Treating Molten Magnesium(mg) Patents (Class 75/600)
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Patent number: 11939644Abstract: A method for regenerating different types of copper-containing aluminum alloys using aluminum alloy scrap from aeronautical industry includes detecting a chemical composition of said aluminum alloy scrap and optionally adding a suitable amount of a metal or alloy additive according to a composition requirement of a target aluminum-copper alloy, thereby obtaining a mixture of aluminum alloy scrap and metal or alloy additive; vacuum smelting the mixture of aluminum alloy scrap and metal or alloy additive in a vacuum furnace, wherein impurities are removed and an aluminum alloy solution is formed; filtering the aluminum alloy solution using a filter to obtain a melt comprising a target aluminum alloy composition; and casting the target aluminum alloy composition from said melt.Type: GrantFiled: July 25, 2019Date of Patent: March 26, 2024Assignee: The Boeing CompanyInventors: Zhi Sun, Chunwei Liu, Xuan Wei, Hongbin Cao, Pengcheng Yan
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Patent number: 11229974Abstract: To enable welding in a state in which aluminum plating in a desired welding region is removed at a desired high accuracy, a plating layer (103) in a welding region (151) and a plating layer (104) in a welding region (152) are removed using an alkaline solution to form a preprocessed aluminum plated steel sheet (101a), and a plating layer (123) in a welding region (153) and a plating layer (124) in a welding region (154) are removed using an alkaline solution to form a preprocessed aluminum plated steel sheet (121a).Type: GrantFiled: November 18, 2016Date of Patent: January 25, 2022Assignee: G-TEKT CORPORATIONInventors: Shoko Ueno, Akihiko Uchida
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Patent number: 9181607Abstract: Provided are an apparatus and a method for producing an inexpensive Mg2Si1-xSnx polycrystal that can be effectively used as thermoelectric conversion materials that can be expected to have a high performance index by doping if necessary.Type: GrantFiled: March 16, 2011Date of Patent: November 10, 2015Assignees: IBARAKI UNIVERSITY, SHOWA KDE CO., LTD.Inventors: Haruhiko Udono, Yohiko Mito
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Patent number: 9169542Abstract: This invention aims to provide a recycled magnesium alloy having a good corrosion resistance and a process for producing the same. The process of the present invention comprises an adjusting step of adjusting composition of molten metal of a magnesium alloy so as to comprise, by mass: Al: 5 to 10%, Zn: not less than 1% and not less than three times of Cu content (%), Mn: 0.1 to 1.5% and the remainder: Mg and impurities with or without one or more reforming elements. While the upper limit of the Al content is restricted to a low level, the Zn content is increased in accordance with the Cu content. Therefore, the recycled magnesium alloy produced by this process can effectively suppress corrosion caused by Cu, which is one of corrosion-causing elements.Type: GrantFiled: June 9, 2010Date of Patent: October 27, 2015Assignees: KABUSHIKI KAISHA TOYOTA CHUO KENKYUSHO, TOYOTA JIDOSHA KABUSHIKI KAISHAInventors: Hiroyuki Kawabata, Naohisa Nishino, Sonoko Nishino, Yasushi Iwata, Yoshikazu Genma, Tsuyoshi Seguchi
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Patent number: 8932385Abstract: The disclosure provides a method and apparatus for inerting the surface of a metal charge in an induction furnace. The process generally involves use of a porous plug positioned near the surface of the metal charge. Argon (or other blanket gases) is flushed through the porous plug to back fill the volume of the induction furnace above the metal charge with an inert gas.Type: GrantFiled: October 26, 2011Date of Patent: January 13, 2015Assignee: Air Liquide Industrial U.S. LPInventor: Terence D. La Sorda
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Patent number: 8784579Abstract: A process of grain refining magnesium metal or magnesium based alloy including the step of a) providing a melt of the magnesium metal or magnesium based alloy, said melt including a grain refining agent in an amount effective to induce grain refinement of said magnesium or magnesium based alloy upon solidification, wherein the grain refining agent is vanadium metal, where said grain refinement comprises a reduction in average grain size of at least 50% (percent) as compared with the average grain size without addition of said grain refining agent.Type: GrantFiled: April 20, 2009Date of Patent: July 22, 2014Inventor: Joka Buha
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Patent number: 8668762Abstract: The present invention relates to a desulfurizing agent of improved oxidation resistance, ignition resistance and productivity, and a method for manufacturing the desulfurizing agent. The desulfurizing agent may include a plurality of magnesium-aluminum alloy grains with grain boundaries, and a compound of one selected from consisting of magnesium and aluminum and one selected from consisting of alkaline metal and alkaline earth metal, the compound exists in the grain boundaries and is not inside but outside of the magnesium-aluminum alloy grains.Type: GrantFiled: December 6, 2012Date of Patent: March 11, 2014Assignee: Korea Institute of Industrial TechnologyInventors: Shea Kwang Kim, Jung Ho Seo, Dong In Jang
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Publication number: 20140050608Abstract: A method for reducing impurities in magnesium comprises: combining a zirconium-containing material with a molten low-impurity magnesium including no more than 1.0 weight percent of total impurities in a vessel to provide a mixture; holding the mixture in a molten state for a period of time sufficient to allow at least a portion of the zirconium-containing material to react with at least a portion of the impurities and form intermetallic compounds; and separating at least a portion of the molten magnesium in the mixture from at least a portion of the intermetallic compounds to provide a purified magnesium including greater than 1000 ppm zirconium. A purified magnesium including at least 1000 ppm zirconium and methods for producing zirconium metal using magnesium reductant also are disclosed.Type: ApplicationFiled: August 14, 2012Publication date: February 20, 2014Applicant: ATI PROPERTIES, INC.Inventors: Scott Coffin, Arnel M. Fajardo
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Patent number: 8613789Abstract: A process for producing particle-reinforced composite materials through utilization of an in situ reaction to produce a uniform dispersion of a fine particulate reinforcement phase. The process includes forming a melt of a first material, and then introducing particles of a second material into the melt and subjecting the melt to high-intensity acoustic vibration. A chemical reaction initiates between the first and second materials to produce reaction products in the melt. The reaction products comprise a solid particulate phase, and the high-intensity acoustic vibration fragments and/or separates the reaction products into solid particles that are dispersed in the melt and are smaller than the particles of the second material. Also encompassed are particle-reinforced composite materials produced by such a process.Type: GrantFiled: November 10, 2011Date of Patent: December 24, 2013Assignee: Purdue Research FoundationInventors: Qingyou Han, Zhiwei Liu
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Patent number: 8540797Abstract: A method to introduce ceramic particles into liquid metal through the polymeric precursor route by cross-linking organic precursor into a hard polymer, which is added to the liquid melt for in-situ pyrolysis of the organic into the ceramic phase. The starting material, the organic, for the above process can be in the form of a liquid or a solid. If it is a solid it is usually dissolved into a solvent to create a liquid form. The organic is then cross linked either directly by a thermal process, by adding a catalyst, or by the well known sol-gel process into a hard polymer. It is this hard polymer which is then pyrolyzed into a high temperature ceramic material by the process outlined above.Type: GrantFiled: July 29, 2008Date of Patent: September 24, 2013Assignee: Indian Institute of ScienceInventors: Rishi Raj, Mirle Krishnegowda Surappa, Sudarshan
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Publication number: 20130199337Abstract: Provided are an apparatus and a method for producing an inexpensive Mg2Si1-xSnx polycrystal that can be effectively used as thermoelectric conversion materials that can be expected to have a high performance index by doping if necessary.Type: ApplicationFiled: March 16, 2011Publication date: August 8, 2013Inventors: Haruhiko Udono, Yohiko Mito
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Publication number: 20120301383Abstract: The present invention relates to new compositions of matter, particularly metals and alloys, and methods of making such compositions. The new compositions of matter exhibit long-range ordering and unique electronic character.Type: ApplicationFiled: March 20, 2012Publication date: November 29, 2012Inventor: Christopher J. Nagel
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Publication number: 20120156087Abstract: This invention aims to provide a recycled magnesium alloy having a good corrosion resistance and a process for producing the same. The process of the present invention comprises an adjusting step of adjusting composition of molten metal of a magnesium alloy so as to comprise, by mass: Al: 5 to 10%, Zn: not less than 1% and not less than three times of Cu content (%), Mn: 0.1 to 1.5% and the remainder: Mg and impurities with or without one or more reforming elements. While the upper limit of the Al content is restricted to a low level, the Zn content is increased in accordance with the Cu content. Therefore, the recycled magnesium alloy produced by this process can effectively suppress corrosion caused by Cu, which is one of corrosion-causing elements.Type: ApplicationFiled: June 6, 2010Publication date: June 21, 2012Applicants: TOYOTA JIDOSHA KABUSHIKI KAISHA, KABUSHIKI KAISHA TOYOTA CHUO KENKYUSHOInventors: Hiroyuki Kawabata, Naohisa Nishino, Sonoko Nishino, Yasushi Iwata, Yoshikazu Genma, Tsuyoshi Seguchi
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Patent number: 8202346Abstract: A method for filtering molten magnesium or magnesium alloys is provided. The method includes the steps of: providing an organic foam; impregnating the organic foam with a slurry comprising metal particles; heating the impregnated organic foam to a temperature sufficient to volatilize the organic foam thereby forming a porous metal foam comprising no more than 0.5 wt % nickel; sintering the porous metal foam; passing molten magnesium or magnesium alloy through the porous metal foam thereby forming purified molten magnesium or magnesium alloy; and cooling the purified molten magnesium or magnesium alloy.Type: GrantFiled: June 24, 2009Date of Patent: June 19, 2012Assignee: Porvair, PLCInventor: Leonard S. Aubrey
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Publication number: 20110236249Abstract: Provided are a magnesium-based alloy and a manufacturing method thereof. In the method, a magnesium alloy is melted into liquid phase, and an alkaline earth metal oxide is added into a molten magnesium alloy. The alkaline earth metal oxide is exhausted through surface reduction reaction between the melt and the alkaline earth metal oxide. Alkaline earth metal produced by the exhaustion reacts with Mg and/or other alloying elements in the magnesium alloy so that an intermetallic compound is formed. The magnesium prepared by the method is excellent in fluidity and hot-tearing resistance. To this end, the alkaline earth metal oxide added is CaO, and the added amount of CaO is 1.4 to 1.7 times the target weight of Ca to be contained in the final Mg alloy.Type: ApplicationFiled: March 24, 2011Publication date: September 29, 2011Applicant: KOREA INSTITUTE OF INDUSTRIAL TECHNOLOGYInventors: Shae K. KIM, Jung-Ho SEO
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Patent number: 8016911Abstract: A method of using a protective gas composition comprising a fluorine-containing organic compound and a carrier gas for preventing a rapid oxidation or combustion of a molten magnesium/magnesium alloy alloy in a magnesium or magnesium alloy production process.Type: GrantFiled: June 28, 2010Date of Patent: September 13, 2011Assignee: Central Glass Company, LimitedInventors: Yasuo Hibino, Ryoichi Tamai, Satoru Okamoto, Fuyuhiko Sakyu
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Publication number: 20110036466Abstract: A process of grain refining magnesium metal or magnesium based alloy including the step of a) providing a melt of the magnesium metal or magnesium based alloy, said melt including a grain refining agent in an amount effective to induce grain refinement of said magnesium or magnesium based alloy upon solidification, wherein the grain refining agent is vanadium metal, where said grain refinement comprises a reduction in average grain size of at least 50% (percent) as compared with the average grain size without addition of said grain refining agent.Type: ApplicationFiled: April 20, 2009Publication date: February 17, 2011Inventor: JOKA BUHA
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Publication number: 20100326237Abstract: The present invention relates to new compositions of matter, particularly metals and alloys, and methods of making such compositions. The new compositions of matter exhibit long-range ordering and unique electronic character.Type: ApplicationFiled: February 23, 2010Publication date: December 30, 2010Inventor: Christopher J. Nagel
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Patent number: 7854787Abstract: A method is provided for removing a coating from a coated magnesium alloy product. The method includes a first treatment step of immersing the coated magnesium alloy product in a first alkaline solution, and a second treatment step of immersing the magnesium alloy product, which has undergone the first treatment step, in a second alkaline solution or in an acid solution. The second alkaline solution is different from the first alkaline solution.Type: GrantFiled: July 26, 2006Date of Patent: December 21, 2010Assignee: Fujitsu LimitedInventors: Kota Nishii, Koichi Kimura
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Patent number: 7550027Abstract: In order to provide a method for supplying a cover gas which has sufficient preventive effects of oxidation-combustion and prevents cost-increase by containing a necessary and sufficient amount of fluoroketone in the cover gas which is supplied in a melting furnace of magnesium, the present invention provides a method for supplying a cover gas containing fluoroketone in a melt furnace to prevent oxidation and combustion of a melt of magnesium in the melt furnace, wherein the moisture concentration of gas in the melt furnace is measured, and the concentration of fluoroketone in the cover gas is adjusted to a range from 1/50 to 1/5 relative to the moisture concentration.Type: GrantFiled: October 31, 2007Date of Patent: June 23, 2009Assignee: Taiyo Nippon Sanso CorporationInventors: Hiroshi Sanui, Yuji Nomura, Hidetoshi Ohta
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Publication number: 20080105087Abstract: In order to provide a method for supplying a cover gas which has sufficient preventive effects of oxidation-combustion and prevents cost-increase by containing a necessary and sufficient amount of fluoroketone in the cover gas which is supplied in a melting furnace of magnesium, the present invention provides a method for supplying a cover gas containing fluoroketone in a melt furnace to prevent oxidation and combustion of a melt of magnesium in the melt furnace, wherein the moisture concentration of gas in the melt furnace is measured, and the concentration of fluoroketone in the cover gas is adjusted to a range from 1/50 to 1/5 relative to the moisture concentration.Type: ApplicationFiled: October 31, 2007Publication date: May 8, 2008Applicant: TAIYO NIPPON SANSO CORPORATIONInventors: Hiroshi Sanui, Yuji Nomura, Hidetoshi Ohta
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Patent number: 6808679Abstract: A magnesium-based casting alloy having good salt-spray corrosion resistance and improved creep resistance, tensile yield strength and bolt-load retention, particularly at elevated temperatures of at least 150° C., is provided. The inventive alloy comprises, in weight percent, 2 to 9% aluminum and 0.5 to 7% strontium, with the balance being magnesium except for impurities commonly found in magnesium alloys. A method of making an oxidation-resistant alloy melt, and the alloy melt prepared by such a method, are also provided. The alloy melt comprises magnesium as a primary alloying metal, and aluminum and strontium as secondary alloying metals, while the inventive method comprises: melting the alloying metals under an atmosphere of an inert gas selected from a mixture of carbon dioxide and sulfur fluoride gas, a mixture of nitrogen and sulfur dioxide gas, and combinations thereof.Type: GrantFiled: November 27, 2001Date of Patent: October 26, 2004Assignee: Noranda, Inc.Inventors: Mihriban Ozden Pekguleryuz, Pierre Labelle, Pierre Vermette
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Publication number: 20040107799Abstract: In a method of melting metal of a predetermined liquidus temperature, particularly a non-iron metal, such as magnesium, in a heated melting chamber into which solid metal is introduced and where a stream is generated, the parameters of flow are chosen such that the melting time is, in maximum, half the melting time without this stream under the condition that the temperature of the molten metal, when measured at at least one place in a distance of 5 mm in maximum from the solid metal, does not fall below liquidus temperature. To this end, an apparatus may be provided comprising at least one pump in a melting chamber having an associated heating device. This pump sucks the melt through at least one inlet opening and discharges the melt through at least one outlet opening. Both inlet opening and outlet opening are arranged within the melt bath of the melting chamber.Type: ApplicationFiled: November 20, 2003Publication date: June 10, 2004Inventors: Erich Rauch, Alfred Sigmund
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Publication number: 20030226424Abstract: A method is provided for removing a coating from a coated magnesium alloy product. The method includes a first treatment step of immersing the coated magnesium alloy product in a first alkaline solution, and a second treatment step of immersing the magnesium alloy product, which has undergone the first treatment step, in a second alkaline solution or in an acid solution. The second alkaline solution is different from the first alkaline solution.Type: ApplicationFiled: November 18, 2002Publication date: December 11, 2003Applicant: FUJITSU LIMITEDInventors: Kota Nishii, Koichi Kimura
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Patent number: 6616729Abstract: A method of grain refining cast magnesium alloy includes adding to a magnesium alloy melt containing aluminum and manganese, pure carbon powder, or a carbon source in combination with niobium pentoxide or vanadium pentoxide.Type: GrantFiled: July 30, 2002Date of Patent: September 9, 2003Assignees: Seiko Idea Center Co., Ltd.Inventors: Tetsuichi Motegi, Kiichi Miyazaki, Yoshitomo Tezuka, Kiyotaka Yoshihara, Eiji Yano
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Patent number: 6607578Abstract: A continuous vacuum refining method of molten metals, wherein impurities in the molten metal are eliminated by evaporation by stirring the molten metal (1) in the molten liquid stirring part B in the evacuated and pre-heated vacuum chamber, the molten liquid is transferred from the stirring part B to the tapping part C in the chamber through connecting holes, the molten liquid is continuously guided into the vessel in the refined molten liquid recovery chambers (10a), (10b) through the recovery passageways (8a), (8b) connected to the tapping part C, the recovery chamber being evacuated and connected with the passageway, and the refined molten liquid (9) is recovered after returning the pressure to the atmospheric pressure, wherein the molten liquid is discharged using plural passageways and plural recovery chambers connected with the respective passageways with alternating the recovery chamber. An apparatus employed for this method.Type: GrantFiled: November 21, 2001Date of Patent: August 19, 2003Assignees: Kobe Steel, Ltd., Showa Denka K.K., Sky Aluminum Co., Ltd., Nippon Light Metal Company, Ltd., The Furukawa Electric Co., Ltd, Mitsubishi Aluminum Co., Ltd.Inventors: Mitsuhiro Otaki, Kensuke Mori
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Publication number: 20020121158Abstract: A continuous vacuum refining method of molten metals, wherein impurities in the molten metal are eliminated by evaporation by stirring the molten metal (1) in the molten liquid stirring part B in the evacuated and pre-heated vacuum chamber, the molten liquid is transferred from the stirring part B to the tapping part C in the chamber through connecting holes, the molten liquid is continuously guided into the vessel in the refined molten liquid recovery chambers (10a), (10b) through the recovery passageways (8a), (8b) connected to the tapping part C, the recovery chamber being evacuated and connected with the passageway, and the refined molten liquid (9) is recovered after returning the pressure to the atmospheric pressure, wherein the molten liquid is discharged using plural passageways and plural recovery chambers connected with the respective passageways with alternating the recovery chamber. An apparatus employed for this method.Type: ApplicationFiled: November 21, 2001Publication date: September 5, 2002Inventors: Mitsuhiro Otaki, Kensuke Mori
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Patent number: 5908488Abstract: The magnesium melting furnace (1) has a plurality of chambers. The material to be melted is fed into a melting chamber (2) through a charging chute (20), one end of which terminates under the surface of the melting bath. The melt is slowly transferred into a holding chamber (4) through a passage (3) situated in the lower third of a dividing wall (11) above a layer of impurities settling at the bottom (14) of the melting chamber (2). The melt slowly flows through the holding chamber (4), with impurities rising to the surface or settling on the bottom (15). The purified melt flows through a second passage (5) situated in the lower third of a second dividing wall (12) into a metering chamber (6). The melt can be removed from the metering chamber (6) through a transfer pipe (28) using a metering pump (27). The magnesium melting furnace (1) makes it possible to simultaneously melt, purify and remove the magnesium in metered quantities.Type: GrantFiled: July 2, 1996Date of Patent: June 1, 1999Assignees: Schmitz + Apelt LOI Industrieofenanlagen GmbH, Rauch Fertigungstechnik Ges. m.h.H.Inventors: Dominik Schroder, Erich Rauch
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Patent number: 5762680Abstract: An apparatus for distribution of magnesium or magnesium alloys from a central melting unit (2) into a casting shop with one or more casting machines (3) has a tube furnace (1) extending from a central melting unit (2) into the casting shop. The tube furnace (1) is equipped with outlets (6) at the top for the mounting of a transfer tube (7) for the supply of metal to one or more holding furnaces (4) arranged at each casting machine. The tube furnace is preferably placed inside a steel cover (8) and is positioned just beneath the metal level in the holding furnace (4). The tube furnace (1) and transfer tubes (7) are provided with heating elements (11) with an outer insulation (12). The transfer tubes (7) have an air inlet (9). Two or more tube furnaces could be placed in the steel cover (8). The metal is transferred by the act of gravity.Type: GrantFiled: September 24, 1996Date of Patent: June 9, 1998Assignee: Norsk Hydro a.s.Inventors: Olav Holta, H.ang.kon Westengen
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Patent number: 5536295Abstract: An apparatus for the processing of molten metal including a crucible furnace for receiving magnesium scrap and for converting the magnesium scrap into molten metal, a robotic arm positioned so as to extend into the molten metal in the crucible furnace and having a three-axis range of motion. The robotic arm has a connector formed thereon so as to receive a tool. The tool can be a pump which is connected to the robotic arm means so as to transfer the molten metal from the crucible furnace to another location. The pump includes a pump nozzle which is connected to the robotic arm and extends from the robotic arm into the molten metal, an outlet conduit fixedly positioned relative to the crucible furnace, and a pump connected to the pump nozzle and to the outlet conduit. A mixer member is attachable to the connector of the robotic arm to as to extend into the molten metal for the purpose of pushing the magnesium scrap into the molten metal.Type: GrantFiled: May 15, 1995Date of Patent: July 16, 1996Assignee: Garfield Alloys, Inc.Inventor: Charles M. Slovich
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Patent number: 5531806Abstract: A process for preparing a high strength magnesium alloy comprising heating a melt comprised of a base metal of magnesium, greater than 0.5% of lithium, and at least one alkali metal impurity selected from the group consisting of sodium, potassium, rubidium and cesium, the total alkali metal present in an amount greater than 5 ppm, to a temperature of about 50.degree. to 200.degree. C. above the melting point of alloy being refined in a vacuum for a sufficient time to reduce the aggregate concentration of alkali metal impurities in the melt to less than about 5 ppm as measured by GDMS.Type: GrantFiled: April 19, 1995Date of Patent: July 2, 1996Assignee: Comalco Aluminium LimitedInventor: Donald Webster