Abstract: A continuous hydrogen pulverization method of a rare earth permanent magnetic alloy includes: providing a hydrogen adsorption room, a heating dehydrogenation room and a cooling room in series, applying hydrogen adsorption, heating dehydrogenation and cooling on a rare earth permanent magnetic alloy in the production device at the same time, wherein collecting and storing under an inert protection atmosphere can also be provided. Continuous production is provided under vacuum and the inert protection atmosphere in such a manner that an oxygen content of the pulverized powder is low and a proportion of single crystal in the powder is high.

Abstract: A process for obtaining tantalum powder from tantalum containing scrap material is provided. The process includes selecting source material, such as from sintered anodes for capacitors, hydriding the source material, milling to desired particle size and surface area, dehydriding, deoxidizing, agglomerating, sifting, and acid treating to obtain tantalum powder of a desired size and purity.

Abstract: A method for producing a metal powder product involves: Providing a supply of a precursor metal powder; combining the precursor metal powder with a liquid to form a slurry; feeding the slurry into a pulsating stream of hot gas; and recovering the metal powder product.

Abstract: It is to propose a method of producing super-micro powders of pure metal-alloy in which cheap materials can be used and the production is efficient. In the production method of pure metal super-micro powder by heating a starting material containing a metal chloride and reducing the resulting vapor of the metal chloride with hydrogen gas, an elementary metal constituting the metal chloride is added to the starting material containing the metal chloride and a metal chloride having a large valence among metal chlorides having two or more valence is used as the metal chloride. Also, in the production method of alloy super-micro powder, a metal chloride is used as one to (number of all alloying components—1) alloying components in the starting material and an elemental metal is used as the other alloying component.

Abstract: The present invention relates to the a method for manufacturing high strength ultra-fine/nano-structured aluminum/aluminum nitride or aluminum alloy/aluminum nitride composites using mechanical milling or mechanical alloying process which is conducted in the nitride-forming atmosphere such as nitrogen gas (N), ammonia gas (NH) or mixed gas including both gases, subsequent heat treatment process, and hot consolidation process. Also, high strength ultra-fine/nano-structured Al/ALN or Al alloy/ALN composite materials fabricated by the method of present invention have superior mechanical strength and heat resistance to those fabricated by conventional powder metallurgy process or liquid processes.

Abstract: Densified molybdenum metal powder and method for producing same. Densified molybdenum powder has substantially generally spherical particles, surface area to mass ratio of no more than about 0.5 m2/g as determined by BET analysis, and a flowability greater than about 32 s/50g as determined by a Hall Flowmeter. A method for producing densified molybdenum metal powder includes providing a supply of precursor material of molybdenum metal powder particles reduced from ammonium molybdate; providing a supply of reducing gas; densifying the precursor material in the presence of the reducing gas; and producing the densified molybdenum metal powder.

Abstract: The present invention relates to an economically excellent method for manufacturing ultra fine tungsten carbide-cobalt composite powder having tungsten compound and cobalt compound as its raw material. More particularly, the present invention provides a manufacturing method comprising a process for mixing tungsten compounds, cobalt compounds, grain-grown inhibitor compounds and oxide in a mechanical method, a calcination process for removing ammonia and moisture of the mixed powder and forming it into an composite oxide, a reduction process for manufacturing said calcined powder into pure metal powder, a mixing process for adding carbon source to said reduced powder, and a carburization process for manufacturing the mixed powder into a tungsten carbide-cobalt composite powder, which is the final form. Using the manufacturing method of the present invention, ultra-fine tungsten carbide-cobalt composite powder having an ultra-fine particle size of 0.1˜0.2 ?m, 0.2˜0.3 ?m,0.3˜0.

Abstract: The invention concerns an iron powder for fortifying foodstuff. The powder consists of a reduced iron powder having irregularly shaped particles, wherein the iron powder has a ratio AD:PD less than 0.3, wherein AD is the apparent density in g/cm3, and PD is the particle density in g/cm3. The specific surface area of the powder particles is above 300 m2/kg as measured by the BET method and the average particle size is between 5-45 ?m.

Abstract: Provided are silver-containing powders and a method and apparatus for manufacturing the silver-containing particles of high quality, of a small size and narrow size distribution. An aerosol is generated from liquid feed and sent to a furnace, where liquid in droplets in the aerosol is vaporized to permit formation of the desired particles, which are then collected in a particle collector. The aerosol generation involves preparation of a high quality aerosol, with a narrow droplet size distribution, with close control over droplet size and with a high droplet loading suitable for commercial applications.

Abstract: Produce metal particles offering high purity and uniform granular shape and size: by forming a combustion chamber comprising an injector nozzle for mixture gas of oxygen and hydrogen, an ignition device and a material metal feeder in the upper space of a high-pressure water tank filled with inert gas; igniting inside the combustion chamber via the ignition device the injector nozzle for mixture gas of oxygen and hydrogen and melting (vaporize) the material fed by the material metal feeder; and then causing the produced molten metal droplets to contact high-pressure water and let the resulting metallic particles to precipitate in water.

Abstract: Manufacture health ornaments such as necklaces, bracelets and wristbands that provide sufficient health-promoting function and effective therapeutic action for a long time, by burning a gaseous mixture of oxygen and hydrogen in high-pressure water, using the resultant gas to heat and granulate titanium material, and combining the obtained titanium powder with an elastomer material.

Abstract: The manufacture of pure, fine spherical powders has always been a problem for many materials, particularly for high-melting and highly reactive materials such as titanium, tantalum, vanadium and zirconium. The present invention provides a process and apparatus for producing such powders by rapidly heating course powders containing a gas or gases to near or above their melting point, whereby the contained gas erupts explosively to form many fine particles of the host material. The fine particles are typically, but not necessarily spheroidal, depending upon the process conditions at the time of eruption and immediately thereafter. Methods are described for producing, collecting, handling, storing and passivating said fine powders.

Abstract: The invention relates to a process for the production of metallic and metal-ceramic composite components by powder injection molding of a system comprising a metal composite powder, a binder and optionally a ceramic component, where the metal composite powder used is mixed with a protecting liquid in an inert atmosphere before the mixing with the binder. The invention furthermore relates to molybdenum/copper and tungsten/copper composite powders which have a primary metal particle size of predominantly <2 ?m, an oxygen content of <0.8% by weight and optionally a ceramic component, to the use of these composite powders for the production of composite components by powder injection molding, and to a process for the preparation of composite powders in which oxides of molybdenum or tungsten and of copper are mixed, dry-ground and reduced using hydrogen at a temperature of from 800 to 1050° C., and a ceramic component is optionally admixed with the resultant metal composite powder.

Abstract: When a chromium-iron-based alloy, preferably a chromium-iron-based alloy having a chromium content of about 60 to about 95 mass % is subjected to heat treatment at about 500 to about 1,300° C., and subsequently to grinding treatment by use of an impact mill, grindability of the chromium-iron-based alloy is improved, and running cost can be reduced. In addition, the resultant powdery thermal spraying material exhibits stable fluidity during spray coating, and thus a uniform coating can be formed.

Abstract: A magnetic powder of an Sm—Fe—N alloy, which has a mean particle diameter of 0.5 to 10 &mgr;m, and either an average acicularity of 75% or above or an average sphericity of 78% or above. The powder exhibits an extremely high residual magnetization and an extremely high coercive force, since particles characterized by the above acicularity or sphericity have particle diameters approximately equal to that of the single domain particle and nearly spherical particle shapes. The powder can be produced by preparing an Sm—Fe oxide by firing a coprecipitate corresponding to the oxide, mixing the obtained oxide with metallic calcium and subjecting the mixture to reduction/diffusion and nitriding successively.

Abstract: A fine powder of metallic copper, suitable as a material for electroconductive pastes, and having a BET diameter of 3 &mgr;m or less, large crystallite size, high dispersibility and particles of high sphericity and a process for producing the same. More specifically, a fine powder of metallic copper having a BET diameter of 3 &mgr;m or less, particles of high sphericity and crystallites of 0.1 to 10 &mgr;m in size, and more preferably containing oxygen at 0.3% by weight or less. Moreover, the fine powder of metallic copper can be produced stably and efficiently by blowing an ammonia-containing gas onto molten copper kept at 1120° C. More specifically, it can be produced more stably and efficiently by blowing ammonia at 0.015 L/minute or more per unit area (cm2) of the molten copper.

Abstract: Methods for making hydrogen storage tanks may include disposing a substantially solid block of hydrogen-absorbing alloy within an activation vessel. Hydrogen gas may then be introduced into the activation vessel under conditions that will cause the hydrogen-absorbing alloy to absorb hydrogen and crack or break apart. Preferably, a substantially powdered hydrogen-absorbing alloy is formed thereby. Thereafter, the substantially powdered hydrogen-absorbing alloy can be transferred from the activation vessel to a hydrogen storage tank without substantially exposing the powered hydrogen-absorbing alloy to oxygen. The hydrogen-absorbing alloy is preferably ingot-shaped when introduced into the activation vessel. Further, the substantially powdered hydrogen-absorbing alloy is preferably produced by continuously breaking the ingot-shaped hydrogen-absorbing alloy within the activation vessel due to volume expansion caused by the hydrogen-absorbing alloy having absorbed hydrogen.

Abstract: To produce a hydrogen absorbing alloy powder, a starting powder and a plurality of balls are thrown into a container of a ball mill, and then, the inside of the container is maintained in a hydrogen atmosphere to conduct a mechanical alloying.

Abstract: The cost-effective titanium powder is manufactured by (a) magnesium-thermic reduction of titanium chlorides characterized by the formation of a hollow block of the reaction mass having an open cavity in the center of the block, (b) thermal-vacuum separation of the hollow block from excessive Mg and MgCl2 at 850-950° C. and residual pressure of 10−2-10−3 mm Hg, (c) cooling of obtained titanium hollow block in a H2-contained atmosphere at an excessive hydrogen pressure, (d) crushing the hydrogenated titanium block, (e) grinding the crushed titanium pieces into the powder combined with a hydro-metallurgical treatment of obtained titanium powder in a diluted aqueous solution of at least one chloride selected from magnesium chloride, sodium chloride, potassium chloride, or titanium chloride, and (f) drying and, optionally dehydrating the titanium powder ground to a predetermined particle size.

Abstract: A process for producing metallic powders a chlorination step for continuously producing chloride gas of metal by reacting metal with chlorine gas, and a reduction step for continuously reducing the metallic chloride gas by reacting the metallic chloride gas produced in the chlorination step with reducing gas. Regulating the feed rate of the chlorine gas can control the feed rate of the metallic chloride gas, whereby the particle diameters of produced metal powders can be stably controlled. Thus, the invention can make the particle diameters stable and arbitrarily control the diameters in the range of 0.1 to 1.0 &mgr;m.

Abstract: A procedure for making zinc particles of a size, shape and composition such that the particles can be subsequently used in a process for manufacturing zinc parts from such particles in either molten or powder form includes the initial step of heating zinc to a temperature at least as high as 720.degree. C. The molten zinc is passed through a screen having small openings, on the order of about 1/4".times.1/4" into a cooling region formed by a movable surface which is at a temperature of on the order of about -200.degree. C. The zinc forms small particles as it passes through the openings in the screen and essentially instantaneously solidifies as it contacts the movable surface. Thereafter, the solidified zinc particles are subjected to a grinding process to reduce their size to a powder having a surface area in the range of 2 mm.sup.2 to 20 mm.sup.2.

Abstract: A method for preparing controlled phase alloys useful for engineering and hydrogen storage applications. This novel method avoids melting the constituents by employing vapor transport, in a hydrogen atmosphere, of an active metal constituent, having a high vapor pressure at temperatures .apprxeq.300 C. and its subsequent condensation on and reaction with the other constituent (substrate) of an alloy thereby forming a controlled phase alloy and preferably a single phase alloy. It is preferred that the substrate material be a metal powder such that diffusion of the active metal constituent, preferably magnesium, and reaction therewith can be completed within a reasonable time and at temperatures .apprxeq.300 C. thereby avoiding undesirable effects such as sintering, local compositional inhomogeneities, segregation, and formation of unwanted second phases such as intermetallic compounds.

Abstract: A method of producing iron powder comprises the step of providing a supply of iron oxide powder of a size less than 1000 microns which is then heated in a reducing agent atmosphere to a temperature between 1000.degree. F. and 2100.degree. F., thus resulting in the iron oxide powder being reduced to iron powder, cooling the iron powder in an inert gas atmosphere to a temperature below 150.degree. F. and milling to a median particle size diameter of less than or equal to 20 microns.

Abstract: A hydrogen occluded alloy and a process for producing the above alloy are disclosed. The above process mechanically forms the hydrogen occluded alloy having improved initial discharging characteristics. In the above process, either a powdered LaNi.sub.5 alloy or rare earth metals, such as la, Ce, Pr and Nd, and a powdered CaCu.sub.5 alloy of Mm-Mn-Ni-Al-Co alloys is mixed with a powdered Laves alloy of Zr-Mn-V-Cr-Ni alloys into a powdered alloy mixture. Thereafter, the alloy mixture is applied with a mechanical impact by a high energy ball mill with an attritor, thereby mechanically forming the hydrogen occluded alloy. The above process easily controls the manganese component while producing the hydrogen occluded alloy through the mechanical alloying.

Abstract: A method for the manufacture of finely divided particles of palladium, palladium oxide or mixtures thereof comprising the sequential steps:A. Forming an unsaturated solution of thermally decomposable palladium-containing compound in a thermally volatilizable solvent;B. Forming an aerosol consisting essentially of finely divided droplets of the solution from step A. dispersed in an inert carrier gas;C. Heating the aerosol to an operating temperature above the decomposition temperature of the palladium-containing compound, but below the melting point of palladium metal by which finely divided particles of palladium, palladium oxide or mixtures thereof are formed and densified; andD. Separating the particles of palladium, palladium oxide or mixtures thereof from the carrier gas, reaction by-products and solvent volatilization products.

Abstract: The invention relates to a method for producing metal powders from reactive metals, when the employed raw materials are metal ions in a liquid phase. According to the invention, the metal ions are first reduced into metal in a molten salt electrolysis. The obtained reduction products are further subjected to a high-temperature treatment, for example by means of plasma, in order to improve the powder qualities of the metal. The metal to be treated is for instance titanium or zirconium.

Abstract: A process for producing salt free titanium powder by reacting zinc and a titanium halide in the presence of a reducing agent to form a solid zinc titanium product. Titanium halide vapor is introduced into a liquid alloy of zinc and the reducing agent at a temperature between 650.degree.-907.degree. C. The titanium halide is introduced beyond the titanium solubility limit in zinc to precipitate a zinc titanium intermetallic compound and also produce a liquid halide salt. The intermetallic compound forms and accumulates at an interface between the salt and liquid alloy. The compound is periodically removed from the interface, crushed into a powder, and the zinc is evaporatively separated from the titanium to produce pure titanium powder. The process preferably occurs above the peritectic decomposition temperature of Zn.sub.3 Ti, and most preferably above the peritectic decomposition temperature of Zn.sub.2 Ti, to maximize the titanium content of the resulting product.

Abstract: A method is disclosed for producing an agglomerated molybdenum plasma spray powder with a controlled level of oxygen which comprises forming a relatively uniform mixture of agglomerated powders containing molybdenum dioxide and one or more ammonium-containing compounds of molybdenum wherein the mixture has an oxygen content of greater than about 25% by weight and reducing the mixture in a moving bed furnace at a temperature of from about 700.degree. C. to about 1000.degree. C. for a sufficient time to remove a portion of the oxygen therefrom and form reduced molybdenum powder agglomerates having an oxygen content of no greater than about 25% by weight. The reduction takes place in the direction from the outside surface of the agglometates to the inside surface.

Abstract: A process for producing finely divided spherical iron group based metallic powders comprises forming an aqueous solution containing a source of the appropriate metal sources in a mineral acid, forming a reducible iron group based material from the solution, reducing the material to iron group based metal powder particles, subjecting the metal particles to a high temperature zone to melt a portion of the particles and to form droplets and cooling the droplets to form an essential spherical iron group based metallic powders.

Abstract: The process for producing crushed zirconium sponge having particle configurations which enhance its compactability, wherein conventionally produced, as-reduced, non-sintered zirconium sponge pieces are loaded into a vacuum furnace, the furnace is heated under partial vacuum at a temperature of up to about 400.degree. C. for a sufficient period to essentially demoisturize and degas the sponge, the temperature is raised to at least about 700.degree. C. and the vacuum terminated, H.sub.2 is fed in a carefully controlled manner into the furnace over a period of several hours in a total amount comprising from about 0.05 to about 0.8% by weight of the sponge, the furnace is cooled, the cooled sponge is pacified, the sponge is removed from the furnace and crushed, the crushed sponge is loaded into a vacuum furnace, the furnace is heated at from about 950.degree. C. to about 1100.degree. C.