Metallic Patents (Class 148/24)
  • Patent number: 9724786
    Abstract: Various embodiments of a metal cored wires, hardband alloys, and methods are disclosed. In one embodiment of the present invention, a hardbanding wire comprises from about from about 16% to about 30% by weight chromium; from about 4% to about 10% by weight nickel; from about 0.05% to about 0.8% by weight nitrogen; from about 1% to about 4% by weight manganese; from about 1% to about 4% by weight carbon from about 0.5% to about 5% by weight molybdenum; from about 0.25% to about 2% by weight silicon; and the remainder is iron including trace elements. The hardband alloy produced by the metal cored wire meets API magnetic permeability specifications and has improved metal to metal, adhesive wear resistance compared to conventional hardband alloys.
    Type: Grant
    Filed: November 12, 2013
    Date of Patent: August 8, 2017
    Assignee: Postle Industries, Inc.
    Inventor: Christopher J. Postle
  • Patent number: 9721599
    Abstract: A suspension board with circuit includes a metal supporting board, an insulating base layer formed on one side of the metal supporting board in a thickness direction thereof, a conductive layer, and an insulating cover layer formed on the one side of the insulating base layer to cover the conductive layer. Either one of the insulating base layer and the insulating cover layer includes an opening extending therethrough in the thickness direction. The conductive layer includes a wire formed on the one side of the insulating base layer, and a connection terminal electrically connected to the wire and exposed from the opening to be capable of electrical connection to an electronic element. The suspension board with circuit further includes a protective layer for protecting the connection terminal exposed from the opening.
    Type: Grant
    Filed: June 4, 2015
    Date of Patent: August 1, 2017
    Assignee: NITTO DENKO CORPORATION
    Inventor: Takatoshi Sakakura
  • Patent number: 9610655
    Abstract: A solder paste includes a flux and powder mixed with the flux, where the powder includes first powder and second powder mixed with each other. The first powder may be a tin (Sn) and at least one metal dissolved in the tin (Sn), and the second powder may be a copper (Cu) powder, the surface of which is coated with silver (Ag).
    Type: Grant
    Filed: May 7, 2014
    Date of Patent: April 4, 2017
    Assignee: LG INNOTEK CO., LTD.
    Inventor: Deok Ki Hwang
  • Patent number: 9604315
    Abstract: Provided is a welding method and electrodes (wires) with aluminum as a primary deoxidizer and a basic flux system for joining a workpieces with weld metal of comparable strengths and enhanced toughness. For instance, provided is a welding wire, comprising an aluminum content configured to act as a primary deoxidizer, and an overall composition configured to produce a weld deposit comprising a basic slag over a weld bead, wherein the aluminum content is configured to kill the oxygen in the weld pool, and wherein the oxygen comprises oxygen provided by a shielding gas or produced by heating of welding filler materials. Further provided is a welding method comprising arc welding a workpiece using an electrode having aluminum as a primary deoxidizer under a gas shield to produce a bead of weld deposit and a basic slag over the weld bead.
    Type: Grant
    Filed: October 19, 2015
    Date of Patent: March 28, 2017
    Assignee: ILLINOIS TOOL WORKS INC.
    Inventors: Mario Anthony Amata, Joseph C. Bundy
  • Patent number: 9597753
    Abstract: A solder paste whereby metal does not flow out of a joint during a second or subsequent reflow heating stage. The solder paste excels in terms of temporal stability and exhibits high joint strength at room temperature and at high temperatures. The solder paste comprises a powdered metal component and a flux component, the powdered metal component comprising: 10-70 mass % of a powdered intermetallic compound comprising copper and tin and 30-90 mass % of a solder powder including tin as a main component. Neither the powdered intermetallic compound nor the solder powder contains a copper-only phase, inhibiting the elution of copper ions into the flux.
    Type: Grant
    Filed: March 28, 2014
    Date of Patent: March 21, 2017
    Assignee: Senju Metal Industry Co., Ltd.
    Inventors: Motoki Koroki, Shunsaku Yoshikawa, Sakie Okada, Taro Itoyama, Hideyuki Komuro, Naoko Hirai, Keitaro Shimizu
  • Patent number: 9573836
    Abstract: The present invention concerns a bushing assembly comprising: (a) a liquid glass feeding unit arranged upstream of and in fluid communication with, (b) a first and second tip plate assemblies (1A, 1B) extending along a longitudinal direction, arranged side by side, and each surrounded by side walls and end walls and, the first and second tip plate assemblies being separated from one another by a stiffening rib structure (21) extending along said longitudinal direction, characterized in that, the feeding unit comprises a glass distribution manifold (2), which defines two separate fluid communication paths to the first and second tip plate assemblies (1A, 1B), and in that, the stiffening rib structure (21) forms an integral part of the floor of the manifold (2).
    Type: Grant
    Filed: May 17, 2013
    Date of Patent: February 21, 2017
    Assignee: 3B-Fibreglass sprl
    Inventors: Philippe Simon, Dimitri Laurent, Utku Ahmet Özden, Christoph Broeckmann, Alexander Bezold
  • Patent number: 9572255
    Abstract: An electronic device has a printed substrate having land electrodes and a chip-type electronic component having external electrodes formed on a surface of a component element body. The land electrodes and the external electrodes are bonded via a solder to form electrode bonding parts. A thermosetting resin is filed between the electrode bonding parts. The bonding material contains solder particles having a melting point T1, a thermosetting resin having a curing temperature T2 that is higher than the melting point T1, and an activating agent having an activation temperature T3 that is lower than the curing temperature T2. The viscosity of the contained components except the solder particles at the melting point T1 is 0.57 Pa·s or less, and the melting point T1 and the activation temperature T3 satisfy T1?T3<50° C.
    Type: Grant
    Filed: March 25, 2014
    Date of Patent: February 14, 2017
    Assignee: MURATA MANUFACTURING CO., LTD.
    Inventors: Akihiro Nomura, Hidekiyo Takaoka
  • Patent number: 9541366
    Abstract: A spark generating tube includes a single tube and a pyrotechnical mixture. The single tube only has a single layer of plastic material, such as ethylene vinyl acetate (EVA) and polyethylene. The pyrotechnical mixture has formed a thin layer in contact with the single layer of the single tube. The pyrotechnical contains an oxidizer, a reducing agent, a substance with low temperature of Tammann and an agent for lubricating and adhering, wherein the agent for lubricating and adhering is either talc or graphite, and the reducing agent can be an aluminum powder in microscale. During the process for manufacturing a spark generating tube, the mixture of the oxidizers and additives is formed separately from the reducing agent. The final mixture is obtained only in the single tube formed with an extruder. In this way, only a very small amount of pyrotechnic mixture is formed at any instant.
    Type: Grant
    Filed: August 25, 2014
    Date of Patent: January 10, 2017
    Assignee: IBQ INDUSTRIAS QUIMICAS S/A
    Inventor: Marco Antonio Falquete
  • Patent number: 9529333
    Abstract: A method of assembling a device including first and second parts, the method including: taking the first and second parts; assembling the first and second parts provided by their arrangement so a gap is present between the first and second parts; taking a metal alloy, chosen for its ability to become at least partially amorphous; shaping the metal alloy to fill the gap between the first and second parts to join them and thereby form the device, the metal alloy having been subject to a treatment allowing the alloy to become at least partially amorphous, at a latest at a time of the shaping. The metal alloy is subject to a temperature increase above the melting temperature thereof causing the alloy to lose any local crystalline structure, the increase followed by cooling to a lower temperature than vitreous transition temperature thereof allowing the material to become at least partially amorphous.
    Type: Grant
    Filed: June 22, 2011
    Date of Patent: December 27, 2016
    Assignee: The Swatch Group Research and Development Ltd.
    Inventors: Yves Winkler, Stewes Bourban, Alban Dubach
  • Patent number: 9527168
    Abstract: A titanium oxide raw material for a welding material, which can achieve the improvement in a bead shape and high-speed welding. The titanium oxide raw material has the form of particles and has a composition containing 58.0 to 99.0 mass % of TiO2, 2.5 mass % or less of Si, 3.0 mass % or less of Al, 5.0 mass % or less of Mn, 35.0 mass % or less of Fe, 5.0 mass % or less of Mg and 2.0 mass % or less of Ca, wherein the surface of each of the particles is coated with an oxide and/or a composite oxide of at least one element selected from Ti, Fe, Mn, Al and Si and the atom percentages of Ti, Fe, Mn, Al, Si and O in the oxide and/or the composite oxide fulfill the following three formulae.
    Type: Grant
    Filed: January 25, 2012
    Date of Patent: December 27, 2016
    Assignee: Kobe Steel, Ltd.
    Inventors: Eri Yamamoto, Norio Masaie, Akiyoshi Kataoka
  • Patent number: 9515044
    Abstract: Provided is an electronic device which includes a conductor allowing an electric signal to transmit therethrough, the conductor containing a plurality of species of metal components having different melting points, and internally having a constituent concentration gradient produced as a result of diffusion of the metal components.
    Type: Grant
    Filed: October 14, 2015
    Date of Patent: December 6, 2016
    Assignee: Napra Co., Ltd.
    Inventor: Shigenobu Sekine
  • Patent number: 9504168
    Abstract: A fluxing-encapsulant material and method of use thereof in a thermal compression bonding (TCB) process is described. In an embodiment, the TCB process includes ramping the bond head to 250° C.-300° C. at a ramp rate of 50° C./second-100° C./second. In an embodiment, the fluxing-encapsulant material comprising one or more epoxy resins having an epoxy equivalent weight (EEW) of 150-1,000, a curing agent, and a fluxing agent having a mono-carboxylic acid or di-carboxylic acid and a pKa of 4-5.
    Type: Grant
    Filed: September 30, 2011
    Date of Patent: November 22, 2016
    Inventors: Sivakumar Nagarajan, Sandeep Razdan, Nisha Ananthakrishnan, Craig J. Weinman, Kabirkumar J. Mirpuri
  • Patent number: 9498853
    Abstract: The present invention provides an amorphous caesium aluminum fluoride complex, a process for its production and the use of the complex as a flux, in particular for the soft soldering of aluminum.
    Type: Grant
    Filed: December 20, 2006
    Date of Patent: November 22, 2016
    Inventors: Gerd J. Harms, Hartmut Hofmann, Klaus-Peter Lehmann, Alexander Schiedt
  • Patent number: 9475154
    Abstract: Electrodes for depositing hardfacing alloys containing boron, carbon, chromium, manganese, and silicon on the surface of metal components that are subjected to high thermal and mechanical stresses. The deposited hardfacing alloys have from about 2.5 to about 14.0 atomic percent boron and have a hardness on the Rockwell “C” scale of at least about 65 HRC in the first layer of the weld deposit.
    Type: Grant
    Filed: May 30, 2013
    Date of Patent: October 25, 2016
    Assignee: Lincoln Global, Inc.
    Inventors: Daniel J Langham, Badri K Narayanan
  • Patent number: 9227273
    Abstract: There is provided a high-temperature Pb-free solder paste having the strength required to join electronic parts to a substrate and having excellence in wettability and workability. The solder paste formed by mixing a solder alloy and a flux, the solder alloy consisting of, based on the total mass of the solder alloy as 100 mass %: 0.4 to 13.5 mass % of Zn, at least one of 0.01 to 2.0 mass % of Cu or 0.03 to 0.7 mass % of Al, and a balance being Bi except for inevitable impurities.
    Type: Grant
    Filed: November 18, 2011
    Date of Patent: January 5, 2016
    Assignee: SUMITOMO METAL MINING CO., LTD.
    Inventor: Takashi Iseki
  • Patent number: 9209155
    Abstract: The present invention aims to provide a method for producing a semiconductor device, the method being capable of achieving high reliability by suppressing voids. The present invention also aims to provide a flip-chip mounting adhesive for use in the method for producing a semiconductor device. The present invention relates to a method for producing a semiconductor device, including: step 1 of positioning a semiconductor chip on a substrate via an adhesive, the semiconductor chip including bump electrodes each having an end made of solder; step 2 of heating the semiconductor chip at a temperature of the melting point of the solder or higher to solder and bond the bump electrodes of the semiconductor chip to an electrode portion of the substrate, and concurrently to temporarily attach the adhesive; and step 3 of removing voids by heating the adhesive under a pressurized atmosphere, wherein the adhesive has an activation energy ?E of 100 kJ/mol or less, a reaction rate of 20% or less at 2 seconds at 260° C.
    Type: Grant
    Filed: August 5, 2013
    Date of Patent: December 8, 2015
    Assignee: SEKISUI CHEMICAL CO., LTD.
    Inventors: Sayaka Wakioka, Hiroaki Nakagawa, Yoshio Nishimura, Shujiro Sadanaga
  • Patent number: 9107332
    Abstract: A printed circuit board includes a base, a circuit pattern, a solder mask, an activated metal layer, a plurality of metal seed layers, and a plurality of metal bumps. The conductive circuit pattern is formed on the base, to include a plurality of conductive pads. The solder mask is formed on a surface of the conductive circuit pattern and portions of the base are exposed from the circuit pattern. The solder mask includes blind vias corresponding to the pads, and laser-activated catalyst. The activated metal layer is obtained by laser irradiation at the wall of the blind via. The activated metal layer is in contact with the solder mask. The metal seed layer is formed on the activated metal layer and the pads. Each metal bump is formed on the metal seed layer, and each metal bump protrudes from the solder mask.
    Type: Grant
    Filed: April 16, 2013
    Date of Patent: August 11, 2015
    Assignee: Zhen Ding Technology Co., Ltd.
    Inventor: Wen-Hung Hu
  • Patent number: 9095936
    Abstract: The present invention relates to variable melting point solder formulations. The solder is comprised of at least one base metal or base metal alloy, preferably alloyed with at least one melting point depressant metal, such that the solidus point of the solder composition is reduced to an initial solidus temperature. Said base metal or base metal alloy, alloyed with at least one melting point depressant metal is mixed with at least one additive metal or additive metal alloy. When heated to a process temperature above said initial solidus temperature, a reaction occurs between the melting point depressant metal, and the additive metal, such that solidification occurs at the process temperature via the formation of intermetallic phases, effectively increasing the solidus of the base metal, and of the overall solder.
    Type: Grant
    Filed: August 26, 2011
    Date of Patent: August 4, 2015
    Assignee: DYNAJOIN CORPORATION
    Inventors: Douglas J. McIsaac, Mark A. Whitney, Stephen F. Corbin
  • Patent number: 9085051
    Abstract: Certain example embodiments of this invention relate to silver pastes that are capable of making an electrical connection with at least one conductive layer in a layer stack, even where the at least one conductive layer is protected by one or more strong dielectric layers, and/or methods of making the same. Certain example embodiments include a chemically modified silver paste that may be cured or fired using a standard glass tempering furnace (e.g., an electrical or gas-fuelled furnace) or a short-wave infrared heating process at temperatures below 750 degrees C. In certain example embodiments, the fluorine causes apertures or micro-factures in the dielectric layer(s), which allows the silver in the paste to move therethrough (e.g., by capillary action) to form a contact with the conductive layer(s).
    Type: Grant
    Filed: March 29, 2010
    Date of Patent: July 21, 2015
    Assignee: Gaurdian Industries Corp.
    Inventor: Jemssy Alvarez
  • Publication number: 20150136461
    Abstract: A solder alloy of a tin-silver-copper solder alloy, containing tin, silver, antimony, bismuth, copper, and nickel, and substantially does not contain germanium, relative to the total amount of the solder alloy, the silver content is more than 1.0 mass % and less than 1.2 mass %, the antimony content is 0.01 mass % or more and 10 mass % or less, and the bismuth content is 0.01 mass % or more and 3.0 mass % or less.
    Type: Application
    Filed: June 25, 2013
    Publication date: May 21, 2015
    Inventors: Yoji Imamura, Kazuki Ikeda, JinYu Piao, Tadashi Takemoto
  • Publication number: 20150125281
    Abstract: A multi-component braze filler alloy comprising at least 70% by weight MarM509A superalloy with the remainder MarM509B superalloy is diffusion brazed to a CM247 alloy base substrate, such as a gas turbine blade or vane. It is shown that generally higher braze temperatures lead to improved results including the possibility of re-welding such a brazed component, resulting in a re-repaired brazed component capable of continued commercial service.
    Type: Application
    Filed: November 4, 2013
    Publication date: May 7, 2015
    Inventors: Petya M. Georgieva, James A. Yarbrough
  • Publication number: 20150110548
    Abstract: The present disclosure provides compositions and methods for forming three-dimensional structures atop substrates. These structures may be formed and processed so as to braze together two substrates. The structures may be controllably formed in three dimensions so as to accommodate virtually any substrate geometry or configuration. The structures may also be disposed so as to maintain spacing between two surfaces.
    Type: Application
    Filed: October 22, 2014
    Publication date: April 23, 2015
    Inventor: Aarne H. Reid
  • Publication number: 20150090367
    Abstract: A flux for soldering includes a base resin, a solvent, and an activating agent. The base resin contains a rosin. An amount of the rosin to be incorporated is from 0% by weight to 30% by weight with respect to a total amount of the base resin. The activating agent includes a compound having a plurality of carboxyl groups on a cyclohexyl structure represented by a general formula (1). X is (a) one or more carboxyl groups, or (b) one or more carboxyl groups and at least one selected from a hydrogen atom, chloro group, bromo group, alkyl group, and cyclohexyl group. A position of the X is not limited. A number of the X is one or more. The X may have either one of the (a) and (b) alone, or a plurality of the (a) and (b) in combination.
    Type: Application
    Filed: September 25, 2014
    Publication date: April 2, 2015
    Applicant: TAMURA CORPORATION
    Inventors: Masahiro TSUCHIYA, Akira KITAMURA, Momoko SEINO, Masaya ARAI
  • Publication number: 20150086776
    Abstract: The present invention relates to a blend of at least one boron source and at least one silicon source, wherein the blend comprises boron and silicon in a weight ratio boron to silicon within a range from about 5:100 to about 2:1, wherein silicon and boron are present in the blend in at least 25 wt %, and wherein the at least one boron source and the at least one silicon source are oxygen free except for inevitable amounts of contaminating oxygen, and wherein the blend is a mechanical blend of powders, and wherein particles in the powders have an average particle size less than 250 ?m. The present invention relates further to a composition comprising the blend a substrate applied with the blend, a method for providing a brazed product, and uses.
    Type: Application
    Filed: March 27, 2013
    Publication date: March 26, 2015
    Applicant: ALFA LAVAL CORPORATE AB
    Inventors: Per Sjödin, Kristian Walter
  • Publication number: 20150075676
    Abstract: The object of the present invention is to provide a soldering-flux-oriented novel base resin that enhances the fluidity of a soldering flux and both the visco-stability and adhesion of a solder paste, while improving the color tone and anti-crack property of the flux residue. The present invention is directed to a base resin for a soldering flux, the base resin comprising a rosin (A) containing at least 15 wt % of a pimarane-type resin acid (a-1), at least 1 wt % of a labdane-type resin acid (a-2), and at least 50 wt % of an abietane-type resin acid that has no conjugated double bond (a-3).
    Type: Application
    Filed: May 13, 2013
    Publication date: March 19, 2015
    Applicant: ARAKAWA CHEMICAL INDUSTRIES, LTD.
    Inventors: Yasushi Funakoshi, Takashi Nakatani, Tetsuya Yoshimoto
  • Publication number: 20150069638
    Abstract: According to one embodiment, a metallic particle paste includes a polar solvent and particles dispersed in the polar solvent and containing a first metal. A second metal different from the first metal is dissolved in the polar solvent.
    Type: Application
    Filed: July 22, 2014
    Publication date: March 12, 2015
    Applicant: Kabushiki Kaisha Toshiba
    Inventors: Daisuke HIRATSUKA, Tomohiro IGUCHI, Masayuki UCHIDA
  • Publication number: 20150068713
    Abstract: The invention relates to a solder powder for connecting components made of aluminium or aluminium alloys by brazing, in particular a brazing powder for connecting heat exchanger components. The solder powder consists of powder particles on an aluminium-silicon base having a weight fraction of more than 12% by weight of silicon, wherein the powder particles have been produced by a rapid solidification and contain uniformly distributed silicon primary crystal precipitations in the eutectic aluminium-silicon alloy structure. Coating with such a solder powder leads to a uniform distribution of the silicon on the surface of the component coated with solder powder and thus to the same good soldering results.
    Type: Application
    Filed: March 20, 2013
    Publication date: March 12, 2015
    Inventors: Norbert William Sucke, Lothar Löchte, Martin Grzesik
  • Publication number: 20150059928
    Abstract: Provided is flux which is capable of suppressing increase in the viscosity of solder paste during its storage and is also capable of improving the fusibility of a solder alloy. In the flux which contains an activator and a solvent and forms solder paste by being mixed with a granular solder alloy, this flux contains a solvent of monoalkyl propylene glycol series. It is preferable that the solvent of monoalkyl propylene glycol series is butyl propylene triglycol or butyl propylene diglycol. It is also preferable that a contented amount of the solvent of monoalkyl propylene glycol series is equal to or more than 75% but equal to or less than 100% relative to a contented amount of all the solvents.
    Type: Application
    Filed: April 5, 2012
    Publication date: March 5, 2015
    Applicant: Senju Metal Industry Co., Ltd.
    Inventors: Tomohiro Yamagame, Daisuke Minakuchi
  • Patent number: 8968488
    Abstract: A cream solder obtained by kneading an Sn—Ag—Cu alloy together with a flux, wherein the Sn—Ag—Cu alloy includes a mixture of a first powdery alloy and a second powdery alloy, the first powdery alloy is represented by an Sn—Ag phase diagram having a solid-liquid coexistence region and has a given silver amount which is larger than that in the eutectic composition (3.5 wt. % silver), and the second powdery alloy has a silver amount which is that in the eutectic composition (3.5 wt. % silver) or which is close to that in the eutectic composition and is smaller than that in the first powdery alloy. This cream solder has excellent strength and thermal stability, and satisfactory bonding properties. It is based on an inexpensive Sn—Ag—Cu solder alloy. It is suitable for use as a high-temperature-side lead-free solder material conformable to temperature gradation bonding. Also provided is a method of soldering.
    Type: Grant
    Filed: July 3, 2007
    Date of Patent: March 3, 2015
    Assignees: Fuji Electric Co., Ltd., Nihon Handa Co., Ltd.
    Inventors: Mitsuo Yamashita, Tomoaki Goto, Takeshi Asagi
  • Publication number: 20150053753
    Abstract: The present invention addresses the problem of providing a composite nanometal paste which is relatively low in price and is excellent in terms of bonding characteristics, thermal conductivity, and electrical property. The present invention is a copper-filler-containing composite nanometal paste that contains composite nanometal particles each comprising a metal core and an organic coating layer formed thereon. The metal paste contains a copper filler and contains, as binders, first composite nanometal particles and second composite nanometal particles which differ from the first composite nanometal particles in the thermal decomposition temperature of the organic coating layer, wherein the mass proportion W1 of the organic coating layer in the first composite nanometal particles is in the range of 2-13 mass %, the mass proportion W2 of the organic coating layer in the second composite nanometal particles is in the range of 5-25 mass %, and these particles satisfy the relationships W1.
    Type: Application
    Filed: March 30, 2012
    Publication date: February 26, 2015
    Applicants: Applied Nanoparticle Laboratory Corporation, Shindengen Electric Manufacturing Co., Ltd.
    Inventors: Teruo Komatsu, Ryo Matsubayashi
  • Patent number: 8961709
    Abstract: A solder paste using a Sn—Ag base, Sn—Cu base, or similar alloy powder has a high melting point, so it causes thermal damage to electronic devices. Sn—Ag—In base lead-free solder alloys having a low melting temperature have been studied, but they are difficult to use because they cause much occurrence of chips standing up during reflow. The present invention forms a solder paste by separating a Sn—Ag—In base lead-free solder into first and second solder alloy powders for which the difference in their peak temperatures measured by differential thermal analysis is at least 10° C. and blends the mixed powders with a flux.
    Type: Grant
    Filed: March 9, 2004
    Date of Patent: February 24, 2015
    Assignee: Senju Metal Industry Co., Ltd.
    Inventors: Kunihito Takaura, Kaichi Tsuruta, Hiroshi Kawanakago, Hiroshi Takahashi
  • Patent number: 8950652
    Abstract: A sintering method is provided which allows components to be joined to each other in a stable way, wherein the processing temperature is less than 200° C. and stable contact points are produced, which have low porosity and also high electrical and thermal conductivity. The method for joining components includes (a) providing a sandwich arrangement having at least (a1) one component 1, (a2) one component 2, and (a3) a metal paste located between component 1 and component 2, and (b) sintering the sandwich arrangement. The metal paste contains (A) 75-90 weight percent of at least one metal present in the form of particles having a coating containing at least one organic compound, (B) 0-12 weight percent of at least one metal precursor, (C) 6-20 weight percent of at least one solvent, and (D) 0.1-15 weight percent of at least one sintering agent selected from the group comprising (i) organic peroxides, (ii) inorganic peroxides, and (iii) inorganic acids.
    Type: Grant
    Filed: September 3, 2010
    Date of Patent: February 10, 2015
    Assignee: Heraeus Materials Technology GmbH & Co. KG
    Inventors: Michael Schäfer, Wolfgang Schmitt, Jian Zeng
  • Patent number: 8950653
    Abstract: A sintering method allows components to be joined to each other in a stable way at a processing temperature of less than 200° C., producing stable contact points having low porosity and high electrical and thermal conductivity. The method includes (a) providing a sandwich arrangement having at least a first component, a second component, and a metal paste located between the first and second components, and (b) sintering the sandwich arrangement. The metal paste includes (A) 75-90 wt. % of at least one metal present in the form of particles having an organic compound-containing coating, (B) 0-12wt % of at least one metal precursor, (C) 6-20wt % of at least one solvent, and (D) 0.1-15 wt % of at least one sintering agent selected from (i) salts of C1-C4 organic acids, (ii) esters of C1-C4 organic acids, and (iii) carbonyl complexes.
    Type: Grant
    Filed: September 3, 2010
    Date of Patent: February 10, 2015
    Assignee: Heraeus Materials Technology GmbH & Co. KG
    Inventors: Michael Schäfer, Wolfgang Schmitt, Jian Zeng
  • Publication number: 20150035137
    Abstract: There are provided a solder joint structure, a power module using the joint structure, a power module substrate with a heat sink and a method of manufacturing the same, as well as a solder base layer forming paste which is disposed and fired on a metal member to thereby react with an oxide film generated on the surface of the metal member and form the solder base layer on the metal member, capable of suppressing the occurrence of waviness and wrinkles on the surface of the metal member even at the time of loading the power cycle and heat cycle and improving the joint reliability with a joint member.
    Type: Application
    Filed: February 14, 2013
    Publication date: February 5, 2015
    Inventors: Shuji Nishimoto, Kimihito Nishikawa, Yoshiyuki Nagatomo
  • Publication number: 20150027768
    Abstract: The present invention provides a solder bump formation resin composition which ensures resist (e.g., dry film) removability and which exhibits excellent solder bonding performance, even when the working substrate is placed at high temperature during reflowing, baking, or a similar process. The solder bump formation resin composition contains (A) at least one species selected from among an alkali-dissoluble thermoplastic resin having an acid value (mgKOH/g) of 110 or higher, an unsaturated fatty acid polymer having an acid value of 80 or higher, and an unsaturated fatty acid-aliphatic unsaturated compound copolymer having an acid value of 50 or higher; (B) a solvent; and (C) a solder powder, and contains no activating agent.
    Type: Application
    Filed: July 25, 2014
    Publication date: January 29, 2015
    Inventors: Yasuhiro TAKASE, Kazuki HANADA, Kazunori KITAMURA
  • Publication number: 20150027589
    Abstract: A solder paste which solves any nozzle clogging that suddenly occurs in a case of being used in a discharging method and which also realizes residue-free because flux is decomposed by heating during soldering. In the solder paste produced by mixing solder powders with the flux, the flux is flux containing polyalkyl-methacrylate of not less than 1.0 mass % and less than 2.0 mass % as methacrylate polymer of an amount such that it prevents the solder powders from being sedimented at ordinary temperature and it is decomposed or evaporated in the process of heating during the soldering, and containing stearic acid amide of not less than 5.0 mass % and less than 15.0 mass %, as viscosity modifier, wherein viscosity is 50 through 150 Pa·s. It is preferable that the content of flux in the solder paste is not less than 11 mass % and less than 13 mass %.
    Type: Application
    Filed: December 25, 2012
    Publication date: January 29, 2015
    Applicants: Senju Metal Industry Co., Ltd., Denso Corporation
    Inventors: Sakie Okada, Motoki Koroki, Hiroaki Iseki, Taro Itoyama, Yoshitsugu Sakamoto, Hiromasa Hayashi
  • Publication number: 20150028085
    Abstract: The occurrence of uneven drying in the center and end of a surface of a bonding layer during a desolvation process of a pre-drying step is reduced to ensure highly reliable bonding without peeling of a bonding surface even after repeated exposure to heat shock after bonding. The bonding material of the present invention to achieve the object contains silver nanoparticles coated with organic substance having 6 or less carbon atoms and having an average primary particle diameter of 10 to 30 nm as main silver particles, silver nanoparticles coated with an organic substance having 6 or less carbon atoms and having an average primary particle diameter of 100 to 200 nm as secondary silver particles, two kinds of solvents having different boiling points, and a dispersant.
    Type: Application
    Filed: January 20, 2012
    Publication date: January 29, 2015
    Applicant: DOWA ELECTRONICS MATERIALS CO., LTD.
    Inventors: Keiichi Endoh, Satoru Kurita, Minami Nagaoka
  • Publication number: 20150030837
    Abstract: The present invention relates to an intermediate product for joining and coating by brazing comprising a base metal and a blend of boron and silicon, said base metal having a solidus temperature above 1040° C., and the intermediate product has at least partly a surface layer of the blend on the base metal, wherein the boron in the blend is selected from a boron source, and the silicon in the blend is selected from a silicon source, and wherein the blend comprises boron and silicon in a ratio of boron to silicon within a range from about 3:100 wt/wt to about 100:3 wt/wt. The present invention relates also to a stacked intermediate product, to an assembled intermediate product, to a method of brazing, to a brazed product, to a use of an intermediate product, to a pre-brazed product, to a blend and to paint.
    Type: Application
    Filed: March 27, 2013
    Publication date: January 29, 2015
    Applicant: ALFA LAVAL CORPORATE AB
    Inventors: Per Sjödin, Kristian Walter
  • Publication number: 20150021377
    Abstract: A method of forge welding includes placing at least two components for welding together, adjacent each other and with an exothermic flux mixture placed between the components. The exothermic flux mixture is heated to initiate an exothermic reaction and the faying surfaces of the two components are pressed together. The components being welded may be tubular, in particular pipes. Apparatus for the method of forge welding and exothermic flux mixtures for the method of forge welding are also provided.
    Type: Application
    Filed: February 22, 2013
    Publication date: January 22, 2015
    Applicant: TUBEFUSE APPLICATIONS B.V.
    Inventors: Wayne RUDD, Hu Chun YI, Jeremy Joseph ITEN
  • Publication number: 20150014399
    Abstract: The present invention provides a conductive paste for die bonding comprising a metal powder and an organic solvent, the metal powder comprising: one or more metal particles selected from a silver powder, a palladium powder, and a copper powder, the metal particles having a purity of 99.9% by mass or higher and an average particle size of 0.01 ?m to 1.0 ?m; and a coating layer made of gold covering at least part of the metal particles. The conductive paste according to the present invention can suppress the occurrence of defects such as voids in a bonded part when a semiconductor element or the like is die-bonded to a substrate.
    Type: Application
    Filed: March 21, 2013
    Publication date: January 15, 2015
    Applicant: TANAKA KIKINZOKU KOGYO K.K.
    Inventors: Toshinori Ogashiwa, Masayuki Miyairi, Akikazu Shioya
  • Publication number: 20150008022
    Abstract: Provided are a conductive particle and a conductive material which are capable of decreasing the connection resistance and suppressing generation of voids in a connection structure when the connection structure is obtained by electrically connecting electrodes. The conductive particle according to the present invention has a solder at a conductive surface, wherein a group including a carboxyl group is covalently bonded to the surface of the solder; and the conductive material according to the present invention includes the conductive particles and a binder resin.
    Type: Application
    Filed: February 19, 2013
    Publication date: January 8, 2015
    Inventors: Ryohei Masui, Takashi Kubota, Hideaki Ishizawa
  • Patent number: 8925789
    Abstract: A method is provided for connecting at least two components, in which a sintering preform is used. This preform includes a carrier having a surface that has at least one structuring element containing hardened paste, wherein the hardened paste contains: (a) metal particles having a coating that contains at least one organic compound; and (b) at least one sintering aid selected from the group consisting of (b1) organic peroxides, (b2) inorganic peroxides, (b3) inorganic acids, (b4) salts of organic acids, wherein the organic acids have 1-4 carbon atoms, (b5) esters of organic acids, wherein the organic acids have 1-4 carbon atoms, and (b6) carbonyl complexes. The surface of the carrier having the hardened paste is not reactive to the constituents of the paste.
    Type: Grant
    Filed: September 2, 2011
    Date of Patent: January 6, 2015
    Assignee: Heraeus Materials Technology GmbH & Co. KG
    Inventors: Michael Schäfer, Wolfgang Schmitt
  • Publication number: 20140345750
    Abstract: Pre-flux coating for the manufacturing of components by brazing, in particular manufacturing of heat exchangers of aluminium components including one or more fluxes and filler material. The coating is composed of one ore more fluxes in the form of potassium aluminum fluoride K1-3AIF4.6, potassium trifluoro zincate, KZnF3, lithium aluminum fluoride Li3AIF6, filler material in the form of metallic Si particles, Al—Si particles and/or potassium fluoro silicate K2S1F6, and additive in the form of alumminium oxide and/or other suitable oxide or material forming a post braze ceramic layer, and further including solvent and binder containing at least 10% by weight of a synthetic resin which is based, as its main constituent, on methacrylate homopolymer or methacrylate copolymer.
    Type: Application
    Filed: September 6, 2012
    Publication date: November 27, 2014
    Inventors: Dagmar Steiner, Jan Halvor Nordlien, Jeffrey L. Insalaco
  • Patent number: 8888932
    Abstract: A lead-free solder alloy which can be used for soldering of vehicle-mounted electronic circuits and which exhibits high reliability is provided. The alloy consists essentially of Ag: 2.8-4 mass %, In: 3-5.5 mass %, Cu: 0.5-1.1 mass %, if necessary Bi: 0.5-3 mass %, and a remainder of Sn. In is at least partially in solid solution in the Sn matrix.
    Type: Grant
    Filed: July 17, 2008
    Date of Patent: November 18, 2014
    Assignee: Senju Metal Industry Co., Ltd.
    Inventors: Yuji Kawamata, Minoru Ueshima, Tomu Tamura, Kazuhiro Matsushita, Masashi Sakamoto
  • Publication number: 20140332116
    Abstract: A solder paste includes a flux and powder mixed with the flux, where the powder includes first powder and second powder mixed with each other. The first powder may be a tin (Sn) and at least one metal dissolved in the tin (Sn), and the second powder may be a copper (Cu) powder, the surface of which is coated with silver (Ag).
    Type: Application
    Filed: May 7, 2014
    Publication date: November 13, 2014
    Applicant: LG INNOTEK CO., LTD.
    Inventor: Deok Ki Hwang
  • Patent number: 8882934
    Abstract: In solder powder having an average particle size of 5 ?m or less and constituted by a center core and a covering layer covering the center core, wherein the center core consists of an intermetallic compound of silver and tin, or silver and the intermetallic compound of silver and tin, the covering layer consists of tin, and an intermediate layer which consists of an intermetallic compound of copper and tin is interposed between the center core and the covering layer so that at least a part of the center core is covered thereby.
    Type: Grant
    Filed: August 22, 2012
    Date of Patent: November 11, 2014
    Assignee: Mitsubishi Materials Corporation
    Inventors: Sho Nakagawa, Hiroki Muraoka, Kanji Kuba, Yousuke Kawamura
  • Publication number: 20140285039
    Abstract: An aluminum wire body, in which an aluminum or aluminum alloy electric wire and a metal to be joined are joined by solder, wherein the solder includes an oxide glass including vanadium and a conducting particle. Preferably, the conducting particle contained in the solder is 90% by volume or less and the oxide glass is 20% by volume to 90% by volume. Further preferably, the oxide glass includes 40% by mass or more of Ag2O in terms of oxides and the glass transition point is 180° C. or less.
    Type: Application
    Filed: February 11, 2014
    Publication date: September 25, 2014
    Applicant: Hitachi, Ltd.
    Inventors: Takuya AOYAGI, Motomune KODAMA, Takashi NAITO, Tadashi FUJIEDA, Yuichi SAWAI, Masanori MIYAGI, Haruo AKAHOSHI, Norihisa IWASAKI
  • Patent number: 8840700
    Abstract: The present invention provides conductive metal compositions for electronic applications, and methods of preparation and uses thereof. More specifically, the present invention provides metallic particle transient liquid phase sintering compositions containing blended formulations of metal and metal alloy components that form interconnected conductive metallurgical networks with increased stability, resistance to thermal stress and ability to mitigate CTE mismatch between materials.
    Type: Grant
    Filed: November 5, 2010
    Date of Patent: September 23, 2014
    Assignee: Ormet Circuits, Inc.
    Inventors: Catherine Shearer, Kenneth C. Holcomb, G. Delbert Friesen, Michael C. Matthews
  • Publication number: 20140263588
    Abstract: A solder and methods of forming an electrical interconnection are shown. Examples of solders include gallium based solders. A solder including gallium is shown that includes particles of other solders mixed with a gallium based matrix. Methods of applying a solder are shown that include swiping a solder material over a surface that includes a resist pattern. Methods of applying a solder are also shown that include applying a solder that is immersed in an acid solution that provides a fluxing function to aid in solder adhesion.
    Type: Application
    Filed: March 13, 2013
    Publication date: September 18, 2014
    Inventors: Ting Zhong, Rajashree Raji Baskaran, Aleksandar Aleks Aleksov
  • Publication number: 20140252607
    Abstract: The present invention relates to a reflow film containing a thermoplastic resin which is dissolvable in a solvent, and solder particles, wherein the solder particles are dispersed in the film, and also relates to a solder bump formation method which comprises: (A) a step of mounting the reflow film on the electrode surface side of a substrate, (B) a step of mounting and fixing a flat plate, (C) a step of heating, and (D) a step of dissolving and removing the reflow film, and herewith, a reflow film is provided which, by causing localization of the solder component on the electrodes of the substrate by self-assembly, exhibits excellent storage properties, transportability and handling properties during use, and can form solder bumps or solder joints selectively on only the electrodes.
    Type: Application
    Filed: October 26, 2012
    Publication date: September 11, 2014
    Applicant: Hitachi Chemical Company, Ltd.
    Inventors: Kazuhiro Miyauchi, Naoya Suzuki, Nozomu Takano, Yukihiko Yamashita