With Organic Treating Agent (e.g., Solvent, Surfactant, Or Reactant Yielding Soluble Product, Etc.) Patents (Class 134/22.14)
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Patent number: 8257508Abstract: The invention relates to a method and apparatus relate for the liquefaction of natural gas. In another aspect, the present invention concerns the deriming the interior surfaces of a cryogenic heat exchanger employed in the liquefaction of natural gas. In another aspect, the present invention concerns the utilization of a pump to derim the interior surfaces of a cryogenic heat exchanger.Type: GrantFiled: January 27, 2010Date of Patent: September 4, 2012Assignee: ConocoPhillips CompanyInventors: Karl L. Herzog, Jon M. Mock
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Patent number: 8257509Abstract: The present invention relates to a method and an apparatus for liquefying natural gas.Type: GrantFiled: February 16, 2011Date of Patent: September 4, 2012Assignee: ConocoPhillips CompanyInventors: Karl L. Herzog, Jon M. Mock
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Patent number: 8246906Abstract: A method for antimicrobial treatment (e.g. antimicrobial treatment of food packaging and equipment) comprising applying to microbes a composition containing a diluting solvent (e.g., water), an antimicrobially-active solvent having a density different from the density of the diluting solvent, and an optional cosolvent, surfactant, or additional antimicrobial agent, wherein the amount of antimicrobially-active solvent or additional antimicrobial agent is sufficiently high and the amount of cosolvent or surfactant is sufficiently low so that the composition will provide greater than a 1-log order reduction in the population of bacteria or spores of Bacillus cereus within 10 seconds at 60° C. Preferred methods of the invention employ compositions containing an additional antimicrobial agent such as peroxyacetic acid. Compositions for use in the method can be prepared as concentrates, and used full strength or in diluted form.Type: GrantFiled: February 9, 2009Date of Patent: August 21, 2012Assignee: Ecolab USA Inc.Inventors: Robert D. P. Hei, Guang-jong J. Wei, David A. Halsrud, Kim R. Smith, Teresa C. Podtburg
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Patent number: 8216383Abstract: Disclosed herein is a method and treatment system for rapid cleaning and protecting of automotive cooling systems containing controlled atmosphere brazed aluminum heat exchangers. The method and treatment system can optionally include a conditioning (passivating) step. The treatment system can comprise three different parts: (1) cleaner or cleaning solution; (2) conditioner or conditioning solution; and (3) compatible CAB aluminum protective heat transfer fluid.Type: GrantFiled: July 6, 2010Date of Patent: July 10, 2012Assignee: Prestone Products CorporationInventors: Bo Yang, Aleksei V. Gershun, Peter M. Woyciesjes
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Patent number: 8211239Abstract: A method for cleaning used beer kegs employing an aqueous solution of phosphoric acid, nitric acid and one or more surfactants, e.g., a detergent and/or wetting agent. Preferably, the aqueous cleaning solution has a total nitric acid content of 12 wt % or less. Complete cleaning can be achieved without using any caustic. The cleaning solution can be recycled repeatedly to clean multiple kegs on numerous occasions over a period of time, e.g., several weeks.Type: GrantFiled: September 18, 2009Date of Patent: July 3, 2012Assignee: Birko CorporationInventor: Dana J. Johnson
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Patent number: 8172952Abstract: A method for reducing noxious sulfur species including hydrogen sulfide in sewage collection systems including force mains is disclosed, where the method involves administering a an effective amount of a composition including a water soluble sulfur scavenger and an oil soluble sulfur scavenger in the presence of sufficient surfactant to produce a homogeneous product.Type: GrantFiled: February 21, 2007Date of Patent: May 8, 2012Assignee: Clearwater International, LLCInventors: Mark J. Wanner, Ron Anderson, Thomas P. Wilson, Jr.
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Patent number: 8163102Abstract: A composition is provided for use in cleaning a surface of a cementitious material. The composition includes HCI, urea, complex substituted keto-amine-hydrochloride, an alcohol, an ethoxylate, and a ketone. A method of using the composition includes applying the composition to a surface from which it is desired to clean a cementitious material and removing the composition and released cementitious material from the surface. Methods are also provided for performing hydraulic fracturing of an oil or a gas well; for adjusting a pH of a drilling fluid; for adjusting and maintaining a pH of a process fluid; for solubilizing calcium carbonate in an aqueous suspension or dispersion of calcium carbonate; for removing a foulant in a fluid-handling element; adjusting a pH and lowering a salt level of turf.Type: GrantFiled: May 10, 2011Date of Patent: April 24, 2012Assignee: Green Products & Technologies, LLCInventor: John T. MacDonald
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Patent number: 8142714Abstract: The invention relates to the use of a cleaning agent that contains surfactants and has a pH value of at least 11 when diluted in an aqueous solution and ready for use. Said cleaning agent is used to destabilize prions during mechanical and manual cleaning and/or disinfection of medical and/or surgical instruments and appliances. It has been recognized that this combination enables a reliable destabilization of prions during the mechanical reconditioning of surgical instruments.Type: GrantFiled: January 28, 2003Date of Patent: March 27, 2012Assignee: Chemische Fabrik Dr. Weigert GmbH & Co. KGInventors: Petra Tiarks, Jurgen Staffeldt
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Patent number: 8128755Abstract: Disclosed are cleaning solvents and cleaning methods for metallic compounds deposited on the equipment that supplies organometallic compounds to the manufacturing tool in the photovoltaic industry or the semiconductor industry. The cleaning solvents and the cleaning methods disclosed not only selectively remove the metallic compound without corroding the equipment, but also improve the ordinary cleaning process. Moreover, the cleaning solvents and the cleaning methods disclosed improve maintenance costs for the supply system because the equipment may be cleaned without being detached from the supply system.Type: GrantFiled: June 17, 2010Date of Patent: March 6, 2012Assignee: L'Air Liquide Societe Anonyme pour l'Etude Et L'Exploitation des Procedes Georges ClaudeInventor: Yoichi Sakata
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Patent number: 8124011Abstract: A method for sterilizing a plastic bottle in an aseptic filling system according to which at least an inner surface or an outer surface of a bottle is sterilized by injecting a heated sterilizing fluid at 65° C.-90° C. while maintaining internal pressure of the bottle at 1 kPa-20 kPa.Type: GrantFiled: October 29, 2010Date of Patent: February 28, 2012Assignee: Toyo Seikan Kaisha, Ltd.Inventors: Takeshi Iwashita, Yonosuke Takahara, Kenichi Kominami, Ken Isogawa
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Patent number: 8075699Abstract: A paper-roll core that is a soluble, disposable carrier for cleaning and/or disinfecting chemicals. The paper-roll cores are toilet paper roll cores and paper towel roll cores and are rapidly soluble in water and may release cleansers, disinfectants, colors, etc., upon dissolving. Described are: methods of using, manufacturing, advertising, and distributing the paper-roll cores; and methods of advertising and distributing such paper-roll cores to children, who will particularly enjoy the novelty; and methods of modifying existing paper-roll core manufacturing equipment to manufacture soluble cleanser-dispensing paper-roll cores.Type: GrantFiled: February 17, 2011Date of Patent: December 13, 2011Assignee: The Procter & Gamble CompanyInventor: George H. Butler, III
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Publication number: 20110259371Abstract: A method for cleaning a drain line of a dialysis machine downstream of a filtration unit. The method includes closing inlet and outlet valves of the filtration unit, and closing a bypass valve along a bypass line that connects a source line to a drain line. The method also includes configuring the balancing chamber such that flow is permitted only via the drain line, flowing an amount of a cleaning agent into the drain line through a cleaning agent valve, and rinsing the cleaning agent from the drain line with a rinse fluid.Type: ApplicationFiled: April 26, 2010Publication date: October 27, 2011Applicant: FRESENIUS MEDICAL CARE HOLDINGS, INC.Inventors: Christian Schlaeper, Martin Joseph Crnkovich
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Patent number: 7976640Abstract: A method for the on-line cleaning of a heat exchanger used with petroleum process fluids which create coke deposits of asphaltenic origin on the exchanger tubes. The asphaltenes are removed by re-dissolution in a solvent oil of high solubility power for the asphaltenes. Certain asphaltenic crudes are useful as solvents in view of their chemical similarity to the asphaltene coke precursors; also useful are refined petroleum fractions such as gas oils which are also characterized by their solvency for asphaltenes. The solvent oil may be admitted to the heat exchanger following withdrawal of the process fluid and then allowed to soak and dissolve the asphaltene coke precursors after which the resulting solution may be withdrawn and the exchanger returned to use without being at any time disconnected from its associated process unit.Type: GrantFiled: March 29, 2006Date of Patent: July 12, 2011Assignee: ExxonMobil Research & Engineering CompanyInventors: Douglas S. Meyer, Glen B. Brons, Ryan E. Vick, Douglas P. Bryant, Gary L. Novosad
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Patent number: 7976638Abstract: A composition for removing particulate matter from integrated circuit substrates, including (a) one or more metal ion-free base; (b) a water-soluble metal ion-free onium salt of a polyhedral silsesquioxane; (c) an oxidizing agent; and (d) metal ion-free water, and a composition obtained by combining ingredients including (a), (b), (c) and (d). A process for removing particulate matter from a surface of an integrated circuit device, including applying to the surface the composition including (a), (b), (c) and (d) or applying to the surface the composition obtained by combining ingredients including (a), (b), (c) and (d).Type: GrantFiled: November 12, 2008Date of Patent: July 12, 2011Assignee: Sachem, Inc.Inventor: Jianjun Hao
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Patent number: 7956137Abstract: A polymerisation reactor comprising one or more circulation loops with one or more inlets for raw material, one or more outlets, and a circulation pump for circulating a reactor charge within the circulation loop. A by-pass line for by-passing the circulation pump connects a point of the loop upstream of the pump with a point downstream of the pump, both points being provided with a three way valve.Type: GrantFiled: January 9, 2007Date of Patent: June 7, 2011Assignee: Celanese International CorporationInventor: David Charles Adams
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Publication number: 20110114323Abstract: Generating heat within a combination solvent/acid system removes undesirable deposits from petroleum reservoir formations (especially the near well-bore region), oilfield equipment, and petroleum processing equipment. An exothermic reaction occurs between the solvent and the acid and the heat evolved helps remove organic solid deposits. The acids may include organic acid compounds, such as sulfonic acids, sulfuric acid and nitric acid. The solvents may include terpene- and terpene-derivative-containing solvents, including, but not necessarily limited to, limonene, pinene, dipentene, myrcene, turpentines and compounds having at least one double bond, such as methyl furan, dienes, styrene, vinyl acetate and the like. The exothermic reaction produces a great amount of heat, and together with using certain acids and solvents already known as effective to remove paraffin and asphaltene deposition, removing such deposits is improved.Type: ApplicationFiled: November 5, 2010Publication date: May 19, 2011Applicant: Baker Hughes IncorporatedInventors: David W. Jennings, Samuel Asomaning, Michael E. Newberry
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Patent number: 7938909Abstract: An automated method for determining the cleaning operation of a water treatment or water distribution apparatus or system to which one or more substances are added, the method comprising the steps of: (a) conducting one or more measurements of a property of the or an added substance; (b) comparing the property measurement s) from step (a) with at least one reference value for that property; and (c) determining when the comparison in step (b) is within, above or below a pre-determined range or level for that property. The determination in step (c) can consider whether the cleaning operation has been successfully carried out. The present invention automates and therefore optimizes the cleaning operation of the water treatment or distribution apparatus or system such that expensive periods of non-operation during sanitization or cleaning are minimized both in terms of frequency and duration.Type: GrantFiled: August 8, 2005Date of Patent: May 10, 2011Assignee: Veolia Water Solutions & Technoloiges SupportInventors: Alan Denton Mortimer, Lee Underwood
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Patent number: 7931753Abstract: A method to remove deposits containing magnetite and copper from a container, particularly from a steam generator of a nuclear power plant. In a first step, the container is treated using an alkaline cleaning solution containing a complexing agent forming a soluble complex with iron ions, a reducing agent, and an alkalizing agent. In a second step a further complexing agent forming a more stable complex with iron III ions than the complexing agent used in the first step and an oxidant are added to the cleaning solution of the first step present in the container.Type: GrantFiled: September 8, 2009Date of Patent: April 26, 2011Assignee: Areva NP GmbHInventors: Konrad Bitter, Ursula Hollwedel, Enkhtsetseg Batchuluun
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Patent number: 7919446Abstract: Compositions comprise a purine compound; an alcohol amine; a quaternary ammonium salt; an amino acid, and optionally an antioxidant. The compositions are useful in post-CMP cleaning processes. One particular advantage of these compositions is that they can effectively remove slurry contamination without increasing the roughness of the copper surface.Type: GrantFiled: December 26, 2008Date of Patent: April 5, 2011Assignee: Intermolecular, Inc.Inventors: Zachary M. Fresco, Anh Duong, Chi-I Lang, Nikhil Kalyankar, Nicole Rutherford, Alexander Gorer
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Patent number: 7909935Abstract: The present invention is directed to a method of cleaning an interior surface of a fluid delivery system. The method comprises introducing a first liquid into the fluid delivery system and contacting the interior surface with the first liquid; forming a slurry by introducing a particulate into the first liquid and contacting the interior surface with the slurry; introducing a second liquid into the fluid delivery system and contacting the interior surface with the second liquid; and introducing a third liquid into the fluid delivery system and contacting the interior surface with the third liquid. The first liquid is substantially soluble or substantially insoluble in the second liquid, the second liquid is substantially insoluble in the third liquid, and the particulate is substantially insoluble in the first and second liquids and substantially soluble in the third liquid.Type: GrantFiled: October 10, 2008Date of Patent: March 22, 2011Assignee: PPG Industries Ohio, Inc.Inventors: Jonathan N. Warren, Phillip J. Beauchamp, Finn Bergishagen, Denise A. Palumbo
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Patent number: 7906069Abstract: A method for sterilizing a plastic bottle in an aseptic filling system according to which at least an inner surface or an outer surface of a bottle is sterilized by injecting a heated sterilizing fluid at 65° C.-90° C. while maintaining internal pressure of the bottle at 1 kPa-20 kPa.Type: GrantFiled: August 4, 2006Date of Patent: March 15, 2011Assignee: Toyo Seikan Kaisha, Ltd.Inventors: Takeshi Iwashita, Yonosuke Takahara, Kenichi Kominami, Ken Isogawa
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Patent number: 7799145Abstract: The present invention is a cleaning composition for use with firearms and industrial items in which all of the components of the composition are biodegradable. The selected components of the composition also have a combined flashpoint of over 200° F. The low volatility of the composition enhances the safety factor by its reduced flammability in conjunction with the low odor and other benefits obtained by the biodegradability of the composition. The composition essentially comprises a hydrocarbon solvent and a lubricant which effectively removes the fouling present within the interior arm of a firearm bore and at the same time lubricates and protects the firearm bore to help prevent the formation of rust.Type: GrantFiled: September 16, 2008Date of Patent: September 21, 2010Inventor: John A. Thompson
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Patent number: 7794785Abstract: To provide a pattern formation method capable of forming a pattern by cleaning a liquid droplet ejection head without causing problems during the liquid droplet ejection operation, when the liquid droplet ejection head stored with a storage solution is used again, a pattern formation method includes: filling a passage including a liquid droplet ejection head and a conduit to feed a functional solution to the liquid droplet ejection head with purified water; filling the passage with a solvent dissolving both the purified water and a solvent contained in the functional solution, filling the passage with the solvent contained in the functional solution, surface treating a substrate by forming a lyophobic film on a region surrounding a pattern formation region defined on the substrate; and disposing liquid droplets on the pattern formation region with the liquid droplet ejection head.Type: GrantFiled: April 20, 2004Date of Patent: September 14, 2010Assignee: Seiko Epson CorporationInventor: Hidekazu Moriyama
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Publication number: 20100147333Abstract: Non-high solvency dispersive power (non-HSDP) crude oil with increased fouling mitigation and on-line cleaning effects includes a base non-HSDP crude oil and an effective amount of resins isolated from a high solvency dispersive power (HSDP) crude oil, and method of making same. Also, methods of using such non-HSDP crude oil for on-line cleaning of a fouled crude oil refinery component, for reducing fouling in a crude oil refinery component, and in a system capable of experiencing fouling conditions associated with particulate or asphaltene fouling.Type: ApplicationFiled: December 11, 2008Publication date: June 17, 2010Applicant: ExxonMobil Research and Engineering CompanyInventors: Chris A. Wright, Glen B. Brons, Sharon A. Feiller, George A. Lutz
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Patent number: 7736537Abstract: Chlorofluorocarbon replacement solvents include a main component (first solvent) and a property-modification component (second solvent). The resulting solvent mixtures meet or exceed the solvency, flammability, and compatibility requirements for CFC's while providing similar or improved environmental and toxicological properties. These solvent mixtures can be used in conjunction with refrigeration or heat pumps, electronics, implantable prosthetic devices, oxygen systems, and optical equipment.Type: GrantFiled: October 1, 2008Date of Patent: June 15, 2010Assignee: Mainstream Engineering Corp.Inventors: Dustin Zastrow, John Meyer, Lisa Patton
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Patent number: 7731803Abstract: The present invention is directed to a composition, and a process employing same, for descaling, cleaning and inhibiting the corrosion of process equipment made of steel by including an inhibitory effective amount of acridine orange in the composition.Type: GrantFiled: November 14, 2003Date of Patent: June 8, 2010Assignee: Saudi Arabian Oil CompanyInventor: Abdulghani Jaralla
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Publication number: 20100078047Abstract: A method, composition and apparatus for cleaning an internal surface of a narrow diameter channel.Type: ApplicationFiled: September 30, 2008Publication date: April 1, 2010Inventors: Mohamed Emam Labib, Stanislav S. Dukhin, Joseph J. Murawski, Yacoob Tabani, Ching-Yue Lai
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Patent number: 7682460Abstract: The method for cleaning chemical process and hydrocarbon processing apparatuses is performed by establishing a closed flow circulation loop, under specific operating conditions and in the presence of hydrocarbon-based fluids. The cleaning method is monitored by performing chemical/physical analysis. After cleaning the apparatus(es) can be immediately inserted back into the process. An optional degassing step can also be performed, in case the apparatus(es) has to be disassembled for inspection of maintenance.Type: GrantFiled: June 10, 2003Date of Patent: March 23, 2010Inventor: Marcello Ferrara
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Patent number: 7650930Abstract: A process for the solution polymerization of olefins with improved on-stream time is provided. The solution polymerization process of the current invention comprises a method for the on-line removal of foulant material from one or more heat exchangers downstream of a polymerization reactor. Removal of foulant material is accomplished by deliberately applying a positive pressure differential across a heat exchanger. In the process of the current invention, reactor shut down is not required for the purpose of cleaning foulant material from a heat exchanger.Type: GrantFiled: August 22, 2008Date of Patent: January 26, 2010Assignee: NOVA Chemical (International) S.A.Inventors: Eric Cheluget, Arun Sood, Rob VanAsseldonk, Ryan McCabe
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Publication number: 20090229632Abstract: An apparatus and method for cleaning passageways and the like with a two-phase mixture of gas under pressure and an aqueous cleaning solution. The two-phase cleaning mixture is generated in a module and is passed out of the module at a predetermined rate that determines droplet size, velocity and droplet density at the pipeline surface to be cleaned. The droplets impact the walls of the passageway to be cleaned, thereby fragmenting, eroding and removing contaminants in said passageway. These are then flushed out of the passageway by the two-phase flow. The flow of cleaning solution can be steady or pulsed. The apparatus and process include a clean-in-place system that is useful in food, beverage, pharmaceutical and similar process industries.Type: ApplicationFiled: January 16, 2009Publication date: September 17, 2009Applicant: Princeton Trade and TechnologyInventors: Mohamed Emam Labib, Chung-Yue Lai, Yacoob Tabani
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Patent number: 7575642Abstract: A composition comprising a polypropylene glycol, a polyethylene glycol ester, an amine, and optionally an alcohol. The composition can be used as a purge solution to clean paint equipment.Type: GrantFiled: January 31, 2008Date of Patent: August 18, 2009Assignee: BASF CorporationInventors: David Law, Gregory W Drewno, Robert Ball, Michael J Anchor
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Patent number: 7566409Abstract: Chlorofluorocarbon replacement solvents include a main component (first solvent) and a property-modification component (second solvent). The resulting solvent mixtures meet or exceed the solvency, flammability, and compatibility requirements for CFC's while providing similar or improved environmental and toxicological properties. These solvent mixtures can be used in conjunction with refrigeration or heat pumps, electronics, implantable prosthetic devices, oxygen systems, and optical equipment.Type: GrantFiled: January 24, 2008Date of Patent: July 28, 2009Assignee: Mainstream Engineering CorporationInventors: Dustin Zastrow, John Meyer, Lisa Patton
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Patent number: 7556654Abstract: Methods are disclosed for cleaning a material by applying a cleaning composition having one or more biosurfactants and one or more enzymes to the material. During use, the material is agitated with the cleaning composition. The cleaning composition can be used as a fabric cleaner, carpet cleaner, deodorizer, disinfectant, all purpose cleaner, kitchen counter cleaner, window cleaner, bar soap additive, septic and sewage cleaner, driveway and street cleaner, circuit board cleaner, wheel cleaner, toxic waste cleaner, clean-room cleaner, oil spill cleaner, soil treatment, or metal cleaner.Type: GrantFiled: April 17, 2006Date of Patent: July 7, 2009Inventor: Micheal Nero
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Publication number: 20090149683Abstract: An oil or gas treating fluid is provided by processing the waste stream from biodiesel production.Type: ApplicationFiled: December 5, 2007Publication date: June 11, 2009Applicant: CAM CHEMICAL MANUFACTURING LLCInventors: Spencer S. Awbrey, H. Casey Riney
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Patent number: 7531048Abstract: A cleaning method for a combustor comprises positioning a spray portion of a nozzle through an igniter plug boss and spraying an acid solution inside the combustion chamber. The acid solution impinges the inner liner and the outer liner, dissolving contaminant deposits inside the effusion holes. The nozzle can have a second spray portion outside the combustion chamber to provide acid solution to the radially outward surface of the outer liner. After cleaning, distilled water is sprayed through the nozzle to remove the acid solution residue from the combustor. The used acid solution and distilled water can be collected, filtered and pumped through the nozzle to provide a recirculating cleaning/rinsing system.Type: GrantFiled: February 7, 2005Date of Patent: May 12, 2009Assignee: Honeywell International Inc.Inventors: Gregory O. Woodcock, Robert W. Mahar, William Tesch, Richard A. Bonvouloir, John C. Saunders, Udo Schuelke
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Publication number: 20090107529Abstract: A method and device provide for delivering fluid for cleaning and/or decontamination to a lumen in a medical device. A tube having a plurality of openings therethrough is inserted into the lumen of the medical device the fluid is flowed through the tube, out of the openings and into the lumen.Type: ApplicationFiled: October 31, 2007Publication date: April 30, 2009Inventors: Szu-Min Lin, Robert C. Platt, Peter C. Zhu
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Publication number: 20090101177Abstract: The present invention relates to a composition based on 1,1,1,3,3-pentafluorobutane (HFC-365 mfc), that can be used in deposition, cleaning, degreasing and drying applications. Its object is also a fluid for cleaning internal heat-transfer systems. The object of the present invention is also a method for dissolving oil and for cleaning.Type: ApplicationFiled: July 20, 2005Publication date: April 23, 2009Inventors: Laurent Caron, Jean-Pierre Lallier, Gerard Guilpain
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Publication number: 20090095324Abstract: An underground cable (2) comprises a housing (4) filled with conductive elements (6) and an insulating oil (12). To remove the insulating oil and prevent contamination, a visco-elastic formulation is prepared, suitably from cross-linked polyvinylalcohol, and introduced into the cable (2). The fluid is forced through the cable whereby it removes insulating oil therefrom.Type: ApplicationFiled: April 25, 2007Publication date: April 16, 2009Applicant: AGT Sciences LimitedInventors: Nicholas John Crowther, Donald Eagland
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Publication number: 20090078285Abstract: The invention relates to a method for keeping vacuum piping, particularly the vacuum piping (2, 3, 4) of the waste systems of ships and similar, clean, or for assisting it. The device according to the invention is used to feed acid and bacteria are fed to the end of each vacuum pipe run (3). The feeding takes place mainly automatically by means of controllable hose pumps (102), provided a predefined vacuum prevails in the vacuum pipe run (3).Type: ApplicationFiled: April 10, 2006Publication date: March 26, 2009Inventors: Tauno Marttinen, Mika Laakso, Kaj Pelamo
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Publication number: 20090020140Abstract: Methods and compositions for purging and cleaning a semiconductor fabrication system are disclosed herein. In general, the disclosed methods utilize solvents comprising hydrofluoroethers. Hydrofluoroethers are non-toxic and have low moisture content, preventing heat generation from organometallic precursor hydrolysis. In an embodiment, a method of cleaning a semiconductor fabrication system comprises dissolving at least one chemical precursor used in semiconductor fabrication in at least one delivery line with a solvent to clean the at least one delivery line. The solvent generally comprises a hydrofluoroether. The methods and compositions may be used in a variety of semiconductor film deposition processes.Type: ApplicationFiled: June 9, 2008Publication date: January 22, 2009Applicant: AIR LIQUIDE ELECTRONICS U.S. LPInventors: Zhiwen WAN, Ashutosh Misra, Ziyun Wang
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Publication number: 20090020142Abstract: The method is a method of rinsing an endoscope in an endoscope cleaner placed in a vessel. The method includes a step of charging a surfactant into a vessel in addition to water to fill the vessel with a first rinse water containing the surfactant, a step of rinsing the endoscope placed in the vessel with the first rinse water, a step of supplying only water into the vessel after rinsing with the first rinse water to fill the vessel with a second rinse water that does not contain the surfactant and a step of rinsing the endoscope with the second rinse water. In the method, the action of the surfactant contained in the detergent is effectively utilized in a rinsing treatment of the endoscope while the endoscope is rinsed to thereby ensure that re-deposition of dirt is suppressed to enhance the overall cleaning efficiency.Type: ApplicationFiled: July 15, 2008Publication date: January 22, 2009Applicant: FUJIFILM CorporationInventor: Kuniaki MIYAKO
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Patent number: 7459029Abstract: A cleaning apparatus of organic substances attached to a vapor-deposition mask for low molecular weight organic EL devices comprises a first stage for treating a vapor-deposition mask with a derivative of pyrrolidone, a second stage for rinsing the vapor-deposition mask with water, and a third stage for rinsing the vapor-deposition mask with flowing water. The cleaning apparatus also comprises a fourth stage for treating the vapor-deposition mask with ethanol, a fifth stage for drying the vapor-deposition mask, and a carrying means that carries the vapor-deposition mask to each stage in sequence. It is desirable to adopt N-methyl-2-pyrrolidone as the derivative of pyrrolidone.Type: GrantFiled: December 1, 2004Date of Patent: December 2, 2008Assignee: Seiko Epson CorporationInventors: Toshiko Hosoda, Shinichi Yotsuya
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Patent number: 7449072Abstract: A method and apparatus for removing solid or semi-solid material from within a container, for example removing an energetic material from the casing of an explosive shell. The method is applicable to the demilitarization of aged or obsolete explosive ordnance, for example mortar rounds, and uses ultrasonic energy rather than heat like previous methods. An item to be demilitarized and cleaned is immersed in a fluid contained within a vessel. An ultrasonic probe or wand is inserted into the submerged item, in proximity with the material to be removed. The fluid is the medium for transmitting sonic energy from the probe to the material to fracture and mobilize the material. Mobilized particulates are expelled from the casing, and settle to the bottom of the fluid vessel for collection. At the conclusion of the process, the emptied container shell, now relatively clean, is retrieved from the vessel and salvaged as desired.Type: GrantFiled: July 20, 2006Date of Patent: November 11, 2008Assignee: TPL, Inc.Inventors: Randal Johnson, Catherine Malins
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Patent number: 7435301Abstract: Disclosed are a cleaning solution for preventing damage of a silicon germanium layer when cleaning a semiconductor device including the silicon germanium layer and a cleaning method using the same. The cleaning solution of a silicon germanium layer includes from about 0.01 to about 2.5 percent by weight of a non-ionic surfactant with respect to 100 percent by weight of the cleaning solution, about 0.05 to about 5.0 percent by weight of an alkaline compound with respect to the cleaning solution and a remaining amount of pure water. The damage to an exposed silicon germanium layer can be prevented when cleaning a silicon substrate having a silicon germanium layer. Impurities present on the surface portion of the silicon germanium layer can be effectively removed.Type: GrantFiled: April 13, 2005Date of Patent: October 14, 2008Assignee: Samsung Electronics Co., Ltd.Inventors: Chang-Sup Mun, Doo-Won Kwon, Hyung-Ho Ko, Chang-Ki Hong, Sang-Jun Choi
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Publication number: 20080216872Abstract: There is obtained an MOCVD oriented vaporizer which eliminates a phenomenon that thin-film materials are adhered to a portion of the vaporizer near and around a spout thereof. A carrier gas/small amount oxidizing gas supply part supplies a carrier gas, which is supplied through an internally formed gas passage and which contains a material solution, to a vaporization part; a bubble prevention/material solution supply part supplies a material for preventing generation of bubbles of the carrier gas containing the material solution, and the material solution, into the carrier gas; a solvent vaporization restricting/cooling system restricts vaporization of a solvent; and a swirl flow preventing gas supply part supplies a gas for preventing occurrence of swirl flows near a gas outlet of the vaporization part.Type: ApplicationFiled: February 18, 2004Publication date: September 11, 2008Inventors: Hisayoshi Yamoto, Ryoichi Sakai, Masafumi Shoji, Kazuya Akuto, Ken Nagaoka, Hiroshi Watanuki
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Publication number: 20080202562Abstract: A composition for removing copper from a surface comprises a polyphosphonic acid, a primary amine, and water. Optionally, the composition may also comprise a dialkanolamine and/or a trialkanolamine, a degreaser, and/or a surfactant. The pH of the composition is between 9.0 and 12.5. The method of removing copper from a surface, which may be a gun bore, involves contacting the surface with the composition.Type: ApplicationFiled: October 15, 2007Publication date: August 28, 2008Inventor: Ted M. Schlosser
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Patent number: 7410544Abstract: A method for cleaning a metal plating tank is provided herein. In accordance with the method, the tank is exposed to a first acid (103), after which the tank is exposed to a second acid in the presence of a first oxidizing agent (107).Type: GrantFiled: April 21, 2006Date of Patent: August 12, 2008Assignee: Freescale Semiconductor, Inc.Inventors: Sam S. Garcia, Edward Acosta, Varughese Mathew
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Patent number: 7375065Abstract: A composition for cleaning a fluid delivery system includes an agent which controls the rheology of the fluid so that its apparent viscosity decreases as the fluid is subjected to a shear force. In particular applications, the viscosity of the composition is greater than 600 centipoise when it is not subject to any shear and less than 600 centipoise when subject to a shear of at least 10 1/sec. The fluid may be thixotropic or a Bingham plastic, in some instances. In a specific embodiment, the viscosity of the composition is greater than 3000 centipoise when it is not subject to shear, less than 3000 centipoise at a shear of 10 1/sec, less than 1000 centipoise at a shear of 30 1/sec, and less than 600 centipoise at a shear of 60 1/sec. Also disclosed are methods for cleaning a fluid delivery system with these compositions.Type: GrantFiled: December 21, 2004Date of Patent: May 20, 2008Assignee: Gage Products CompanyInventors: Jeffrey Maxwell, Stephen Summerfield
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Patent number: 7367350Abstract: A film processing device using vaporized liquid source capable of confirming the flow control accuracy of flow control equipment such as a mass flow controller (15) controlling the flow of the liquid source without separating the flow control equipment from piping and disassembling the piping, comprising a bypass passage (41) for bypassing a part of a washing fluid feed passage (32) for feeding washing fluid to a liquid source feed passage (12) and a flowmeter such as an MFM (42), wherein the washing fluid is allowed to flow to the mass flow controller (15) through the MFM (42), and the flow of the washing fluid detected by the MFM (42) is compared with a target flow set in the mass flow controller (15) to check whether the mass flow controller (15) operates normally or not.Type: GrantFiled: February 7, 2003Date of Patent: May 6, 2008Assignee: Tokyo Electron LimitedInventors: Daisuke Toriya, Kenji Homma, Akihiko Tsukada, Kouji Shimomura
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Patent number: RE42248Abstract: A cleaning apparatus of organic substances attached to a vapor-deposition mask for low molecular weight organic EL devices comprises a first stage for treating a vapor-deposition mask with a derivative of pyrrolidone, a second stage for rinsing the vapor-deposition mask with water, and a third stage for rinsing the vapor-deposition mask with flowing water. The cleaning apparatus also comprises a fourth stage for treating the vapor-deposition mask with ethanol, a fifth stage for drying the vapor-deposition mask, and a carrying means that carries the vapor-deposition mask to each stage in sequence. It is desirable to adopt N-methyl-2-pyrrolidone as the derivative of pyrrolidone.Type: GrantFiled: March 26, 2009Date of Patent: March 29, 2011Assignee: Seiko Epson CorporationInventors: Toshiko Hosoda, Shinichi Yotsuya