With Organic Treating Agent (e.g., Solvent, Surfactant, Or Reactant Yielding Soluble Product, Etc.) Patents (Class 134/22.14)
  • Patent number: 11021418
    Abstract: The present invention relates to a method for olefin oligomerization, and can provide a method for olefin oligomerization. The method includes the steps of: introducing an oligomerization transition metal catalyst, olefin monomers, and a solvent into a reactor and performing an olefin oligomerization reaction to produce an oligomer; introducing a catalyst deactivator to a reaction product of the oligomerization reaction to deactivate the catalyst, with the catalyst deactivator including at least one functional group containing at least one selected from the group including oxygen, phosphor, nitrogen, and sulfur and having a number average molecular weight of 400 or more; separating the oligomer through distillation in a distiller; and separating the catalyst deactivator through the bottom end of the distiller.
    Type: Grant
    Filed: July 18, 2018
    Date of Patent: June 1, 2021
    Assignees: SK Innovation Co., Ltd., SK Global Chemical Co., Ltd.
    Inventors: Sungreal Son, Hyoseung Park, Inhyoup Song, So Hee Sim, Chansaem Park, Woosung Jung
  • Patent number: 10711115
    Abstract: A process for extruding polypropylene comprising extruding a composition comprising a polypropylene and a second acid scavenger and less than about 10 ppm of a nucleating agent.
    Type: Grant
    Filed: May 24, 2018
    Date of Patent: July 14, 2020
    Assignee: Milliken & Company
    Inventors: Kemper D. Lake, Jr., Christopher T. Kochanowicz, Joseph J. Peterson, Clifford S. Bynum, Keith A. Keller
  • Patent number: 10383343
    Abstract: An installation and method for producing and/or processing confectionery masses which are made from at least one liquid raw material and granular and/or powdery raw materials. The installation includes at least a first mixing container and at least one further product-processing device. The first mixing container has at least one raw-material inlet and a product outlet and a mixing device for mixing the raw materials at least largely homogeneously. At least the mixing container includes at least one spraying device in an upper container region, which at least one spraying device serves to feed the at least one liquid raw material, wherein at least one outlet cone of the spraying device is directed, at least in some regions, toward an inner wall surface of the first mixing container.
    Type: Grant
    Filed: August 18, 2016
    Date of Patent: August 20, 2019
    Assignee: NETZSCH-Feinmahltechnik GmbH
    Inventors: Theron Harbs, Holger Moeschl, Lars-Peter Weiland, Sergio Devegili
  • Patent number: 10302236
    Abstract: The present invention provides methods and methods for curing a leakage in a pipeline, the method including at least one gel pig and at least one sealant composition; wherein the at least one gel pig and the at least one sealant composition form a pig train, adapted to move along the pipeline to a region of the leakage and to seal the leakage.
    Type: Grant
    Filed: December 18, 2015
    Date of Patent: May 28, 2019
    Assignee: Curapipe System Ltd.
    Inventors: Samuel Perstnev, Boris Natapov, Alexander Perstnev, Reonald Ukhanov, Peter Paz
  • Patent number: 10209038
    Abstract: A curtain of a flexible fabric is provided that is deployable to create a physical and visual barrier between an employee and a person perpetuating a crime such as a robbery or assault. The barrier can be in the form of a curtain that is electrified with an extreme high voltage, similar to a stun gun, and which prevents the assailant from approaching an employee or a restricted area. The curtain can be mounted in any area where it is beneficial to limit site and access of a trespasser or an assailant, such as between a cashier at a convenience store and the store's open retail area. The curtain can also be used to create temporary safe rooms or deployed within hallways of a restricted area to limit movement of an intruder.
    Type: Grant
    Filed: July 28, 2016
    Date of Patent: February 19, 2019
    Inventor: Christopher D. Wallace
  • Patent number: 10202514
    Abstract: The present invention relates to graffiti removal compositions and the use thereof for the removal of graffiti from surfaces. The compositions comprise (i) alkyl esters of one or more soybean oil fatty acids; (ii) one or more aliphatic diesters of dicarboxylic acids; (iii) one or more compounds of the formula R2C(0)OR3, wherein R2 is a C1-C20 alkyl and R3 is C1-C20 alkyl; and (iv) a surfactant.
    Type: Grant
    Filed: June 18, 2015
    Date of Patent: February 12, 2019
    Assignee: GUARD IT SOLUTIONS PTY LTD
    Inventors: Anthony Leenan, Peter Richardt
  • Patent number: 9791108
    Abstract: A method of hydraulic fracturing is provided which uses metal silicides to generate significant pressure inside a wellbore. The method comprises injecting a fracturing fluid and an aqueous or reacting fluid into the wellbore to react with the fracturing fluid. The fracturing fluid comprises metal silicide, which may be uncoated or coated, and hydrocarbon fluid. The reacting fluid comprises water or a solvent. A method of removing buildup in pipelines such as subsea pipelines which uses metal silicides to generate heat and pressure inside the pipeline is also provided. The method comprises injecting an organic slug and an aqueous slug. The organic slug comprises metal silicide and hydrocarbon fluid. The aqueous slug comprises water. Alternatively, there is also provided a method for purifying flowback water produced from a hydraulic fracturing process comprising adding metal silicide to the flowback water produced from a hydraulic fracturing process.
    Type: Grant
    Filed: May 4, 2017
    Date of Patent: October 17, 2017
    Assignee: SIGNA CHEMISTRY, INC.
    Inventors: Paul H. Krumrine, III, James S. Falcone, Jr., Michael Lefenfeld
  • Patent number: 9758877
    Abstract: Methods and compositions are disclosed for inhibiting corrosion on metal surfaces of gas turbine air compressors. The methods comprise contacting the metal surfaces with a corrosion inhibiting composition comprising at least one filming amine.
    Type: Grant
    Filed: February 28, 2014
    Date of Patent: September 12, 2017
    Assignee: General Electric Company
    Inventors: Sal Esposito, Anthony M. Rossi, Mel Joseph Esmacher, Rebecca Evelyn Hefner, Trevor James Dale, Kelsey Elizabeth Beach
  • Patent number: 9017488
    Abstract: A process for quickly removing hydrocarbon contaminants and noxious gases in a safe and effective manner from catalytic reactors, other media packed process vessels and associated equipment in the vapor phase without using steam. The cleaning agent contains one or more solvents, such as terpenes or other organic solvents. The cleaning agent is injected into contaminated equipment, along with a carrier gas, in the form of a cleaning vapor.
    Type: Grant
    Filed: July 16, 2014
    Date of Patent: April 28, 2015
    Assignee: Refined Technologies, Inc.
    Inventors: Cody Nath, Barry Baker, Sean Sears
  • Patent number: 8999072
    Abstract: Disclosed are methods and apparatus for cleaning heat exchangers and similar vessels by introducing chemical cleaning solutions and/or solvents while maintaining a target temperature range by direct steam injection into the cleaning solution. The steam may be injected directly into the heat exchanger or into a temporary side stream loop for recirculating the cleaning solution or admixed with fluids being injected to the heat exchanger. The disclosed methods are suitable for removing metallic oxides from a heat exchanger under chemically reducing conditions or metallic species such as copper under chemically oxidizing conditions. In order to further enhance the heat transfer efficiency of heating cleaning solvents by direct steam injection, mixing on the secondary side of the heat exchanger can be enhanced by gas sparging or by transferring liquid between heat exchangers when more than one heat exchanger is being cleaned at the same time.
    Type: Grant
    Filed: December 3, 2009
    Date of Patent: April 7, 2015
    Assignee: Westinghouse Electric Company LLC
    Inventors: Robert D. Varrin, Jr., Michael J. Little
  • Publication number: 20150083165
    Abstract: Methods for on-line cleaning hot parts of a gas turbine during its operation are provided. A cleaning agent composition is injected into a hot gas path of the gas turbine, and includes a liquid carrier and a descaling material suspending in the liquid carrier. The descaling material includes at least one oxide, in an anhydrous or a hydrated form, that is derived from calcium, magnesium, titanium, iron, aluminium, silicon in the form of silicates having non-fibrous structures, or phosphorus in the form of alkaline-earth phosphates. Cleaning agents are also provided for use in a gas turbine.
    Type: Application
    Filed: March 25, 2014
    Publication date: March 26, 2015
    Applicant: General Electric Company
    Inventor: Michel Moliere
  • Patent number: 8986461
    Abstract: A cleaning composition and process to remove carbon deposits from combustion equipment components is provided. The de-carbonizing composition is packaged in certain embodiments in an aerosol propellant. The inventive composition is also readily used as a liquid or an atomized mist that is readily introduced into the intake manifold through a tube tolerant of engine inlet operational temperatures and conditions. The invention introduces the composition by a process that precludes the need for engine disassembly.
    Type: Grant
    Filed: March 17, 2014
    Date of Patent: March 24, 2015
    Assignee: Illinois Tool Works, Inc.
    Inventors: Mark E. Hischier, Gregory Hewgill
  • Patent number: 8957005
    Abstract: A silicon wafer cleaning agent includes at least a water-based cleaning liquid, and a water-repellent cleaning liquid for providing water-repellent to an uneven pattern at least at recessed portions during a cleaning process. The water-repellent cleaning liquid is a liquid composed of a water-repellent compound containing a reactive moiety which is chemically bondable to Si in the silicon wafer, and a hydrophobic group, or is a liquid wherein 0.1 mass % or more of the water-repellent compound relative to the total quantity of 100 mass % of the water-repellent cleaning liquid and an organic solvent are mixed and contained therein. A cleaning process wherein a pattern collapse is easily induced can be improved by using the cleaning agent.
    Type: Grant
    Filed: September 15, 2010
    Date of Patent: February 17, 2015
    Assignee: Central Glass Company, Limited
    Inventors: Soichi Kumon, Masanori Saito, Takashi Saio, Hidehisa Nanai, Yoshinori Akamatsu
  • Patent number: 8951467
    Abstract: An embodiment prevents equipment fouling (deposition of unwanted material) in an oil recovery system via implementing passivation of metallic components. By preventing or at least slowing or inhibiting corrosion of equipment or components via passivation, such as passivating heat exchangers, metallic piping, and the like, an embodiment in turn reduces fouling thereof. Other embodiments are described and claimed.
    Type: Grant
    Filed: March 15, 2013
    Date of Patent: February 10, 2015
    Assignee: Chemtreat, Inc.
    Inventors: Robert Wright Bedinger, III, Benjamin Edward Niemaseck, Mark Jason Puchovich, John Richardson
  • Patent number: 8945314
    Abstract: A solid composition includes a polysaccharide hybrid polymer composition and a hydratable salt. In one embodiment, the polysaccharide hybrid polymer composition includes a polysaccharide residue present in an amount from approximately 5% to 90% by weight of the polysaccharide hybrid polymer composition and a residue of at least one ethylenically unsaturated monomer present in an amount from approximately 10% to 75% by weight of the polysaccharide hybrid polymer composition.
    Type: Grant
    Filed: July 30, 2012
    Date of Patent: February 3, 2015
    Assignee: Ecolab USA Inc.
    Inventors: Kerrie E. Walters, Carter Silvernail
  • Patent number: 8940679
    Abstract: The present invention relates to compositions for deodorizing and cleaning, in particular solid compositions in the form of effervescent tablets which can be reconstituted in water to obtain solutions for cleaning and deodorizing. The compositions comprise one or more Bacillus subtilis strain(s), one or more surfactant(s), one or more fragrance(s), one or more descaling agent(s), and one or more effervescent agent(s). The invention further relates to a kit comprising such tablets, as well as methods for obtaining cleaning and deodorizing tablets and solutions and their use for cleaning and deodorizing.
    Type: Grant
    Filed: January 25, 2013
    Date of Patent: January 27, 2015
    Assignee: Pollets S.A.
    Inventor: Abdelhamid Jabrane
  • Publication number: 20140352731
    Abstract: A cleaning composition suitable for removing soil from a variety of surfaces and a method of using the same are provided. Cleaning compositions according to embodiments of the present invention include at least one carbonate ester, including, for example, ethylene carbonate, propylene carbonate, trimethylene carbonate, and combinations thereof. Depending on the specific application, the compositions may also include at least one surfactant and/or at least one thickener. Cleaning compositions as described herein may be particularly useful for removing soil from surfaces of pipes, vessels, and other equipment associated with the production and/or processing of oil and/or natural gas, such as, for example, equipment associated with a hydraulic fracturing process.
    Type: Application
    Filed: May 31, 2013
    Publication date: December 4, 2014
    Inventors: Tony Atabong, Curtis Shaw
  • Publication number: 20140311529
    Abstract: The present invention relates to [1] a detergent composition for endoscope washers, including a nonionic surfactant (A) represented by the following formula (1), a branched-chain fatty acid having not less than 6 and not more than 10 carbon atoms or a salt thereof (B), a defoaming agent (C) and water, R—O—[(EO)m/(PO)n]—H??(1) wherein R represents a branched-chain alkyl group having not less than 7 and not more than 9 carbon atoms; EO represents an ethanediyloxy group; PO represents a propanediyloxy group; m and n each represent an average molar number of addition of the ethanediyloxy or propanediyloxy group in which m is a number of not less than 1 and not more than 30, and n is a number of not less than 2 and not more than 50; and the mark “/” represents that EO and PO may be added either in a random form or in a block form, and an order of addition of EO and PO is optional; and [2] a method of washing an endoscope using an endoscope washer, including the step of washing the endoscope with a mixture inclu
    Type: Application
    Filed: May 28, 2013
    Publication date: October 23, 2014
    Inventors: Masaya Nishio, Tatsuya Sakai
  • Patent number: 8853144
    Abstract: A composition includes a polysaccharide graft polymer composition. In one embodiment, the polysaccharide graft polymer composition includes a polysaccharide residue present in an amount from about 5% to about 90% by weight of the polysaccharide graft polymer composition and a residue of at least one ethylenically unsaturated monomer present in an amount from about 10% to about 75% by weight of the polysaccharide graft polymer composition.
    Type: Grant
    Filed: July 30, 2012
    Date of Patent: October 7, 2014
    Assignee: Ecolab USA Inc.
    Inventors: Carter Silvernail, Erik C. Olson, Klin Rodrigues
  • Patent number: 8841246
    Abstract: A composition includes a polysaccharide hybrid polymer composition. In one embodiment, the polysaccharide hybrid polymer composition includes a polysaccharide residue present in an amount from about 5% to about 90% by weight of the polysaccharide hybrid polymer composition and a residue of at least one ethylenically unsaturated monomer present in an amount from about 10% to about 75% by weight of the polysaccharide hybrid polymer composition.
    Type: Grant
    Filed: July 30, 2012
    Date of Patent: September 23, 2014
    Assignee: Ecolab USA Inc.
    Inventors: Carter Silvernail, Erik C. Olson, Klin Rodrigues
  • Patent number: 8821646
    Abstract: An irrigation system cleaning formulation contains a sufficient concentration of a water-soluble organic acid which has a pK(1)a of less than about 4.0. A cleansing irrigation water contains a sufficient amount of such cleaning formulation, and a method of cleaning an irrigation system uses such cleaning formulation.
    Type: Grant
    Filed: November 18, 2008
    Date of Patent: September 2, 2014
    Inventors: John C. Miller, Deborah L. Miller
  • Publication number: 20140238437
    Abstract: The present invention comprises a method and system for the in-situ cleaning of a heat exchanger tube bundle of carbonaceous deposits. Using the method and system, an organic solvent is brought into fluid communication with one or more heat exchanger tube bundles in a closed system. The closed system is formed at the site of operation of the heat exchanger tube bundles and without having to remove the heat exchanger tube bundles from their shells or other associated equipment. Once the closed system is formed, the organic solvent is brought to a temperature at which it is effective to remove carbonaceous deposits from the heat exchanger tube bundle and flowed through the equipment associated with the heat exchanger tube bundles so as to contact the heat exchanger tube bundles and remove carbonaceous deposits that have formed therein.
    Type: Application
    Filed: February 26, 2014
    Publication date: August 28, 2014
    Applicant: T5 TECHNOLOGIES, INC.
    Inventors: Michael Tomkins, Robert Larsen
  • Publication number: 20140238444
    Abstract: The present invention provides a cleaning method by which the performance of a microchip can be recovered and a cleaning liquid. A method for cleaning a microfluidic device comprising: cleaning a channel that is formed in the microfluidic device, has a surface having a polymer coating, and has been brought into contact with a sample containing nucleic acid and/or protein, by bringing the channel into contact with a cleaning liquid comprised only of an organic solvent having solubility in at least the same volume of water at 25° C., or a cleaning liquid containing 50 vol % or more of the organic solvent in a buffer solution. The method wherein the buffer solution has a pH of 8 to 10. The method wherein the buffer solution further contains 3 to 8M of a protein denaturant. The method wherein the buffer solution has a pH of 2 to 4.
    Type: Application
    Filed: February 27, 2013
    Publication date: August 28, 2014
    Applicant: SHIMADZU CORPORATION
    Inventor: Akihiro Arai
  • Patent number: 8765021
    Abstract: The present invention relates to an aqueous treatment composition for inhibiting corrosion and acid attack on metallic surfaces that comprises a thiourea organic derivative, a polyalkoxylated terpene nonionic surfactant and an acid. The invention also relates to a process for cleaning industrial metallic equipment, in particular heat exchangers in which a heat transfer fluid, generally based on air or on water, flows, with a view to cleaning them and removing scale and other soiling.
    Type: Grant
    Filed: March 26, 2009
    Date of Patent: July 1, 2014
    Assignee: Rhodia Operations
    Inventor: Jean-Emile Zanetto
  • Patent number: 8734589
    Abstract: A heat exchanger may be cleaned by introducing compressed nitrogen and a flushing composition through an injection device.
    Type: Grant
    Filed: August 23, 2012
    Date of Patent: May 27, 2014
    Assignee: The Rectorseal Corporation
    Inventors: Eva Ackerman, Yanwei Cen, William Francis Flynn, Richard Garza
  • Patent number: 8691731
    Abstract: Generating heat within a combination solvent/acid system removes undesirable deposits from petroleum reservoir formations (especially the near well-bore region), oilfield equipment, and petroleum processing equipment. An exothermic reaction occurs between the solvent and the acid and the heat evolved helps remove organic solid deposits. The acids may include organic acid compounds, such as sulfonic acids, sulfuric acid and nitric acid. The solvents may include terpene- and terpene-derivative-containing solvents, including, but not necessarily limited to, limonene, pinene, dipentene, myrcene, turpentines and compounds having at least one double bond, such as methyl furan, dienes, styrene, vinyl acetate and the like. The exothermic reaction produces a great amount of heat, and together with using certain acids and solvents already known as effective to remove paraffin and asphaltene deposition, removing such deposits is improved.
    Type: Grant
    Filed: November 5, 2010
    Date of Patent: April 8, 2014
    Assignee: Baker Hughes Incorporated
    Inventors: David W. Jennings, Samuel Asomaning, Michael E. Newberry
  • Patent number: 8685173
    Abstract: The present invention is generally directed toward methods of cleaning and descaling surfaces contaminated with food soils, especially clean-in-place systems. More particularly, the methods according to the present invention also provide for sanitizing of surfaces contaminated with food soils. Thus, there is provided a single cleaning cycle that may clean, sanitize, and descale food-soiled surfaces, and in certain embodiments, without the need for a pre-rinse step, using an acidic detergent composition comprising a fatty alkyl-1,3-diaminopropane or salt thereof in the presence of an acid selected from the group consisting of inorganic acids, organic acids, and mixtures thereof.
    Type: Grant
    Filed: July 16, 2009
    Date of Patent: April 1, 2014
    Assignee: DeLaval Holding AB
    Inventors: Fahim U. Ahmed, Bruno Van Den Bossche
  • Patent number: 8679366
    Abstract: A composition includes a polysaccharide graft polymer composition and 2-phosphonobutane-1,2,4-tricarboxylic acid. In one embodiment, the polysaccharide graft polymer composition includes a polysaccharide residue present in an amount from approximately 5% to approximately 90% by weight of the polysaccharide graft polymer composition and a residue of acrylic acid, methacrylic acid or a combination thereof present in an amount from approximately 10% to approximately 75% by weight of the polysaccharide graft polymer composition.
    Type: Grant
    Filed: July 30, 2012
    Date of Patent: March 25, 2014
    Assignee: Ecolab USA Inc.
    Inventors: Carter Silvernail, Erik C. Olson
  • Patent number: 8673089
    Abstract: Methods of using an aldimine of formula (I) as cleaning agent or ingredient of a cleaning agent composition for reactive polyurethane compositions, especially for reactive polyurethane hot melt adhesives. It has been found that such cleaning agents can greatly reduce the quantity of wastes and in particular mixtures of blocked and nonblocked reactive polyurethane compositions can be used without problem for gluing, without the gluing being negatively influenced in its properties, especially its thermal stability.
    Type: Grant
    Filed: November 26, 2010
    Date of Patent: March 18, 2014
    Assignee: Sika Technology AG
    Inventors: Doreen Janke, Kai Paschkowski
  • Patent number: 8673088
    Abstract: A device for combining multiple components into a foam mixture and dispensing the foam mixture into a pipe is described. The multiple components are combined immediately prior to dispensing, which maximizes activity for labile, biologically active components whose degradation accelerates upon combining components. Embodiments of the device are relatively light weight and adapted to removably couple to sewer cleaning vehicles.
    Type: Grant
    Filed: September 17, 2010
    Date of Patent: March 18, 2014
    Inventor: Thomas P. Suiter, II
  • Patent number: 8668779
    Abstract: A method of simultaneously cleaning and disinfecting an industrial water system is described and claimed. The method involves the addition to the water of the industrial water system of a Compound selected from the group consisting of the alkali salts of chlorite and chlorate and mixtures thereof; and an acid, followed by allowing the water in the industrial water system to circulate for several hours. The reaction of the alkali salts of chlorite and chlorate and acid produces chlorine dioxide in-situ in the water of the industrial water system. The chlorine dioxide kills microorganisms and the acid acts to remove deposits upon the water-contact surfaces of the equipment. This cleaning and disinfecting method works in a variety of industrial water systems including cooling water systems.
    Type: Grant
    Filed: April 30, 2002
    Date of Patent: March 11, 2014
    Assignee: Nalco Company
    Inventors: Andrew J. Cooper, Jasbir S. Gill, Amit Gupta, Robert F. Kelly, Douglas G. Kelley, Eric R. Myers
  • Patent number: 8647443
    Abstract: A method of cleaning an automatic biochemical analyzer, wherein the cleaning solution includes: at least one anionic surfactant, at least one nonionic surfactant, an alkali metal hydroxide, an alkali metal citrate, and a buffering agent stabilizing the pH value above 13.0. In some embodiments, the cleaning solution provides low residual rate of proteins, low residual rate of lipids, desirable within-batch repeatability in clinical testing, low level of cross-contamination, and low level of reactant deposit after cleaning, without affecting test results of the biochemical analyzer. In some embodiments, the cleaning solution has no corrosive effects on the liquid path and reaction cup of the analyzer. The ingredients of the cleaning solution may also be biodegradable.
    Type: Grant
    Filed: May 20, 2011
    Date of Patent: February 11, 2014
    Assignee: Shenzhen Mindray Bio-Medical Electronics Co., Ltd.
    Inventors: Yuping Zhang, Mulong Liu, Wenjuan Xu, Jun Cheng
  • Patent number: 8636918
    Abstract: A composition includes an anionic polysaccharide hybrid polymer composition and 2-phosphonobutane-1,2,4-tricarboxylic acid. In one embodiment, the polysaccharide hybrid polymer composition includes a polysaccharide residue present in an amount from approximately 5% to approximately 90% by weight of the polysaccharide hybrid polymer composition and a residue of at least one ethylenically unsaturated monomer present in an amount from approximately 10% to approximately 75% by weight of the polysaccharide hybrid polymer composition.
    Type: Grant
    Filed: July 30, 2012
    Date of Patent: January 28, 2014
    Assignee: Ecolab USA Inc.
    Inventors: Carter Silvernail, Erik C. Olson
  • Patent number: 8632638
    Abstract: Disclosed is a method for cleaning deposits from one or more parts of an engine fuel delivery system, the method comprising introducing into the engine fuel delivery system a cleaning composition comprising (a) one or more aromatic hydrocarbon solvents; and (b) one or more propylene glycol ethers.
    Type: Grant
    Filed: November 15, 2011
    Date of Patent: January 21, 2014
    Assignee: Chevron Oronite Company LLC
    Inventors: Felicia Simpson-Green, Damon Vaudrin
  • Patent number: 8628625
    Abstract: A method that uses an L-?-dipalmitoleoyl-phosphatidylcholine (DPPC) surfactant based device that reacts with a substance in a known manner, to detect a substance of interest or to extract a substance of interest from a material is provided. The principles of the present invention are particularly useful in detecting/measuring a substance that is harmful to a human, and also to extracting NACL from saltwater.
    Type: Grant
    Filed: October 1, 2007
    Date of Patent: January 14, 2014
    Inventor: Mark L. Witten
  • Publication number: 20130333729
    Abstract: Disclosed is a dry cleaning method for removing a composition represented by a compositional formula of MgaZnbOHc (0?a?1, 0?b?1, 0?c?1, and 0.5?a+b?1), which accumulates in a film formation chamber or in an exhaust pipe of an apparatus for forming a composition represented by a compositional formula of MgXZn1?XO (0?x?1) into a film, by using a cleaning gas. This method is characterized by that a cleaning gas containing ?-diketone is used and that the composition is removed by reacting the composition accumulated with the cleaning gas at a temperature of from 100° C. to 400° C. It is possible by this method to remove the composition without opening the apparatus.
    Type: Application
    Filed: January 19, 2012
    Publication date: December 19, 2013
    Applicant: Central Glass Company, Limited
    Inventors: Tomonori Umezaki, Yuta Takeda
  • Patent number: 8608863
    Abstract: A method for cleaning a component comprises a first stage including the steps of: (i) loading a component into the cleaning chamber of a flush station, (ii) directing a deionized water stream through first filter means, (iii) introducing carbon dioxide into the filtered water stream, (iv) directing the carbonated water stream into a fluid passage to be cleaned in the component, and (v) collecting the dirty water stream after it passes through the component and directing the collected dirty water stream through second filter means for reuse. The method can further include a second stage including the steps of: (vi) loading the component into a testing chamber of a testing station, (vii) directing a deionized water stream through third filter means, (viii) directing the filtered water stream into the fluid passage in the component, and (ix) collecting the water stream after it passes through the component and directing the collected water stream into a particle counter.
    Type: Grant
    Filed: December 8, 2010
    Date of Patent: December 17, 2013
    Assignee: Parker-Hannifin Corporation
    Inventor: Jerome Francis Stremel, III
  • Patent number: 8562751
    Abstract: A dry cleaning method of a substrate processing apparatus includes forming a metal oxide by oxidizing a metal film adhered to the inside of a processing chamber of the substrate processing apparatus; forming a complex by reacting the metal oxide with ?-diketone; and sublimating the complex to be removed. A cleaning gas containing oxygen and ?-diketone is supplied into the processing chamber while heating the inside of the processing chamber. A flow rate ratio of oxygen to ?-diketone in the cleaning gas is set such that a formation rate of the metal oxide is lower than a formation rate of the complex.
    Type: Grant
    Filed: January 17, 2012
    Date of Patent: October 22, 2013
    Assignees: Tokyo Electron Limited, Central Glass Company, Limited
    Inventors: Isao Gunji, Yusaku Izawa, Hitoshi Itoh, Tomonori Umezaki, Yuta Takeda, Isamu Mori
  • Publication number: 20130239991
    Abstract: A composition for treating a water system to remove scale, microorganisms and biofilm, and corrosion by-products. The composition comprises chelating agents and a surfactant. Depending on the water system being treated, the composition may be a solid dissolved by water in the system being treated or may be a pre-mixed foam or aerosol. A treatment system particularly suitable for flowing water systems comprises a container for holding such a treatment composition and mixing it with a portion of water from the water system, a filter for removing solids dislodged during treatment, and a corrosion monitor. A method for using such a treatment composition comprises draining substantially all existing water in the water system, filling or rinsing the system with fresh water, contacting the treatment composition with substantially all parts of the water system, and draining the treatment composition from the system before resuming normal operations.
    Type: Application
    Filed: January 18, 2013
    Publication date: September 19, 2013
    Applicant: NCH Corporation
    Inventors: Adrian Denvir, David F. Vela, Christina B. Burton, Katrell D. Copeland, Scott M. Boyette, Robert C. Pearce, III
  • Publication number: 20130233350
    Abstract: A method and system for removing hydrocarbon deposits from a heat exchanger tube bundle using an organic solvent. After contact with a heat exchanger tube bundle, the contaminated organic solvent may be treated to remove solids, base waters, and/or suspended hydrocarbons, and then again contacted with a heat exchanger tube bundle for the removal of hydrocarbon deposits. This allows for the removal of hydrocarbon deposits from a heat exchanger tube bundle in an efficient and environmentally friendly manner. The treatment of the heat exchanger tube bundle is also preferably performed using a method and system by which, through contact of the heat exchanger tube bundle with an organic solvent, a large percentage of hydrocarbon deposits are removed from the heat exchanger tube bundle in a short period of time.
    Type: Application
    Filed: March 7, 2012
    Publication date: September 12, 2013
    Inventors: Michael Tomkins, Robert Larsen, Gary L. Gardner
  • Publication number: 20130192649
    Abstract: The present invention relates to the acidic cleaning in the beer industry, and more particularly an improved process for acidic cleaning of the various elements and vessels that are used in the preparation of beer and other and other related fermented beverages, said cleaning being carried out by using a formulation comprising at least one alkane sulphonic acid.
    Type: Application
    Filed: March 13, 2013
    Publication date: August 1, 2013
    Applicant: ARKEMA FRANCE
    Inventor: Arkema France
  • Patent number: 8492473
    Abstract: A purging compound for purging an extruder of polyamides or other polar thermoplastic resins for transitioning to the extrusion of a non-polar thermoplastic resin, includes a non-polar base polymer compounded with an ethylene-methacrylate copolymer, up to 15% of a mineral, and about 1% of a suitable antioxidant.
    Type: Grant
    Filed: March 23, 2011
    Date of Patent: July 23, 2013
    Assignee: Ingenia Polymers Corp.
    Inventors: Sushanta Dhar Roy, Viraj Triokekar, Salvatore D'Uva, Ed Hindy
  • Patent number: 8480812
    Abstract: A process for quickly removing hydrocarbon contaminants and noxious gases in a safe and effective manner from catalytic reactors, other media packed process vessels and associated equipment in the vapor phase without using steam. The cleaning agent contains one or more solvents, such as terpenes or other organic solvents. The cleaning agent is injected into contaminated equipment, along with a carrier gas, in the form of a cleaning vapor.
    Type: Grant
    Filed: June 4, 2009
    Date of Patent: July 9, 2013
    Assignee: Refined Technologies, Inc.
    Inventors: Cody Nath, Barry Baker, Sean Sears
  • Patent number: 8444770
    Abstract: A method for cleaning components of a system for filling holes in a printed circuit board with a fluid fill material includes removing the components being a dispensing head and a manifold connected to the dispensing head preferably as a single unit. The single unit is retained in that format. Excess fluid material from the dispensing head and manifold is evacuated preferably by passing air through the dispensing head and manifold. Then the dispensing head and manifold is placed in a cleaning tub, and the manifold is attached to a solvent pump line. The dispensing head and manifold is flushed with a flow of solvent from the solvent pump line; and excess solvent from the dispensing head and manifold is evacuated, by passing air through the dispensing head and manifold.
    Type: Grant
    Filed: June 29, 2009
    Date of Patent: May 21, 2013
    Assignee: TTM Technologies, Inc.
    Inventors: Tadd Hohlfelder, Brad Moran, Rubin Matthews, Thomas Gannon
  • Patent number: 8361238
    Abstract: A process is provided for removing polymeric fouling on process equipment surfaces to restore the efficiency of such equipment. This is accomplished by contacting the fouled equipment with a solvent comprising at least one non-aromatic hydrocarbon compound, or a mixture of one or more non-aromatic organic compounds and one or more aromatic hydrocarbon compounds, for a period of time sufficient to remove the polymeric fouling.
    Type: Grant
    Filed: January 4, 2012
    Date of Patent: January 29, 2013
    Assignee: Perigee Solutions International, LLC
    Inventors: Michael R. Dorton, Gary L. Gardner, Sr.
  • Patent number: 8353990
    Abstract: A process is provided for chemically decontaminating the surface of a metallic component. In a first treatment step, an oxide layer formed on the component by corrosion of the material of the component is detached from the surface of the component with a first aqueous treatment solution containing an organic decontamination acid. In a subsequent second treatment step, the surface which is at least partially freed of the oxide layer is treated with an aqueous solution containing an active component for removing particles which adhere to the surface. The active component is formed of at least one anionic surfactant from the group including sulphonic acids, phosphonic acids, carboxylic acids and salts of those acids.
    Type: Grant
    Filed: August 17, 2011
    Date of Patent: January 15, 2013
    Assignee: Areva NP GmbH
    Inventors: Rainer Gassen, Luis Sempere Belda, Werner Schweighofer, Bertram Zeiler
  • Patent number: 8344198
    Abstract: A processes is provided to inhibit or limit the decomposition of a halide-containing olefin oligomerization catalyst system during recovery of an oligomerization product. The process includes deactivation of an olefin oligomerization catalyst system present in an olefin oligomerization reactor effluent stream by contact with an alcohol under conditions that minimize potential for deactivated catalyst system decomposition. Such conditions include minimization of the water content of the deactivation agent and concentration of the deactivation agent.
    Type: Grant
    Filed: March 15, 2004
    Date of Patent: January 1, 2013
    Assignee: Chevron Phillips Chemical Company LP
    Inventors: Warren M. Ewert, Bruce E. Kreischer, Ronald D. Knudsen
  • Publication number: 20120285489
    Abstract: [Problem] An object of the present invention is to provide pipe cleaning means that can effectively control introduction of viable bacteria to an inside of an apparatus and contamination occurring in the apparatus and particularly provide a pipe cleaning method and a pipe cleaning mechanism in a luminescence measurement apparatus. [Solution] A cleaning method of a pipe of a luminescence measurement apparatus (10) according to the present invention includes a bacteriolytic process of supplying a sterilization reagent into a supply pipe for hot water or a reagent in the luminescence measurement apparatus (10) and sterilizing an inside of the supply pipe, an ATP removal process of supplying an ATP removal reagent into the supply pipe after the sterilization of the inside of the supply pipe and removing ATP inside the supply pipe, and a process of replacing the ATP removal reagent in the supply pipe with pure water.
    Type: Application
    Filed: January 21, 2011
    Publication date: November 15, 2012
    Inventor: Noe Miyashita
  • Patent number: 8298345
    Abstract: A heat exchanger may be cleaned by introducing compressed nitrogen and a flushing composition through an injection device.
    Type: Grant
    Filed: September 11, 2009
    Date of Patent: October 30, 2012
    Assignee: The Rectorseal Corporation
    Inventors: Eva Ackerman, Yanwei Cen, William Francis Flynn, Richard Garza
  • Patent number: 8298481
    Abstract: A method for sterilizing a plastic bottle in an aseptic filling system according to which at least an inner surface or an outer surface of a bottle is sterilized by injecting a heated sterilizing fluid at 65° C.-90° C. while maintaining internal pressure of the bottle at 1 kPa-20 kPa.
    Type: Grant
    Filed: October 18, 2011
    Date of Patent: October 30, 2012
    Assignee: Toyo Seikan Kaisha, Ltd.
    Inventors: Takeshi Iwashita, Yonosuke Takahara, Kenichi Kominami, Ken Isogawa