Including Comminution Patents (Class 75/354)
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Patent number: 10185683Abstract: A bus interface system is disclosed that includes a master bus controller and a slave bus controller that are coupled by a bus line. The slave bus controller includes a decoder that allows for data to be transmitted along just the bus line. The decoder includes an oscillator, a first counter, and a comparison circuit. The oscillator is configured to be enabled by data pulses defined by the input data signal and generate oscillation pulses while enabled. The first counts the oscillation pulses and indicates a number of the oscillation pulses generated during a time slot. The comparison circuit is configured to this number with a reference number and generate a data output that represents a first logical value in response to the number being greater than the reference parameter and represents a second logical value in response to the number being less than the reference parameter.Type: GrantFiled: December 18, 2014Date of Patent: January 22, 2019Assignee: Qorvo US, Inc.Inventors: Christopher Truong Ngo, Alexander Wayne Hietala, Christian Rye Iversen, Ruediger Bauder
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Patent number: 10030450Abstract: A polycrystalline compact comprises a plurality of diamond grains of micron size, submicron size, or both, and a plurality of crushed diamond nanoparticles disposed in interstitial spaces between the plurality of diamond grains. A method of forming a polycrystalline compact comprises combining a plurality of micron and/or submicron-sized diamond grains and a plurality of crushed diamond nanoparticles to form a mixture and sintering the mixture in a presence of a binder to form a polycrystalline hard material comprising a plurality of inter-bonded diamond grains and diamond nanoparticles. Cutting elements comprising a polycrystalline compact and earth-boring tools bearing such compacts are also disclosed.Type: GrantFiled: July 3, 2013Date of Patent: July 24, 2018Assignee: Baker Hughes IncorporatedInventor: Anthony A. DiGiovanni
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Patent number: 9068250Abstract: A high-strength, pre-coated, titanium or titanium-alloy material component is provided that includes a titanium or titanium-alloy material article having ultra-fine, submicron grain size microstructure and an organic coating of phenolic resin applied to the surface of the article. The article is prepared from a coarse grain titanium or titanium-alloy powder material that is cryomilled into an ultra-fine, submicron grain material, degassed, and densified. The densified material is formed or otherwise processed into a article, and pre-coated with an organic coating containing phenolic resin prior to installation or assembly.Type: GrantFiled: October 8, 2010Date of Patent: June 30, 2015Assignee: The Boeing CompanyInventor: Steven G. Keener
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Publication number: 20150099183Abstract: Electrodes employing as active material metal nanoparticles synthesized by a novel route are provided. The nanoparticle synthesis is facile and reproducible, and provides metal nanoparticles of very small dimension and high purity for a wide range of metals. The electrodes utilizing these nanoparticles thus may have superior capability. Electrochemical cells employing said electrodes are also provided.Type: ApplicationFiled: March 19, 2014Publication date: April 9, 2015Applicant: Toyota Motor Engineering & Manufacturing North America, Inc.Inventors: Nikhilendra Singh, Michael Paul Rowe
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Publication number: 20150096887Abstract: Electrodes employing as active material iridium nanoparticles synthesized by a novel route are provided. The nanoparticle synthesis is facile and reproducible, and provides iridium nanoparticles of very small dimension and high purity for a wide range of metals. The electrodes utilizing these nanoparticles have excellent efficiency catalyzing the electrolytic production of oxygen from water.Type: ApplicationFiled: July 10, 2014Publication date: April 9, 2015Inventors: Kenneth J. McDonald, Michael Paul Rowe
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Publication number: 20150099118Abstract: Electrodes for metal-air batteries and the metal-air batteries employing such electrodes are provided. The electrodes include metal nanoparticles synthesized via a novel route. The nanoparticle synthesis is facile and reproducible, and provides metal nanoparticles of very small dimension and high purity for a wide range of metals. The electrodes utilizing these nanoparticles thus may have superior capability. Electrochemical cells employing said electrodes are also provided.Type: ApplicationFiled: June 17, 2014Publication date: April 9, 2015Inventors: Fuminori Mizuno, Michael Paul Rowe, Ryan Daniel Desautels
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Patent number: 8979972Abstract: Disclosed herein is a method of manufacturing a metal flake, including the steps of: applying metal ink containing an organic metal compound onto a substrate; calcining the metal ink applied on the substrate to form a thin metal film; separating the formed thin metal film from the substrate; and pulverizing the separated thin metal film. The method of manufacturing a metal flake is characterized in that the thickness and size of metal flakes can be easily adjusted, metal flakes having excellent conductivity and gloss can be obtained, and metal flakes can be mass-produced using environmentally friendly and economical methods.Type: GrantFiled: August 24, 2009Date of Patent: March 17, 2015Assignee: Inktec Co., Ltd.Inventors: Kwang Choon Chung, Hyun Nam Cho, Dong Rip Kim, Ji Hoon Yoo
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METHOD FOR MANUFACTURING METAL NANOPOWDER BY WIRE-EXPLOSION AND APPARATUS FOR MANUFACTURING THE SAME
Publication number: 20150000469Abstract: There are provided a method and an apparatus for manufacturing a metal nanopowder having a uniform particle size distribution by uniformly applying current to a center portion of the metal wire and a surface portion thereof. The method includes increasing a surface roughness of a metal wire; supplying the metal wire having the increased surface roughness to an electrode in a reaction chamber; and wire-exploding the metal wire by supplying electrical energy to the electrode.Type: ApplicationFiled: September 17, 2013Publication date: January 1, 2015Applicant: SAMSUNG ELECTRO-MECHANICS CO., LTD.Inventors: Sung Ho LEE, Kwan LEE, Jung Wook SEO -
Patent number: 8911529Abstract: Low cost spherical titanium and titanium powder alloy powder is produced by impinging a stream of an inert gas, such as argon, on the surface of a molten pool of titanium or sponge and alloying elements.Type: GrantFiled: April 13, 2012Date of Patent: December 16, 2014Assignee: Materials & Electrochemical Research Corp.Inventors: James C. Withers, Raouf O. Loutfy
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Publication number: 20140202286Abstract: A metal powder production method and a metal powder production device capable of reducing the size of the device, reducing costs, and obtaining spherical metal powder are provided. Supply means supplies a downward flow of molten metal, and a plurality of jet burners emit flame jets to the downward flow of the molten metal supplied from the supply means. Each of the jet burners is provided to emit the flame jet from the same angle and from each of positions rotationally symmetrical with each other with respect to the downward flow of the molten metal.Type: ApplicationFiled: May 18, 2012Publication date: July 24, 2014Applicants: HARD INDUSTRY YUGEN KAISHA, TOHOKU TECHNO ARCH CO., LTD.Inventors: Yoshihiko Yokoyama, Takuichi Yamagata, Torao Yamagata
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Patent number: 8734714Abstract: The present invention discloses a method for recovering rare earth particulate material from an assembly comprising a rare earth magnet and comprises the steps of exposing the assembly to hydrogen gas to effect hydrogen decrepitation of the rare earth magnet to produce a rare earth particulate material, and separating the rare earth particulate material from the rest of the assembly. The invention also resides in an apparatus for separating rare earth particulate material from an assembly comprising a rare earth magnet. The apparatus comprises a reaction vessel having an opening which can be closed to form a gas-tight seal, a separation means for separating the rare earth particulate material from the assembly, and a collection means for collecting the rare earth particulate material. The reaction vessel is connected to a vacuum pump and a gas control system, and the gas control system controls the supply of hydrogen gas to the reaction vessel.Type: GrantFiled: June 27, 2011Date of Patent: May 27, 2014Assignee: The University of BirminghamInventors: Ivor Rex Harris, Andrew Williams, Allan Walton, John Speight
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Patent number: 8702836Abstract: The invention relates to a method of forming solid particles from a sample, which includes the step of exposing the sample to a focused acoustic field having an acoustic wave variable, until the solid particles achieve a desired state of particularization. The acoustic wave variable may be selected based, at least in part, on the desired state of particularization. The sample may be exposed to the focused acoustic field through a medium.Type: GrantFiled: November 20, 2007Date of Patent: April 22, 2014Assignee: Covaris, Inc.Inventors: James A. Laugharn, Jr., Edwin Rudd
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Patent number: 8657915Abstract: The present invention provides a metal powder composed of tantalum or niobium that achieves both sinterability and fluidity and the manufacturing method thereof. The present invention also provides a tantalum or niobium powder that enables the manufacturing of an anode for a solid electrolytic capacitor in which holes are formed for a conductive polymer-containing solution to pass through, without using a hole molding material or pore forming material. Furthermore, the present invention provides an anode for a solid electrolytic capacitor that enables the manufacturing of a high-volume and low ESR solid electrolytic capacitor. The present invention further provides a manufacturing method of a metal powder that allows the manufacturing of a metal powder of a given diameter range from a raw powder at high yield, without requiring a lot of work and time.Type: GrantFiled: May 31, 2006Date of Patent: February 25, 2014Assignee: Global Advanced Metals Japan, K.K.Inventors: Yujiro Mizusaki, Isao Sugiyama, Hitoshi Iijima, Osamu Kubota
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Publication number: 20130313309Abstract: A conductive bonding material includes: a solder component including a metal foamed body of a first metal having at least one pore, the pore absorbs melted first metal when the metal foamed body is heated at a temperature higher than the melting point of the first metal, and a second metal having a melting point lower than the melting point of the first metal.Type: ApplicationFiled: March 28, 2013Publication date: November 28, 2013Inventors: Masayuki KITAJIMA, Takatoyo YAMAKAMI, Takashi KUBOTA, Kuniko ISHIKAWA
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Patent number: 8545596Abstract: The invention concerns alloyed zinc powders for alkaline batteries and a method to manufacture such powders. The powders are characterized by the presence of particles pierced with at least one hole. This appears to benefit the high drain discharge capacity while preserving the process ability of the powder, and the shelf life and the gassing behavior of the batteries. The invented powders can be manufactured using centrifugal atomization in a cooled, oxygen-depleted atmosphere.Type: GrantFiled: November 29, 2011Date of Patent: October 1, 2013Assignee: UmicoreInventors: Christophe Henninot, Yvan Strauven
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Publication number: 20130209308Abstract: A method of making a nanoscale metallic powder is disclosed. The method includes providing a base material comprising a metallic compound, wherein the base material is configured for chemical reduction by a reductant to form a metallic material. The method also includes forming a powder of the base material, the powder comprising a plurality of powder particles, the powder particles having an average particle size that is less than about 1 micron. The method further includes disposing the powder particles into a reactor together with the reductant under an environmental condition that promotes the chemical reduction of the base material and formation of a plurality of particles of the metallic material.Type: ApplicationFiled: February 15, 2012Publication date: August 15, 2013Applicant: Baker Hughes IncorporatedInventors: Oleg A. Mazyar, Michael H. Johnson, David Ernest Rodrigues
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Publication number: 20120291593Abstract: The present invention relates to the tantalum powder and the process for preparing the same, and also relates to the electrolytic capacitor anode made of the tantalum powder. More particularly, the present invention relates to the tantalum powder having a BET surface area not more than 0.530 m2/g, Fisher mean particle size not less than 3.00 ?m. The present invention relates to the process for preparing the tantalum powder, wherein the tantalum powder is prepared through reducing tantalum compound with a reducing agent, wherein the tantalum powder as seed is added during reduction, and said tantalum powder as seed is the tantalum powder that has been milled.Type: ApplicationFiled: August 2, 2012Publication date: November 22, 2012Inventors: Guoqi Yang, Wenfeng Shi, Xifang Bao, Yong Li, Zhongxiang Li, Zhangong Dong, Xiaoyan Yang
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Patent number: 8273149Abstract: The present invention provides a nanowire production method that is simpler than conventional nanowire production methods, and that makes it easier to control the size and shape of the nanowires by using a technique completely different from the conventional ones. A powder particle containing a metal element is divided into nanometer-size wires containing the metal element by irradiating a suspension of the powder particles with a femtosecond laser. The present invention also makes it possible to divide the nanometer-size wires thus formed into nanometer-size particles containing the metal element by irradiating further the nanometer-size wires with the femtosecond laser.Type: GrantFiled: June 20, 2007Date of Patent: September 25, 2012Assignee: Kyoto UniversityInventors: Yasuhiko Shimotsuma, Kiyotaka Miura, Kazuyuki Hirao, Mitsuo Kawasaki, Osamu Kajita, Takafumi Iwamoto, Eitaro Yasuda, Shigeyuki Kimura
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Patent number: 8257464Abstract: The present invention relates to pulverulent materials suitable for storing hydrogen, and more particularly to a method of preparing such a material, in which: (A) a composite metallic material having a specific granular structure is prepared by co-melting the following mixtures: a first metallic mixture (m1), which is an alloy (a1) of body-centered cubic crystal structure, based on titanium, vanadium, chromium and/or manganese, or a mixture of these metals in the proportions of the alloy (a1); and a second mixture (m2), which is an alloy (a2), comprising 38 to 42% zirconium, niobium, molybdenum, hafnium, tantalum and/or tungsten and 56 to 60 mol % of nickel and/or copper, or else a mixture of these metals in the proportions of the alloy (a2), with a mass ratio (m2)/(m1+m2) ranging from 0.1 wt % to 20 wt %; and (B) the composite metallic material thus obtained is hydrogenated, whereby the composite material is fragmented (hydrogen decrepitation).Type: GrantFiled: February 22, 2007Date of Patent: September 4, 2012Assignee: Centre National de la Recherche Scientifique (C.N.R.S.)Inventors: Jean Charbonnier, Patricia De Rango, Daniel Fruchart, Salvatore Miraglia, Sophie Rivoirard, Natalia Skryabina
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Publication number: 20120111148Abstract: In certain embodiments, a material comprising one or more semiconductive substances is vaporized to generate a vapor phase condensate. The vapor phase condensate is allowed to form nanoparticles. The nanoparticles are annealed to yield substantially spherical nanoparticles.Type: ApplicationFiled: November 8, 2010Publication date: May 10, 2012Applicant: Raytheon CompanyInventor: Kalin Spariosu
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Publication number: 20120103134Abstract: It is described a manganese pellet production from non-calcinated manganese ore, comprising the following phases: (a) ore size preparation through ore classification by function of particle size, smaller or equal to 1 mm particles being maintained from the ore particle fraction process so as to have a smaller or equal to 1 mm size, as well as the comminution of these particles; (b) flux addition; (c) agglomerant addition; (d) pelletizing resulting in crude pellets; and (e) thermal processing through crude pellet drying, pre-heating and heating.Type: ApplicationFiled: July 27, 2009Publication date: May 3, 2012Applicant: VALE S.A.Inventors: Washington Luiz Mafra, João Batista Conti de Souza
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Publication number: 20120096989Abstract: The invention concerns alloyed zinc powders for alkaline batteries and a method to manufacture such powders. The powders are characterized by the presence of particles pierced with at least one hole. This appears to benefit the high drain discharge capacity while preserving the process ability of the powder, and the shelf life and the gassing behavior of the batteries. The invented powders can be manufactured using centrifugal atomization in a cooled, oxygen-depleted atmosphere.Type: ApplicationFiled: November 29, 2011Publication date: April 26, 2012Applicant: UMICOREInventors: Christophe HENNINOT, Yvan STRAUVEN
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Patent number: 8118906Abstract: A method of recycling ruthenium (Ru) and Ru-based alloys comprises steps of: providing a solid body of Ru or a Ru-based alloy; segmenting the body to form a particulate material; removing contaminants, including Fe, from the particulate material; reducing the sizes of the particulate material to form a powder material; removing contaminants, including Fe, from the powder material; reducing oxygen content of the powder material to below a predetermined level to form a purified powder material; and removing particles greater than a predetermined size from the purified powder material. The purified powder material may be utilized for forming deposition sources, e.g., sputtering targets.Type: GrantFiled: October 29, 2007Date of Patent: February 21, 2012Assignee: Heraeus Inc.Inventors: Wuwen Yi, William Heckman, Bernd Kunkel, Carl Derrington, Patrick Griffin
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Patent number: 8101006Abstract: A centrifugal impact atomization process for producing zinc or zinc alloy powder from molten zinc. A stream of molten zinc is injected onto the surface of a spinning disk contained within an atomization chamber. The disk has a cup shaped cavity having an open end, opposing closed end and integral side walls. The disk may have baffles protruding into the open cavity core within the disk. The baffles may have straight or curved side surfaces. The disk is rotated at high speeds between about 10,000 and 15,000 rpm (revolutions per minute). The oxygen content in the chamber is preferably between about 1 and 6 vol %. Zinc powder is produced having more smaller size particles. Zinc alkaline cells utilizing such zinc product as anode active material show improved performance, especially as power source in high discharge services such as digital cameras.Type: GrantFiled: April 22, 2008Date of Patent: January 24, 2012Assignee: The Gillette CompanyInventors: Michael J. Zuraw, Peter B. Harris
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Patent number: 8088193Abstract: A method for making nanoparticles includes the steps of dipping a metal element in a solution that contains metallic ions or ions with a metal, wherein the metal element has a lower electronegativity or redox potential than that of the metal in the ions, and rubbing the metal element to make nanoparticles. Another method for making nanoparticles includes the steps of dipping a metal element in a solution that contains metallic ions or ions with a metal, wherein the metal element has a lower electronegativity or redox potential than that of the metal in the ions, and applying sonic energy to at least one of the metal element and solution. A further method for making copper nanoparticles includes the step of adding ascorbic acid to a copper salt solution.Type: GrantFiled: December 17, 2007Date of Patent: January 3, 2012Inventors: Taofang Zeng, Chunwei Wu
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Publication number: 20110283835Abstract: A metal powder manufacturing device for manufacturing a metal powder includes a feed for supplying a molten metal, a fluid spout unit, and a course modification unit. The fluid spout unit further includes a channel and an orifice. The channel is provided below the feed, allowing passing of the molten metal supplied from the feed. The orifice is opened at a bottom end of the channel, spouting a fluid into the channel. The above course modification unit is provided below the fluid spout unit, and forcibly changes the traveling direction of a dispersion liquid. This dispersion liquid is composed of multiple fine droplets dispersed into the fluid. The above droplets are a resultant of a breakup caused by a contact between the molten metal and the fluid ejected from the orifice. Here, the dispersion liquid is transported so that the droplets is cooled and solidified in the dispersion liquid in order to manufacture the metal powder.Type: ApplicationFiled: August 3, 2011Publication date: November 24, 2011Applicant: SEIKO EPSON CORPORATIONInventor: Atsushi WATANABE
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Patent number: 8034156Abstract: A method for producing a decomposer of an organic halogenated compound comprises subjecting an iron powder produced beforehand to plastic deformation that gives the iron powder particles a flat shape. Further, an iron powder and a copper salt powder are mechanically mixed in a ball mill to produce a copper salt-containing iron particle powder in which the particles of the two powders are joined. In this case, the method for producing the decomposer of an organic halogenated compound is characterized in that the iron powder is mechanically deformed to give the particles a flat shape.Type: GrantFiled: March 22, 2006Date of Patent: October 11, 2011Assignee: Dowa Eco-System Co., Ltd.Inventors: Masami Kamada, Taishi Uehara
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Publication number: 20110233480Abstract: There is provided a producing method of metal fine particles or metal oxide fine particles for producing metal fine particles or metal oxide fine particles by atomizing raw materials by performing processes including an oxidizing process and a reducing process to the raw materials composed of metal or a metal compound.Type: ApplicationFiled: March 23, 2011Publication date: September 29, 2011Applicants: HITACHI CABLE, LTD., TOHOKU UNIVERSITYInventors: Yamato HAYASHI, Yoshihiro SEKIGUCHI, Hirotsugu TAKIZAWA, Dai ISHIKAWA, Tomiya ABE
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Publication number: 20110011207Abstract: A metal powder production system includes a vacuum chamber having a vacuum chamber interior, a stock feed mechanism communicating with the vacuum chamber interior, a radiation source provided in the vacuum chamber interior, a cooling chamber having a cooling chamber interior communicating with the vacuum chamber interior and a container communicating with the cooling chamber interior. A metal powder production method is also disclosed.Type: ApplicationFiled: September 28, 2010Publication date: January 20, 2011Inventor: Victor Blakemore Slaughter
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Patent number: 7871537Abstract: A method for fabricating a magnesium-based hydrogen storage material according to the present invention comprises a) forming a mixture of a magnesium hydride powder and a transition metal halide powder, b) adding the mixture and balls into a vessel, c) filling the vessel with an inert gas or hydrogen, and d) subjecting the mixture to high energy ball milling.Type: GrantFiled: November 14, 2007Date of Patent: January 18, 2011Assignee: Korea Institute of Science and TechnologyInventors: Jae-Hyeok Shim, Seon-Ah Jin, Young-Whan Cho
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Publication number: 20100294079Abstract: The present invention provides a method and facility for preventing crumbling and powderization of green pellets when producing high strength green pellets using a powder feedstock and using the pellets in a rotary hearth reducing furnace and for efficiently reducing the same. It comprises kneading by a kneader 5 a feedstock of a powder of a fine particle size (20 to 80 wt % having size of not more than 10 ?m) including a metal oxide and carbon-bearing powder fed from a feed storage tank 1 and producing green pellets by a pan type pelletizer 7. The green pellets are screened by a pellet screen 9, then dried by a pellet dryer 11 and reduced by firing in a rotary hearth reducing furnace 13. At that time, the green pellets are continuously conveyed to prevent crumbling.Type: ApplicationFiled: July 29, 2010Publication date: November 25, 2010Applicant: Nippon Steel CorporationInventors: Tetuharu Ibaraki, Hiroshi Oda, Shoji Imura, Masaharu Takahashi
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Patent number: 7829014Abstract: The invention is a high-strength, pre-coated, titanium or titanium-alloy material component comprising a titanium or titanium-alloy material article having ultra-fine, submicron grain size microstructure and an organic coating of phenolic resin applied to the surface of the article. The article is prepared from a coarse grain titanium or titanium-alloy powder material that is cryomilled into an ultra-fine, submicron grain material, degassed, and densified. The densified material is formed or otherwise processed into a article, and pre-coated with an organic coating containing phenolic resin prior to installation or assembly.Type: GrantFiled: November 5, 2004Date of Patent: November 9, 2010Assignee: The Boeing CompanyInventor: Steven G. Keener
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Publication number: 20100272888Abstract: In a method for producing a starting material (M, N, N?) for the production of a wear layer (420), a coating (40) with a composition which corresponds to that of the wear layer (420) which is to be produced is chemically undissolved from its substrate (30) and is detached as a solid body, and that the starting material (M, N, N?) is formed by the layer material (60) of the detached coating (40).Type: ApplicationFiled: July 9, 2007Publication date: October 28, 2010Inventors: Rene Jabado, Jens Dahl Jensen, Ursus Krüger, Daniel Körtvelyessy, Volkmar Lüthen, Ralph Reiche, Michael Rindler, Raymond Ullrich
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Publication number: 20100263766Abstract: A method according to one embodiment includes combining an amorphous iron-based alloy and at least one metal selected from a group consisting of molybdenum, chromium, tungsten, boron, gadolinium, nickel phosphorous, yttrium, and alloys thereof to form a mixture, wherein the at least one metal is present in the mixture from about 5 atomic percent (at %) to about 55 at %; and ball milling the mixture at least until an amorphous alloy of the iron-based alloy and the at least one metal is formed.Type: ApplicationFiled: April 20, 2009Publication date: October 21, 2010Inventors: Cheng Kiong Saw, William A. Bauer, Jor-Shan Choi, Sumner Daniel Day, Joseph C. Farmer
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Publication number: 20100226070Abstract: The present invention relates to the tantalum powder and the process for preparing the same, and also relates to the electrolytic capacitor anode made of the tantalum powder. More particularly, the present invention relates to the tantalum powder having a BET surface area not more than 0.530 m2/g, Fisher mean particle size not less than 3.00 ?m. The present invention relates to the process for preparing the tantalum powder, wherein the tantalum powder is prepared through reducing tantalum compound with a reducing agent, wherein the tantalum powder as seed is added during reduction, and said tantalum powder as seed is the tantalum powder that has been milled.Type: ApplicationFiled: March 5, 2010Publication date: September 9, 2010Inventors: Guoqi Yang, Wenfeng Shi, Xifang Bao, Yong Li, Zhongxiang Li, Zhangong Dong, Xiaoyan Yang
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Publication number: 20100167078Abstract: Disclosed are a method for fabricating nanopowders, nano ink containing the nanopowders and micro rods, and nanopowders containing nanoparticles, nano clusters or mixture thereof, milled from nano fiber composed of at least one kind of nanoparticles selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, nano ink containing the nanopowders and microrods, the method comprising spinning a spinning solution containing at least one kind of precursor capable of composing at least one kind selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, crystallizing or amorphizing the spun precursor to produce nano fiber containing at least one kind of nanoparticles selected from a group consisting of metal, nonmetal, metal oxide, metal compound, nonmetal compound and composite metal oxide, and milling the nano fiber to fabricate nanopowders containing nanoparticles, nano clusters orType: ApplicationFiled: December 23, 2009Publication date: July 1, 2010Inventors: Il Doo KIM, Seung hun CHOI
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Patent number: 7601198Abstract: Ammonium hexachlororuthenate is produced by adding ammonium chloride to a hydrochloric acid solution containing ruthenium. The ammonium hexachlororuthenate is baked to obtain the ruthenium powder. When the moisture content of the ammonium hexachlororuthenate is high, the baked product is so hard sintered product that its pulverization is not easy. In accordance with the present invention, the following steps are carried out. Hydrochloric acid solution containing ruthenium is held at a temperature of 80 to 95° C. for three hours or longer. The ammonium chloride is then added to the hydrochloric acid solution which is stirred by a stirring mill at the rotation of 200 revolutions per minute or more. The hydrochloric acid solution is held at a temperature of from 85 to 95° C. for 1 hour while being stirred at 200 rpm. The resultant precipitate of ammonium hexachlororuthenate is filtered. The inventive crystals of precipitated ammonium hexachlororuthenate has 10 mass % or less of moisture content.Type: GrantFiled: January 28, 2008Date of Patent: October 13, 2009Assignee: Nippon Mining & Metals Co., Ltd.Inventors: Hifumi Nagai, Yuji Kawano
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Publication number: 20090193935Abstract: The present invention relates to the a method for manufacturing high strength ultra-fine/nano-structured aluminum/aluminum nitride or aluminum alloy/aluminum nitride composites using mechanical milling or mechanical alloying process which is conducted in the nitride-forming atmosphere such as nitrogen gas (N), ammonia gas (NH) or mixed gas including both gases, subsequent heat treatment process, and hot consolidation process. Also, high strength ultra-fine/nano-structured Al/ALN or Al alloy/ALN composite materials fabricated by the method of present invention have superior mechanical strength and heat resistance to those fabricated by conventional powder metallurgy process or liquid processes.Type: ApplicationFiled: May 30, 2006Publication date: August 6, 2009Applicant: Dynamaterials Co., Inc.Inventors: Kwang Seon Shin, Seung Hoon Yu
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Patent number: 7531022Abstract: A liquid for the preparation of powder mixtures on the basis of hard metals, comprising water and an inhibitor, wherein the inhibitor is in the form of at least one of the following materials: polyvinyllactam or wax emulsion, or the inhibitor is in the form of at least one of the following materials: carboxylic acid, amines or their derivatives.Type: GrantFiled: October 13, 2005Date of Patent: May 12, 2009Assignee: Zschimmer & Schwarz GmbH & Co. KG Chemische FabrikenInventors: Peter Quirmbach, Michael Hölzgen, Alfred Vuin
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Patent number: 7524355Abstract: A method is disclosed for producing an energetic metastable nano-composite material. Under pre-selected milling conditions a mixture of powdered components are reactively milled. These components will spontaneously react at a known duration of the pre-selected milling conditions. The milling is stopped at a time at which the components have been compositionally homogenized to produce nanocomposite powder, but prior to said known duration, and thereby before the spontaneous reaction occurs. The milled powder is recovered as a highly reactive nanostructured composite for subsequent use by controllably initiating destabilization thereof.Type: GrantFiled: November 12, 2004Date of Patent: April 28, 2009Assignee: New Jersey Institute of TechnologyInventors: Edward Leonid Dreizin, Mirko Schoenitz
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Publication number: 20090080145Abstract: The present invention provides a metal powder composed of tantalum or niobium that achieves both sinterability and fluidity and the manufacturing method thereof. The present invention also provides a tantalum or niobium powder that enables the manufacturing of an anode for a solid electrolytic capacitor in which holes are formed for a conductive polymer-containing solution to pass through, without using a hole molding material or pore forming material. Furthermore, the present invention provides an anode for a solid electrolytic capacitor that enables the manufacturing of a high-volume and low ESR solid electrolytic capacitor. The present invention further provides a manufacturing method of a metal powder that allows the manufacturing of a metal powder of a given diameter range from a raw powder at high yield, without requiring a lot of work and time.Type: ApplicationFiled: May 31, 2006Publication date: March 26, 2009Inventors: Yujiro Mizusaki, Isao Sugiyama, Hitoshi Iijima, Osamu Kubota
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Publication number: 20090074607Abstract: The present invention is directed to flotation of refractory gold sulfide ores in which the ore is ground, floated, the tailings reground, and refloated to produce gold-bearing concentrates.Type: ApplicationFiled: September 11, 2008Publication date: March 19, 2009Applicant: BARRICK GOLD CORPORATIONInventors: Daniel Hillier, Barun Gorain, Jacques McMullen
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Publication number: 20090068488Abstract: An object of the present invention is to provide a method for producing granulated metallic iron superior in rust resistance. Another object of the present invention is to provide a method for producing such granulated metallic iron. In the method, the granulated metallic iron is produced by agglomerating a material mixture including an iron-oxide-containing material and a carbonaceous reducing agent; charging and heating the agglomerated material mixture in a moving hearth-type reducing furnace to reduce the iron oxide in the material mixture with the carbonaceous reducing agent to obtain hot granulated metallic iron; and cooling the hot granulated metallic iron, wherein the hot granulated metallic iron is cooled while its relative position is changed; and an oxide coating is formed on the surface of the hot granulated metallic iron by bringing moisture into contact with almost the entire surface of the hot granulated metallic iron.Type: ApplicationFiled: March 24, 2006Publication date: March 12, 2009Applicant: Mesabi Nugget LLCInventors: Koji Tokuda, Osamu Tsuge
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Publication number: 20090025841Abstract: Surface-modified metal fuels, which improve the stability in storage of pyrotechnics and methods for manufacturing such fuels, are provided. Improved storage stability is conferred either by alloying the precursor metal prior to the powder production process, or by forming an enhanced stability coating on the surface of the metal powders during the powder production process.Type: ApplicationFiled: July 3, 2008Publication date: January 29, 2009Inventor: Paul Smith
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Publication number: 20080307925Abstract: This invention relates to a method for producing titanium by reaction of titanium tetrachloride with magnesium in a reactor, wherein the temperature in the reactor is above the melting point of magnesium and below the melting point of magnesium chloride, wherein the reaction results in formation of particles comprising titanium, and wherein the particles are removed from the reactor and processed in order to recover the titanium.Type: ApplicationFiled: October 14, 2005Publication date: December 18, 2008Applicant: COMMONWEALTH SCIENTIFIC AND INDUSTRIAL RESEARCH OR ORGANIZATIONInventors: Grant Ashley Wellwood, Christian Doblin
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Patent number: 7459007Abstract: The present invention provides a metallic composition, which includes a plurality of ultra-fine copper flakes having at least one desirable feature, such as oxidation resistance and excellent dispersibility in a non-aqueous system. Also provided is a method for forming compositions having a plurality of ultra-fine copper flakes, and the metallic composition produced therewith.Type: GrantFiled: March 15, 2005Date of Patent: December 2, 2008Assignee: Clarkson UniversityInventors: Dan V. Goia, Corina Goia
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Publication number: 20080264205Abstract: A method for making nanoparticles includes the steps of dipping a metal element in a solution that contains metallic ions or ions with a metal, wherein the metal element has a lower electronegativity or redox potential than that of the metal in the ions, and rubbing the metal element to make nanoparticles. Another method for making nanoparticles includes the steps of dipping a metal element in a solution that contains metallic ions or ions with a metal, wherein the metal element has a lower electronegativity or redox potential than that of the metal in the ions, and applying sonic energy to at least one of the metal element and solution. A further method for making copper nanoparticles includes the step of adding ascorbic acid to a copper salt solution.Type: ApplicationFiled: December 17, 2007Publication date: October 30, 2008Inventors: Taofang ZENG, Chunwei Wu
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Publication number: 20080233420Abstract: The present invention relates to a high-purity tantalum flake powder, produced by a hydride-dehydride process including: (a) cold working tantalum metal into a thin sheet; (b) hydriding the thin sheet, forming a brittle tantalum foil; (c) adjusting the tantalum foil to a desired particle size; and (d) removing hydrogen from the tantalum foil by vacuum sintering, forming a tantalum flake powder. In accordance with the present invention, tantalum flake is produced by sizing ultra-thin tantalum foil via the hydride-dehydride process. Tantalum is an extremely malleable metal and can be cold worked into extremely thin sheets less than 1 micron thick. Once hydrided, this foil is brittle, and can be easily sized by suitable milling processes. The hydrogen is removed by vacuum sintering, resulting in an extremely thin Ta metal flake.Type: ApplicationFiled: March 23, 2007Publication date: September 25, 2008Inventors: Colin G. McCracken, Scott M. Hawkins
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Patent number: 7407526Abstract: The invention concerns an iron powder for fortifying foodstuff. The powder consists of a reduced iron powder having irregularly shaped particles, wherein the iron powder has a ratio AD:PD less than 0.3, wherein AD is the apparent density in g/cm3, and PD is the particle density in g/cm3. The specific surface area of the powder particles is above 300 m2/kg as measured by the BET method and the average particle size is between 5-45 ?m.Type: GrantFiled: November 24, 2004Date of Patent: August 5, 2008Assignee: Höganäs ABInventors: Bo Hu, Fredrik Eklund, Nils Jonsson, Fredrik Persson
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Patent number: 7361204Abstract: Methods, systems and apparatus for producing a variable, known number of nanoparticles of various materials in an expanding mist in a vacuum or enclosure. The configurations allow for this mist of small particles to be produced in bursts, at repetition rates over a wide range of frequencies. The technique produces an isotropically expanding mist of particles. Direct applications of the invention can be used for the development of high power short wavelength incoherent light sources for applications in EUV lithography (EUVL), advanced microscopy, precision metrology, and other fields.Type: GrantFiled: November 5, 2004Date of Patent: April 22, 2008Assignee: Research Foundation of the University of Central FloridaInventors: Martin Richardson, Chiew-Seng Koay, Kazutoshi Takenoshita