide, tantalum nitride, tungsten carbide, titanium diboride, and boron carbide. The metal phase consists essentially of a combination of nickel and aluminum having a ratio of nickel to aluminum of from about 85:15 to about 88:12, and 0-5% of an additive selected from the group consisting of titanium, zirconium, hafnium, vanadium, niobium, tantalum, chromium, molybdenum, cobalt, boron, and/or carbon.
    Type: Grant
    Filed: May 13, 1991
    Date of Patent: December 21, 1993
    Assignee: Valenite Inc.
    Inventors: Sergej T. Buljan, Helmut Lingertat, Steven F. Wayne
  • Patent number: 5264021
    Abstract: A compacted and consolidated aluminum-based alloy material is obtained by compacting and consolidating a rapidly-solidified material having a composition represented by the general formula: Al.sub.a Ni.sub.b X.sub.c M.sub.d or Al.sub.a' Ni.sub.b X.sub.c M.sub.d Q.sub.e, where X is one or two elements selected from La and Ce or an Mm; M is Zr or Ti; Q is one or more elements selected from Mg, Si, Cu and Zn, and a, a', b, c, d and e are, in atomic percentages, 84.ltoreq.a.ltoreq.94.8, 82.ltoreq.a'.ltoreq.94.6, 5.ltoreq.b .ltoreq.10, 0.1.ltoreq.c.ltoreq.3, 0.1.ltoreq.d.ltoreq.3, and 0.2.ltoreq.e.ltoreq.2. According to the production process of the invention, powder or flakes obtained by rapidly solidifying are compacted, followed by compressing, forming and consolidating by conventional plastic working operations. The consolidated material has an elongation sufficient to withstand secondary working operations. Moreover, the material retains the excellent properties of its raw material as they are.
    Type: Grant
    Filed: August 14, 1992
    Date of Patent: November 23, 1993
    Assignee: Yoshida Kogyo K.K.
    Inventors: Kazuhiko Kita, Makoto Kawanishi, Hidenobu Nagahama
  • Patent number: 5256183
    Abstract: Particle reinforced composite material produced by mixing granules of a composite material formed by rapidly solidifying a melt comprising a based light metal matrix and particles of a non-metallic reinforced material with granules of unreinforced host metal matrix, compacting the mixture and applying a shear deformation on said mixture.
    Type: Grant
    Filed: January 23, 1992
    Date of Patent: October 26, 1993
    Assignee: Norsk Hydro a.s.
    Inventors: Wolfgang W. Ruch, Lars Auran, Nils Ryum
  • Patent number: 5224983
    Abstract: A rapidly solidified zirconium containing aluminum lithium alloy powder consisting essentially of the formula Al.sub.bal Li.sub.a Cu.sub.b Mg.sub.c Zr.sub.d where "a" ranges from 2.1 to 3.4 wt %, "b" ranges from about 0.5 to 2.0 wt %, "c" ranges from 0.2 to 2.0 wt % and "d" ranges from greater than about 0.6 to 1.8 wt %, the balance being aluminum. The powder is degassed in a vacuum at a temperature of at least about 450.degree. C. Components consolidated from the powder exhibit high tensile strength and elongation together with excellent notched impact toughness.
    Type: Grant
    Filed: June 24, 1992
    Date of Patent: July 6, 1993
    Assignee: Allied-Signal Inc.
    Inventors: Jerry C. LaSalle, Derek Raybould, Santosh K. Das, Edward V. Limoncelli
  • Patent number: 5217583
    Abstract: A dimensionally stable combustion synthesis product of a composition containing at least 20% by weight of a particulate combustible material; at least 15% by weight of a particulate filler material capable of providing desired mechanical and electrical properties; and up to 35% by weight of a particulate inorganic binder having a melting point lower than the combustion synthesis temperature. Electrodes suitable for electrochemical processing are a preferred product form, particularly electrodes for use in the electrowinning of aluminum from its oxide.
    Type: Grant
    Filed: January 30, 1991
    Date of Patent: June 8, 1993
    Assignee: University of Cincinnati
    Inventors: Jainagesh A. Sekhar, Sarit B. Bhaduri
  • Patent number: 5199971
    Abstract: The present invention relates to parts, such as a drive gear and driven gear, for use in a rotary gear pump exhibiting good sliding characteristics against a pump case made of light metals such as aluminum alloys. These parts are obtained by subjecting aluminum alloy powders, which have been solidified at a cooling rate of 100.degree. C./sec or more, or aluminum alloy powders having particle diameters of 350 .mu.m or less, to powder compacting and hot extrusion and optionally further to hot forging, or subjecting the aluminum alloy powders to powder forging.
    Type: Grant
    Filed: December 19, 1989
    Date of Patent: April 6, 1993
    Assignee: Sumitomo Electric Industries, Ltd.
    Inventor: Kiyoaki Akechi
  • Patent number: 5174955
    Abstract: A heat-resisting aluminum alloy contains manganese ranging from 6 to 8% by weight, iron ranging from 0.5 to 2% by weight, zirconium ranging from 0.03 to 0.5% by weight, and copper ranging from 2 to 5% by weight, the balance being essentially aluminum. The aluminum alloy has been confirmed to be high in mechanical strength both at ordinary temperatures and at high temperatures while to be suitable for producing an article by using so-called atomization process.
    Type: Grant
    Filed: July 22, 1986
    Date of Patent: December 29, 1992
    Assignee: Nissan Motor Co., Ltd.
    Inventors: Masahiko Shioda, Syunsuke Suzuki, Akira Matsuyama, Yoshihiro Maki
  • Patent number: 5171381
    Abstract: The invention comprises an alloy having improved intermediate temperature properties at temperatures up to about 316.degree. C. The alloy contains (by weight percent) about 1-6% X contained as an intermetallic phase in the form of Al.sub.3 X. X is at least one selected from the group consisting of Nb, Ti and Zr. The alloy also contains 0.1-4% strengthener selected from the group consisting of Si and Mg. In addition, the alloy contains about 1-4% C and 0.1-2% O present as aluminum carbides and oxides for grain stabilization.
    Type: Grant
    Filed: February 28, 1991
    Date of Patent: December 15, 1992
    Assignee: Inco Alloys International, Inc.
    Inventors: Prakash K. Mirchandani, Arunkumar S. Watwe, Walter E. Mattson
  • Patent number: 5169461
    Abstract: The alloy of the invention has improved intermediate temperature properties at temperatures up to about 482.degree. C. The alloy contains (by weight percent) a total of about 6-12% X contained as an intermetallic phase in the form of Al.sub.3 X. X is selected from the group consisting of Nb, Ti and Zr. The alloy also contains about 0.1-4% strengthener selected from the group consisting of Co, Cr, Mn, Mo, Ni, Si, V, Nb when Nb is not selected as X and Zr when Zr is not selected as X. In addition, the alloy contains about 1-4% C and about 0.1-2% O.
    Type: Grant
    Filed: June 6, 1991
    Date of Patent: December 8, 1992
    Assignee: Inco Alloys International, Inc.
    Inventors: Arunkumar S. Watwe, Prakash K. Mirchandani, Walter E. Mattson
  • Patent number: 5167480
    Abstract: A rivet is formed from a friction-actuated extrustion. The extrusion is produced by a process that utilizes a comminuted rapidly solidified aluminum alloy ribbon as the in-feed for a continuous friction-actuated extruder. Gumming and flow problems are eliminated. The extruded product is devoid of surface blistering. The extrusion is converted into a rivet that has improved ambient and elevated temperature mechanical properties.
    Type: Grant
    Filed: February 4, 1991
    Date of Patent: December 1, 1992
    Assignee: Allied-Signal Inc.
    Inventors: Paul S. Gilman, Michael S. Zedalis
  • Patent number: 5166105
    Abstract: This invention relates generally to a novel method of preparing self-supporting bodies, and to novel products made thereby. In its more specific aspects, this invention relates to a method of producing self-supporting bodies comprising one or more boron-containing compounds, e.g., a boride or a boride and a carbide, by reactive infiltration of a molten parent metal actinide into (1) a bed or mass containing boron carbide and, optionally, (2) at least one of a boron donor material (i.e., a boron-containing material) and a carbon donor material (i.e., a carbon-containing material), (3) a bed or mass comprising a mixture of a boron donor material and a carbon donor material and, optionally, (4) one or more inert fillers in any of the above masses, to form the body.
    Type: Grant
    Filed: December 10, 1990
    Date of Patent: November 24, 1992
    Assignee: Lanxide Technology Company, LP
    Inventor: Paul V. Kelsey
  • Patent number: 5154780
    Abstract: This invention is characterized by working which improves metal formability. This is contrary to the usual result of working metals, where formability decreases during working.
    Type: Grant
    Filed: June 22, 1990
    Date of Patent: October 13, 1992
    Assignee: Aluminum Company of America
    Inventor: M. K. Premkumar
  • Patent number: 5152829
    Abstract: A rapidly solidified aluminum base alloy consists essentially of the formula Al.sub.bal Fe.sub.a Si.sub.b X.sub.c, wherein X is at least one element selected from the group consisting of W,Ta,Nb, "a" ranges from 3.0 to 7.1 at %, "b" ranges from 1.0 to 3.0 at %, "c" ranges from 0.25 to 1.25 at % and the balance is aluminum plus incidental impurities, with the provisos that the ratio [Fe+X]:Si ranges from about 2.33:1 to 3.33:1 and that the ratio Fe:X ranges from about 16:1 to 5:1. The alloy exhibits high strength, ductility and fracture toughness and is especially suited for use in high temperature structural applications such as gas turbine engines, missiles, airframes and landing wheels.
    Type: Grant
    Filed: June 3, 1991
    Date of Patent: October 6, 1992
    Assignee: Allied-Signal Inc.
    Inventors: David J. Skinner, Michael S. Zedalis
  • Patent number: 5145513
    Abstract: A process for the preparation of composite materials consisting essentially of an oxide phase and a metal phase is effected by grinding a mixture of at least one oxide precursor of the metal phase of the composite with at least one reducing agent, the reducing agent being a precursor of the oxide phase. The grinding being performed in a high energy mechanical grinder for a sufficient length of time so that at least 80 percent of the oxide precursor is reduced to metal or to a metal alloy. The process is particularly valuable for the preparation of oxide/metal composite materials which have improved mechanical, electrical or radiation absorption properties.
    Type: Grant
    Filed: April 12, 1991
    Date of Patent: September 8, 1992
    Assignee: Centre National de le Recherche Scientifique
    Inventors: Paolo Matteazzi, Gerard Le Caer, Elizabeth Grosse-Bauer
  • Patent number: 5141819
    Abstract: A net shaped ceramic-reinforced aluminum matrix composite is formed by forming a permeable mass of ceramic material with a defined surface boundary having a barrier, and contracting a molten aluminum-magnesium alloy with the permeable mass of ceramic material in the presence of a gas comprising from about 10 to 100% nitrogen, by volume, balance nonoxidizing gas, e.g. hydrogen or argon. Under these conditions, the molten alloy spontaneously infiltrates the ceramic mass under normal atmospheric pressures until it reaches the barrier. A solid body of the alloy can be placed adjacent to a permeable bedding of ceramic material having a barrier, and brought to the molten state, preferably to at least about 700.degree. C., in order to form the net shape aluminum matrix composite by infiltration. In addition to magnesium, auxiliary alloying elements may be employed with aluminum. The resulting composite products may contain a discontinuous aluminum nitride phase in the aluminum matrix.
    Type: Grant
    Filed: February 19, 1991
    Date of Patent: August 25, 1992
    Assignee: Lanxide Technology Company, LP
    Inventors: Michael K. Aghajanian, Terry D. Claar
  • Patent number: H1411
    Abstract: Magnesium lithium based alloys prepared by mechanical alloying are disclosed.
    Type: Grant
    Filed: November 12, 1992
    Date of Patent: February 7, 1995
    Inventor: Uday V. Deshmukh