Abstract: A method for treatment of a hexachlorodisilane and its hydrolyzed product is disclosed. It comprises adding a hexachlorodisilane or its hydrolyzed product into a sulfuric acid solution for reaction.
Type:
Grant
Filed:
May 23, 2018
Date of Patent:
February 4, 2020
Assignee:
National Kaohsiung University of Science and Technology
Abstract: Embodiments of the present invention include a filter element for decomposing contaminants including a substrate, and a photocatalytic composition comprising at least a photocatalyst. The embodiments of the present invention also includes a system for decomposing contaminants including a substrate, and a photocatalytic composition comprising at least a photocatalyst; and a method using the system.
Abstract: Yield of products of increased purity from a fluidized bed reactor where silicon is produced or consumed is enhanced by purging with inert gas, purging with hydrogen gas, and purging with a chlorosilane-containing gas. The purging with hydrogen is conducted at an elevated temperature.
Abstract: According to aspects of the present disclosure, a ternary alloy includes a dual-phase microstructure including a first phase and a second phase. The first phase defines a hexagonal close-packed structure with a stoichiometric ratio of Al4Fe1.7Si. The second phase defines a face-centered cubic structure with a stoichiometric ratio of Al3Fe2Si. The dual-phase microstructure is stable above about 800° C., and the dual-phase microstructure has a first-phase abundance greater than about 50 parts by weight and a second-phase abundance less than about 50 parts by weight based on 100 parts by weight of the ternary alloy.
Abstract: An aqueous cobalt chloride solution refinement method, in which metallic nickel is washed with an acidic liquid having a pH of not more than 2.5 before the metallic nickel is brought into contact with the aqueous solution containing cobalt chloride. Since the metallic nickel is washed with the acidic liquid having a pH of not more than 2.5, a passive film on a surface of the metallic nickel is removed and therefore, when the metallic nickel comes in contact with the aqueous solution containing cobalt chloride, an impurity more noble than the metallic nickel can be precipitated by a cementation reaction. In addition, since the metallic nickel is only washed with acid to be brought into contact with the aqueous solution containing cobalt chloride, impurities can be easily removed from the aqueous solution containing cobalt chloride.
Abstract: An ultrahigh-strength spring steel, used as steel for a vehicle engine valve spring may include 0.5 to 0.7 wt % of C, 1.3 to 2.5 wt % of Si, 0.6 to 1.2 wt % of Mn, 0.6 to 1.5 wt % of Cr, 0.01 to 0.5 wt % of Mo, 0.01 to 0.9 wt % of Ni, 0.5 wt % or less (excluding 0 wt %) of V, 0.5 wt % or less (excluding 0 wt %) of Nb, 0.3 wt % or less (excluding 0 wt %) of Ti, 1.0 wt % or less (excluding 0 wt %) of Co, 0.1 wt % or less (excluding 0 wt %) of B, 0.3 wt % or less (excluding 0 wt %) of W, 0.3 wt % or less (excluding 0 wt %) of Cu, 0.3 wt % or less (excluding 0 wt %) of Al, 0.03 wt % or less (excluding 0 wt %) of N, 0.003 wt % or less (excluding 0 wt %) of O, and a remainder of Iron (Fe) and inevitable impurities.
Type:
Grant
Filed:
November 14, 2016
Date of Patent:
November 26, 2019
Assignee:
Hyundai Motor Company
Inventors:
Sung Chul Cha, Min Woo Kang, Hye Min Jo, Seung Hyun Hong
Abstract: An aluminum-alloy sheet for a bus bar has a chemical composition containing Mg: 0.3%-0.9% (mass %, likewise below), Si: 0.2%-1.2%, Cu: 0.2% or less, and Fe: 0.5% or less, the remainder being Al and unavoidable impurities. In addition, acicular particles containing Mg and Si are present in the Al matrix at 900-4,000 particles/?m2. In addition, Fe-based particles present in the above-mentioned Al matrix have an average circle-equivalent diameter of 5 ?m or less, and the number of particles having a circle-equivalent diameter of more than 2 ?m is 10,000 particles/mm2 or less.
Abstract: A source of phosphate for agriculture and food industry comprises a phosphate salt in solid form of formula Mn(HPO4)y.zH2O in which M is Na, K, NH4, n=2, and y=1; or M is Ca, n=1, y=1; or M is Al or Fe, n=2, y=3; and in which z is 0, 1 or 2, wherein said phosphate salt has a phosphate content expressed as a P2O5 content of between 30 and 50% by weight of the phosphate salt, and it has a cadmium content lower than 0.40 ppm.
Abstract: The invention relates to a method for purifying halogenated oligosilanes in the form of a pure compound or a mixture of compounds with respectively at least one direct Si—Si bond, the substituents thereof being exclusively made from halogen or from halogen and hydrogen and in the composition thereof, the atomic ratio of the substituents:silicon is at least 3:2, by the action of at least one purification agent on the halogenated oligosilane and by isolating the halogenated oligosilanes with improved purity. According to prior art, halogenated monosilanes such as HSiCl3 are purified by treating with organic compounds, preferably polymers, containing amino groups, and are separated from said mixtures. Based on the contained amino groups, said method can not be used for halogenated oligosilanes as the secondary reactions lead to a decomposition of the products. The novel method is used to provide the desired products in a high yield and purity without using the amino groups.
Type:
Grant
Filed:
September 7, 2015
Date of Patent:
October 29, 2019
Assignee:
PSC POLYSILANE CHEMICALS GMBH
Inventors:
Christian Bauch, Sven Holl, Matthias Heuer
Abstract: A nanocrystalline bainitic steel consisting of, by weight percentage: 0.3% to 0.6% carbon; 9.0% to 20.0% nickel; up to 10% cobalt; 1.0% to 4.5% aluminium; up to 0.5% molybdenum; up to 0.5% manganese; up to 0.5% tungsten; up to 3.0% chromium; and the balance being iron and impurities.
Type:
Grant
Filed:
February 23, 2017
Date of Patent:
October 29, 2019
Assignee:
ROLLS-ROYCE plc
Inventors:
Paul O Hill, Steve W Ooi, Christopher N Hulme-Smith, Harshad K Bhadeshia, Martin J Rawson, Mathew J Peet
Abstract: The reaction tube for preparing hydrogen cyanide comprises a cylindrical tube composed of ceramic, a catalyst comprising platinum applied to the inner wall of the tube and also at least one insert composed of ceramic, having three or four fins pointing from the tube axis to the inner wall of the tube, which is inserted into the cylindrical tube, wherein the fins divide the tube interior space into substantially straight channels with substantially identical circle segment cross sections and wherein the mean gap between the ends of the fins and the inner wall of the tube is in the range of 0.1 to 3 mm. In the method for preparing hydrogen cyanide, ammonia and at least one aliphatic hydrocarbon having 1 to 4 carbon atoms are reacted in the reaction tube at 1000 to 1400° C.
Type:
Grant
Filed:
October 2, 2014
Date of Patent:
October 15, 2019
Assignee:
Evonik Degussa, GmbH
Inventors:
Martin Steffan, Martin Steurenthaler, Thomas Müller, Martin Körfer, Steffen Krill
Abstract: Provided are a high-strength steel sheet for containers and a method for producing the high-strength steel sheet. The high-strength steel sheet for containers has a composition containing, by mass, C: 0.0010% to 0.10%, Si: 0.04% or less, Mn: 0.10% to 0.80%, P: 0.007% to 0.100%, S: 0.10% or less, Al: 0.001% to 0.100%, N: 0.0010% to 0.0250%, and the balance being Fe and inevitable impurities. The difference between the dislocation density at the uppermost layer of the high-strength steel sheet in the thickness direction and the dislocation density at a depth of ¼ of the thickness of the high-strength steel sheet from the surface is 1.94×1014 m?2 or less. The high-strength steel sheet has a tensile strength of 400 MPa or more and a fracture elongation of 10% or more.
Type:
Grant
Filed:
April 23, 2015
Date of Patent:
September 17, 2019
Assignee:
JFE Steel Corporation
Inventors:
Masaki Tada, Hayato Saito, Katsumi Kojima, Hiroki Nakamaru
Abstract: Described herein are methods for the bromine-facilitated synthesis of fluoro-sulfur compounds, that include SF4, SF5Cl, SF5Br and SF6. The methods described herein generally require lower temperature and pressure, produce higher yields, require less time, do not use corrosive or costly reactants and solvents that are commonly used in the synthesis of the fluoro-sulfur compounds, and do not produce deleterious waste products when compared to previously-used methods.
Abstract: Production of polycrystalline silicon in substantially closed-loop processes and systems is disclosed. The processes and systems generally involve disproportionation of trichlorosilane to produce silane or dichlorosilane and thermal decomposition of silane or dichlorosilane to produce polycrystalline silicon.
Abstract: The present invention relates to a process for treating a biomass (1) mixed with water in order to produce, independently, combustible solids (14) and drinking water (12) and biogas (13A, 13B), and also to a device for treating a biomass (1) mixed with water in order to produce, independently, combustible solids (14), drinking water (12) and biogas (13A, 13B).
Abstract: A polycrystalline silicon rod is synthesized by the Siemens method (S101). After the polycrystalline silicon rod is covered from above with a plastic bag whose inner surface has been washed, and housed in the plastic bag in a reactor (S103), the polycrystalline silicon rod is removed out of the reactor (S104), and heat-sealed and stored in an enclosed state (S105). According to the present invention, steps conventionally considered as essential, such as washing, etching, and water washing, are not always necessary, and therefore the concentrations of fluorine ions, nitrate ions, and nitrogen dioxide ions remaining on the surface can each be less than 0.2 ppbw. In addition, by covering with the plastic bag, the metal contamination levels decrease significantly. Moreover, when the handling according to the present invention is performed, surface contamination hardly proceeds even if the polycrystalline silicon rod is stored for a long period.
Abstract: The present invention relates to a method for purifying raw phosphoric acid by adding ashes originating from waste incineration plants, as well as calcium hydroxide and at least one sulfide, and by wet-chemical digestion for obtaining (producing) calcium sulfate, pure phosphoric acid, metal salt solution and/or calcium hydrogen phosphates (e.g. triple superphosphate).
Abstract: The invention relates generally to heaters and methods of using the heaters. In certain embodiments, a heater includes a pressure shell having a cylindrical heating cavity, an annular heat shield disposed within the cylindrical heating cavity, and at least one heating element disposed within an interior volume of the annular heat shield. In another embodiment, a method of preparing a trichlorosilane includes introducing a reactant stream comprising silicon tetrachloride into a heater, passing electrical current through a heating element to heat the reactant stream, and introducing the heated reactant stream into a reactor.
Abstract: The present invention relates to an apparatus and a method for producing polycrystalline silicon having a reduced amount of boron compound impurities. Especially, the boron compounds are removed from the process for producing polycrystalline silicon, while the trichlorosilane is purified by distillation. The invention feeds condensed liquid trichlorosilane into a primary distillation tower below the liquid level inside the primary distillation tower thereby scrubbing the boron impurities upon contact inside the primary distillation tower. There result is trichlorosilane leaving the primary distillation tower with total amount of boron at least 10 times less.
Type:
Grant
Filed:
January 16, 2018
Date of Patent:
May 21, 2019
Assignees:
MITSUBISHI POLYCRYSTALLINE SILICON AMERICA CORPORATION (MIPSA), MITSUBISHI MATERIALS CORPORATION
Abstract: [Problem] To provide a novel production method for pentachlorodisilane and to obtain pentachlorodisilane having a purity of 90 mass % or more by carrying out this production method. [Solution] A production method provided with: a high-temperature reaction step in which a raw material gas containing vaporized tetrachlorosilane and hydrogen is reacted at a high temperature in order to obtain a reaction product gas containing trichlorosilane; a pentachlorodisilane generation step in which the reaction product gas obtained in the high-temperature reaction step is brought into contact with a cooling liquid obtained by circulative cooling of a condensate that is generated by cooling the reaction product gas, the reaction product gas is quickly cooled, and pentachlorodisilane is generated within the condensate; and a recovery step in which the generated pentachlorodisilane is recovered.
Type:
Grant
Filed:
September 25, 2015
Date of Patent:
May 21, 2019
Assignees:
DENKA COMPANY LIMTIED, L'AIR LIQUIDE SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE