Abstract: A method of characterizing the structure of a void sensitized liquid energetic material, which method comprises defining the material in terms distribution function, the distribution function representing the fraction of liquid energetic material that occurs at a given point within the void sensitized liquid energetic material.
Type:
Grant
Filed:
December 13, 2012
Date of Patent:
October 9, 2018
Assignee:
Orica International Pte Ltd
Inventors:
John Cooper, Ian John Kirby, Vladimir Sujansky, Sek K Chan
Abstract: Apparatuses and methods for separating regenerated catalyst are provided. In one embodiment, an apparatus for separating regenerated catalyst includes a regeneration vessel including a catalyst bed section. The apparatus includes a catalyst settler physically separated from the catalyst bed section by a wall extending within the regeneration vessel. The catalyst overflowing the catalyst bed section flows over the wall and enters the catalyst settler. The apparatus further includes a pipe in fluid communication with the catalyst settler and configured to deliver regenerated catalyst from the regeneration vessel to another vessel.
Type:
Grant
Filed:
July 31, 2014
Date of Patent:
August 7, 2018
Assignee:
UOP LLC
Inventors:
Miladin Crnkovic, Paolo Palmas, Richard A. Johnson, II, Thomas William Lorsbach
Abstract: A solar light (heat) absorption material which has an excellent solar light (heat) absorbing ability and a simple structure, and may be used as a low-cost and high-performance heat absorption/accumulation material. Also, a solar light (heat) absorption/control building component including the solar light (heat) absorption material that allows for easy change of its solar light (heat) absorption/control ability. The material includes particles dispersed into a liquid medium having a specific heat ranging from 0.4 to 1.4 cal/g/° C. and a melting point of 5° C. or lower. The dispersed particles have L*value of 30 or less as determined by the CIE-Lab color system (light source D65).
Type:
Grant
Filed:
August 20, 2014
Date of Patent:
July 10, 2018
Assignees:
University of the Ryukyus, Osaka Gas Co., Ltd.
Abstract: Methods and apparatuses for regenerating catalysts and methods of inhibiting corrosion in catalyst regenerating apparatuses are provided. An exemplary apparatus includes: a metal vessel configured to receive a spent catalyst stream and contact at least a portion of the spent catalyst stream with an oxygen containing environment at a sufficiently high temperature to burn coke present in the spent catalyst stream; a refractory material overlying at least a portion of an inner surface of the metal vessel; and a corrosion inhibiting material in contact with at least a portion of the inner surface of the metal vessel and disposed between the inner surface and at least a portion of the refractory material, wherein the corrosion inhibiting material is heat stable at a temperature of at least up to about 400° F. (about 204° C.) and inhibits contact of an acid environment with the inner surface of the metal vessel.
Type:
Grant
Filed:
October 28, 2014
Date of Patent:
July 3, 2018
Assignee:
UOP LLC
Inventors:
Paolo Palmas, James W. Althoff, Sanford Allan Victor
Abstract: Provided is a gas generating composition which can maintain stable combustion performance even under variation of ambient temperature. The gas generating composition includes (a) a fuel and (b) an oxidizing agent and meets the following requirements (I) and (II): (I) a combustion temperature at a time of ignition and combustion at any ambient temperature within a range of ?40° C. to 85° C. is a melting point of a substance included in a combustion residue; and (II) a difference between combustion temperatures at the time of ignition and combustion at ambient temperatures of ?40° C. and 85° C. is less than 125 K.
Abstract: The present invention relates to a method for preparing an adsorbent for phosphorus adsorption and an adsorbent prepared by the method. More specifically, the present invention is based on the fact that phosphorus has a strong affinity for the surface of metal oxides or hydroxides, and relates to a method for preparing an adsorbent for phosphorus adsorption, which comprises absorbing and coating expanded vermiculite with aluminum and heating the coated vermiculite at high temperature to produce aluminum oxide on the surface of the expanded vermiculite so that the adsorption of phosphorus at the coordination of the oxide can be achieved with very high efficiency by a strong attraction between phosphorus ions and aluminum ions, and to an adsorbent prepared by the method.
Type:
Grant
Filed:
July 28, 2014
Date of Patent:
May 29, 2018
Inventors:
Taeyoon Lee, Junheok Lim, Jeakeun Lee, Jahyun Kim
Abstract: This invention relates to the construction of a rocket motor and fuel system thereof and, in particular to a new and useful Viscous Liquid Monopropellant (VLM) rocket motor containing a liquid propellant that is pumped into the combustion chamber, atomized and then ignited. The atomization step significantly increases the surface area of the propellant, delivering faster burn rates and smoother combustion. VLM is a non-Newtonian fluid containing both oxidizers and fuels. These monopropellants are comprised of a variety of liquid and solid components, mixed together to form a homogenous fluid, although heterogeneous in composition. The solid constituents are retained within the liquid phase by dispersion, suspension, bonding or chemical emulsification techniques, so as when a motive force is applied to the propellant, all the constituents are also transported, and held in correct proportion while doing so.
Abstract: A desensitizing agent and method which desensitizes triacetone triperoxide (TATP). The agent includes a common polymer dissolved in a volatile solvent, which allows for direct, rapid application on-site, providing for safer movement and transport of the explosive. Drop heights in impact test results of treated TATP were twice that of neat TATP or TATP treated with conventional agents. The agent is composed of non-toxic, inexpensive components with the polymer delivered in a solvent vehicle, which quickly volatilizes after application and exhibits compatibility with TATP and conventional explosives.
Type:
Grant
Filed:
February 20, 2014
Date of Patent:
April 17, 2018
Assignee:
The United States of America as Represented by the Secretary of the Navy
Abstract: Paper microfluidic devices for testing for explosives are provided, along with methods of fabricating and using the same. One or more channels are formed on a paper substrate, and a test spot is formed in at least one of the channels. The channels can be hydrophobic. A test reagent is provided in the test spot and tests for explosives.
Type:
Grant
Filed:
March 17, 2014
Date of Patent:
February 13, 2018
Assignee:
The Florida International University Board of Trustees
Inventors:
Bruce McCord, Inge Corbin, Lucas Blanes
Abstract: The present invention relates generally to an advanced oxidation process for providing advanced oxidation products to an environment. More particularly, the present invention provides a wick structure and hydrophilic granules for use in an advanced oxidation process, and methods of making the same. The wick structure and hydrophilic granules may be configured to collect and concentrate water vapor, so that the water vapor may subsequently be used to generate advanced oxidation products that react with and neutralize compounds in an environment, including microbes, odor causing chemicals, and other organic and inorganic chemicals.
Abstract: Ceramic catalyst carriers that are mechanically, thermally and chemically stable in a ionic salt monopropellant decomposition environment, high temperature catalysts for decomposition of liquid high-energy-density monopropellants and ceramic processing techniques for producing spherical catalyst carrier granules are disclosed. The ceramic processing technique is used to produce spherical catalyst carrier granules with controlled porosities and desired composition and allows for reproducible packing densities of catalyst granules in thruster chambers. The ceramic catalyst carrier has excellent thermal shock resistance, good compatibility with the active metal coating and metal coating deposition processes, melting point above >2300° C., chemical resistance to steam, nitrogen oxides and nitric acid, resistance to sintering to prevent void formation, and the absence of phase transition associated with volumetric changes at temperatures up to and beyond 1800° C.
Abstract: The present invention is a red-light-emitting composition based upon a potassium periodate oxidizer formulation, which is useful as the illuminant in the US military's M662 40 mm red star parachute projectile, and which composition is composed of readily commercially available ingredients—ingredients that are environmentally friendly. Further, the subject inventive potassium periodate formulation provides significant enhanced illumination and safety versus the current military M662 illuminant which is based upon potassium perchlorate oxidizer formulation.
Type:
Grant
Filed:
March 19, 2015
Date of Patent:
January 2, 2018
Assignee:
The United States of America as Represented by the Secretary of the Army
Abstract: What is disclosed is a method for preparing a catalyst system and a catalyst system for polymerizing or copolymerizing an ?-olefin. Catalyst component (A) is obtained by a process of reacting a magnesium complex (A-1) containing acid salts of group IB-VIIIB elements formed by contacting a magnesium halide with an acid salt solution of group IB-VIIIB metals or spherical particles adducts, an internal electron donor (A-2) of diester or diether or composite compounds, and a titanium compound (A-3). The catalyst compound (A) is contacted with a silicon compound (B) and an organoaluminium compound (C) to complete the catalyst system providing a good balance of catalyst performance in terms of activity and stereo-specificity.
Abstract: A method for processing an edge of a catalyst-supporting honeycomb structure in an exhaust gas denitration apparatus, in which an exhaust gas denitration apparatus equipped with a denitration catalyst-supporting honeycomb structure in which a corrugated plate-like inorganic fiber sheet and a flat plate-like inorganic fiber sheet, each supporting thereon a denitration catalyst containing a silica sol, titania particles, and ammonium metavanadate as a whole primary denitration catalyst layer, are alternately laminated, the edge of gas inlet side of the denitration catalyst-supporting honeycomb structure having the whole primary denitration catalyst layer is dipped in a denitration catalyst-containing slurry for edge processing composed of a silica sol, titania particles or kaolin particles, and ammonium metatungstate to form a coating layer of the denitration catalyst-containing slurry in the edge of the honeycomb structure, and this is dried and then calcinated to form an edge secondary denitration catalyst la
Type:
Grant
Filed:
December 17, 2012
Date of Patent:
October 31, 2017
Assignee:
Hitachi Zosen Corporation
Inventors:
Seigo Yamamoto, Susumu Hikazudani, Naoe Hino, Kana Shimizu
Abstract: Provided are: a hydrotreating catalyst for hydrocarbon oil having a hydrodesulfurization activity additionally improved by: simultaneously and continuously adding an aqueous solution of an acidic compound containing titanium and an aqueous solution containing an alkaline compound to a hydrosol containing an alumina hydrate particle at a temperature of 10 to 100° C. and a pH of 4.5 to 6.5; washing the resultant to remove a contaminating ion; forming the washed product after dehydration so as to have a moisture content at which it is formable; drying the resultant; impregnating the dried product with a catalytic component aqueous solution containing at least one kind of periodic table group 6 metal compound, at least one kind of periodic table group 8-10 metal compound, at least one kind of phosphorus compound, and at least one kind of saccharide; and drying the resultant; a manufacturing method for the catalyst; and a hydrodesulfurization treatment method for hydrocarbon oil using the catalyst.
Type:
Grant
Filed:
March 22, 2011
Date of Patent:
October 3, 2017
Assignee:
CHIYODA CORPORATION
Inventors:
Shinichi Inoue, Yukitaka Wada, Akihiro Mutou, Takeo Ono
Abstract: There are disclosed energetic nanoparticle compositions and materials containing silicon and other energetic elements, and methods of manufacturing the same, including reacting silicon nanoparticles and unsaturated alkene or alkyne to form covalently bonded surface coatings passivated against surface oxidation, for combination with a fuel, explosive or oxidizer.
Abstract: Apparatuses and methods are provided for regenerating catalyst particles. In one embodiment, a method for regenerating catalyst particles includes passing the catalyst particles through a halogenation zone and a drying zone. The method feeds drying gas to the drying zone and passes a first portion of the drying gas from the drying zone to the halogenation zone. The method includes removing a second portion of the drying gas from the drying zone and injecting a halogen gas into the second portion of the drying gas. Further, the method includes delivering the halogen gas and the second portion of the drying gas to the halogenation zone. In the method, substantially all of the drying gas fed to the drying zone enters the halogenation zone.
Type:
Grant
Filed:
August 27, 2014
Date of Patent:
August 15, 2017
Assignee:
UOP LLC
Inventors:
Ka Lok, Jennifer J Ozmen, William Yanez, Mary Wier, Richard Gaicki
Abstract: An improved method of preparing tetranitroglycoluril (TNGU) via the in situ decomposition of a nitrimino group with elimination of nitrogen without the use of dinitrogen pentoxide. The compound is useful as a high energy, high density explosive or propellant oxidizer.
Type:
Grant
Filed:
September 29, 2014
Date of Patent:
July 4, 2017
Assignee:
The United States of America as represented by the Secretary of the Army
Inventors:
William Matthew Sherrill, Eric Christopher Johnson
Abstract: An effective, safe and economical method of manufacture of an insensitive high explosive molding powder usable as a booster HE. The method preferably involving the steps of adding a binder and a crystalline high explosive to water, grinding that suspension in a bead mill until the crystalline high explosive is nano-sized, and precipitating the binder and crystalline high explosive using a spray dryer. Alternatively, an aqueous suspension of the crystalline high explosive can be ground in the bead mill and the binder subsequently added, prior to spray drying. A fatty alcohol, water defoaming/dispersant/surfactant agent can be added to the dissolved binder/suspended crystalline high explosive, to aid in the manufacturability.
Type:
Grant
Filed:
March 18, 2014
Date of Patent:
June 20, 2017
Assignee:
The United State of America as Represented by the Secretary of the Army
Inventors:
Rajen B. Patel, Victor Stepanov, Ashok Surapaneni, Anthony DiStasio
Abstract: The present invention provides a modular installation (1) for carrying out a method of manufacturing an explosive emulsion precursor comprising at least three containers: —a first container (100) for preparing an aqueous phase, including a dissolution first tank (110); and —at least one second and/or third container (200, 300) including a second tank for preparing oily phase (210) and a third tank for preparing emulsion (310); and —at least one fourth and/or fifth container (400, 500) including means (410) for feeding heat and means (510) for feeding electrical energy; and —said first, second and/or third containers (100, 200, 300) being juxtaposed over at least a portion of one of their walls (100a, 300b, 200b) and being provided with openings (170, 370a, 275, 375, 270b) in their walls.