Abstract: A resonator assembly for executing measurements on a sample within a constant magnetic field B0 by means of magnetic resonance is disclosed. It comprises a resonator portion defining a longitudinal axis and an axial direction. The resonator portion has, along the axial direction, a hollow cavity for exciting electron resonance within the sample. A coupling portion is provided adjacent the resonator portion and has, along the longitudinal axis, a stepped through being electrically conductive at its inner surface. A first, middle section of the stepped through configures the hollow cavity. A second and a third, lateral section adjacent axially opposed sides of the hollow cavity are each dimensioned such that a basic mode being resonant within the hollow cavity is unable to propagate within the second and the third section. A coil is wound around the resonator portion for additionally exciting a nuclear resonance within the sample.

Abstract: A superconducting magnet configuration (4; 14) for generating a homogeneous magnetic field B0 in an examination volume (4b), has an interior radial superconducting main field coil (1) which is disposed rotationally symmetrically about an axis (z-axis) and an oppositely driven coaxial radially exterior superconducting shielding coil (2) is characterized in that the magnet configuration (4; 14) consists of the main field coil (1), the shielding coil (2), and a ferromagnetic field formation device (3; 18), wherein the ferromagnetic field formation device (3; 18) is located at the radially inside of the main field coil (1), the main field coil (1) consisting of an unstructured solenoid coil or of several radially nested unstructured solenoid coils (15, 16) which are driven in the same direction, the axial extent Labs of the shielding coil (2) being smaller than the axial extent Lhaupt of the main field coil (1), wherein the axial magnetic field profile (5) generated by the main field coil (1) and the shielding co

Abstract: A winding machine (1) for winding solenoid-shaped coils (21) with band-shaped conductors (6), comprising a winding means (3) which holds a circular-cylindrical coil core (2) of a coil (21) to be wound, and a winding drive which rotates a coil core (2), which is held in the winding means (3), about a winding axis W, wherein the winding means (3) can be moved in a first direction A by an axial drive, the direction A preferably extending approximately parallel to the winding axis W, is characterized in that the winding means (3) can be rotated about a pivot axis S by a pivot drive, wherein the pivot axis S extends perpendicularly to the direction A. The winding machine winds a solenoid-shaped coil with several layers of a band-shaped conductor without damaging the band-shaped conductor, in particular, when the band-shaped conductor contains brittle superconducting material.

Abstract: A superconducting magnetic field coil (1; 21; 31; 41; 51; 61) comprising at least one coil section (42; 43) which is wound in layers, is characterized in that, in at least one layer (11, 12, 13, 14, 101, 102, 103, 104) of the coil section (42; 43) N (with N?2), superconducting wire sections (A, B, C, D, E) are wound in parallel, such that the windings of the N wire sections (A, B, C, D, E) are adjacent to each other and the N wire sections (A, B, C, D, E) are connected in series. The inventive magnetic field coil can be produced at highly reduced costs, in particular, when the magnetic field coil has a comparatively large layer length.

Abstract: A superconducting magnet system with a superconducting magnet coil system, which is disposed in a cryogenic fluid tank (2) of a cryostat (1), and an exchangeable refrigerator (5; 31) which is operated in a vacuum container (8) and is provided to re-liquefy the cryogenic fluid flowing through a tubular conduit (4; 21) is characterized in that the tubular conduit (4; 21) is rigidly installed in the cryostat (1). The refrigerator reaches its optimum performance during operation in a vacuum, and can be easily exchanged in case of a defect.

Abstract: A method and an apparatus serve the purpose of determining the fat or oil content of a sample. The sample is dried under the action of a microwave field and is examined under the action of a radio-frequency signal and of a constant magnetic field by means of nuclear magnetic resonance. The sample is exposed to the microwave field, the radio-frequency signal and the magnetic field at the same measuring place in a common measuring chamber. The apparatus has a microwave source for drying the sample, a magnetic system for generating a nuclear magnetic resonance magnetic field in the sample, and a nuclear magnetic resonance measuring arrangement for irradiating radio-frequency signals into the sample and for receiving excited nuclear magnetic resonance signals from the sample. The microwave source, the magnetic system and the nuclear magnetic resonance measuring arrangement are connected to a common measuring chamber in which the sample is located.

Abstract: A cryostat configuration has a magnet coil system (2) disposed in a helium tank (1), and a horizontal room temperature bore (3) which provides access to a volume under investigation in the center of the magnet coil system (2). The helium tank (1) contains undercooled liquid helium at a temperature of less than 3.5 K, in particular of approximately 2 K, and the cryostat configuration has at least one vertical tower structure (4) on its upper side for filling in and evaporating helium. The tower structure (4) contains a container (5) with liquid helium of 4.2 K which is separated from the helium tank (1) by a thermal barrier (7), and the helium tank (1) contains an undercooling unit (9). This yields a compact cryostat configuration which achieves continuous, stable long-term operation with an undercooled high-field magnet coil.

Abstract: A nuclear magnetic resonance (NMR) resonator (1; 31) comprising an inductive section (6) and a capacitive section (6a), wherein the inductive section (6) is band-shaped and surrounds a substantially cylindrical volume under investigation (5), wherein the capacitive section (6a) is formed from one or more discrete capacitor(s) (13; 13a, 13b, 13c, 13d), and wherein the ends (7, 8) of the band-shaped inductive section (6) are connected through one or several capacitor(s) (13; 13a, 13b, 13c, 13d) of the capacitive section (6a), is characterized in that the inductive section (6) is formed from a dielectric flexible foil (2) which is conductively coated on both sides and the ends (7, 8) of the band-shaped inductive section (6) overlap, wherein the outer coating (4) of the inner end (7) is electrically conductingly connected to the inner coating (3) of the outer end (8), with one or more through-connections (10) being provided in the area of the inner end (7) of the band-shaped inductive section (6), and the outer c

Abstract: A sample exchange device (1), in particular, for an NMR spectrometer, comprising a circumferential chain (22), sample receptacles (7) which are disposed on the chain (22) at equal distances and are connected to each other via webs (23), and a measuring or transfer position (9), wherein each sample receptacle (7) can be moved to the measuring or transfer position (9) by moving the chain (22), characterized in that a chain guidance is provided which guides the circumferential chain (22) along a meandering path. The inventive sample exchange device is particularly economic and does not impair the analysis of the samples.

Abstract: In a method for the acquisition of data relating to multi-dimensional NMR spectra (designated as the SHARC protocol—SHaped, ARrayed aCquisition Protocol), crossed signals are shifted at will in frequency space using selective pulses and frequency dependent folding.

Abstract: A nuclear magnetic resonance (NMR) magic angle spinning (MAS) probe head (1; 61) for measuring a measuring substance in an MAS rotor (21a-21c), comprises a bottom box (3) and a tube (2) mounted to the bottom box (3) and projecting from the bottom box, wherein, in the area of the end (5) of the tube (2) facing away from the bottom box (3), an MAS stator (7; 62) is disposed within the tube (2) for receiving an MAS rotor (21a-21c), and with a pneumatic sample changing system for supplying and discharging an MAS rotor (21a-21c) to/from the MAS stator (7; 62). A transport conduit (10) is provided for pneumatically transferring an MAS rotor (21a-21c) within the transport conduit (10), wherein the transport conduit (10) extends in the inside of the tube (2) from the bottom box (3) to the MAS stator (7; 62). The probe head realizes fast change between different MAS rotors and facilitates RF shielding and keeping of defined extreme temperature conditions.

Abstract: A method for coupling a gas chromatograph (21) to an NMR spectrometer, wherein the carrier gas present at the outlet of a separating column (23) of the gas chromatograph (21) including a sample contained in the carrier gas is supplied via a heated transfer line (1) to a collecting device (2) for the sample contained in the carrier gas, is characterized in that the carrier gas containing the sample is introduced into a collecting liquid (8) in the collecting device (2), and the sample is collected in the collecting liquid (8), wherein the collecting liquid (8) is suitable as an NMR solvent for the sample. The sample loss of the coupling method is reduced.

Abstract: A method for cooling a cryostat configuration (1, 1?) during transport, wherein the cryostat configuration (1) comprises a superconducting magnet coil (2) in a helium tank (8) containing liquid helium (9), which is surrounded by at least one radiation shield (10), wherein the cooling inside the cryostat configuration (1, 1?) in stationary operation is performed entirely without liquid nitrogen by means of a refrigerator, characterized in that during transport, the refrigerator is switched off and instead, liquid nitrogen (6) is conducted from an external nitrogen vessel (4) via a supply tube (7) from the nitrogen vessel (4) to the cryostat configuration (1, 1?) and brought into thermal contact with the radiation shield (10) by means of a thermal contact element (11) in the cryostat configuration (1, 1?). In this way, the consumption of liquid helium during transport can be greatly reduced and the possible transport time of a charged superconducting magnet configuration increased.

Abstract: A method for spectrometric investigation of a plurality of samples dissolved in a solvent comprises: (a) guiding a first solvent with a sample through an SPE cartridge for concentrating the sample in the cartridge; (b) positioning the cartridge in a carrier for a plurality of cartridges; (c) repeating steps (a) and (b) for a desired number of samples; (d) drying the concentrated samples through removal of the residual first solvent, in particular, dehydration or evaporation; (e) dissolving each sample in a second solvent, transferring these dissolved samples from the cartridges to a spectrometer and acquiring a spectrum of each sample. All samples are dried together in step (d) subsequent to steps (b) and (c) while the cartridges with samples are positioned in the carrier. The drying process is thereby considerably accelerated in a straightforward technical manner.

Abstract: A superconducting magnet configuration (4; 14) for generating a homogeneous magnetic field B0 in an examination volume (4b), has an interior radial superconducting main field coil (1) which is disposed rotationally symmetrically about an axis (z-axis) and an oppositely driven coaxial radially exterior superconducting shielding coil (2) is characterized in that the magnet configuration (4; 14) consists of the main field coil (1), the shielding coil (2), and a ferromagnetic field formation device (3; 18), wherein the ferromagnetic field formation device (3; 18) is located at the radially inside of the main field coil (1), the main field coil (1) consisting of an unstructured solenoid coil or of several radially nested unstructured solenoid coils (15, 16) which are driven in the same direction, the axial extent Labs of the shielding coil (2) being smaller than the axial extent Lhaupt of the main field coil (1), wherein the axial magnetic field profile (5) generated by the main field coil (1) and the shielding co

Abstract: A resonator assembly for executing measurements on a sample within a constant magnetic field B0 by means of magnetic resonance is disclosed. It comprises a resonator portion defining a longitudinal axis and an axial direction. The resonator portion has, along the axial direction, a hollow cavity for exciting electron resonance within the sample. A coupling portion is provided adjacent the resonator portion and has, along the longitudinal axis, a stepped through being electrically conductive at its inner surface. A first, middle section of the stepped through configures the hollow cavity. A second and a third, lateral section adjacent axially opposed sides of the hollow cavity are each dimensioned such that a basic mode being resonant within the hollow cavity is unable to propagate within the second and the third section. A coil is wound around the resonator portion for additionally exciting a nuclear resonance within the sample.

Abstract: In a method for determining an absolute number of electron spins in an extended sample (3) with the assistance of an apparatus for measuring magnetic resonance, the extended sample (3) is disposed within a measurement volume (2) of a radiofrequency RF resonator (1) of the apparatus during an electron spin resonance measurement (ESR).

Abstract: An apparatus for analyzing a measuring substance which is dissolved in a solvent, comprising a conduit (4) for transporting the dissolved measuring substance from a feed means (3) to a measuring location (12), wherein the feed means (3) is designed to optionally feed a solvent or dissolved measuring substance into the conduit (4), is characterized in that the conduit (4) is designed, at least partially, as a polycapillary area (9) which has N parallel connected capillaries (21a, 21b, 21c; 62a, 62b), such that the individual capillaries (21a, 21b, 21c; 62a, 62b) have identical flow times from the feed means (3) to the measuring location (12) and wherein N?2. The apparatus improves the signal-to-noise ratio of the analysis.

Abstract: A superconducting magnet configuration with a magnet coil (1) of inductance L which is disposed in a cryostat (7) at a cryogenic temperature, for generating a temporally stable magnetic field, in a working volume, which is suitable for NMR measurements, and with current feed lines to an external current source (3) via which a current of a current strength IPS can be supplied, wherein, at a cryogenic temperature, the magnet coil (1) can be exclusively short-circuited via a switch (5), is characterized in that the switch (5) is normally conducting and comprises a mechanically operable bridge (6) with an ohmic resistance R1 which can be predetermined. The inventive magnet configuration ensures straightforward stable permanent operation via a mains supply even at high currents (>1000 A) and also effective discharge of the energy released during a quench.

Abstract: A nuclear magnetic resonance (NMR) resonator (1; 31) comprising an inductive section (6) and a capacitive section (6a), wherein the inductive section (6) is band-shaped and surrounds a substantially cylindrical volume under investigation (5), wherein the capacitive section (6a) is formed from one or more discrete capacitor(s) (13; 13a, 13b, 13c, 13d), and wherein the ends (7, 8) of the band-shaped inductive section (6) are connected through one or several capacitor(s) (13; 13a, 13b, 13c, 13d) of the capacitive section (6a), is characterized in that the inductive section (6) is formed from a dielectric flexible foil (2) which is conductively coated on both sides and the ends (7, 8) of the band-shaped inductive section (6) overlap, wherein the outer coating (4) of the inner end (7) is electrically conductingly connected to the inner coating (3) of the outer end (8), with one or more through-connections (10) being provided in the area of the inner end (7) of the band-shaped inductive section (6), and the outer c