Patents Examined by Aileen B. Felton
  • Patent number: 9663413
    Abstract: The invention relates to a primer composition, to a method for producing the same and to the use of said primer composition.
    Type: Grant
    Filed: December 18, 2006
    Date of Patent: May 30, 2017
    Assignee: RUAG AMMOTEC GMBH
    Inventors: Ulrich Bley, Rainer Hagel, Aleksej Hoschenko, Peter Simon Lechner
  • Patent number: 9650307
    Abstract: A method of producing DEMN eutectic comprises reacting a reactant mixture comprising ethylenediamine and diethylenetriamine with aqueous nitric acid to form a reaction mixture comprising diethylentriamine trinitrate and ethylenediamine dinitrate. The reaction mixture is combined with methylnitroguanidine and nitroguanidine to form an aqueous slurry. Water is removed from the aqueous slurry. A method of producing an energetic composition, and a system for producing DEMN eutectic are also described.
    Type: Grant
    Filed: March 14, 2013
    Date of Patent: May 16, 2017
    Assignee: Orbital ATK, Inc.
    Inventors: Stephen P. Velarde, Harold E. Johnston
  • Patent number: 9650309
    Abstract: A method for gas atomization of oxygen-reactive reactive metals and alloys wherein the atomized particles are exposed as they solidify and cool in a very short time to multiple gaseous reactive agents for the in-situ formation of a protective reaction film on the atomized particles. The present invention is especially useful for making highly pyrophoric reactive metal or alloy atomized powders, such as atomized magnesium and magnesium alloy powders. The gaseous reactive species (agents) are introduced into the atomization spray chamber at locations downstream of a gas atomizing nozzle as determined by the desired powder or particle temperature for the reactions and the desired thickness of the reaction film.
    Type: Grant
    Filed: April 10, 2013
    Date of Patent: May 16, 2017
    Assignee: Iowa State University Research Foundation, Inc.
    Inventors: Iver E. Anderson, Andrew D. Steinmetz, David J. Byrd
  • Patent number: 9623399
    Abstract: A method of surface modification of an alumina carrier. The method includes: 1) dissolving a soluble kazoe in deionized water to yield a kazoe aqueous solution; 2) submerging an alumina carrier in the kazoe aqueous solution and drying the alumina carrier in a vacuum environment; 3) placing the dried alumina carrier in a reactor, adding silicon tetrachloride and Grignard reagent dropwise to the reactor, sealing the reactor and heating it to a constant temperature, and maintaining the constant temperature for between 3 and 18 hours, where a volume ratio of the added silicon tetrachloride and the alumina carrier is between 0.5:1 and 5:1, the constant temperature is controlled to be between 160 and 350° C.; and 4) cooling the reactor, filtering, washing, and drying the alumina carrier in the vacuum environment.
    Type: Grant
    Filed: September 4, 2014
    Date of Patent: April 18, 2017
    Assignee: SUNSHINE KAIDI NEW ENERGY GROUP CO., LTD.
    Inventors: Shenke Zheng, Dechen Song, Xiaodong Zhan
  • Patent number: 9617195
    Abstract: A smoke producing method and device of the present disclosure produces a non-incendiary, organic-polymerization based, smoke-producing reaction. The method of generating smoke comprises initiating a frontal polymerization reaction by heating a composition comprising a monomer compound that exothermically polymerizes upon initiation with an initiator compound and an initiator compound that initiates polymerization of the monomer compound present at a mass concentration that is at least five percent of the mass concentration of the monomer compound. The polymerization of the monomer compound is exothermic, and in one embodiment the concentration of initiator compound is at least five percent of the concentration of monomer compound. The smoke mainly comprises thermal decomposition products of the initiator compound.
    Type: Grant
    Filed: May 7, 2013
    Date of Patent: April 11, 2017
    Assignee: POLARIS SENSOR TECHNOLOGIES, INC.
    Inventors: Peter S. Erbach, R. Michael Banish
  • Patent number: 9617193
    Abstract: An energetic material composite comprising fuel particles and a hydrated compound is disclosed. The energetic material composite is formed by dispersing fuel particles, which have a negative standard reduction potential relative to a standard hydrogen electrode, in a solvent containing dissolved hydrate, followed by a removal of solvent. When initiated, the fuel particles react with the water bound in the hydrated compound to release energy and hydrogen gas.
    Type: Grant
    Filed: February 25, 2011
    Date of Patent: April 11, 2017
    Assignee: NCC NANO, LLC
    Inventors: Kurt A. Schroder, Ronald Ian Dass
  • Patent number: 9605114
    Abstract: Optically sensitized binders which are energetic polyphosphazenes tailored at the molecular level to achieve enhanced absorption of electromagnetic radiation by having attached thereto a chromophore to absorb light and therefore ignite the binder in use.
    Type: Grant
    Filed: June 20, 2013
    Date of Patent: March 28, 2017
    Assignee: The Secretary of State for Defence
    Inventors: Peter Golding, Anthony John Bellamy, Alessandro Enzo Contini
  • Patent number: 9573856
    Abstract: A micro-explosive material is provided. The micro-explosive material can include a carbon nanotube and a solid oxidizer attached to the carbon nanotube. The carbon nanotube with the solid oxidizer attached thereto is operable to burn per an exothermic chemical reaction between the carbon nanotube and the solid oxidizer such that a controlled burn and/or an explosive burn is provided. The micro-explosive material can be used as a heat generator, a gas generator, a micro-thruster, a primer for use with a larger explosive material, and the like.
    Type: Grant
    Filed: February 14, 2012
    Date of Patent: February 21, 2017
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Luke M. Currano, Madan Dubey, Ronald G. Polcawich
  • Patent number: 9573857
    Abstract: A method of forming composite materials includes mixing a first metal precursor with a chelating agent to form a first metal-chelate complex. The first metal-chelate complex is added to a polymer binder having terminating hydroxyl groups to form a polymer binder-first metal-chelate. The polymer binder first metal-chelate complex is mixed with an aluminum precursor. The aluminum precursor decomposes forming aluminum nanoparticles dispersed in a continuous phase material having metallic aluminum cores. At least one of the first metal-chelate complex and the first metal is dissolved in the continuous phase. The aluminum nanoparticles can have a passivating coating layer thereon provided by the polymer binder, or can have a passivating coating layer formed by including an epoxide, alcohol, carboxylic acid, or amine in the adding that forms passivating compound(s) which add further protection that can provide complete protection from oxidation of the metallic aluminum cores by air.
    Type: Grant
    Filed: March 12, 2013
    Date of Patent: February 21, 2017
    Assignees: University of Central Florida Research Foundation, Inc., The Texas A&M University System
    Inventors: David L. Reid, Sudipta Seal, Eric Petersen
  • Patent number: 9573858
    Abstract: A method for improving the characteristics of energetic materials uses amorphous metals as one or more reactant of said materials. Improvements in properties and energy release characteristics for a wide range of energetic materials are obtained thereby, particularly in terms of processability, mechanical properties, and ignition behavior for solid energetic materials.
    Type: Grant
    Filed: March 25, 2010
    Date of Patent: February 21, 2017
    Inventor: Alan H. Brothers
  • Patent number: 9556078
    Abstract: A gas generator is provided, the gas generator having a propellant cushion that prevents movement of propellant tablets or grains by providing a bias thereagainst. Furthermore, the cushion is formed from an auto-igniting material thereby functioning not only as a cushion, but also as an enhanced auto-ignition charge.
    Type: Grant
    Filed: April 7, 2009
    Date of Patent: January 31, 2017
    Assignee: TK Holdings Inc.
    Inventor: Deborah L. Hordos
  • Patent number: 9541366
    Abstract: A spark generating tube includes a single tube and a pyrotechnical mixture. The single tube only has a single layer of plastic material, such as ethylene vinyl acetate (EVA) and polyethylene. The pyrotechnical mixture has formed a thin layer in contact with the single layer of the single tube. The pyrotechnical contains an oxidizer, a reducing agent, a substance with low temperature of Tammann and an agent for lubricating and adhering, wherein the agent for lubricating and adhering is either talc or graphite, and the reducing agent can be an aluminum powder in microscale. During the process for manufacturing a spark generating tube, the mixture of the oxidizers and additives is formed separately from the reducing agent. The final mixture is obtained only in the single tube formed with an extruder. In this way, only a very small amount of pyrotechnic mixture is formed at any instant.
    Type: Grant
    Filed: August 25, 2014
    Date of Patent: January 10, 2017
    Assignee: IBQ INDUSTRIAS QUIMICAS S/A
    Inventor: Marco Antonio Falquete
  • Patent number: 9517361
    Abstract: The invention provides methods for encapsulating nanometric particles inside of micro-sized crystals. An exemplary embodiment involves crystallizing a solution including nanometric particles, a micelle-forming material, a nonpolar dispersant for the micelle-forming material and a crystal-forming material to form crystal-encapsulated nanometric particles. Also provided are compositions or materials which include or are formed using the crystal encapsulated nanoparticles, such compositions and materials can include propellants, cosmetics, composite structures, energetics, and pharmaceutical compositions/materials.
    Type: Grant
    Filed: October 15, 2012
    Date of Patent: December 13, 2016
    Assignee: Purdue Research Foundation
    Inventors: David A. Reese, Steven F. Son, Allen Hoe Yan
  • Patent number: 9480965
    Abstract: Disclosed is a method for preparing a granulated inorganic adsorbent for radionuclides including slurry forming, solidification, drying and hardening, granulation, and washing steps: blending a dihydrogen phosphate, a powdered inorganic adsorbent raw material and a setting time regulator in water to form a slurry; adding sintered magnesia into the slurry, and blending the mixture to form a solidified slurry; setting the solidified slurry on a disk member, and naturally drying to hardening in a specific temperature range to form a hardened solid material; smashing the hardened solid material and performing vibration sieving by using a screen to obtain a granulated inorganic adsorbent for radionuclides containing residual reagents; washing the granulated inorganic adsorbent for radionuclides containing residual reagents with water, to remove the residual reagents to complete preparation, where the adsorption capacity of the granulated inorganic adsorbent for radionuclides thus prepared is in the range of 0.
    Type: Grant
    Filed: October 30, 2014
    Date of Patent: November 1, 2016
    Assignee: INSTITUTE OF NUCLEAR ENERGY RESEARCH ATOMIC ENERGY COUNCIL, EXECUTIVE YUAN
    Inventors: Li-Ching Chuang, Chi-Hung Liao, Jen-Chieh Chung, Kou-Min Lin, Sheng-Wei Chiang, Kuang-Li Chien, Zhe-Cheng Hu, Wen-Chi Tsai
  • Patent number: 9469573
    Abstract: This invention relates to a method of manufacturing a salt-coated heat paper, including preparing a powder mixture by mixing a fuel powder with an oxidant powder; preparing a slurry by adding an organic coagulant, after mixing the powder mixture with glass fibers; obtaining a heat paper by a papermaking process utilizing the slurry; primarily drying the heat paper by pressing; coating the heat paper with a salt solution; and secondarily drying the heat paper.
    Type: Grant
    Filed: October 28, 2014
    Date of Patent: October 18, 2016
    Assignee: AGENCY FOR DEFENSE DEVELOPMENT
    Inventors: Chaenam Im, Jungmin Lee, Seungho Kang, Haewon Cheong
  • Patent number: 9463452
    Abstract: A hydrotreating catalyst for hydrocarbon oil having a hydrodesulfurization activity additionally improved by: simultaneously and continuously adding an aqueous solution of an acidic compound containing titanium and an aqueous solution containing an alkaline compound to a hydrosol containing an alumina hydrate particle at a temperature of 10 to 100° C. and a pH of 4.5 to 6.5; washing the resultant to remove a contaminating ion; forming the washed product after dehydration so as to have a moisture content at which it is formable; drying the resultant; impregnating the dried product with a catalytic component aqueous solution containing periodic table group 6 metal compound, periodic table group 8-10 metal compound, phosphorus compound, and saccharide; and drying the resultant; a manufacturing method for the catalyst; and a hydrodesulfurization treatment method for hydrocarbon oil using the catalyst.
    Type: Grant
    Filed: April 16, 2014
    Date of Patent: October 11, 2016
    Assignee: CHIYODA CORPORATION
    Inventors: Shinichi Inoue, Yukitaka Wada, Akihiro Mutou, Takeo Ono
  • Patent number: 9429104
    Abstract: Embodiments of the invention relate to systems and methods for casting hybrid rocket motor fuel grains. In one embodiment, a method for casting a rocket motor fuel grain can be provided. The method can include providing a positive image of a port made from at least one material. The method can further include disposing at least one fuel material around at least a portion of the positive image of the port. Further, the method can include removing the at least one material, wherein a negative image of the port is formed in the at least one fuel material.
    Type: Grant
    Filed: August 1, 2012
    Date of Patent: August 30, 2016
    Assignee: The Aerospace Corporation
    Inventor: Jerome Keith Fuller
  • Patent number: 9415373
    Abstract: A method of making a structured, doped, cerium oxide nanoparticle includes (a) forming a first reaction mixture including cerium(III), an optional metal ion other than cerium, a base, a stabilizer, and a solvent, (b) contacting the first reaction mixture with an oxidant, (c) forming a cerium oxide nanoparticle core by heating the product of step (b), (d) forming a second reaction mixture by combining with the first reaction mixture one or more metal ions other than cerium, and an optional additional quantity of cerium(III), and (e) forming a shell surrounding the core of cerium oxide by heating the second reaction mixture to produce a product dispersion of structured cerium oxide nanoparticles.
    Type: Grant
    Filed: March 8, 2011
    Date of Patent: August 16, 2016
    Assignee: CERION, LLC
    Inventors: Kenneth J. Reed, Albert Gary DiFrancisco, Richard K. Hailstone, Gary R. Prok, Thomas D. Allston
  • Patent number: 9399602
    Abstract: The invention relates to a method of producing a range of particulate energetic materials with tailored particle sizes and extremely narrow particle size distributions. The use of membrane emulsification apparatus provides a means of formulating explosives with a selectable particle size, without the use of milling techniques to physically reduce the size of the particulates.
    Type: Grant
    Filed: December 7, 2012
    Date of Patent: July 26, 2016
    Assignee: ROXEL (UK ROCKET MOTORS) LIMITED
    Inventor: Matthew James Ian Williamson
  • Patent number: 9394853
    Abstract: A strain measurement device includes a reference material, and a displacement sensor configured to detect relative changes in distance between the sensor and the reference material. At least one of the displacement sensor and the reference material is coupled with a pre-cured elastomeric material. The displacement sensor generates a data signal to a processor that is configured to determine a strain of another elastomeric material based at least in part on the data signal received from the sensor. A displacement sensor and a reference material may be positioned within an elastomeric material within a casing of a solid rocket motor for determining strain experienced by the elastomeric material, such as the propellant of the solid rocket motor. A method includes installing a sensor of an elastomeric material. Another method includes determining strain of an elastomeric material of a solid rocket motor.
    Type: Grant
    Filed: October 12, 2011
    Date of Patent: July 19, 2016
    Assignee: Orbital ATK, Inc.
    Inventors: John L. Shipley, Russell A. Crook, Robert P. Graham, Lydia L. Biegert, David H. Johnson